3.1 Generation of Measurement Conditions
3 - 12
Hold
Time
The end temperature can be held for the set time.
Input range
Dry .................... 0 to 100 s
Ash .................... 0 to 100 s
Atomize ............. 1 to 20 s
Clean ................. 1 to 20 s
(1 to 10 s for Pyro Tube C HR and D
HR)
Cool ................... 12 to 100 s
NOTE
: The limits on the ramp time and hold time vary with the
temperature program developed and are dependent on the
temperature of the cuvette in one measurement session.
Set the limits to meet the following criteria.
1500
C
≦
Cuvette temperature <2000
C
The sum of the ramp time and the hold
time: less than 100 s.
2000
C
≦
Cuvette temperature <2500
C
The sum of the ramp time and the hold
time: less than 25 s.
2500
C
≦
Cuvette temperature <2800
C
The sum of the ramp time and the hold
time: less than 20 s.
2800
C
≦
Cuvette temperature
The sum of the ramp time and the hold
time: less than 10 s.
Gas
Flow
Specifies the flow rate of carrier gas. For stages other
than atomization, set 200 mL/min usually for purging
solvent vapor and sample vapor. In the atomizing
stage, absorption sensitivity is enhanced by increasing
atomic vapor density at a reduced gas flow rate. The
carrier gas is passed through to protect the cuvette. If
the gas flow rate is set to a low value, the life of the
cuvette will be reduced.
Input value: 0, 10, 30, 200 mL/min
Содержание ZA3000 Series
Страница 267: ...3 1 11 3 43 Fig 3 31 Parameter List Window Common conditions The setting of method is thus completed ...
Страница 357: ...5 5 Twin Injection 5 28 Fig 5 24 Dialog Box for Confirming Nozzle Position 7 Click Start measurement ...
Страница 423: ...9 3 5 9 11 Fig 9 14 Diagnosis Log Dialog Box ...
Страница 449: ...10 5 Reflecting on Analysis Conditions 10 24 Fig 10 16 Method Window Unmark the checkbox ...
Страница 455: ...INDEX 4 V Verify 3 34 W Working curve graph 4 1 Wavelength accuracy 9 1 ...
Страница 456: ...INSTRUCTION MANUAL 7J1 9027 000 Ver 1 February 2016 MODEL HFS 4 HYDRIDE FORMATION SYSTEM ...