260
Maintenance
Checking the Spray Pattern
Once you have thoroughly flushed out the nebulizer with deionized water and
removed the nebulizer/end cap, you can follow these steps to check the nebulizer
spray pattern:
1. Set the nebulizer argon flow to
0.6 L/min.
2. Place the sample capillary tubing in a beaker of deionized water and start the
pump at a rate of 1.5 mL/min.
3. Check the spray pattern on a paper towel. You should see a fine, even spray of
uniform sample droplets.
If the spray pattern is not even or the nebulizer is sputtering, the nebulizer tips
should be inspected for clogging and cleaned or replaced as necessary. See the
following procedure.
Complete replacement of the nebulizer/end cap assembly may be necessary if the
GemTips are not seated properly inside the cap (see the next figure) or if the end
cap does not fit properly on the spray chamber.
Disassembling the Cross-Flow Nebulizer
Disassemble the nebulizer if it is necessary to clean or replace the GemTips. The
Cross-Flow nebulizer has two GemTips. The sample tip is a clear sapphire and the
argon tip is a red ruby.
These tips are
not
interchangeable.
For this reason, we
recommend that you first remove one GemTip, clean or replace it, then remove the
other.
When checking the spray pattern of the nebulizer, pump only use
deionized water. Do
not
use any other solution.
Avertissement:
Lors de la vérification du motif de pulvérisation du
nébuliseur, pompe utiliser uniquement de l'eau déminéralisée. Ne pas
utiliser toute autre solution.
!
Warning
Содержание AVIO 500
Страница 1: ...AVIO 500 Customer Hardware and Service Guide ICP OPTICAL EMISSION ...
Страница 2: ......
Страница 3: ...Avio 500 Customer Hardware and Service Guide ...
Страница 12: ...Contents 10 ...
Страница 30: ...28 ...
Страница 31: ...C h a p t e r 1 ...
Страница 32: ......
Страница 33: ...Safety Practices 1 ...
Страница 58: ...56 Safety Practices ...
Страница 59: ...C h a p t e r 2 ...
Страница 60: ......
Страница 76: ...74 Preparing Your Laboratory ...
Страница 77: ...C h a p t e r 3 ...
Страница 78: ......
Страница 79: ...System Description 3 ...
Страница 94: ...92 System Description Figure 3 7 GemCone nebulizer and end cap N0680504 also shown in cross sectional view ...
Страница 115: ...C h a p t e r 4 ...
Страница 116: ......
Страница 137: ...135 Installing the Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 152: ...150 Installation Figure 4 22 Scott Spray Chamber Clip Assembly in Place ...
Страница 195: ...193 Shipping Lists 09290798 USB Cable Table 4 6 Spares Available Continued ...
Страница 196: ...194 Installation ...
Страница 197: ...C h a p t e r 5 ...
Страница 198: ......
Страница 209: ...207 Quick Change Adjustable Torch Module Figure 5 1 Quartz Torch Item Description 1 Plasma Induction Plates 2 Torch 2 1 ...
Страница 217: ...215 Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 316: ...314 Maintenance ...
Страница 317: ...C h a p t e r 6 ...
Страница 318: ......
Страница 339: ...337 RF Generator Sample Introduction System Troubleshooting Form Figure 6 2 Normal plasma at 3mm position ...
Страница 340: ...338 Troubleshooting Figure 6 3 Rounded Plasma due to sample or air getting around the outside typically subtle air leak ...
Страница 342: ...340 Troubleshooting Figure 6 5 Injector too far forward ...
Страница 343: ...341 RF Generator Sample Introduction System Troubleshooting Form Figure 6 6 No Aux Gas torch may be glowing ...
Страница 344: ...342 Troubleshooting Figure 6 7 Air leak or spray chamber temperature too high ...
Страница 345: ...343 RF Generator Sample Introduction System Troubleshooting Form Figure 6 8 Thin plasma due to leak in plasma gas line ...
Страница 346: ...344 Troubleshooting ...
Страница 354: ......