Maintenance
73
Leak Checking
Checking for leaks is actually checking the integrity of the vacuum system. You
observe masses 4 (helium), 18 (water), 28 (nitrogen), and 32 (oxygen).
To leak-check the system, follow this procedure:
1.
Ensure that all connections are made to the mass spectrometer.
2.
Set the GC split flow to 50 mL/min by pressing the PSSI injector icon on the
Clarus GC touch screen. On the next screen, press the split flow setpoint and
use the up and down arrow or keypad
buttons to set the split flow
to 50mL. For example, if the capillary injector is in position 1 and you selected
split flow in the PPC configuration software, the following screen is displayed.
The total flow (split vent + septum purge + column) is displayed in the lower
left of the screen. The split vent flow setpoint is displayed in the setpoint box
in the lower right.
3.
Start the TurboMass software by clicking on the Windows
Start
button at the
bottom left of the screen and select
TurboMass
under the
Programs/TurboMass/TurboMass
path, or double-click on the TurboMass icon if
it is on your Windows desktop.
The initial TurboMass window is displayed.
Summary of Contents for Clarus SQ 8 MS Series
Page 1: ...CLARUS SQ 8 MS Hardware Guide GAS CHROMATOGRAPHY ...
Page 2: ......
Page 3: ...Clarus SQ 8 MS Hardware Guide ...
Page 8: ......
Page 9: ...Warnings and Safety Information 1 ...
Page 10: ......
Page 18: ...Label Location and Content Figure 1 Front View of Clarus SQ 8 T ...
Page 46: ......
Page 47: ...Introduction 2 ...
Page 48: ......
Page 52: ......
Page 53: ...About the Clarus GC MS System 3 ...
Page 54: ......
Page 64: ......
Page 67: ...Maintenance 65 Maintenance 4 ...
Page 68: ......
Page 69: ...Maintenance 67 ...
Page 98: ...Clarus SQ 8 MS Hardware Guide 96 Figure 19 Inserting the Plug Handle and Sight ...
Page 148: ...Troubleshooting 5 ...
Page 149: ...Troubleshooting 147 ...
Page 178: ...TurboMass Software Installation 176 ...
Page 179: ...Index ...
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