ORBECO SP600, Instruction Manual, Page: 136 / 334

134 SP600 Spectrophotometer 01/2008
1.1 Methods
Hydrazine
with Liquid Reagent
0.005 – 0.6 mg/l N
2
H
4
/ 5 – 600 μg/l N
2
H
4
Use two clean vials (24 mm Ø) and mark one as blank for
zeroing.
1. Fill a clean vial with 10 ml deionized water (this is the
blank).
2. Add 1 ml VARIO Hydra 2 Rgt Solution into the vial
(Note 3).
3. Close the vial tightly with the cap and swirl several
times to mix the contents.
4. Place the vial (the blank) in the sample chamber making
sure that the marks are aligned.
5. Press ZERO key.
6. Remove the vial from the sample chamber.
7. Fill the second clean vial with 10 ml of water sample
(this is the sample).
8. Add
1 ml VARIO Hydra 2 Rgt Solution
into the vial.
9. Close the vial tightly with the cap and swirl several
times to mix the contents.
10. Place the vial (the blank) in the sample chamber making
sure that the marks are aligned.
11. Press
TEST
key.
Wait for a reaction period of 12 minutes .
After the reaction period is finished the measurement
starts automatically.
The result is shown in the display as Hydrazine.
prepare Zero
press ZERO
Zero accepted
prepare Test
press TEST
Countdown
12:00
2 0 6