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System Description
Spectrometer
Polychromator:
The high energy (f/6.7) echelle-based polychromator is a
PerkinElmer design. The resolution of the system is 0.006 nm at 200 nm. The 80
by 160 mm echelle grating has 79 lines per mm and a blaze angle of 63.4 degrees.
On the Avio 500, the cross disperser for the UV region is a grating (374 lines/mm)
with Schmidt correction incorporated into its surface. The Schmidt correction
performs aberration correction for the 400 mm radius camera sphere.
The cross disperser for the visible region on dual detector mode is a 60-degree
prism.
The entire optical system is enclosed in a purged and thermostated optical
enclosure.
Thermostating:
The polychromator is thermostated to 39 °C. The thermostating
includes the transfer optics along with the polychromator.
Plasma Viewing:
The viewing position can be optimized by the software with all
configurations.
Shutter and Mercury Recalibration System:
The computer-controlled motor
operated shutter automatically opens and closes for each sample. By closing the
shutter between each sample, the first transfer mirror is protected from long
exposures to the intense UV radiation of the plasma thus extending the useful
lifetime of the mirror. A mercury lamp is built into the entrance shutter mechanism
and can be viewed when the shutter is closed to monitor the mercury emission line
at 253 nm and automatically update the system wavelength calibration. Frequency
of the automatic recalibration is user selectable between 0 and 1000 minutes and
can be varied during an autosampler analysis.
Detector:
The patented PerkinElmer Segmented-array Charge-coupled-device
Detector
(SCD)
Electronics:
Correlated double sampling data acquisition electronics reduce
electronic noise.
Содержание AVIO 500
Страница 1: ...AVIO 500 Customer Hardware and Service Guide ICP OPTICAL EMISSION ...
Страница 2: ......
Страница 3: ...Avio 500 Customer Hardware and Service Guide ...
Страница 12: ...Contents 10 ...
Страница 30: ...28 ...
Страница 31: ...C h a p t e r 1 ...
Страница 32: ......
Страница 33: ...Safety Practices 1 ...
Страница 58: ...56 Safety Practices ...
Страница 59: ...C h a p t e r 2 ...
Страница 60: ......
Страница 76: ...74 Preparing Your Laboratory ...
Страница 77: ...C h a p t e r 3 ...
Страница 78: ......
Страница 79: ...System Description 3 ...
Страница 94: ...92 System Description Figure 3 7 GemCone nebulizer and end cap N0680504 also shown in cross sectional view ...
Страница 115: ...C h a p t e r 4 ...
Страница 116: ......
Страница 137: ...135 Installing the Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 152: ...150 Installation Figure 4 22 Scott Spray Chamber Clip Assembly in Place ...
Страница 195: ...193 Shipping Lists 09290798 USB Cable Table 4 6 Spares Available Continued ...
Страница 196: ...194 Installation ...
Страница 197: ...C h a p t e r 5 ...
Страница 198: ......
Страница 209: ...207 Quick Change Adjustable Torch Module Figure 5 1 Quartz Torch Item Description 1 Plasma Induction Plates 2 Torch 2 1 ...
Страница 217: ...215 Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 316: ...314 Maintenance ...
Страница 317: ...C h a p t e r 6 ...
Страница 318: ......
Страница 339: ...337 RF Generator Sample Introduction System Troubleshooting Form Figure 6 2 Normal plasma at 3mm position ...
Страница 340: ...338 Troubleshooting Figure 6 3 Rounded Plasma due to sample or air getting around the outside typically subtle air leak ...
Страница 342: ...340 Troubleshooting Figure 6 5 Injector too far forward ...
Страница 343: ...341 RF Generator Sample Introduction System Troubleshooting Form Figure 6 6 No Aux Gas torch may be glowing ...
Страница 344: ...342 Troubleshooting Figure 6 7 Air leak or spray chamber temperature too high ...
Страница 345: ...343 RF Generator Sample Introduction System Troubleshooting Form Figure 6 8 Thin plasma due to leak in plasma gas line ...
Страница 346: ...344 Troubleshooting ...
Страница 354: ......