Setting Up Oven and Inlet Temperature Programs . 65
Setting a Coolant Timeout Value
The purpose of the coolant timeout value is to conserve coolant. If you select a coolant timeout value
when you configure the Clarus GC, the coolant solenoid shuts off if a GC run is not started within this time
period after the oven becomes "READY" (reaches the initial set temperature). Once the coolant shuts off,
the Clarus GC remains not ready and the following message will appear,
Coolant Timed Out:Touch OK
to Continue
.
NOTE: The coolant timeout must be greater than the equilibration time.
When you press
OK
, the coolant solenoid will then operate again and the oven will cool to the initial
temperature.
NOTE: When using a POC or PSS injector with the subambient accessory, the injector temperature must not be set
below the oven temperature. You can minimize coolant consumption if using the oven subambient with the
PSS or POC installed but not being used, by deconfiguring the PSS or POC.
Setting a Coolant Cut-In Temperature
The coolant cut-in temperature is the temperature below which the coolant starts to cool the oven. The
default temperature is 60
°
C. The allowable cut-in temperature range is 30
°
C
-
110
°
C. We recommend
that for every
°
C above a room temperature of 20
°
C, you increase the cut-in temperature by 1
°
C.
For example: A room temperature of 20
°
C uses a default temperature of 60
°
C, whereas a room
temperature of 25
°
C uses a 65
°
C cut-in temperature. Examples for setting up isothermal, 1, and 2 ramp
programs follow.
NOTE: Higher cut-in temperatures cause more coolant to be consumed, but can cool the oven to the initial
temperature more rapidly.
Setting Up an Isothermal Program
Setting up an isothermal program requires entering the following information in the sequence shown:
•
Initial oven temperature (Temp 1)
•
The total run time for the initial temperature (Time 1)
•
A temperature rate increase of 0 (Rate 1).
Содержание CLARUS 590 GC
Страница 1: ...CLARUS 590 GC User s Guide GAS CHROMATOGRAPHY ...
Страница 9: ...About This Manual 9 Flame Ionization Detector FID 270 TCD 273 Autosampler 277 Index 279 ...
Страница 10: ...10 Clarus 590 GC User s Guide ...
Страница 11: ...1 Introduction ...
Страница 12: ...12 Clarus 590 GC User s Guide ...
Страница 21: ...2 Touch Screen Navigation ...
Страница 22: ...22 Clarus 590 GC User s Guide ...
Страница 48: ...48 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Страница 50: ...50 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Страница 59: ...3 Using the Active Method ...
Страница 60: ...60 Clarus 590 GC User s Guide ...
Страница 109: ...4 Setting Up the Detectors ...
Страница 110: ...110 Clarus 590 GC User s Guide ...
Страница 197: ...5 Using the Method Editor ...
Страница 198: ...198 Clarus 590 GC User s Guide ...
Страница 207: ...6 Using the Tools Menu ...
Страница 208: ...208 Clarus 590 GC User s Guide ...
Страница 224: ...224 Clarus 590 GC User s Guide ECD PID NPD FPD ...
Страница 225: ...Detectors 225 Output Configured ...
Страница 262: ...262 Clarus 590 GC User s Guide ...
Страница 263: ...7 Setting up a Typical Analysis ...
Страница 264: ...264 Clarus 590 GC User s Guide ...
Страница 279: ...Index ...
Страница 280: ...280 Clarus 590 GC User s Guide ...