171
Instrument Start-up
•
Air/N
2
Shear gas: 5.5 to 8.25 bar or 80-120 psig.
•
N
2
gas: 2.75 to 8.25 bar or 40-120 psig.
3. Make sure that the torch is correctly installed, the torch compartment door is
shut, and the EMO switch is released.
4. Make sure the drain vessel is empty.
5. Switch on the spectrometer, and if required, the autosampler.
6. Switch on the chiller.
7. Switch on the computer and start the ICP software.
8. In the in the
Instrument
tab, click on
Plasma Control
and ignite the plasma.
Allow the torch to warm up for 30 minutes before you start making measurements.
Instrument Start-up
First turn on the gases and water chiller. Then use the Main Instrument switch to
turn on the spectrometer. Once the plasma has been ignited, you should wait one
half hour for the system to stabilize before running samples.
The spectrometer initialization is completed when the spectrometer sends a
"system ready" message to the computer.
Note
It is recommended to leave the main power switch to the instrument is in
the
ON
position to maintain spectrometer thermal equilibrium.
Do
not
block the main power switch because it functions as the
disconnecting device for the instrument's power.
If the instrument is turned off (via the power switch) for more than 24
hours the instrument will require, once it is turned on, two hours to
initialize and warm up before the instrument can operate at peak
performance.
Содержание AVIO 500
Страница 1: ...AVIO 500 Customer Hardware and Service Guide ICP OPTICAL EMISSION ...
Страница 2: ......
Страница 3: ...Avio 500 Customer Hardware and Service Guide ...
Страница 12: ...Contents 10 ...
Страница 30: ...28 ...
Страница 31: ...C h a p t e r 1 ...
Страница 32: ......
Страница 33: ...Safety Practices 1 ...
Страница 58: ...56 Safety Practices ...
Страница 59: ...C h a p t e r 2 ...
Страница 60: ......
Страница 76: ...74 Preparing Your Laboratory ...
Страница 77: ...C h a p t e r 3 ...
Страница 78: ......
Страница 79: ...System Description 3 ...
Страница 94: ...92 System Description Figure 3 7 GemCone nebulizer and end cap N0680504 also shown in cross sectional view ...
Страница 115: ...C h a p t e r 4 ...
Страница 116: ......
Страница 137: ...135 Installing the Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 152: ...150 Installation Figure 4 22 Scott Spray Chamber Clip Assembly in Place ...
Страница 195: ...193 Shipping Lists 09290798 USB Cable Table 4 6 Spares Available Continued ...
Страница 196: ...194 Installation ...
Страница 197: ...C h a p t e r 5 ...
Страница 198: ......
Страница 209: ...207 Quick Change Adjustable Torch Module Figure 5 1 Quartz Torch Item Description 1 Plasma Induction Plates 2 Torch 2 1 ...
Страница 217: ...215 Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 316: ...314 Maintenance ...
Страница 317: ...C h a p t e r 6 ...
Страница 318: ......
Страница 339: ...337 RF Generator Sample Introduction System Troubleshooting Form Figure 6 2 Normal plasma at 3mm position ...
Страница 340: ...338 Troubleshooting Figure 6 3 Rounded Plasma due to sample or air getting around the outside typically subtle air leak ...
Страница 342: ...340 Troubleshooting Figure 6 5 Injector too far forward ...
Страница 343: ...341 RF Generator Sample Introduction System Troubleshooting Form Figure 6 6 No Aux Gas torch may be glowing ...
Страница 344: ...342 Troubleshooting Figure 6 7 Air leak or spray chamber temperature too high ...
Страница 345: ...343 RF Generator Sample Introduction System Troubleshooting Form Figure 6 8 Thin plasma due to leak in plasma gas line ...
Страница 346: ...344 Troubleshooting ...
Страница 354: ......