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Thermo Scientific 146i, Инструкция по эксплуатации


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Optional Equipment

Mounting Options

9-18

Model 146

i

 Instruction Manual

Thermo Fisher Scientific

Содержание 146i

Страница 1: ...Model 146i Instruction Manual Dynamic Gas Calibrator Part Number 102482 00 30Jan2008 ...

Страница 2: ...ons terms and pricing are subject to change Not all products are available in all countries Please consult your local sales representative for details Thermo Fisher Scientific Air Quality Instruments 27 Forge Parkway Franklin MA 02038 1 508 520 0430 www thermo com aqi ...

Страница 3: ...ientific has contracted with one or more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on Thermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive a...

Страница 4: ......

Страница 5: ...s the procedures for calibrating the analyzer and describes the required equipment Chapter 5 Preventive Maintenance provides maintenance procedures to ensure reliable and consistent instrument operation Chapter 6 Troubleshooting presents guidelines for diagnosing analyzer failures isolating faults and includes recommended actions for restoring proper operation Chapter 7 Servicing presents safety a...

Страница 6: ...ignored WARNING A hazard is present or an unsafe practice can result in serious personal injury if the warning is ignored CAUTION The hazard or unsafe practice could result in minor to moderate personal injury if the warning is ignored Equipment Damage The hazard or unsafe practice could result in property damage if the warning is ignored Safety and Equipment Damage Alerts in this Manual Alert Des...

Страница 7: ... using soap and water Equipment Damage Do not attempt to lift the analyzer by the cover or other external fittings Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component This adjustment should only be performed by an instrument service technician Handle all printed circuit boards b...

Страница 8: ...able from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com aqi 1 866 282 0430 1 508 520 0430 Symbol Description Marking of electrical and electronic equipment which applies to electrical and electronic equipment falling under the Directive 2002 96 EC WEEE and the equipment that has been pu...

Страница 9: ...nspection 2 1 Setup Procedure 2 1 Remote Interconnections 2 1 Inputs 2 1 Outputs 2 1 Connecting External Devices 2 1 Terminal Board PCB Assemblies 2 1 Startup 2 1 Operation 3 1 Display 3 1 Pushbuttons 3 1 Soft Keys 3 1 Software Overview 3 1 Power Up Screen 3 1 Run Screen 3 1 Main Menu 3 1 Operation 3 1 Flow Modes 3 1 Standby 3 1 Gas Dilution 3 1 Permeation Oven 3 1 O3 3 1 Photometer 3 1 Gas Setup ...

Страница 10: ...3 2 Program Menu 3 2 Program Cycle 3 2 Period Hours 3 2 Next Cycle 3 2 Events 3 2 Instrument Controls Menu 3 2 Temperature Compensation 3 2 Pressure Compensation 3 2 Datalogging Settings 3 2 Communication Settings 3 2 I O Configuration 3 2 Screen Contrast 3 2 Service Mode 3 2 Date Time 3 2 Diagnostics Menu 3 2 Program Version 3 2 Voltages 3 2 Flows 3 2 Temperatures 3 2 Pressure 3 2 Analog Input Re...

Страница 11: ...ion 3 3 Analog Input Calibration 3 3 Permeation Oven Settings 3 3 Lamp Setting 3 3 Intensity Check 3 3 O3 Response Coefficient 3 3 Display Pixel Test 3 3 Restore User Defaults 3 3 Password 3 3 Set Password 3 4 Lock Instrument 3 4 Change Password 3 4 Remove Password 3 4 Unlock Instrument 3 4 Calibration 4 1 Mass Flow Controllers 4 1 Photometer Calibration 4 1 Calibration Using a Model 49i PS 4 1 Oz...

Страница 12: ... Checkout without Photometer Option 7 1 Mass Flow Controller Replacement 7 1 Pump Replacement Photometer option 7 1 Fan Replacement Rear Panel 7 1 Ran Replacement Mass Flow Controllers 7 1 Analog Output Testing 7 1 Analog Output Calibration 7 1 Analog Input Calibration 7 1 Calibrating the Input Channels to Zero Volts 7 2 Calibrating the Input Channels to Full Scale 7 2 I O Expansion Board Replacem...

Страница 13: ... 3 Pressure Regulator s Adjustment 7 3 Ambient Temperature Calibration 7 3 Service Locations 7 3 System Description 8 1 Hardware 8 1 Flow System 8 1 Precision Gas Dilution 8 1 Ozone Generation 8 1 Gas Phase Titration 8 1 Permeation Tube Oven 8 1 Photometer 8 1 Detector System 8 1 Pressure Transducer 8 1 Ozonator 8 1 Ozonator Lamp Power Supply 8 1 Photometer Lamp Power Supply 8 1 Photometer Tempera...

Страница 14: ...8 2 Digital Relay Outputs 8 2 Digital Inputs 8 2 Serial Ports 8 2 RS 232 Connection 8 2 RS 485 Connection 8 2 Ethernet Connection 8 2 External Accessory Connector 8 3 Optional Equipment 9 1 Ozonator 9 1 Photometer 9 1 Zero Air Source 9 1 Permeation Oven 9 1 Permeation Tube Installation 9 1 Computation of Concentrations 9 1 Oven Installation and Configuration 9 1 Permeation Tube Oven Calibration 9 ...

Страница 15: ...asurement Configuration B 1 Hardware Configuration B 1 Communications Configuration B 1 I O Configuration B 1 Record Layout Definition B 1 Format Specifier for ASCII Responses B 1 Format Specifier for Binary Responses B 1 Format Specifier for Front Panel Layout B 1 MODBUS Protocol C 1 Serial Communication Parameters C 1 TCP Communication Parameters C 1 Application Data Unit Definition C 1 Function...

Страница 16: ...Contents xii Model 146i Instruction Manual Thermo Fisher Scientific ...

Страница 17: ...inal Board Views 2 2 Figure 2 8 25 Pin Terminal Board Views 2 2 Figure 3 1 Front Panel Display 3 4 Figure 3 2 Front Panel Pushbuttons 3 4 Figure 3 3 Flowchart of Menu Driven Software 3 4 Figure 3 4 Pin Out of Rear Connector 3 4 Figure 4 1 Photometer Calibration Flow Schematic 4 1 Figure 4 2 Ozonator Control Check Flow Schematic 4 1 Figure 5 1 Inspecting and Cleaning the Fan Filter 5 2 Figure 5 2 R...

Страница 18: ... 7 12 Photometer Components 7 3 Figure 7 13 Replacing the Ozonator 7 3 Figure 7 14 Removing the Glass Chamber Assembly 7 3 Figure 7 15 Replacing the Glass Chamber Assembly 7 3 Figure 7 16 Replacing the Pressure Regulator 7 3 Figure 8 1 Hardware Components 8 3 Figure 9 1 Cal Oven Therm Resistor Screen 9 2 Figure 9 2 Cal Gas Therm Bath Screen 9 2 Figure 9 3 Cal Gas Therm Resistor Screen 9 2 Figure 9...

Страница 19: ...escriptions 6 1 Table 6 7 Measurement Interface Board Connector Pin Descriptions 6 1 Table 6 8 Solenoid Connector Board Pin Descriptions 6 1 Table 6 9 Ozonator Power Supply Connector Pin Descriptions 6 1 Table 6 10 Photometer Power Supply Connector Pin Descriptions 6 1 Table 7 1 Model 146i Replacement Parts 7 3 Table 7 2 Model 146i Cables 7 3 Table 7 3 External Device Connection Components 7 3 Tab...

Страница 20: ...Contrast Levels B 2 Table B 10 Reply Termination Formats B 2 Table B 11 Analog Current Output Range Values B 2 Table B 12 Analog Voltage Output Range Values B 2 Table B 13 Default Output Assignment B 2 Table C 1 Read Coils for 146i C 1 Table C 2 Read Registers for 146i C 2 Table C 3 Write Coils for 146i C 2 ...

Страница 21: ...lity In the Model 146i these components are integrated into a single microprocessor controlled unit The instrument can be controlled locally via the front panel interface or remotely using a datalogger or computer The standard Model 146i hardware plumbing configuration comprises gas and zero air flow controllers as shown in Figure 1 1 The basic unit can handle three gas standards controlled by ind...

Страница 22: ...tion tube oven as shown in Figure 1 3 Accuracy is achieved since both the release rate of the permeation tube gas and the flow of zero air through the zero air mass flow controller are known and the temperature of the permeation tube is stable Temperature stability of the permeation tube is accomplished by allowing only a small amount of zero air to enter the permeation tube oven to be heated The ...

Страница 23: ...lows through the zero air solenoid and through the zero air mass flow controller then through the ozonator to the manifold and to the external internal solenoid to become the sample gas I The other stream flows from the zero air bulkhead to the sample reference solenoid in the photometer and is used as the reference gas Io Alternately the sample gas may be pulled from an external source through th...

Страница 24: ...Introduction Principle of Operation 1 4 Model 146i Instruction Manual Thermo Fisher Scientific Figure 1 1 Standard Gas Dilution System Figure 1 2 Standard Gas Dilution System with Ozonator Option ...

Страница 25: ...of Operation Thermo Fisher Scientific Model 146i Instruction Manual 1 5 Figure 1 3 Standard Gas Dilution System with Permeation Tube Oven Option Figure 1 4 Standard Gas Dilution with Ozonator and Permeation Tube Oven Options ...

Страница 26: ...peration 1 6 Model 146i Instruction Manual Thermo Fisher Scientific Figure 1 5 Standard Gas Dilution System with Photometer Option Figure 1 6 Standard Gas Dilution System with Ozonator Permeation Tube Oven and Photometer Options ...

Страница 27: ...ollers Response time as measured at output of manifold to 99 of final value Less than one minute for low flows Faster for high flow for gas phase titration mode response time increases to 4 minutes Meets or exceeds U S EPA Dynamic Parameters specification requirements for gas phase titration Operating temperature 0 45 C Power Requirements 100 VAC 50 60 Hz 115 VAC 50 60 Hz 220 240 VAC 50 60 Hz 275 ...

Страница 28: ...puts Up to 8 24 VDC external solenoids can be controlled by Model 146i Analog outputs 6 voltage outputs 0 100 mV 1 5 10 V User selectable 5 of full scale over under range 12 bit resolution user selectable for measurement input Optional 6 current outputs 0 20 mA or 4 20 mA Digital outputs 1 power fail relay Form C 10 relays Form A user selectable alarm output relay logic 100 mA 200 VDC Digital inpu...

Страница 29: ... rear of the unit Although one person can lift the unit it is desirable to have two persons lifting one by grasping the bottom in the front and the other by grasping the bottom in the rear Unpacking and Inspection The Model 146i is shipped complete in one container If there is obvious damage to the shipping container when you receive the instrument notify the carrier immediately and hold for inspe...

Страница 30: ...nts 3 Remove the packing material Figure 2 1 Figure 2 1 Remove the Packing Material 4 If the photometer option is installed includes pump remove the three shipping screws Figure 2 2 Figure 2 2 Remove the Shipping Screws Units without Optional I O Board Units with Optional I O Board Remove Packing Remove Packing 2 pieces 2 pieces Shipping Screws 3 ...

Страница 31: ...ll scale flows of the zero air controller at a pressure between 10 and 40 psi 2 Connect the standard gas cylinders to the ports labeled A B and C 3 Install the permeation tube using the following procedure applicable only if the permeation option is installed a Remove the instrument cover and locate the permeation oven Component Layout on page 7 8 b Release the latches on the sides of the oven cov...

Страница 32: ...top Figure 2 3 Keep glass clean by using Kimwipes or similar material to handle glass e Place permeation tube in chamber f Attach glass chamber to top assembly by gently pushing together with a slight twisting motion Figure 2 3 g Replace glass chamber assembly into oven until top of assembly is flush or slightly below oven top Figure 2 4 Knurled Screw Glass Chamber Assembly Oven Top Top Assembly G...

Страница 33: ...ould be less than 10 feet Verify that there is no restriction in this line 5 Connect a suitable recording device to the rear panel connector For detailed information about connecting to the instrument refer to Connecting External Devices on page 2 10 External Device Connection Components on page 7 7 Terminal Block and Cable Kits on page 9 11 Instrument Controls Menu in the Operation chapter For de...

Страница 34: ...y input settings with corresponding relay outputs Inputs The Model 146i is controllable through the 37 pin male rear panel connector Refer to the following tables when selecting the appropriate gas gas span level and ozonator or permeation oven level for the Model 146i Note These are the default settings that can be changed by the operator A 1 indicates contact closure to ground and 0 indicates no...

Страница 35: ...zonator or permeation oven level gas Gas Bit 3 Pin 23 Gas Bit 2 Pin 4 Gas Bit 1 Pin 3 Gas Type 0 0 0 Gas Off 0 0 1 Gas A 0 1 0 Gas B 0 1 1 Gas C 1 0 0 Gas D 1 0 1 Gas E 1 1 0 Gas F Span Bit 3 Pin 25 Span Bit 2 Pin 6 Span Bit 1 Pin 24 Span Level 0 0 0 Span 0 0 0 1 Span 1 0 1 0 Span 2 0 1 1 Span 3 1 0 0 Span 4 1 0 1 Span 5 1 1 0 Manual Oz Perm Bit 4 Pin 9 Oz Perm Bit 3 Pin 27 Oz Perm 2 Pin 8 Oz Perm...

Страница 36: ...They default to Normally Open meaning that the relays are closed when the condition exists and can be user configured as NO or NC Refer to the following tables for the indicated gas gas span level and ozonator or permeation oven level for the Model 146i Pins 1 2 and 3 to report the selected gas 1 indicates contact closure 0 1 1 0 Ozon 5 0 1 1 1 Perm 1 1 0 0 0 Perm 2 1 0 0 1 Perm 3 1 0 1 0 Perm 4 1...

Страница 37: ... 1 0 Gas F Span Bit 3 Pins 6 25 Span Bit 2 Pins 5 24 Span Bit 1 Pins 4 23 Span Level 0 0 0 Span 0 0 0 1 Span 1 0 1 0 Span 2 0 1 1 Span 3 1 0 0 Span 4 1 0 1 Span 5 1 1 0 Manual Oz Perm Bit 7 Pins10 29 Oz Perm Bit 8 Pins 9 28 Oz Perm 9 Pins 8 27 Oz Perm Bit 10 Pins 7 26 Ozonator or Permeation Oven Levell 0 0 0 0 Ozon Perm Off 0 0 0 1 Ozon Manual 0 0 1 0 Ozon 1 0 0 1 1 Ozon 2 0 1 0 0 Ozon 3 0 1 0 1 O...

Страница 38: ...rminal block and cable kits optional Individual cables optional For detailed information on the optional connection components refer to the Optional Equipment chapter For associated part numbers refer to External Device Connection Components on page 7 7 Terminal Board PCB Assemblies The following terminal board PCB assemblies are available for iSeries instruments I O terminal board PCB assembly 37...

Страница 39: ...ws Component Side Viewed from Top of Board Assembled Connector See Detail A Detail A See Detail B Detail B Table 2 1 I O Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 Analog1 13 Power_Fail_NC 2 Analog ground 14 Power_Fail_COM 3 Analog2 15 Power_Fail_NO 4 Analog ground 16 TTL_Input1 5 Analog3 17 TTL_Input2 6 Analog ground 18 TTL_Input3 7 Analog4 19 TTL_Input4 8 Ana...

Страница 40: ...mbled Connector See Detail A Detail A See Detail B Detail B Table 2 2 D O Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 Relay1_ContactA 13 Relay7_ContactA 2 Relay1_ContactB 14 Relay7_ContactB 3 Relay2_ContactA 15 Relay8_ContactA 4 Relay2_ContactB 16 Relay8_ContactB 5 Relay3_ContactA 17 Relay9_ContactA 6 Relay3_ContactB 18 Relay9_ContactB 7 Relay4_ContactA 19 Relay...

Страница 41: ... 2 3 identifies the connector pins and associated signals Figure 2 8 25 Pin Terminal Board Views Component Side Viewed from Top of Board Assembled Connector See Detail A Detail A See Detail B Detail B Table 2 3 25 Pin Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 IOut1 13 Analog_In1 2 GND_ISO 14 Analog_In2 3 IOut2 15 Analog_In3 4 GND_ISO 16 GNDD 5 IOut3 17 Analog_...

Страница 42: ...urn the power ON 2 Allow 90 minutes for the instrument to stabilize 3 Set instrument parameters such as gas setup and flow modes to appropriate settings For more information about instrument parameters see the Operation chapter 12 GND_ISO 24 GNDD Table 2 3 25 Pin Terminal Board Pin Descriptions continued Pin Signal Description Pin Signal Description ...

Страница 43: ...ge 3 1 Pushbuttons on page 3 2 Software Overview on page 3 4 Operation on page 3 8 Flow Modes on page 3 9 Gas Setup Menu on page 3 21 Ozonator Setup Menu on page 3 26 Permeation Oven Setup Menu on page 3 28 Photometer Setup Menu on page 3 30 Program Menu on page 3 36 Instrument Controls Menu on page 3 39 Diagnostics Menu on page 3 70 Alarms Menu on page 3 77 Service Menu on page 3 84 Password on p...

Страница 44: ...lay CAUTION If the LCD panel breaks do not to let the liquid crystal contact your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and water The Pushbuttons allow the user to traverse the various screens menus Figure 3 2 Front Panel Pushbuttons Pushbuttons ...

Страница 45: ... case letters to easily distinguish them from the operating screens To exit a help screen press or to return to the previous screen or to return to the Run screen Up Down Left Right The four arrow pushbuttons and move the cursor up down left and right or change values and states in specific screens Enter The is used to select a menu item accept set save a change and or toggle on off functions The ...

Страница 46: ...STUVWXYZ PAGE 0123456789 SAVE OPER MODE DIAGS ALARM The Model 146i utilizes the menu driven software as illustrated by the flowchart in Figure 3 3 The Power Up screen shown at the top of the flowchart is displayed while the instrument is warming up and performing self checks After the warm up period the Run screen is automatically displayed From the Run screen the Main Menu can be displayed by pre...

Страница 47: ...igital Inputs Relay States Solenoid States Test Analog Outputs Instrument Config Contact Info Alarms Ambient Temp O 3 Lamp Temp Perm Oven Temp Pressure Phot Bench Temp Phot Lamp Temp Phot Intensity MB Status Int Bd Status I O Bd Status Service Flow Control Select Cal Pres Temp Zero Flow Cal Gas Flow Cal Pressure Cal Ambient Temp Cal Bench Temp Cal Analog Output Cal Analog Input Cal Perm Oven Setti...

Страница 48: ...n oven and ozonator levels time and alarm status There are 5 values that may be displayed on the run screen that include the following TFLOW total flow in sccm as measured by the zero and gas flow controllers GAS X dilution concentration of gas from selected tank in ppm name is user definable O3 concentration of ozone measured by photometer in ppm PERM concentration from permeation tube in ppm GPT...

Страница 49: ...s in every screen The OZONATOR SETUP PERMEATION OVEN SETUP AND PHOTOMETER SETUP menu items are only displayed if these options are installed The SERVICE menu is visible only when the instrument is in service mode For more information on the service mode see Service Mode later in this chapter Use and to move the cursor up and down Press to select a choice Press to return to the top of the Main Menu...

Страница 50: ...ontrollers are set to provide the previously determined total flow and gas concentration For MANUAL the flow rates for the zero and gas flow controllers may be set directly The next line is used to set the permeation oven output level if installed The allowable modes are OFF PERM 1 through 5 and manual The concentration for these modes is displayed on the right If a gas span value is also selected...

Страница 51: ... up and down to select a mode or setting or change the number in the numeric edit field Press to save the mode switch to numeric entry or save the numeric entry Use and to change the mode or move the cursor in the numeric edit field Press to return to the Main Menu or to return to the Run screen OPERATION GAS A ZFLOW 10000 SCCM MANUAL GFLOW 100 SCCM PERM OFF 0 000 PPM OZONE OFF 0 0 PHOT OFF OPER M...

Страница 52: ...ode is turned back off In the Main Menu choose Standby STANDBY CURRENTLY OFF SET TO ON TOGGLE VALUE OPER MODE DIAGS ALARM The Gas Dilution menu is used to select a gas valve flow and span concentration The Gas A B or C menus set the zero air flow span 0 flow and the total flow output for a maximum of five span settings for each gas Additionally the gas menus let you manually set the zero air and g...

Страница 53: ...s Gas Dilution Gas A F Zero or Span 1 5 GAS A SPAN SELECTION ZERO 0 000 PPM SPAN 1 0 020 PPM SPAN 2 2 000 PPM SPAN 3 0 000 PPM SPAN 4 0 000 PPM SPAN 5 0 000 PPM MANUAL OPER MODE DIAGS ALARM FLOW MODE GAS A SPAN 2 GAS CONC 100 000 PPM TFLOW 1000 SCCM SAVING SAVE FLOW MODE OPER MODE DIAGS ALARM The Gas Manual Flow screen displays the zero air and gas flows and lets the user manually set the zero air...

Страница 54: ... CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Manual Gas Flow screen sets the manual gas flow value for the previously selected gas The screen identifies the minimum and maximum acceptable gas flow rates based on the installed flow controller and lets the user select a flow rate between these two settings If the selected gas flow is lower or higher than the acceptable range TOO LOW or TOO HIGH appe...

Страница 55: ... CONC 00 200 PPM TFLOW 1000 SCCM SAVING SAVE FLOW MODE OPER MODE DIAGS ALARM The Gas Selection screen is used to select the gas to mix with the permeation gas Gas D E and F are available if the six gas option is installed In the Main Menu choose Flow Modes Permeation Oven Gas Mix GAS SELECTION GAS A GAS A GAS B GAS B GAS C GAS C GAS D GAS D GAS E GAS E GAS D GAS F OPER MODE DIAGS ALARM The Gas Spa...

Страница 56: ...SPAN 4 0 000 PPM SPAN 5 0 000 PPM MANUAL OPER MODE DIAGS ALARM FLOW MODE GAS A PERM MIX GAS CONC 02 00 PPM PERM CONC 0 100 PPM TFLOW 1000 SCCM SAVING SAVE FLOW MODE OPER MODE DIAGS ALARM The Permeation Oven Gas Manual Flow screen shows the zero air and gas flows and is used to manually set them for the previously selected gas If the selected zero air flow is lower or higher than the acceptable ran...

Страница 57: ...ODE DIAGS ALARM The Manual Gas Flow screen sets the manual gas flow value for the previously selected gas The screen identifies the minimum and maximum acceptable gas flow rates and lets the user select a flow rate between these two settings If the selected gas flow is lower or higher than the acceptable range TOO LOW or TOO HIGH appears on the screen In the Main Menu choose Flow Modes Permeation ...

Страница 58: ...ODE DIAGS ALARM Five ozonator levels 1 5 can be set using the Ozonator Level Selection screen Once selected the screen reports the new flow mode The user must press to accept and activate these settings The message SAVING is displayed for 3 seconds then removed In the Main Menu choose Flow Modes O3 Transfer Standard Level 1 5 O3 LEVEL SELECTION LEVEL1 20 0 LEVEL2 25 0 LEVEL3 40 0 LEVEL4 60 0 LEVEL...

Страница 59: ...el can be set using the Ozonator GPT Select screen Alternately if Photometer Control is selected then all ozonator levels are shown in parts per million ppm instead of percent The MANUAL screen is used to set the ozonator output to the manual level in ppm or In the Main Menu choose Flow Modes O3 GPT Photometer Control Level 1 5 Manual O3 Adjust GPT Photometer Control O3 LEVEL SELECTION LEVEL1 100 ...

Страница 60: ... C GAS C GAS D GAS D GAS E GAS E GAS F GAS F OPER MODE DIAGS ALARM The Gas Span Selection screen is used to select the span level for the previously selected gas Gas D E and F are available if the six gas option is installed Once selected the screen reports the new flow mode The user must press to accept and activate these settings The message SAVING is displayed for 3 seconds then removed In the ...

Страница 61: ... zero air flow value for the previously selected gas The screen identifies the minimum and maximum acceptable zero air flow rates and lets the user select a flow rate between these two settings If the selected zero air flow is lower or higher Gas Manual Flow Zero Air GAS A SPAN SELECTION ZERO 0 000 SPAN 1 100 0 SPAN 2 80 0 SPAN 3 50 0 SPAN 4 20 0 SPAN 5 10 0 MANUAL OPER MODE DIAGS ALARM GAS A SPAN...

Страница 62: ...or higher than the acceptable range TOO LOW or TOO HIGH appears on the screen In the Main Menu choose Flow Modes O3 GPT Photometer Control Gas A F Level 1 5 Manual Gas MAN GAS A GAS FLOW MINIMUM 004 00 SCCM MAXIMUM 100 00 SCCM SET TO 050 01 SCCM MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Photometer flow mode menu is used to select the photometer measurement mode Available choices in...

Страница 63: ...et the zero air and gas flows for each gas Gas D E and F are available if the six gas option is installed In the Main Menu choose Flow Modes Gas Setup GAS SETUP GAS A GAS A GAS B GAS B GAS C GAS C GAS D GAS D GAS E GAS E GAS F GAS F OPER MODE DIAGS ALARM GAS A SETUP GAS NAME GAS A GAS SOL A TANK CONC 100 000 PPM ZERO 2000 CCM SPAN 1 10 000 PPM SPAN 2 8 000 PPM SPAN 3 5 000 PPMª OPER MODE DIAGS ALA...

Страница 64: ...A for Gas A Solenoid B for Gas B and Solenoid C for Gas C the same default designation system applies to Solenoids D through F if the six gas option is installed Allowable selections are SOLENOID A SOLENOID B SOLENOID C SOLENOID D if installed SOLENOID E if installed and SOLENOID F if installed In the Main Menu choose Gas Setup Gas A F Gas Solenoid GAS A SOLENOID CURRENTLY SOLENOID A SET TO SOLENO...

Страница 65: ...d to select a flow rate between these two settings If the selected zero flow is lower or higher than the acceptable range TOO LOW or TOO HIGH appears on the screen In the Main Menu choose Gas Setup Gas A F Zero GAS A ZERO AIR FLOW MINIMUM 00400 SCCM MAXIMUM 10000 SCCM SET TO 01001 SCCM MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Span menu displays the span concentration and total flo...

Страница 66: ... Changing this valve may affect allowable limits for span flow It is advisable to check this setting In the Main Menu choose Gas Setup Gas A F Span 1 5 Conc GAS A SPAN 1 CONC MINIMUM 00000 040 PPM MAXIMUM 00020 000 PPM SET TO 00010 001 PPM MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Span Flow screen displays the minimum and maximum flows for spans 1 through 5 of each gas Minimum and ...

Страница 67: ...M GAS 030 00 CCM OPER MODE DIAGS ALARM The Manual Zero Air Flow screen sets the manual zero air flow value for the previously selected gas The screen identifies the minimum and maximum acceptable zero air flow rates and lets the user select a flow rate between these two settings If the selected zero air flow is lower or higher than the acceptable range TOO LOW or TOO HIGH appears on the screen In ...

Страница 68: ...MUM 004 00 SCCM MAXIMUM 100 00 SCCM SET TO 030 01 SCCM MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Model 146i can be equipped with an optional internal ozonator The production of ozone is regulated by either changing the flow of zero air or by changing the intensity of the ozone producing lamp The Ozonator Setup menu sets the amount of zero air flow From this menu the ozone generatio...

Страница 69: ...termine a calibration curve an external ozone primary standard such as the Model 49i Primary Standard must be used Due to changes in light intensity flow and ambient temperature the calibration curve is accurate only for a short time after a transfer standard reading is taken Since the setting is not remembered once the instrument is powered down the calibration curve is not retained and must be r...

Страница 70: ...u In the Main Menu choose Permeation Oven Setup PERMEATION OVEN PERMEATION K 1 000 PERMEATION RATE 1000 0 LEVEL 1 0 000 PPM LEVEL 2 0 000 PPM LEVEL 3 0 000 PPM LEVEL 4 0 000 PPM LEVEL 5 0 000 PPM OPER MODE DIAGS ALARM The Permeation K constant screen allow the user to set the multiplier for the permeation tube for a given oven temperature Allowable values are 0 000 to 9 999 If the values selected ...

Страница 71: ...ings In the Main Menu choose Permeation Oven Setup Permeation Rate PERMEATION RATE NG NG MIN CURRENTLY 1000 0 SET TO 01020 0 MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Permeation Level 1 5 screens are used to set minimum and maximum permeation levels These levels can be selected from the Operation or Flow Modes screens Note When a gas is selected and mixed with the permeation oven o...

Страница 72: ... range and to set the custom ranges In the Main Menu choose Photometer Setup Range RANGE GAS UNITS PPM RANGE 5 00 SET CUSTOM RANGES OPER MODE DIAGS ALARM The O3 Range screen defines the concentration range of the analog outputs For example an O3 range of 0 5 ppm sets the analog output to concentrations between 0 and 5 ppm Available operating ranges include 0 05 0 1 0 2 0 5 1 0 2 0 5 0 C1 C2 and C3...

Страница 73: ...IAGS ALARM The analog outputs are arranged on the rear panel connector as shown in Figure 3 4 See Table 3 3 for channels and pin connections Figure 3 4 Pin Out of Rear Connector Table 3 2 Default Analog Outputs Channel Pin Description 1 14 Gas Conc Analog Output 2 33 Gas Conc Analog Output 3 15 None 4 34 None 5 17 None 6 36 None Ground 16 18 19 35 37 Signal Ground ...

Страница 74: ... DIAGS ALARM The Custom Ranges screen is used to define the custom ranges The display shows the current custom range The next line of the display is used to set the range To use the custom full scale range be sure to select it Custom range 1 2 or 3 in the O3 Ranges screen For more information about selecting ranges see O3 Range above In the Main Menu choose Photometer Setup Range Set Custom Ranges...

Страница 75: ...ds In the Main Menu choose Photometer Setup Averaging Time AVERAGING TIME CURRENTLY 90 SEC SET TO 120 SEC ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The Calibration Factors menu displays the calibration factors and is used to make minor compensations to the O3 concentration In the Main Menu choose Photometer Setup Calibration Factors CALIBRATION FACTORS O3 BKG 0 0000 O3 COEF 1 000 RESET USER ...

Страница 76: ...e will show ERROR if the measured concentration is not a valid span value either higher than the selected range or 0 or lower In the Main Menu choose Photometer Setup Calibration Factors O3 Coef O3 COEFFICIENT O3 600 SET COEF TO 1 000 ª INC DEC SAVE VALUE OPER MODE DIAGS ALARM The Reset User Calibration Default screen allows the user to reset the calibration configuration values to factory default...

Страница 77: ... zero calibration ensure the analyzer samples zero air for at least 5 minutes It is important to note the averaging time when calibrating The longer the averaging time the more accurate the calibration will be To be most accurate use the 300 second averaging time In the Main Menu choose Photometer Setup Calibration Cal Zero O3 BACKGROUND O3 0 0000 CURRENTLY 0 0000 SET O3 TO ZERO OPER MODE DIAGS AL...

Страница 78: ...ts the Model 146i s internal computer program to conduct a series of calibration events at preset times and durations Up to 32 calibration events can be programmed Next Event is read only and shows the status of the next event number and time there is no setting screen Each event can be assigned gas span ozonator and permeation levels photometer mode and event set time This function is only availa...

Страница 79: ... current event When disabled the program will not be run at its assigned interval This screen is also used to cancel a running program In the Main Menu choose Program Program Cycle PROGRAM CYCLE STATUS CURRENTLY DISABLED SET TO ENABLED TOGGLE VALUE OPER MODE DIAGS ALARM The Period Hours screen is used select how many hours starting between cycles of the program Valid values are 0 to 999 If 0 is se...

Страница 80: ...A F Zero span level for that gas 1 5 Zero ozonator and permeation levels 1 5 OFF photometer mode I internal E external C control and event duration time in minutes Selecting an event allows detailed setup of that event A maximum of 32 events can be controlled from this menu Note When events are running none of the settings may be changed via the front panel interface except for the program cycle e...

Страница 81: ...part of the event When set to NONE it will leave that event alone it stays the same as it was before the event started If set ON it will turn user outputs on If set OFF it will turn outputs to off In the Main Menu choose Program Events Event 1 32 Press or to toggle and to set following items EVENT 10 ENABLED 32 MIN GAS A 0 212 SCCM SPAN 1 2314 PPM PHOT OFF 0 PPM PERM OFF 0 PPM OZONE OFF 0 USER1 DO...

Страница 82: ...by a thermistor on the Interface board When temperature compensation is off the display shows 0 0 C In the Main Menu choose Instrument Controls Temperature Compensation TEMPERATURE COMPENSATION COMP TEMP 32 6 o C CURRENTLY ON SET TO OFF TOGGLE VALUE OPER MODE DIAGS ALARM The Pressure Compensation screen is used to turn the pressure correction on or off When pressure compensation is on the first li...

Страница 83: ... DATA ERASE LOG SELECT CONTENT COMMIT CONTENT RESET TO DEFAULT CONTENT CONFIGURE DATA LOGGING OPER MODE DIAGS ALARM The Select SREC LREC is used to select short record or long record format for other operations in this menu In the Main Menu choose Instrument Controls Datalogging Settings Select SREC LREC SELECT LOG TYPE CURRENTLY SREC SET TO LREC TOGGLE VALUE OPER MODE DIAGS ALARM The View Logged ...

Страница 84: ...000000 TOTAL LRECS 20 MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Record Display screen read only displays the selected records time date flags 10 01 06 20 05 C008890 10 02 06 20 05 C008890 10 03 06 20 05 C008890 10 04 06 20 05 C008890 ª PGUP DN PAN L R OPER MODE DIAGS ALARM The Date and Time screen is used to set a start date and time for which to view logged data For example if 20 ...

Страница 85: ...nd long records In the Main Menu choose Instrument Controls Datalogging Settings Erase Log The Select Content submenu displays a list of 32 record fields to use and a submenu list of the analog output signal group choices to choose from Choices are Concentrations Other Measurements and Analog Inputs if the I O expansion board is installed This is a temporary list of items for the selected record t...

Страница 86: ...CONCENTRATIONS OTHER MEASUREMENTS ANALOG INPUTS OPER MODE DIAGS ALARM The Concentrations screen allows the user to select the output signal that is tied to the selected field item The selected item is shown by after it Note that at this point pressing indicates that these are proposed changes as opposed to implemented changes To change the selected record format and erase record log file data see ...

Страница 87: ...s OTHER MEASUREMENTS NONE TARGET GFLOW ACTUAL GFLOW TARGET ZFLOW ACTUAL ZFLOW TARGET TFLOW ACTUAL TFLOW ª OPER MODE DIAGS ALARM PRESSURE BENCH TEMP LAMP TEMP O3 LAMP TEMP INTENSITY NOISE The Analog Inputs screen allows the user to select the output signal none or analog inputs 1 8 that is tied to the selected field item The selected item is shown by after it Note that at this point pressing indica...

Страница 88: ...alog output signal group choices see Select Content above In the Main Menu choose Instrument Controls Datalogging Settings Reset to Default Content The Configure Datalogging menu deals with datalogging configuration for the currently selected record type In the Main Menu choose Instrument Controls Datalogging Settings Configure Datalogging Commit Content Reset to Default Content Configure Datalogg...

Страница 89: ...nfigure Datalogging Logging Period Min SET PERIOD FOR SREC CURRENTLY 60 MIN SET TO OFF MIN ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Memory Allocation Percent screen is used to select the percentage of each record type for both short records and long records Percentages between 0 and 100 are available in increments of 10 Changing this value results in log erasure for both short records and lon...

Страница 90: ...figure Datalogging Data Treatment SET LREC DATA TYPE CURRENTLY AVG SET TO MAX ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Communication Settings menu is used with communications control and configuration In the Main Menu choose Instrument Controls Communication Settings COMMUNICATION SETTINGS BAUD RATE INSTRUMENT ID COMMUNICATION PROTOCOL STREAMING DATA CONFIG RS 232 RS 485 SELECTION TCP IP SETT...

Страница 91: ...ments are connected to one computer Valid Instrument ID numbers are from 0 to 127 The Model 146i has a default Instrument ID of 51 For more information about the Instrument ID see Appendix B C Link Protocol Commands or Appendix C MODBUS Protocol In the Main Menu choose Instrument Controls Communication Settings Instrument ID INSTRUMENT ID CURRENTLY 51 SET TO 52 ª CHANGE VALUE SAVE VALUE OPER MODE ...

Страница 92: ...and Analog Inputs if the I O expansion board option is installed In the Main Menu choose Instrument Controls Communication Settings Streaming Data Config STREAMING DATA CONFIG INTERVAL 10 SEC ADD LABELS NO PREPEND TIMESTAMP YES ITEM 1 CONC ITEM 2 TGFLO ITEM 3 AGFLO ITEM 4 TZFLO ª OPER MODE DIAGS ALARM CHOOSE STREAM DATA CONCENTRATIONS OTHER MEASUREMENTS ANALOG INPUTS OPER MODE DIAGS ALARM The Stre...

Страница 93: ...Communication Settings Streaming Data Config Select Item Concentrations CONCENTRATIONS NONE GAS CONC O3 CONC PERM CONC OPER MODE DIAGS ALARM The Other Measurements screen allows the user to select the output signal that is tied to the selected streaming data item The selected item is shown by after it In the Main Menu choose Instrument Controls Communication Settings Streaming Data Config Select I...

Страница 94: ...IN 5 ANALOG IN 6 ª OPER MODE DIAGS ALARM The RS 232 RS 485 Selection screen allows the user to choose between the RS 232 or RS 485 specification for serial communication Note Disconnect the serial cable before changing RS 232 and RS 485 selection to prevent damage to the connected equipment In the Main Menu choose Instrument Controls Communication Settings RS 232 RS 485 Selection Analog Inputs RS ...

Страница 95: ...MASK 255 255 255 0 GATEWAY 0 0 0 0 HOST NAME iSeries OPER MODE DIAGS ALARM The Use DHCP screen is used to specify whether to use DHCP or not In the Main Menu choose Instrument Controls Communication Settings TCP IP Settings Use DCHP DHCP CURRENTLY OFF SET TO ON TOGGLE VALUE CYCLE POWER TO CHANGE DHCP OPER MODE DIAGS ALARM The IP Address screen is used to edit the IP address The IP address can only...

Страница 96: ... 255 255 255 000 MOVE CURSOR ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The Default Gateway screen is used to edit the gateway address In the Main Menu choose Instrument Controls Communication Settings TCP IP Settings Gateway DEFAULT GATEWAY CURRENT 10 209 42 1 SET TO 10 209 42 1 1 MOVE CURSOR ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The host name screen is used to edit the host name W...

Страница 97: ...nu choose Instrument Controls I O Configuration Note The digital outputs may take up to one second after the assigned state occurs to show up on the outputs I O CONFIGURATION OUTPUT RELAY SETTINGS DIGITAL INPUT SETTINGS EXTERNAL SOLENOIDS ANALOG OUTPUT CONFIG ANALOG INPUT CONFIG OPER MODE DIAGS ALARM The Output Relay Settings menu displays a list of the 10 analog output relays available and allows...

Страница 98: ...n or normally closed Press to toggle and set the logic state open or closed OUTPUT RELAY SETUP LOGIC STATE OPEN INSTRUMENT STATE OPER MODE DIAGS ALARM The Instrument State menu allows the user to select the instrument state that is tied to the selected relay output A submenu lists signal types of either alarm or non alarm to choose from In the Main Menu choose Instrument Controls I O Configuration...

Страница 99: ...DIAGS ALARM PHOT LAMP TEMP PHOT INTENSITY O3 LEVEL The Non Alarm status screen allows the user to select the non alarm status for the selected relay output The selected item is shown by after it For more information on the I O connections see Remote Interconnections in the Installation chapter In the Main Menu choose Instrument Controls I O Configuration Output Relay Settings Select Relay Instrume...

Страница 100: ...I O Configuration Digital Input Settings DIGITAL INPUT SETTINGS 1 NOP GAS BIT 1 2 NOP GAS BIT 2 3 NOP GAS BIT 3 4 NOP SPAN BIT 1 5 NOP SPAN BIT 2 6 NOP SPAN BIT 3 7 NOP O3 PERM BIT 1 ª OPER MODE DIAGS ALARM The Logic State screen is used to change the I O relay to either normally open or normally closed The default state is open which indicates that a relay connected between the digital input pin ...

Страница 101: ...CHOOSE ACTION NONE GAS BIT 1 GAS BIT 2 GAS BIT 3 SPAN BIT 1 SPAN BIT 2 SPAN BIT 3 ª OPER MODE DIAGS ALARM O3 PERM BIT 1 O3 PERM BIT 2 O3 PERM BIT 3 O3 PERM BIT 4 PHOTO BIT 1 PHOTO BIT 2 AOUTS TO ZERO AOUTS TO FS The Model 146i can drive up to eight external solenoids You can select the external solenoids with the External Solenoids menu Each solenoid can be connected to the following Gas A B or C ...

Страница 102: ...ed Press to toggle and set the logic state open or closed EXT SOLENOID SETUP LOGIC STATE OPEN INSTRUMENT STATE OPER MODE DIAGS ALARM The Instrument State menu allows the user to select the instrument state that is tied to the selected solenoid output A submenu lists signal types of either alarm or non alarm to choose from In the Main Menu choose Instrument Controls I O Configuration Ext Solenoid S...

Страница 103: ... ALARM AMBIENT TEMP O3 LAMP TEMP PERM GAS TEMP PRESSURE PHOT BENCH TEMP ª OPER MODE DIAGS ALARM PHOT LAMP TEMP PHOT INTENSITY O3 LEVEL The Non Alarm status screen allows the user to select the non alarm status for the selected solenoid output The selected item is shown by after it In the Main Menu choose Instrument Controls I O Configuration Ext Solenoid Settings Select Solenoid Instrument State N...

Страница 104: ...u choose Instrument Controls I O Configuration Analog Output Config OUTPUT CHANNELS ALL VOLTAGE CHANNELS ALL CURRENT CHANNELS VOLTAGE CHANNEL 1 VOLTAGE CHANNEL 2 VOLTAGE CHANNEL 3 VOLTAGE CHANNEL 4 VOLTAGE CHANNEL 5 ª OPER MODE DIAGS ALARM ANALOG OUTPUT CONFIG SELECT RANGE SET MINIMUM VALUE SET MAXIMUM VALUE CHOOSE SIGNAL TO OUTPUT OPER MODE DIAGS ALARM The Select Output Range screen is used to se...

Страница 105: ...screen In the Main Menu choose Instrument Controls IO Configuration Analog Output Config Select Channel Set Minimum or Maximum Value MINIMUM OUTPUT PERCENT SELECTED OUTPUT V ALL CURRENTLY N A SET TO 0000 5 ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM Table 3 3 Analog Output Zero to Full Scale Table Output Zero Value Full Scale 100 Value Gas Conc Zero 0 10 000 ppm O3 Conc Zero 0 Range setting Perm Con...

Страница 106: ...Signal Type to Output screen displays a submenu list of the analog output signal group choices Group choices are Concentrations Other Measurements and Analog Inputs if the I O expansion board option is installed This allows the user to select the output signal to the selected output channel The Concentrations screen is shown below See Table 3 4 below for a list of items for each signal group choic...

Страница 107: ...nput 8 Lamp Temperature O3 Lamp Temperature Intensity Noise The Analog Input Configuration menu displays a list of the 8 analog input channels available for configuration This screen is only displayed if the I O expansion board option is installed Configuration includes entering descriptor units decimal places choice of 1 10 points in the table and corresponding number of points selected In the Ma...

Страница 108: ...rs in length and defaults to IN1 to IN8 user input channel number In the Main Menu choose Instrument Controls I O Configuration Analog Input Config Select Channel Descriptor ANALOG INPUT DESCRIPTOR CURRENTLY IN1 IN1 ABCDEFGHIJKLMN BKSP OPQRSTUVWXYZ PAGE 0123456789 SAVE OPER MODE DIAGS ALARM The Units screen allows the user to enter the units for the selected analog input channel The units are disp...

Страница 109: ... Instrument Controls I O Configuration Analog Input Config Select Channel Decimal Places DECIMAL PLACES CURRENTLY 2 SET TO 3 ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The Number of Table Points screen allows the user to select how many points are used in the conversion table The points range from 2 to 10 with a default of 2 In the Main Menu choose Instrument Controls I O Configuration Analog...

Страница 110: ...a two point table with point 1 0 00 V 000 0 U and point 2 10 00 V 10 0 U In the Main Menu choose Instrument Controls I O Configuration Analog Input Config Select Channel Select Point Volts TABLE POINT 01 VOLTS CURRENTLY 0 00 SET TO 00 00 MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The User Value screen allows the user to set the output value for the corresponding input voltage for the se...

Страница 111: ...eratures In the Main Menu choose Instrument Controls Screen Contrast SCREEN CONTRAST CURRENTLY 50 SET TO 60 ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The Service Mode screen is used to turn the service mode on or off The service mode locks out any remote actions and includes parameters and functions that are useful when making adjustments or diagnosing the Model 146i For more information abo...

Страница 112: ...cess to diagnostic information and functions This menu is useful when troubleshooting the instrument The analog input readings and analog input voltages are only displayed if the I O expansion board option is installed In the Main Menu choose Diagnostics DIAGNOSTICS PROGRAM VERSION VOLTAGES FLOWS TEMPERATURES PRESSURE ANALOG INPUT READINGS ANALOG INPUT VOLTAGES ª OPER MODE DIAGS ALARM DIGITAL INPU...

Страница 113: ...N PRODUCT MODEL 146i VERSION 01 02 12 095 OPER MODE DIAGS ALARM The Voltages menu displays the current diagnostic voltage readings This screen enables the power supply to be quickly read for low or fluctuating voltages without having to use a voltage meter The I O board is only displayed if the I O expansion board option is installed In the Main Menu choose Diagnostics Voltages VOLTAGES MOTHERBOAR...

Страница 114: ...ages INTERFACE BOARD VOLTAGES 3 3 SUPPLY 3 3 V 5 0 SUPPLY 5 0 V 15 0 SUPPLY 15 0 V 15 0 SUPPLY 15 0 V 24 0 SUPPLY 24 0 V PHOTOMTR 12 0 V O3 LAMP 11 6 Vª OPER MODE DIAGS ALARM The I O Board screen read only is used to display the current voltage readings on the I O expansion board This menu is only displayed if the I O expansion board option is installed In the Main Menu choose Diagnostics Voltages...

Страница 115: ...creen read only displays the current ambient temperature bench temperature bench lamp temperature ozone lamp temperature and permeation oven temperature In the Main Menu choose Diagnostics Temperatures TEMPERATURES AMBIENT 30 6 o C BENCH 30 7 o C BENCH LAMP 54 0 o C O3 LAMP 67 0 o C PERM OVEN GAS 40 0 o C PERM OVEN HTR 40 0 o C OPER MODE DIAGS ALARM The Pressure screen read only displays the curre...

Страница 116: ...s screen read only displays the 8 raw analog voltage readings if the I O expansion board option is installed In the Main Menu choose Diagnostics Analog Input Voltages ANALOG INPUT VOLTAGES ANALOG IN 1 6 24 V ANALOG IN 2 4 28 V ANALOG IN 3 0 00 V ANALOG IN 4 0 00 V ANALOG IN 5 0 00 V ANALOG IN 6 0 00 V ANALOG IN 7 0 00 Vª OPER MODE DIAGS ALARM The Digital Inputs screen read only displays the state ...

Страница 117: ...he state of the 10 digital outputs and allows toggling of the state to either on 1 or off 0 The solenoids are restored to their original states upon exiting this screen In the Main Menu choose Diagnostics Solenoid States SOLENOID STATE SOLENOID 1 1 SOLENOID 2 0 SOLENOID 3 0 SOLENOID 4 0 SOLENOID 5 0 SOLENOID 6 0 SOLENOID 7 0ª OPER MODE DIAGS ALARM The Test Analog Outputs menu contains a number of ...

Страница 118: ... normal operation The example below shows the selected output state ALL is set to normal In the Main Menu choose Diagnostics Test Analog Outputs ALL Voltage Channel 1 6 or Current Channel 1 6 SET ANALOG OUTPUTS SETTING ALL OUTPUT SET TO NORMAL SET TO FULL SCALE ª SET TO ZERO RESET TO NORMAL OPER MODE DIAGS ALARM The Instrument Configuration screen displays information on the hardware configuration...

Страница 119: ...he lower or upper limit the status of that item will go from OK to either LOW or HIGH respectively If the alarm is not a level alarm the status will go from OK to FAIL The number of alarms detected is displayed to indicate how many alarms have occurred If no alarms are detected the number zero is displayed To see the actual reading of an item and its minimum and maximum limits move the cursor to t...

Страница 120: ... alarm limits range from 8 to 47 C If the ambient temperature reading goes beyond either the minimum or maximum alarm limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms Ambient Temp AMBIENT TEMPERATURE ACTUAL 30 1 o C MIN 15 0 o C MAX 45 0 o C OPER MODE DIAGS ALARM The Minimum Ambient Temperature alarm limit screen is used to ch...

Страница 121: ...um alarm limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms O3 Lamp Temp O3 LAMP TEMPERATURE ACTUAL 68 8 o C MIN 60 0 o C MAX 80 0 o C OPER MODE DIAGS ALARM The Minimum O3 Lamp Temperature alarm limit screen is used to change the minimum O3 lamp temperature alarm limit The minimum and maximum O3 lamp temperature screens function...

Страница 122: ... Temperature alarm limit screen is used to change the minimum bench temperature alarm limit The minimum and maximum permeation oven temperature screens function the same way In the Main Menu choose Alarms Perm Oven Temp Min or Max POVEN GAS EMPERATURE ACTUAL MIN 40 0 o C SET MIN TO 44 0 o C ª INC DEC SAVE VALUE OPER MODE DIAGS ALARM The Pressure screen displays the current reaction chamber pressur...

Страница 123: ... mmHg SET MIN TO 250 0 mmHg ª INC DEC SAVE VALUE OPER MODE DIAGS ALARM The Photometer Bench Temperature screen displays the current bench temperature and sets the minimum and maximum alarm limits Acceptable alarm limits range from 10 to 50 C If the bench temperature reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Mai...

Страница 124: ...and maximum alarm limits Acceptable alarm limits range from 45 to 65 C If the bench temperature reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms Phot Lamp Temp PHOT LAMP TEMPERATURE ACTUAL 32 3 o C MIN 50 0 o C MAX 60 0 o C OPER MODE DIAGS ALARM The Minimum Photometer Lamp Temp...

Страница 125: ...m limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu In the Main Menu choose Alarms Phot Intensity PHOTOMETER INTENSITY ACTUAL 98425 Hz MIN 45000 Hz MAX 150000 Hz OPER MODE DIAGS ALARM The Minimum Photometer Intensity alarm limit screen is used to change the minimum intensity alarm limit The minimum and maximum photometer intensity screens function the same w...

Страница 126: ...IBRATION BENCH TEMP CALIBRATION ª OPER MODE DIAGS ALARM ANALOG OUT CALIBRATION ANALOG INPUT CALIBRATION PERM OVEN SETTINGS LAMP SETTING INTENSITY CHECK O3 RESPONSE COEFFICIENT DISPLAY PIXEL TEST RESTORE USER DEFAULTS The Flow Control Selection menu is used to select the installed zero air controller and gas controller The zero air and gas controller screens are used when installing new mass flow c...

Страница 127: ...hese settings The mass flow controllers are accurate to only 2 upon delivery from the manufacturer The instrument includes factory set calibration curves to improve this accuracy To achieve an equivalent accuracy when installing new controllers see Zero Flow Calibration later in this chapter In the Main Menu choose Service Flow Control Selection Zero Scale ZERO AIR FLOW CONTROLLER CURRENTLY 5 SLM ...

Страница 128: ...PER MODE DIAGS ALARM The Calibrate Pressure Temperature screen is used only prior to calibrating the flow controllers These values are used to convert from volumetric flow to standard flow in the flow controller calibration screens The flow controllers are calibrated prior to shipment However if you need to re calibrate the flow controllers you can use this screen to enter the pressure and tempera...

Страница 129: ...e only when the instrument is in service mode For more information of the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Zero Flow Calibration ZERO AIR FLOW CAL 5 FS 0 500 SLM 20 FS 2 000 SLM 35 FS 3 500 SLM 50 FS 5 000 SLM 65 FS 6 500 SLM 80 FS 8 000 SLM 95 FS 9 500 SLM OPER MOD...

Страница 130: ...nstrument is in service mode For more information of the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Gas Flow Calibration GAS FLOW CAL SOLENOID A 5 FS 0 500 SCCM 20 FS 2 000 SCCM 35 FS 3 500 SCCM 50 FS 5 000 SCCM 65 FS 6 500 SCCM 80 FS 8 000 SCCM OPER MODE DIAGS ALARM 95 FS 9 ...

Страница 131: ...AS DRIVE 5 STD FLOW 010 22 SCCM VOL FLOW 010 24 SCCM MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Pressure Calibration menu is used to calibrate the pressure sensor to zero span or restore factory default values The pressure calibration is visible only if the photometer option is installed and when the calibrator is in service mode For more information on the service mode see Service ...

Страница 132: ...PRESSURE ZERO CURRENTLY 753 0 mmHg SET TO 0 0 mmHg CONNECT VACUUM PUMP AND SAVE ZERO PRESSURE OPER MODE DIAGS ALARM The Calibrate Pressure Span screen is used to view and set the pressure sensor calibration span point Note The plumbing going to the pressure sensor should be disconnected so the sensor is reading ambient pressure before performing the span calibration The operator should use an inde...

Страница 133: ... Calibration screen is used to view and set the ambient temperature sensor calibration The ambient temperature calibration is visible only when the instrument is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Ambient Temp Calibration Re...

Страница 134: ... in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Bench Temp Calibration CALIBRATE BENCH TEMP CURRENTLY 32 3 o C SET TO 032 5 o C MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Analog Output Calibration menu is a selection of 6 voltage channels and 6 current channels if I O expansion board option is installe...

Страница 135: ...connect a meter to the output and adjust the output until it reads 0 0 V on the meter In the Main Menu choose Service Analog Out Calibration Select Channel Calibrate Zero ANALOG OUTPUT CAL ZERO CONNECT METER TO OUTPUT SELECTED OUTPUT V1 SET TO 100 SAVE VALUE ª INC DEC SET OUTPUT TO 0 0 V OPER MODE DIAGS ALARM The Analog Output Calibrate Full Scale screen is used to calibrate the full scale state o...

Страница 136: ...ible only when the instrument is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician In the Main Menu choose Service Analog Input Calibration ANALOG INPUT CAL INPUT CHANNEL 1 INPUT CHANNEL 2 INPUT CHANNEL 3 INPUT CHANNEL 4 INPUT CHANNEL 5 INPUT CHANNEL 6 INPUT CHANNEL 7 ª ...

Страница 137: ...ect Channel Calibrate Full Scale Hook up a voltage source of 10 V to the analog input channel ANALOG INPUT CAL SPAN PROVIDE VOLTAGE TO INPUT SELECTED INPUT INPUT 1 CURRENTLY 6 24 V SET TO 10 00 V CALIBRATE INPUT TO ZERO OPER MODE DIAGS ALARM The Permeation Oven Settings menu is used for setting up and calibrating the permeation oven option The permeation oven settings are visible only if the perme...

Страница 138: ...er bath or known resistance In the Main Menu choose Service Perm Oven Settings Cal Gas Thermistor CALIBRATE GAS THERMISTOR WATER BATH KNOWN RESISTOR OPER MODE DIAGS ALARM The Calibrate Gas Thermistor Water Bath screen is used to view and set the permeation oven gas temperature to a known temperature value In the Main Menu choose Service Perm Oven Settings Cal Gas Thermistor Water Bath CAL GAS THER...

Страница 139: ...ODE DIAGS ALARM The Calibrate Oven Thermistor screen is used to view and set the permeation oven thermistor resistance to a known resistor value In the Main Menu choose Service Perm Oven Settings Cal Oven Thermistor CAL OVEN THERM RESISTOR CURRENTLY 3850 Ohms SET TO 04000 Ohms MOVE CURSOR ª CHANGE VALUE SAVE OPER MODE DIAGS ALARM The Permeation Oven Setpoint screen is used to select the permeation...

Страница 140: ...hoose Service Perm Oven Settings Factory Cal Gas Therm FACTORY CAL GAS THERM LOW POINT HIGH POINT SET DEFAULTS OPER MODE DIAGS ALARM The Calibrate Gas Thermistor Low Point screen is used to view and set the permeation oven thermistor resistance The low and high point screens function the same way In the Main Menu choose Service Perm Oven Settings Factory Cal Gas Therm Low or High Point CAL GAS THE...

Страница 141: ...en Settings Factory Cal Oven Therm FACTORY CAL OVEN THERM LOW POINT HIGH POINT SET DEFAULTS OPER MODE DIAGS ALARM The Calibrate Oven Thermistor Low Point screen is used to view and set the permeation oven thermistor resistance The low and high point screens function the same way In the Main Menu choose Service Perm Oven Settings Factory Cal Oven Therm Low or High Point Set Defaults Factory Calibra...

Страница 142: ... lamp drive settings are displayed Adjust the lamp setting until the intensity is about 10000 Hz The lamp setting is visible only if the photometer option is installed and when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter In the Main Menu choose Service Lamp Setting BENCH LAMP SETTING INT 100246 Hz LAMP SETTING 61 1 ª CHANGE VAL...

Страница 143: ... For more information on the service mode see Service Mode earlier in the chapter In the Main Menu choose Service Intensity Check INTENSITY CHECK REFERENCE GAS SAMPLE GAS OPER MODE DIAGS ALARM The Reference Gas screen read only sets the valves to route the reference gas through the photometer and displays the intensity and noise In the Main Menu choose Service Intensity Check Reference Gas PHOTOME...

Страница 144: ... the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter In the Main Menu choose Service O3 Response Coefficient O3 RESPONSE COEFFICIENT CURRENTLY 1 000 SET TO 1 250 ª CHANGE VALUE SAVE VALUE OPER MODE DIAGS ALARM The Display Pixel Test is used to test the LCD display The display pixel test is visible only when the instrument is in service...

Страница 145: ... of the settings may be changed via the front panel user interface The items visible under the password menu are determined by the instrument s password status In the Main Menu choose Password PASSWORD MENU SET PASSWORD LOCK INSTRUMENT CHANGE PASSWORD REMOVE PASSWORD UNLOCK INSTRUMENT OPER MODE DIAGS ALARM The Set Password screen is used to set the password to unlock the front panel The set passwo...

Страница 146: ...t is unlocked and the password is set In the Main Menu choose Password Lock Instrument LOCK FRONT PANEL XXXPRESSING ENTER WILLXXXX PREVENT USER FROM CHANGING XCONFIG FROM FRONT PANELXX LOCK AND RETURN TO RUN OPER MODE DIAGS ALARM The Change Password is used to change the password used to unlock the instrument s front panel The change password is shown if the instrument is unlocked In the Main Menu...

Страница 147: ...ssword Remove Password REMOVE PASSWORD XXXPRESSING ENTER WILLXXXX XREMOVE CURRENT PASSWORDXX XXXAND DISABLE LOCKINGXXXX REMOVE PASSWORD OPER MODE DIAGS ALARM The Unlock Instrument screen is used to enter the password to unlock the front panel The unlock instrument is shown if the instrument is locked In the Main Menu choose Password Unlock Instrument ENTER NEW PASSWORD RANGXXXXXE ABCDEFGHIJKLMN BK...

Страница 148: ......

Страница 149: ...curate calibration procedure use a volumetric NIST traceable calibrator with the following step by step calibration procedure 1 Connect a source of clean dry air to the inlet of the mass flow controller 2 Measure barometric pressure and room temperature 3 Connect a suitable flow meter to the mass flow controller outlet 4 Set Model 146i to Gas Drive or Zero Air Flow Calibration as described in the ...

Страница 150: ... primary standard must be used If an ozone analyzer is also available the generation of the calibration curve becomes easier A procedure for both is given below Calibration Using a Model 49i PS Use the following procedure to calibrate the Model 146i using a Model 49i PS Refer to the Photometer Calibration Flow Schematic Figure 4 1 1 Connect the 49i PS OUTPUT to the 146i EXTERNAL SAMPLE port 2 Set ...

Страница 151: ...low Schematic Ozonator Control Check Use the following procedure to perform an ozonator control check Refer to the ozonator control check flow schematic Figure 4 2 1 Connect the 146i OUTPUT port to the 49i PS INPUT port 2 Set ozone concentration at different levels 3 Compare the ozone concentration readings on the 146i and 49i PS ...

Страница 152: ...Calibration Ozonator Control Check 4 4 Model 146i Instruction Manual Thermo Fisher Scientific Figure 4 2 Ozonator Control Check Flow Schematic ...

Страница 153: ...s cleaning the optics and checking the pressure calibration should be performed on a regular basis This chapter includes the following maintenance information and replacement procedures Safety Precautions on page 5 2 Replacement Parts on page 5 2 Accessing the Service Mode on page 5 2 Outside Case Cleaning on page 5 2 Fan Filter Inspection and Cleaning on page 5 3 Photometer Cleaning on page 5 3 M...

Страница 154: ... Mode screen appears 2 Press to toggle the Service Mode to ON 3 Press to return to the Main Menu 4 Return to the procedure Outside Case Cleaning Clean the outside case using a damp cloth being careful not to damage the labels on the case WARNING If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Equipment Damage Some ...

Страница 155: ...hen the photometer is cleaned prior to recalibration The cleanliness of the photometer should also be checked any time the detector frequency drops below 65 kHz since one source of low output is light attenuation due to dirt in the cell Dirt particulates are usually effective ozone removers Use the following procedure to clean the photometer Figure 7 12 1 Turn instrument OFF unplug the power cord ...

Страница 156: ...hat the tube fits into 9 Replace the photometer components following the previous steps in reverse Note It is recommended that the Model 146i be recalibrated if the photometer has been completely disassembled Always check for leaks after replacing any component Refer to Leak Test and Pump Checkout in the Servicing chapter 10 Re install the instrument cover Monitoring Detector Frequency and Noise T...

Страница 157: ...fully warmed up lamp see Troubleshooting Guides on page 6 2 in the Troubleshooting chapter if the noise is excessive Degradation of detector frequency to below 65 kHz indicates either a dirty cell or low lamp output In addition to degrading the measured detector frequency dirt in the cell can decompose the ozone and give erroneous readings Therefore the cell should first be cleaned and the frequen...

Страница 158: ...trument If you need the capillary part number refer to the Replacement Parts List on page 7 5 Ozonator Capillary Replacement Ozonator option Use the following procedure to replace the ozonator capillary Figure 5 2 Equipment Required Ozonator capillary 1 Turn instrument OFF unplug the power cord and remove the cover 2 Unscrew the knurled fitting separate the components and remove the capillary Figu...

Страница 159: ...lowing procedure to replace the pressure regulator capillary Figure 5 3 Equipment Required Pressure regulator capillary 1 Turn instrument OFF unplug the power cord and remove the cover 2 Unscrew the knurled fitting separate the components and remove the capillary Figure 5 3 Capillary Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded...

Страница 160: ...ents with the photometer option use the following procedure to replace the pump capillary Figure 5 4 Equipment Required Pump capillary 1 Turn instrument OFF unplug the power cord and remove the cover 2 Loosen the fitting connecting the capillary to the pump and remove the capillary Figure 5 4 Capillary Equipment Damage Some internal components can be damaged by small amounts of static electricity ...

Страница 161: ...e Pump Replacement Photometer option on page 7 16 in the Servicing chapter Equipment Required Flatblade screwdriver Pump rebuild kit flapper valve and diaphragm 1 Turn instrument OFF unplug the power cord and remove the cover 2 Loosen the fittings and remove both lines going to the pump Capillary Equipment Damage Some internal components can be damaged by small amounts of static electricity A prop...

Страница 162: ... the Pump 4 Remove the screw the securing the diaphragm to piston and remove diaphragm 5 Assemble the pump by following the previous steps in reverse make sure the Teflon white side of the diaphragm is facing up and that the flapper valves cover the holes of the top and bottom plate 6 Test the pump for leaks Refer to Leak Test and Pump Checkout in the Servicing chapter Top Plate Flapper Plate Bott...

Страница 163: ...the same information found in the Diagnostic menu however readings are updated every second in the service mode compared with every 10 seconds in the Diagnostics menu The Technical Support Department at Thermo Fisher Scientific can also be consulted in the event of problems See Service Locations at the end of this chapter for contact information In any correspondence with the factory please note b...

Страница 164: ...20 volts Check instrument fuse Power supply Check power supply voltages Flow controller unstable Leak Perform a leak check see Servicing chapter Flow controller malfunction Replace Flow Controller Solenoid not switching in local mode Instrument in remote mode Put instrument in local mode Solenoid malfunction Check 24 VDC on solenoid connector Check solenoid cable Check solenoid for continuity and ...

Страница 165: ...ator board see Servicing chapter Low ozonator output Leak in ozonator or distribution manifold Check for leaks in ozonator and manifold system see Servicing chapter and repair leak Flow excessively high Check zero air flow valve and reduce flow Ozonator board failure Replace ozonator board see Servicing chapter Weak lamp Check to see that there is a bright blue light when removing the ozone lamp f...

Страница 166: ...rement interface board Replace measurement interface board Cell frequency low or zero Light setting too low Raise lamp setting Service Mode Lamp Setting Contaminated cell Clean cell Defective detector Replace detector module Defective photometer board Replace photometer board Defective measurement interface board Replace measurement interface board Cell noise excessive Contaminated cell Clean cell...

Страница 167: ...Verify averaging time is set properly Leak Perform leak test see Servicing chapter Contaminated optical bench Clean bench and then condition system overnight Table 6 2 Troubleshooting Alarm Messages Alarm Message Possible Cause Action Alarm O3 Lamp Temp Defective ozonator board Replace ozonator board Defective ozonator lamp heater Replace ozonator lamp heater Alarm Lamp Temp Defective photometer b...

Страница 168: ...bleshooting information Oz Level 3 Check Opt Does not reach the level 3 setting See Table 6 1 for troubleshooting information Oz Level 4 Check Opt Does not reach the level 4 setting See Table 6 1 for troubleshooting information Alarm O3 Conc Concentration has exceeded range limit Check to insure range corresponds with expected value If not select proper range Concentration low Check user defined l...

Страница 169: ...vice Disconnect external devices from board and recycle power If alarm persists replace board Internal cables not connected properly Check that all internal cables are connected properly Defective optional I O expansion board Replace board Table 6 2 Troubleshooting Alarm Messages continued Alarm Message Possible Cause Action ...

Страница 170: ...nics 2 Pin P1 DIGITAL OUTPUTS 24V D C P O W E RSU P P LY MO THE RBO AR D D IG ITALO U TP U T BO AR D I OE XP ANSIO N BO AR D J14 J3 F R O NT P ANE L BO AR D J1 LCD DISPLAY KEY PANEL J18 J2 J4 J3 J1 J10 J17 PJ1 PJ3 PJ2 FRONT PANEL POWER SW 16 Pin 4 Pin 8 Pin 34 Pin 3 Pin 2 Pin 3 Pin 3 Pin 3 Pin PJ6 3 Pin IPJ8 3 Pin 8 Pin 11 Pin 2 Pin EXPANSION RS485 ANALOG OUTPUTS DIGITAL INPUTS P1 A P1 B RS232 RS4...

Страница 171: ...UPPLY 8 Pin LAMP HEATER LAMP 6 Pin 2 Pin J2 J1 J3 PHOTOMETER POWER SUPPLY 8 Pin MASS FLOW CONTROLLER 2 6 Pin MASS FLOW CONTROLLER 1 6 Pin DETECTOR 6 Pin J4 PRESSURE 4 Pin J6 J7 J16 J15 J5 J10 J3 J2 PUMP AC 3 Pin AC 2 Pin BENCH TEMP THERM J4 J5 2 Pin 2 Pin J3 2 Pin J1 J2 2 Pin 2 Pin J7 J8 2 Pin 2 Pin J6 2 Pin RC SOL 2 Pin 2 Pin SAMP REF SOL 2 Pin OZ SOL PERM1 SOL 2 Pin 2 Pin PERM2 SOL FAN FAN 2 Pin...

Страница 172: ... Pin Descriptions on page 6 19 Measurement Interface Board Connector Pin Descriptions on page 6 20 Solenoid Connector Board Pin Descriptions on page 6 23 Ozonator Power Supply Connector Pin Descriptions on page 6 24 Photometer Power Supply Connector Pin Descriptions on page 6 25 Table 6 3 Motherboard Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description INTF DATA J...

Страница 173: ...xpansion Board 8 RS485 to Expansion Board SPARE DATA J4 1 5V 2 24V 3 24V 4 Ground 5 Ground 6 Ground 7 RS485 to Spare Board 8 RS485 to Spare Board I O J5 1 Power Fail Relay N C Contact 2 Ground 3 TTL Input 1 4 TTL Input 2 5 Ground 6 TTL Input 5 7 TTL Input 7 8 TTL Input 8 9 TTL Input 10 10 Ground 11 TTL Input 13 Table 6 3 Motherboard Connector Pin Descriptions continued Connector Label Reference De...

Страница 174: ... N O Contact 22 Ground 23 TTL Input 3 24 TTL Input 4 25 TTL Input 6 26 Ground 27 TTL Input 9 28 TTL Input 11 29 TTL Input 12 30 TTL Input 14 31 TTL Input 16 32 Ground 33 Analog Voltage Output 2 34 Analog Voltage Output 4 35 Ground 36 Analog Voltage Output 6 37 Ground SER EN J7 1 Serial Enable Jumper 2 3 3V 24V IN J10 1 24V 2 Ground DIGITAL I O J14 1 5V 2 24V 3 24V Table 6 3 Motherboard Connector P...

Страница 175: ...5 J15 1 RS485 to Rear Panel 2 RS485 to Rear Panel 3 5V 4 5V 5 5V 6 Ground 7 Ground 8 Ground 9 NC 10 NC 11 24V 12 24V 13 24V 14 24V 15 24V 24V MONITOR J17 1 24V Power Monitor 2 Ground FRONT PANEL BD J18 1 Ground 2 Ground 3 LCLK LCD Signal 4 Ground 5 Ground 6 LLP LCD Signal 7 LFLM LCD Signal Table 6 3 Motherboard Connector Pin Descriptions continued Connector Label Reference Designator Pin Signal De...

Страница 176: ... Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 23 Keypad Row 4 Input 24 Keypad Row 3 Input 25 Keypad Col 2 Select 26 Keypad Col 1 Select 27 Keypad Col 4 Select 28 Keypad Col 3 Select 29 Ground 30 Ground 31 Ground 32 Ground 33 24V 34 24V RS232 RS485 A P1 A 1 NC 2 Serial Port 1 RX RS485 IN 3 Serial Port 1 TX RS485 OUT 4 NC 5 Ground 6 NC Table 6 3 Motherboard Connector Pi...

Страница 177: ...S485 OUT 8 Serial Port 2 CTS RS485 IN 9 NC AC IN PJ1 1 AC HOT 2 AC NEUT 3 AC Ground AC 24VPWR PJ2 1 AC HOT 2 AC NEUT 3 AC Ground AC INTF BD PJ3 1 AC HOT 2 AC NEUT 3 AC Ground Table 6 4 Front Panel Board Connector Pin Diagram Connector Label Reference Designator Pin Signal Description MOTHER BOARD J1 1 Ground 2 Ground 3 LCLK LCD Signal 4 Ground 5 Ground 6 LLP LCD Signal Table 6 3 Motherboard Connec...

Страница 178: ...und 19 Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 23 Keypad Row 4 Input 24 Keypad Row 3 Input 25 Keypad Col 2 Select 26 Keypad Col 1 Select 27 Keypad Col 4 Select 28 Keypad Col 3 Select 29 Ground 30 Ground 31 Ground 32 Ground 33 24V 34 24V LCD DATA J2 1 LFLM_5V LCD Signal 2 LLP_5V LCD Signal 3 LCLK_5V LCD Signal 4 LCD_ONOFF_5V LCD Signal 5 5V Table 6 4 Front Panel B...

Страница 179: ...Row 3 Input 4 Keypad Row 4 Input 5 Keypad Col 1 Select 6 Keypad Col 2 Select 7 Keypad Col 3 Select 8 Keypad Col 4 Select LCD BACKLIGHT J4 1 LCD Backlight Voltage 1 2 NC 3 NC 4 LCD Backlight Voltage 2 Table 6 5 I O Expansion Board Optional Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description EXPANSION I O J1 1 Analog Voltage Input 1 2 Analog Voltage Input 2 3 Analo...

Страница 180: ...1 16 Current Output Return 17 Current Output 2 18 Current Output Return 19 Current Output 3 20 Current Output Return 21 Current Output 4 22 Current Output Return 23 Current Output 5 24 Current Output Return 25 Current Output 6 MOTHER BD J2 1 5V 2 24V 3 24V 4 Ground 5 Ground 6 Ground 7 RS485 to Motherboard 8 RS485 to Motherboard Table 6 5 I O Expansion Board Optional Connector Pin Descriptions cont...

Страница 181: ...PI Output 10 SPI Board Select 11 SPI Clock DIGITAL OUTPUTS J2 1 Relay 1 Contact a 2 Relay 2 Contact a 3 Relay 3 Contact a 4 Relay 4 Contact a 5 Relay 5 Contact a 6 Relay 6 Contact a 7 Relay 7 Contact a 8 Relay 8 Contact a 9 Relay 9 Contact a 10 Relay 10 Contact a 11 NC 12 Solenoid Drive Output 1 13 Solenoid Drive Output 2 14 Solenoid Drive Output 3 15 Solenoid Drive Output 4 16 Solenoid Drive Outp...

Страница 182: ...24V 31 24V 32 24V 33 24V 34 24V 35 24V 36 24V 37 24V Table 6 7 Measurement Interface Board Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description AC IN J1 1 AC HOT 2 AC NEUT 3 AC Ground AC PUMP J2 1 AC HOT 2 AC NEUT Switched 3 AC Ground BENCH TEMP J3 1 Bench Temperature Thermistor 2 Ground PRES J4 1 Pressure Sensor Input 2 Ground 3 15V Table 6 6 Digital Output Board...

Страница 183: ...rmistor 4 24V 5 Ground 6 Ozonator Lamp On off Control 7 Ground 8 Ground PHOTOMETER J7 1 Photometer Lamp Intensity Control Voltage Output 2 Photometer Lamp Intensity Control Voltage Input 3 Photometer Heater Thermistor 4 24V 5 Ground 6 Photometer Lamp On Off Control 7 Ground 8 Ground FAN J8 1 24V Fused 2 Ground FAN J9 1 24V Fused 2 Ground 24V IN J10 1 24V 2 Ground DATA J11 1 Ground Table 6 7 Measur...

Страница 184: ...troller 1 Input 2 Mass Flow Controller 1 Output 3 Ground 4 15V 5 15V 6 Ground MFC2 J16 1 Mass Flow Controller 2 Input 2 Mass Flow Controller 2 Output 3 Ground 4 15V 5 15V 6 Ground CONNECTOR BD J17 1 Gas A Solenoid Control 2 Gas C Solenoid Control 3 24V 4 Gas E Solenoid Control 5 Z A Solenoid Control 6 Gas B Solenoid Control 7 Gas D Solenoid Control 8 24V 9 Gas F Solenoid Control 10 EXT INT Solenoi...

Страница 185: ...r Board Pin Descriptions Connector Label Reference Designator Pin Signal Description BRN Gas A Solenoid Control ORG Gas C Solenoid Control RED 24V GRN Gas E Solenoid Control VIO Z A Solenoid Control WHT Gas B Solenoid Control YEL Gas D Solenoid Control RED 24V BLU Gas F Solenoid Control GRA EXT INT Solenoid Control GAS A J1 1 24V 2 Gas A Solenoid Control GAS B J2 1 24V 2 Gas B Solenoid Control GAS...

Страница 186: ...ce Designator Pin Signal Description LAMP J1 1 Ozonator Lamp Voltage Out 2 Ozonator Lamp Voltage Return LAMP HEATER J2 1 Ground 2 Ozonator Lamp Thermistor 1 3 Ozonator Lamp Heater Control 4 Ground 5 24V Heater Current Sense 6 Ozonator Lamp Thermistor 2 INTF J3 1 Ozonator Lamp Intensity Control Voltage Input 2 Ozonator Lamp Intensity Control Voltage Output 3 Ozonator Heater Thermistor 4 24V 5 Groun...

Страница 187: ... International Table 6 10 Photometer Power Supply Connector Pin Descriptions Connector Label Reference Designator Pin Signal Description LAMP J1 1 Photometer Lamp Voltage Out 2 Photometer Lamp Voltage Return LAMP HEATER J2 1 Ground 2 Photometer Lamp Thermistor 1 3 Photometer Lamp Heater Control 4 Ground 5 24V Heater Current Sense 6 Photometer Lamp Thermistor 2 INTF J3 1 Photometer Lamp Intensity C...

Страница 188: ...Troubleshooting Service Locations 6 26 Model 146i Instruction Manual Thermo Fisher Scientific ...

Страница 189: ...r additional service assistance see Service Locations on page 7 54 at the end of this chapter This chapter includes the following parts information testing adjustment and calibration procedures and component replacement procedures Safety Precautions on page 7 3 Firmware Updates on page 7 4 Replacement Parts List on page 7 5 Cable List on page 7 6 External Device Connection Components on page 7 7 R...

Страница 190: ...mp Replacement Photometer option on page 7 31 Photometer Lamp Voltage Adjustment Photometer option on page 7 33 Photometer Lamp Heater Replacement on page 7 33 Photometer Replacement Photometer option on page 7 34 Photometer Board Replacement Photometer option on page 7 35 Detector Replacement Photometer option on page 7 35 Photometer Thermistor Replacement on page 7 36 Photometer Temperature Cali...

Страница 191: ...lacement on page 7 49 Back Pressure Regulator Replacement on page 7 50 Pressure Regulator s Adjustment on page 7 51 Ambient Temperature Calibration on page 7 53 Service Locations on page 7 54 Safety Precautions Read the safety precautions before beginning any procedures in this chapter WARNING The service procedures in this manual are restricted to qualified service representatives If the equipmen...

Страница 192: ...t be worn while handling any internal component Figure 7 1 If an antistatic wrist strap is not available be sure to touch a grounded metal object before touching any internal components When the instrument is unplugged the chassis is not at earth ground Handle all printed circuit boards by the edges Do not remove the LCD panel or frame from the LCD module The polarizing plate is very fragile handl...

Страница 193: ... Supply 101399 00 Transformer 220 240VAC Optional 101863 00 Transformer 100VAC Optional 100880 00 Measurement Interface Board 102590 00 Ozonator 102775 00 Ozonator Lamp 100895 00 Ozonator Board 101023 00 Pressure Transducer 102455 00 Air Regulator Assembly Optional 103209 00 Detector Assembly 102351 00 Photometer Lamp Heater Assembly 102570 00 Photometer 8540 Photometer Lamp 102554 00 Photometer B...

Страница 194: ...r 10 slpm 8094 Mass Flow Controller 20 slpm 4120 Capillary photometer 4121 Capillary ozonator 4121 Capillary pressure gauge 4127 Capillary pump 103199 00 Solenoid sample reference 103205 00 Solenoid ozonator 103334 00 Solenoid perm 1 103200 00 Solenoid perm 2 103207 00 Solenoid reaction chamber 8130 Solenoid zero air 103125 00 Solenoid external internal 103206 00 Solenoid span gas 4291 Charcoal sc...

Страница 195: ...ement Interface Board to Ozonator Board 101267 00 Fan Power Cable 49P747 Mass Flow Controller Cable Assembly Table 7 2 Model 146i Cables continued Part Number Description Table 7 3 External Device Connection Components Part Number Description 101562 00 Terminal Block and Cable Kit DB25 optional 101556 00 Terminal Block and Cable Kit DB37 optional 102645 00 Cable DB37M to Open End Cable Six Feet op...

Страница 196: ...p Solenoids Span Gas Mass Flow Controllers External Internal Solenoid Back Pressure Regulator Reaction Chamber Solenoid Permeation Oven Reaction Pressure Regulator Solenoid Perm 2 Ozonator Capillary Ozonator Capillary Pressure Gauge Capillary Photometer Photometer Capillary Pump Pressure Transducer Chamber Solenoid Sample Reference Solenoid Ozonator DC Power Supply Fan Manifold Solenoid Perm 1 Sol...

Страница 197: ... see Figure 7 3 Figure 7 3 Removing the Measurement Bench and Lowering the Partition Panel Equipment Required Philips screwdriver 1 Turn instrument OFF and unplug the power cord 2 Disconnect the plumbing connections at the rear of the measurement bench Pass Through Connectors Partition Panel Loosen Captive Screw Remove Screw Remove Screws Remove Screw REMOVE SCREWS SLIDE BENCH OUT LOWER PANEL Remo...

Страница 198: ...urely loosen the captive screw at the rear of the measurement bench and pull the measurement bench from the rear of the case 10 Remove the screw at the top rear of the partition panel securing the top of partition panel to the measurement bench and lower the panel being careful not to put excessive tension on the cables 11 Replace the measurement bench by following the previous steps in reverse Fu...

Страница 199: ...to the procedure Leak Test and Pump Checkout with Photometer Option Use the following procedure to check for leaks in the system and to leak test the pump This procedure is for Model 146i instruments that have the photometer option For Model 146i instruments that do not have the photometer option refer to Leak Test and Pump Checkout without Photometer Option WARNING The service procedures in this ...

Страница 200: ...e to scroll to Pressure and press to display the Pressure screen The pressure reading should drop to less than 250 mm Hg If the pump diaphragm is in good condition and the capillary is not blocked it should take less than 20 seconds from the time the inlet is plugged to the time the reading drops below 250 mm Hg If a leak is suspected carefully tighten each fitting until the leak is found and chec...

Страница 201: ... 4 Connect a shutoff valve between the external vacuum pump intake and the vacuum gauge 5 Attach the external vacuum pump vacuum gauge assembly with the vacuum gauge side to the calibrator EXHAUST port 6 Apply vacuum until the gauge stabilizes then trap the vacuum with the shut off valve WARNING The service procedures in this manual are restricted to qualified service representatives If the equipm...

Страница 202: ...edure Mass Flow Controller Replacement Use the following procedure to replace a mass flow controller Figure 7 4 Equipment required Wrenches 7 16 and 9 16 Philips screwdrivers 1 and 2 Flatblade screwdriver New mass flow controller 1 Turn instrument OFF unplug the power cord and remove the cover 2 Loosen all four fittings to mass flow controllers Equipment Damage Some internal components can be dama...

Страница 203: ...ntroller 4 Remove plumbing from flow controllers 5 Disconnect fan electrical connector 6 Remove four screws holding flow controller bracket to floor plate 7 Remove flow controller assembly 8 Remove defective flow controller from bracket by removing the two screws holding flow controller to bracket 9 Install new flow controller by following the above directions in reverse 10 Leak check system and r...

Страница 204: ... 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect pump power line from AC PUMP connector on the measurement interface board Figure 7 5 Replacing the Pump 3 Remove both lines from pump 4 Loosen the four captive screws holding the pump to the mounting plate and remove the pump Equipment Damage Some internal components can be damaged by small amounts of static electricity...

Страница 205: ...ord and remove the cover 2 Remove the measurement bench Refer to Removing the Measurement Bench and Lowering the Partition Panel on page 7 9 3 Pull the power connector off the fan 4 Remove the fan guard from the fan and remove the filter 5 Remove the four fan mounting screws and remove the fan 6 Install a new fan following the previous steps in reverse Equipment Damage Some internal components can...

Страница 206: ...er 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the mass flow controllers Refer to Mass Flow Controller Replacement on page 7 14 3 Disconnect the electrical connection from the fan 4 Remove the fan mounting screws 4 and nuts and remove the fan 5 Install the new fan using the previous steps in reverse Fan Guard Filter Mounting Screws 4 Equipment Damage Some internal com...

Страница 207: ... to the channel to be tested Figure 7 7 shows the analog output pins and Table 7 4 identifies the associated channels 2 From the Main Menu press to scroll to Diagnostics press to scroll to Test Analog Outputs and press The Test Analog Outputs screen appears 3 Press to scroll to the channel corresponding to the rear panel terminal pins where the meter is connected and press The Set Analog Outputs s...

Страница 208: ...og outputs should be adjusted Refer to the Analog Output Calibration procedure that follows 8 Press to reset the analog outputs to normal Figure 7 7 Rear Panel Analog Input and Output Pins Analog Voltage Outputs Current Outputs Analog Voltage Inputs Table 7 4 Analog Output Channels and Rear Panel Pin Connections Voltage Channel Pin Current Channel Pin 1 14 1 15 2 33 2 17 3 15 3 19 4 34 4 21 5 17 5...

Страница 209: ...Figure 7 7 shows the analog output pins and Table 7 4 identifies the associated channels 2 From the Main Menu press to scroll to Service press to scroll to Analog Out Calibration and press The Analog Output Cal screen appears Note If Service is not displayed refer to Accessing the Service Mode on page 7 11 then return to the beginning of this step Ground 16 18 19 35 37 Current Output Return 16 18 ...

Страница 210: ... to select Calibrate Full Scale 8 Use until the meter reads the value shown in the Set Output To line then press to save the value Analog Input Calibration Use the following procedures to calibrate the analog inputs after replacing the optional I O expansion board These procedures include selecting analog input channels calibrating them to zero volts and then calibrating them to full scale using a...

Страница 211: ...ecessary 6 Continue with the Calibrating the Input Channels to Full Scale procedure that follows Calibrating the Input Channels to Full Scale Use the following procedure to calibrate the input channels to full scale by applying a known voltage to the channels Equipment Required DC voltage source greater than 0 volts and less than 10 volts 1 Connect the known DC voltage source to the input channel ...

Страница 212: ...voltage as necessary I O Expansion Board Replacement Optional Use the following procedure to replace the optional I O expansion board Figure 7 8 Note After replacing the optional I O expansion board calibrate the current outputs and the analog voltage inputs See the Analog Output Calibration on page 7 21 and the Analog Input Calibration on page 7 22 in this chapter Equipment Required I O expansion...

Страница 213: ...nel Figure 7 9 4 Pop off the board from the mounting studs and remove the board 5 To install the I O expansion board follow previous steps in reverse Figure 7 8 Replacing the I O Expansion Board Optional Figure 7 9 Rear Panel Board Connectors I O Expansion Board Opt Digital Output Board Motherboard Mounting Studs Motherboard Support Bracket Motherboard Digital Output Board I O Expansion Board ...

Страница 214: ...er 3 Disconnect the digital output board ribbon cable from the motherboard 4 Using the nut driver remove the two standoffs securing the board to the rear panel Figure 7 9 5 Pop off the digital output board from the mounting studs and remove the board 6 To install the digital output board follow previous steps in reverse Motherboard Replacement Use the following procedure to replace the motherboard...

Страница 215: ...fs securing the board to the rear panel 6 Pop off the motherboard from motherboard support bracket and remove the motherboard 7 To install the motherboard follow previous steps in reverse Measurement Interface Board Replacement Use the following procedure to replace the measurement interface board Figure 7 10 Equipment Required Measurement interface board Philips screwdriver Equipment Damage Some ...

Страница 216: ...he top of the board 4 Pop off the measurement interface board from the two mounting studs at the bottom of the board and remove the board Figure 7 10 Replacing the Measurement Interface Board 5 To install the measurement interface board follow previous steps in reverse 6 Re install the measurement bench Refer to Removing the Measurement Bench and Lowering the Partition Panel on page 7 9 Front Pane...

Страница 217: ...ttom support 4 Replace the front panel board by following previous steps in reverse Figure 7 11 Replacing the Front Panel Board and the LCD Module LCD Module Replacement Use the following procedure to replace the LCD module Figure 7 11 Equipment Required Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must b...

Страница 218: ... your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and water Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component Do not remove the panel or frame from the module The polarizing plate is very fragile handl...

Страница 219: ...s a ratio instrument and replacing the lamp does not affect the calibration However after replacing the photometer lamp you must adjust the photometer lamp voltage to ensure proper operation Refer to the Photometer Lamp Voltage Adjustment procedure that follows to adjust the photometer lamp voltage Use the following procedure to replace the photometer lamp Figure 7 12 Equipment required Allen wren...

Страница 220: ... clamp screw 7 Plug the new photometer lamp cable into the LAMP connector on the photometer board 8 Re install the instrument cover 9 Reconnect power and turn instrument ON 10 After lamp has stabilized approximately 15 minutes refer to the Photometer Lamp Voltage Adjustment procedure that follows to adjust the photometer lamp voltage Thermistor Detector Detector Retaining Screw Photometer Lamp Ins...

Страница 221: ...Service is not displayed refer to Accessing the Service Mode on page 7 11 then return to the beginning of this step 2 At the Photometer Lamp Setting screen use to increment decrement the Lamp Setting until Intensity indicates approximately 100 000 Hz 3 Press to save the setting Photometer Lamp Heater Replacement Use the following procedure to replace the photometer lamp heater Figure 7 12 Equipmen...

Страница 222: ...hotometer Allen wrench 7 64 inch Open end wrench 9 16 inch Use the following procedure to replace the photometer 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the plumbing and electrical connections 3 Loosen the four 4 socket head retaining screws securing the photometer to the floor plate Figure 7 12 and remove the photometer 4 Perform the previous steps in reverse...

Страница 223: ...Ozonator Board Replacement Ozonator option on page 7 45 3 Remove the cables from the board 4 Remove the two screws from the top of the board 5 Pop off the board from the bottom mounting studs and remove the board 6 To install the new photometer board follow previous steps in reverse 7 Reinstall the ozonator board Detector Replacement Photometer option Use the following procedure to replace the pho...

Страница 224: ...photometer lamp intensity if necessary via Service Lamp Setting Photometer Thermistor Replacement Use the following procedure to replace the photometer thermistor Figure 7 12 Equipment Required Photometer thermistor Wrench 1 4 inch 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the thermistor electrical connection Equipment Damage Some internal components can be dama...

Страница 225: ... an accurately known 10K resistor to the thermistor input TEMP on the measurement interface board and enter the temperature reading A 1 C change corresponds to a 5 change in resistance thus this alternative procedure can be quite accurate as a check however it clearly is not NIST traceable 3 From the Main Menu press to scroll to Service press to scroll to Temperature Calibration and press The Cali...

Страница 226: ...ut on page 7 8 to locate these solenoids within the instrument If you need the solenoid part number refer to the Replacement Parts List on page 7 5 External Internal solenoid Ozonator solenoid Perm1 and Perm 2 solenoids Reaction chamber solenoid Sample Reference solenoid Span gas solenoids Zero air solenoid Use the following general replacement procedure to replace a solenoid Equipment required So...

Страница 227: ...rocedure to replace the pressure transducer Refer to Component Layout on page 7 8 to locate the pressure transducer within the instrument and refer to Replacement Parts List on page 7 5 if you need the pressure transducer part number Equipment Required Pressure transducer assembly Philips screwdriver short 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect plumbing from ...

Страница 228: ...de by obtaining the current barometric pressure from the local weather station or airport and comparing it to the pressure reading However since these pressures are usually corrected to sea level it may be necessary to correct the reading to local pressure by subtracting 0 027 mm Hg per foot of altitude Do not try to calibrate the pressure transducer unless the pressure is known accurately Use the...

Страница 229: ...en return to the beginning of this step 4 At the Pressure Sensor Cal screen press to select Zero The Calibrate Pressure Zero screen appears 5 Wait at least 10 seconds for the zero reading to stabilize then press to save the zero pressure value 6 Disconnect the pump from the pressure transducer 7 Press to return to the Pressure Sensor Cal screen 8 At the Pressure Sensor Cal screen press to select S...

Страница 230: ... cord 4 Loosen both lamp clamp screws 5 Carefully slide lamp out of ozonator housing 6 Slide insulation off of old lamp and slide onto new lamp cord 7 Carefully insert new lamp into ozonator housing until it bottoms Pull lamp out approximately 1 16 inch to allow for expansion when the lamp warms up and tighten the Allen screws on the clamp 8 Slide the lamp insulation against the ozonator 9 Re conn...

Страница 231: ... 10 3 Disconnect plumbing from the ozonator 4 Remove the ozonator by removing the two screws securing the ozonator to the floor plate and lifting the ozonator straight up 5 Remove the ozonator flange by removing three screws securing the bottom flange and pulling the flange off 6 Remove the ozonator lamp heater block from the ozonator by removing four Allen screws 7 Coat new lamp heater block with...

Страница 232: ...m the LAMP HEATER and LAMP connectors on the ozonator board Figure 7 10 3 Disconnect plumbing from the ozonator 4 Remove the ozonator by removing the two screws securing the ozonator to the floor plate and lifting the ozonator straight up 5 Install new ozonator by following the above procedure in reverse Ensure all fittings are tight 6 Perform a leak test Refer to Leak Test and Pump Checkout in th...

Страница 233: ...oard Philips screwdriver 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the connection cables from the board 3 Remove the two screws from the top of the board 4 Pop off the board from the bottom mounting studs and remove the board 5 To install the new ozonator board follow previous steps in reverse Capillary Equipment Damage Some internal components can be damaged by sma...

Страница 234: ...cover b Remove glass chamber assembly by loosening not removing knurled screw located at the top of the chamber and gently pulling assembly upward Completely remove assembly from oven Figure 7 14 c Separate glass chamber from top assembly by twisting and gently pulling glass away from top Figure 7 14 Keep glass clean by using Kimwipes or similar material to handle glass d Place permeation tube in ...

Страница 235: ...n h Replace oven cover being careful to place tubing and wire in slot of cover 6 Install the new oven by following the previous steps in reverse 7 Check the system for leaks Refer to Leak Test and Pump Checkout in this chapter Figure 7 14 Removing the Glass Chamber Assembly Knurled Screw Glass Chamber Assembly Oven Top Top Assembly Glass Chamber Oven Enclosure ...

Страница 236: ...ch Philips screwdriver 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the plumbing 3 Remove two 2 Allen screws from the top of the holder assembly 4 Remove two 2 Allen screws from the side of the holder assembly Permeation Oven Top See Expanded View Expanded View Chamber Top Oven Top Glass Chamber Assembly Permeation Oven Bottom See Procedure Equipment Damage Some intern...

Страница 237: ...move fitting from bottom of the pressure regulator by holding the assembly in place with a 9 16 inch wrench as shown in Figure 7 16 and loosening the pressure regulator fitting Figure 7 16 Replacing the Pressure Regulator 4 Remove the pressure regulator and replace with a new unit 5 Reconnect plumbing and check for leaks Refer to Leak Test and Pump Checkout in this chapter Equipment Damage Some in...

Страница 238: ...Loosen four 4 captive screws and remove the assembly 4 Remove the pressure transducer 5 Remove the back pressure regulator handle 6 Remove two 2 screws holding the regulator to the bracket 7 Remove the back pressure regulator 8 Install a new back pressure regulator and calibrate 9 After calibration tighten the locking nut securing the position of the back pressure regulator handle 10 Remove flow c...

Страница 239: ...pillary restricting the meter input 2 For instruments equipped with the ozonator option attach the digital flow meter to the gas line immediately preceding the ozonator capillary holder attached to the solenoid valve on the ozonator For instruments equipped with only the permeation oven option attach the digital flow meter in place of the tee fitting between the back pressure regulator input and t...

Страница 240: ...w setting go to Service Flow Control Selection Zero Scale and use the zero flow controller zero scale value listed as the appropriate input for GAS A 7 If the instrument includes an output pressure regulator reduce the output pressure to zero on the gauge 8 Set the back pressure regulator to indicate a flow of 150 sccm on the digital flow meter 9 Change the GAS A flow rate to 400 sccm and observe ...

Страница 241: ...accurately known 10K resistor to the thermistor input AMB TEMP on the measurement interface board and enter the temperature reading A 1 C change corresponds to a 5 change in resistance thus this alternative procedure can be quite accurate as a check however it clearly is not NIST traceable 3 From the Main Menu press to scroll to Service press to scroll to Temperature Calibration and press The Cali...

Страница 242: ...the ambient reading to stabilize use and to enter the known temperature and press to save the temperature value 5 Install the cover Service Locations For additional assistance Thermo Fisher Scientific has service available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com aqi 1 866 282...

Страница 243: ...7 provides an overview of the software organization and detailed information on the software tasks Electronics on page 8 8 describes the system boards assemblies and connectors I O Components on page 8 11 describes the input and output communication functions and components Hardware The Model 146i components include Figure 8 1 Flow system Photometer with photometer lamp optional Pressure transduce...

Страница 244: ...s Each system is described independently While many of the components are shared they may only be necessary for one or two functions These components are only described when the system that requires them is being used Fan I O Expansion Board Optional Digital Output Board Motherboard Measurement Interface Board Ozonator Board Top Photometer Board Bottom Pump Solenoids Span Gas Mass Flow Controllers...

Страница 245: ...the ozone generator or by changing the light intensity In the Model 146i the selected light intensity level is held constant by temperature controlling the lamp and by using a highly stable lamp power supply The flow is held constant by the mass flow controller Gas Phase Titration Gas phase titration in the Model 146i is accomplished by combining the outputs of the precision gas dilution system wi...

Страница 246: ... are necessary for a response of 95 percent Permeation Tube Oven Gas flow through the oven is low approximately 150 sccm to stabilize the permeation tube oven temperature The major portion of the flow bypasses the oven and is directed to the mixing chamber with the stream from the oven This is achieved by using the same back pressure regulator described above for gas phase titration with a capilla...

Страница 247: ...terface board for sample measurement computations Pressure Transducer The pressure transducer measures the pressure of the sample gas Ozonator The internal ozonator operates on the photolytic principle and the ozone level produced is a function of light intensity at 185 nm and gas flow The light intensity is varied by changing the current into the lamp The gas flow is held constant by a pressure r...

Страница 248: ...xternal ozone sample or the internal ozone sample for measurement Span Gas Solenoids Control flow through independent gas inlets depending on the mode being controlled Photometer Capillary Reduces gas flow to the photometer Ozonator Capillary Reduces gas flow to the ozonator Pressure Gauge Capillary Used in conjunction with the pressure regulator to control flow through the ozonator Pump Capillary...

Страница 249: ...on the boards such as analog and digital I O and heater control These processors are controlled over a serial interface with a single high level processor that also controls the front panel user interface The low level processors all run a common piece of firmware that is bundled with the high level firmware and loaded on power up if a different version is detected Each board has a specific addres...

Страница 250: ... time function The background values for O3 are corrected for temperature pressure and span and are subtracted from the ozone calculated to yield a corrected value Output Communication The front panel display serial and Ethernet data ports and analog outputs are used to communicate the results of the measurement calculations The front panel displays the O3 concentration The display is updated ever...

Страница 251: ...es and to output analog voltages that represent the measurement data Connectors located on the motherboard include External Connectors External connectors include External Accessory RS 232 485 Communications two connectors Ethernet Communications I O connector with Power Fail Relay 16 Digital Inputs and 6 Analog Voltage Outputs Internal Connectors Internal connectors include Function key panel and...

Страница 252: ...tput is produced by measuring the pressure difference between the sample gas pressure and ambient air pressure Ozonator Lamp Power Supply The ozonator lamp power supply board includes the circuits that generate high voltage AC to control the lamp heater A transformer outputting high voltage at approximately 15 kHz drives the lamp A resistor in series with the output limits the lamp current The vol...

Страница 253: ...d to output analog currents via a connector located on the rear panel of the instrument It contains local power supplies a DC DC isolator supply a sub processor and analog circuits Eight analog voltage inputs are provided with an input voltage range of 0V to 10VDC Six current outputs are provided with a normal operating range of 0 to 20 mA Front Panel Connector Board The front panel connector boar...

Страница 254: ...ftware configured for any one of the following ranges while maintaining a minimum resolution of 11 bits 0 20 mA 4 20 mA The user can calibrate each analog output zero and span point through firmware At least 5 of full scale over and under range are also supported The analog outputs may be assigned to any measurement or diagnostic channel with a user defined range in the units of the selected param...

Страница 255: ...tal inputs are available which may be programmed to signal instrument modes and special conditions including Zero Gas Mode Span Gas Mode The actual use of these inputs will vary based on instrument configuration The digital inputs are TTL level compatible and are pulled up within the analyzer The active state can be user defined in firmware Serial Ports Two serial ports allow daisy chaining so tha...

Страница 256: ...tor is male a null modem cable is required Data Format 1200 2400 4800 9600 19200 38400 57600 or 115200 BAUD 8 data bits 1 stop bit no parity All responses are terminated with a carriage return hex 0D Refer to Table 8 1 for the DB9 connector pin configuration RS 485 Connection The instrument uses a four wire RS 485 configuration with automatic flow control SD Refer to Table 8 2 for the DB9 connecto...

Страница 257: ...ess may be configured for static addressing or dynamic addressing set using a DHCP server Any serial port protocols may be accessed over Ethernet in addition to the serial port External Accessory Connector The external accessory connector is not used in the Model 146i calibrator This port is used in other models to communicate with smart external devices that may be mounted hundreds of feet from t...

Страница 258: ...System Description I O Components 8 16 Model 146i Instruction Manual Thermo Fisher Scientific ...

Страница 259: ... Mounting Options on page 9 13 Ozonator The internal ozone generator provides easy determination of zero precision and Level 1 span checks The ozone level produced is a function of light intensity at 185 nm and gas flow The light intensity is varied by changing the current into the lamp The gas flow is held constant by a pressure regulator followed by a capillary Photometer The photometer measures...

Страница 260: ...ng as the backpressure regulator In practice rather than measuring the pressure it is the actual flows that are measured while adjusting the pressure regulator Two solenoids under control of the microcomputer are used to change the flow of gas going through the oven to the main stream or to vent Permeation Tube Installation Use the following procedure to install the permeation tube 1 Remove the ov...

Страница 261: ...rmation Note that is assumed that all devices are properly calibrated and that all flows are corrected to 25 C and 1 atm Permeation Tube Where R permeation rate in ng min Q0 flow rate of gas scc min into the charcoal scrubber during span mode K constant for the specific permeant 24 45 MW MW molecular weight Oven Installation and Configuration Use the following procedure to install and configure th...

Страница 262: ... a resistance of approximately 5 KΩ across pins 1 and 2 of POJ1 8 Go to the High Point screen enter the exact value of the resistor and press to calibrate the high resistance point 9 Press to return to the Factory Cal Gas Therm menu 10 Remove resistor from POJ1 and re attach the gas thermistor 11 Connect a resistance of approximately 3 8 KΩ across pins 3 and 4 of POJ3 12 Go to the Factory Cal Oven...

Страница 263: ...corresponds to an error of 1 in release rate The second approach is to note that the thermistors used to measure temperature are interchangeable to better than 0 2 C Thus a 1 resistor of the proper value 4 369 KΩ for 45 C can be used to set the span on the measurement interface board The release rate for the permeation tube is then determined by weight loss in the actual oven being used Setting Pe...

Страница 264: ...Temperature with Water Bath Use the following procedure for setting the measure temperature with water bath 1 Remove the thermistor from the permeation tube oven but leave the thermistor connected to the measurement interface board Insert the thermistor into the water bath next to an NIST traceable thermometer if necessary use an extension cable to reach 2 Turn on the power to the water bath Using...

Страница 265: ...O bulkhead on the rear panel 6 Wait for the permeation gas temperature reading to stabilize Setting Temperature with Known Resistance Use the following procedure to set the gas temperature with an accurate known resistance 1 Remove the thermistor from POJ1 on the measurement interface board 1 Connect a 4 369 KΩ resistor across pins 1 and 2 of POJ1 use a resistance substitution box and an accurate ...

Страница 266: ...permeation gas temperature reading to stabilize Determining Permeation Rate by Weight Loss Use the following procedure to determine the permeation rate by weight loss 1 Make sure the oven has been calibrated as described in the Permeation Tube Oven Calibration procedure described previously 2 Insert the permeation tube carefully Do not touch with fingers 3 Turn on the instrument 4 Wait 48 72 hours...

Страница 267: ...determine the weight loss of permeation tube Determining Release Rate by Transfer Standard Use the following procedure to determine the release rate by transfer standard 1 Make sure the oven has been calibrated as described in the Permeation Tube Oven Calibration procedure described previously Also make sure that the Transfer Standard has been properly calibrated 2 Determine the permeation rate fo...

Страница 268: ...ard to six Span Gas Mass Flow Controller The span gas mass flow controller governs low gas flow to control gas being diluted Span gas mass flow controllers include 25 SCCM 50 SCCM 100 SCCM standard 200 SCCM 500 SCCM Zero Gas Mass Flow Controller The zero gas mass flow controller governs high gas flow to control zero air Zero gas mass flow controllers include 5 SLPM 10 SLPM standard 15 SLPM 20 SLPM...

Страница 269: ...tor to individual numbered terminals Two types of terminal block and cable kits are available One kit is for the DB37 connectors and can be used for either the analog output connector or the relay output connector The other kit is for the DB25 connector and can be used for the optional I O expansion board For associated part numbers refer to External Device Connection Components in the Servicing c...

Страница 270: ...Color Codes for 25 Pin and 37 Pin Cables Pin Color Pin Color 1 BLACK 20 RED BLACK 2 BROWN 21 ORANGE BLACK 3 RED 22 YELLOW BLACK 4 ORANGE 23 GREEN BLACK 5 YELLOW 24 GRAY BLACK 6 GREEN 25 PINK BLACK 7 BLUE End color codes for 25 pin cables continue for 37 pin cables 8 VIOLET 26 PINK GREEN 9 GRAY 27 PINK RED 10 WHITE 28 PINK VIOLET 11 PINK 29 LIGHT BLUE 12 LIGHT GREEN 30 LIGHT BLUE BROWN 13 BLACK WHI...

Страница 271: ...d shown in Figure 9 4 through Figure 9 7 Table 9 3 Mounting Options Mounting Type Description Bench Positioned on bench includes mounting feet and front panel side trim ears EIA rack Mounted in an EIA style rack includes mounting slides and front panel EIA rack mounting ears Retrofit rack Mounted in a Thermo non EIA rack includes mounting slides and retrofit front panel rack mounting ears ...

Страница 272: ...9 14 Model 146i Instruction Manual Thermo Fisher Scientific Figure 9 4 Rack Mount Option Assembly ...

Страница 273: ...Thermo Fisher Scientific Model 146i Instruction Manual 9 15 Figure 9 5 Bench Mounting ...

Страница 274: ...9 16 Model 146i Instruction Manual Thermo Fisher Scientific Figure 9 6 EIA Rack Mounting ...

Страница 275: ...Thermo Fisher Scientific Model 146i Instruction Manual 9 17 Figure 9 7 Retrofit Rack Mounting ...

Страница 276: ...Optional Equipment Mounting Options 9 18 Model 146i Instruction Manual Thermo Fisher Scientific ...

Страница 277: ...h may include biohazard decontamination procedures and other product specific handling instructions and c then if applicable Buyer may return the defective Products to Seller with all costs prepaid by Buyer Replacement parts may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of repaired or replacement Products shall be made ...

Страница 278: ...ling time and materials rates ANY INSTALLATION MAINTENANCE REPAIR SERVICE RELOCATION OR ALTERATION TO OR OF OR OTHER TAMPERING WITH THE PRODUCTS PERFORMED BY ANY PERSON OR ENTITY OTHER THAN SELLER WITHOUT SELLER S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH RESPECT TO THE AFFECTED PRODUCTS THE OBLIGATIONS CREAT...

Страница 279: ...ation on page B 23 Keys Display on page B 25 Measurement Configuration on page B 28 Hardware Configuration on page B 37 Communications Configuration on page B 39 I O Configuration on page B 43 Record Layout Definition on page B 47 Each command sent to the instrument must begin with the American Standard Code for Information Interchange ASCII symbol or byte value equivalent of the instrument s iden...

Страница 280: ...E CR If an incorrect command is sent a bad command message will be received The example below sends the incorrect command set unit ppm instead of the correct command set gas unit ppm Send set unit ppm Receive set unit ppm bad cmd The save and set save params commands stores parameters in FLASH It is important that each time instrument parameters are changed that this command be sent If changes are...

Страница 281: ...p min Reports sets ozonator lamp temperature alarm minimum value B 12 alarm pressure max Reports sets photometer pressure alarm maximum value B 13 alarm pressure min Reports sets photometer pressure alarm minimum value B 13 alarm trig conc o3 Reports sets O3 concentration low alarm trigger value B 13 analog iout range Reports sets analog current output range per channel B 43 analog vin Retrieves a...

Страница 282: ...g down pushbutton B 25 dout Reports sets active logic state for the digital output channel B 45 dtoa Reports outputs of the digital to analog converters per channel B 45 en enter Simulates pressing enter pushbutton B 25 er Returns a brief description of the main operating conditions in the format specified in the commands B 17 erec Returns a brief description of the main operating conditions in th...

Страница 283: ...Reports sets custom level 1 setting of ozonator lamp drive B 32 l1 conc Reports sets custom level 1 concentration for photometer control of ozonator lamp drive B 32 l2 Reports sets custom level 2 setting of ozonator lamp drive B 32 l2 conc Reports sets custom level 2 concentration for photometer control of ozonator lamp drive B 32 l3 Reports sets custom level 3 setting of ozonator lamp drive B 32 ...

Страница 284: ...t for long records ASCII or binary B 19 lrec layout Reports layout of lrec data B 19 lrec mem size Reports maximum number of long records that can be stored B 20 lrec per Reports sets long record logging period B 20 malloc lrec Reports sets memory allocation for long records B 21 malloc srec Reports sets memory allocation for short records B 21 man gas gflow Reports sets gas flow controller manual...

Страница 285: ...esponse coefficient B 25 ri right Simulates pressing right pushbutton B 26 ru run Simulates pressing run pushbutton B 26 save Stores parameters in FLASH B 38 save params Stores parameters in FLASH B 38 sc screen C series legacy command that reports a generic response Use iscreen instead B 27 sp conc Reports sets photometer span concentration for calibration B 25 sp field Reports sets item number a...

Страница 286: ...photometer option is installed Send avg time Receive avg time 5 300 sec set avg time selection This command sets the averaging time according to Table B 2 The example below sets the averaging time to 120 seconds This command is only available if the photometer option is installed Send set avg time 2 Receive set avg time 2 ok Table B 2 Averaging Times Selection Averaging Time seconds 0 60 seconds 1...

Страница 287: ... measured If pressure compensation is on then both pressure readings are the same If pressure compensation is off a pressure of 760 mmHg is used as default pressure even though the actual pressure is 753 4 mmHg The example below shows that the actual reaction chamber pressure is 753 4 mmHg This command is only available if the photometer option is installed Send pres Receive pres 753 4 mmHg actual...

Страница 288: ...r option is installed Send alarm bench lamp temp min Receive alarm bench lamp temp min 52 0 deg C set alarm bench lamp temp min value set alarm bench lamp temp max value These commands set the photometer bench lamp temperature minimum and maximum values to value where value is a floating point number representing bench lamp temperature alarm limits in degrees C The example below sets the bench lam...

Страница 289: ... bench temp max 35 ok alarm conc o3 min alarm conc o3 max These commands report the photometer O3 concentration alarm minimum and maximum value current setting The example below reports the O3 concentration alarm minimum is 20 ppb These commands are only available if the photometer option is installed Send alarm conc o3 min Receive alarm conc o3 min 20 0 ppm set alarm conc o3 min value set alarm c...

Страница 290: ...arm internal temp min 15 0 deg C set alarm internal temp min value set alarm internal temp max value These commands set the internal temperature minimum and maximum values to value where value is a floating point number representing ambient temperature alarm limits in degrees C The example below sets the internal temperature alarm maximum value to 45 0 C Send set alarm internal temp max 45 Receive...

Страница 291: ...number representing pressure alarm limits in millimeters of mercury The example below sets the pressure alarm maximum value to 1000 mmHg These commands are only available if the photometer option is installed Send set alarm pressure max 1000 Receive set alarm pressure max 1000 ok alarm trig conc o3 This command reports the photometer O3 concentration alarm trigger action for minimum alarm to eithe...

Страница 292: ...ve 15 negative 15 positive 5 positive 3 3 Each voltage value is separated by a space Send diag volt mib Receive diag volt mib 24 1 14 9 14 9 4 9 3 2 diag volt iob This command reports the diagnostic voltage measurements on the I O expansion board The sequence of voltages is Positive 24 positive 5 positive 3 3 and negative 3 3 Each voltage value is separated by a space Send diag volt iob Receive di...

Страница 293: ... V lamp voltage o3 This command reports the ozonator lamp voltage in volts This command is only available if the photometer option is installed Send lamp voltage o3 Receive lamp voltage o3 12 3 V oz lamp temp This command reports the current ozonator lamp temperature The example below shows the current ozonator temperature is 68 7 C This command is only available if the photometer option is instal...

Страница 294: ...ed at their normal interval Send set program on Receive set program on ok clr records This command will clear all long and short records that have been saved Send clear records Receive clear records ok set clr lrecs set clr srecs These commands will clear only the long records or only the short records that have been saved The example below clears short records Send set clr srecs Receive set clr s...

Страница 295: ...ive list stream field index variable x x time 1 1 conc 2 2 tgflo 3 3 agflo 4 4 tzflo 5 5 azflo 6 6 ttgflo 7 7 atflo sum 242d er xy lr xy sr xy x 0 1 Reply termination format see set format format command y 0 1 2 Output format see set erec lrec srec format format command These commands report the last long and short records stored or the dynamic data record In the example below the command requests...

Страница 296: ... month 01 to 12 pp day 01 to 31 qq year These commands output long or short records The output format is determined by the set lrec format and set srec format commands The logging time is determined by the set lrec per and set srec per commands In the following example there are 740 long records currently stored in memory When the command lrec 100 5 is sent the instrument counts back 100 records f...

Страница 297: ... format for long records is ASCII with text according to Table B 4 Send lrec format Receive lrec format 01 set erec format format set lrec format format set srec format format These commands set the output format for long and short records and dynamic data according to Table B 4 The example below sets the long record output format to ASCII with text Send set lrec format 1 Receive set lrec format 1...

Страница 298: ...ber of long records that can be stored in memory is 2038 Send lrec mem size Receive lrec mem size 2038 recs 10 blocks lrec per srec per These commands report the long and short records logging period The example below shows that the short record logging period is 5 minutes Send srec per Receive srec per 5 min set srec per value set srec per value value 1 5 15 30 60 These commands set the long and ...

Страница 299: ...d be retrieved using appropriate commands if required Send set malloc lrec 10 Receive set malloc lrec 10 ok set copy sp to lrec set copy sp to srec set copy sp to stream These commands copy the current selections in scratch pad sp into the long record short record or streaming data list The example below copies the current list in scratch pad into the long records list Send set copy sp to lrec Rec...

Страница 300: ...s may be obtained using the command list var aout The set sp field command is used to create a list of variables which can then be transferred into the long record short record or streaming data lists using the set copy sp to lrec set copy sp to srec or set copy sp to stream commands Send set sp field 1 34 Receive set sp field 1 34 ok stream per This command reports the currently set time interval...

Страница 301: ... bkg Receive set cal o3 bkg ok set cal o3 coef This command will auto calibrate O3 coefficients based on O3 span gas concentrations If the mode is incorrect the instrument responds with can t wrong settings The example below shows a successful auto calibration of the O3 coefficient This command is only available if the photometer option is installed Send set cal o3 coef Receive set cal o3 coef ok ...

Страница 302: ...e This command sets the O3 coefficients to user defined values to value where value is a floating point representation of the coefficient The example below sets the O3 coefficient to 1 005 This command is only available if the photometer option is installed Send set o3 coef 1 005 Receive set o3 coef 1 005 ok o3 bkg This command reports the current O3 background The example below reports that the O...

Страница 303: ...mand is only available if the photometer option is installed Send set resp coef 1 500 Receive set resp coef 1 500 ok sp conc This command reports photometer span concentration If the mode is incorrect the instrument responds with can t wrong settings The example below reports the span gas concentration of 50 ppb This command is only available if the photometer option is installed Send sp conc Rece...

Страница 304: ...om left to right Send push enter Receive push enter ok isc iscreen This command retrieves the framebuffer data used for the display on the iSeries instrument It is 19200 bytes in size 2 bits per pixel 4 pixels per byte arranged as 320 by 240 characters The data is sent in RLE encoded form to save time in transmission It is sent as a type 5 binary c_link response with no checksum The RLE encoding c...

Страница 305: ...r rlecount unsigned char rlescreen i while rlecount ptr 0 rlecount else if rlescreen i 0xff unsigned char rlecount unsigned char rlescreen i while rlecount ptr 0xff rlecount To convert this data into a BMP for use with windows it needs to be turned into a 4BPP as that is the smallest windows can display Also note that BMP files are upside down relative to this data i e the top display line is the ...

Страница 306: ...e below reports that Gas A is currently selected Send gas index Receive gas index 1 set gas index index index 0 6 This command sets the current gas index value to index The example below selects Gas D according to Table B 6 Send set gas index 4 Receive set gas index 4 ok Table B 6 Gas Index Values Value Gas Index 0 None 1 Gas A 2 Gas B 3 Gas C 4 Gas D 5 Gas E 6 Gas F sel gas gas man gas a b c d e ...

Страница 307: ... gas solenoids Send sel gas off Receive sel gas off ok gas gas params gas a b c d e f This command returns the parameters for the specified gas Send gas a params Receive gas a params tank ppm 10 000 span 0 zflow 1800 000 span 1 tflow 1000 000 ppm 0 400 span 2 tflow 1000 000 ppm 0 800 span 3 tflow 1000 000 ppm 1 200 span 4 tflow 1000 000 ppm 1 600 span 5 tflow 1000 000 ppm 0 400 manual zflow 1000 0...

Страница 308: ...noid Number Values Value Solenoid Value 1 Solenoid A 2 Solenoid B 3 Solenoid C 4 Solenoid D 5 Solenoid E 6 Solenoid F sel gas gas span gas a b c d e f This command sets the gas gas to span levels 0 1 2 3 4 or 5 The example below sets gas A to span level 1 Send sel gas a span 1 Receive set gas a span 1 ok gas gas span conc spanindex gas a b c d e f spanindex span index 0 6 1 5 reports the span conc...

Страница 309: ...an conc 1 123 45 Receive set gas a span conc 1 123 45 ok gas gas span flow gas a b c d e f spanindex span index 0 6 0 is for zero flow This command reports the target total flow for the specified gas gas and span level spanindex Send gas a span flow 1 Receive gas a span flow 1 123 45 set gas gas span flow value gas a b c d e f spanindex span index 0 6 0 is for zero flow value float This command se...

Страница 310: ...eter option is installed it must be configured for internal or external measurement mode Send l1 Receive l1 10 set l1 value set l2 value set l3 value set l4 value set l5 value These commands set the percentage of the ozonator lamp drive for each of the five custom levels The example below sets the custom level 1 to 10 This command is only available if the ozonator option is installed Also if the p...

Страница 311: ...ere level represents custom levels 1 2 3 4 or 5 The example below sets level 1 Send set level 1 Receive set level 1 ok man gas gas gflow value man gas gas zflow value gas a b c d e f value float These commands set the manual level for zero and gas flows for gas gas in sccm The set command is optional Send set man gas a gflow 202 00 Receive set man gas a gflow 202 00 man ozon level value This comma...

Страница 312: ...tput level 1 This command is only available if the ozonator option is installed Send sel ozon 1 Receive sel ozon 1 ok sel ozon perm off This command turns off the ozonator and permeation oven if these options are present Send set ozon perm off Receive set ozon perm off ok perm This command reports the current permeation oven output level where 0 is off This command is only available if the permeat...

Страница 313: ...he photometer option is installed Send o3 setting Receive o3 setting 1 000E 02 ppb range This commands report photometer O3 range If the mode is incorrect the instrument responds with can t wrong settings The example below reports that the O3 full scale range is set to 5 0 ppm according to Table B 8 This command is only available if the photometer option is installed Send range Receive range 6 500...

Страница 314: ...nt number representing concentration in ppm The example below sets the custom 1 range to 4 5 ppm Send set custom 1 range 4 5 Receive set custom 1 range 4 5 ok pres comp This command reports whether pressure compensation is on or off The example below shows that pressure compensation is on This command is only available if the photometer option is installed Send pres comp Receive pres comp on set p...

Страница 315: ...ands turn the temperature compensation on or off The example below turns temperature compensation off This command is only available if the photometer option is installed Send set temp comp off Receive set temp comp off ok contrast This command reports the screen s level of contrast The example below shows the screen contrast is 50 according to Table B 9 Send contrast Receive contrast 5 50 set con...

Страница 316: ...te 12 01 04 ok set default params This command sets all the parameters to their default values This does not affect the factory calibrated parameters Send set default params Receive set default params ok save set save params This command stores all current parameters in FLASH memory It is important that each time instrument parameters are changed that this command be sent If changes are not saved ...

Страница 317: ... dns Receive addr dns 192 168 1 1 set addr dns address This command sets the dns address where address consists of four numbers ranging from 0 255 inclusive separated by Send set addr dns 192 168 1 1 Receive set addr dns 192 168 1 1 ok addr gw This command reports the default TCP IP gateway address Send addr gw Receive addr gw 192 168 1 1 set addr gw address This command sets the default gateway a...

Страница 318: ...t addr nm 255 255 255 0 Receive set addr nm 255 255 255 0 ok baud This command reports the current baud rate for the serial port RS232 RS485 The example below reports that the current baud rate is 9600 baud Send baud Receive baud 9600 set baud rate rate 1200 2400 4800 9600 19200 38400 57600 115200 This command sets the instrument baud rate The example below sets the instrument s baud rate to 9600 ...

Страница 319: ...e example below shows that the reply format is 00 which means reply with no checksum according to Table B 10 Send format Receive format 00 set format format This command sets the reply termination format where format is set according to Table B 10 The example below sets the reply termination format to checksum Send set format 01 Receive set format 01 ok Table B 10 Reply Termination Formats Format ...

Страница 320: ...etween 0 and 127 inclusive Note sending this command via RS 232 or RS 485 will require the host to use the new id for subsequent commands 5 Send set instrument id 52 Receive set instrument id 52 ok mode This command reports what operating mode the instrument is in local service or remote The example below shows that the instrument is in the remote mode Send mode Receive mode remote set mode local ...

Страница 321: ... Receive analog iout range 4 2 set analog iout range channel range This command sets analog current output channel to the channel range where channel is between 1 and 6 inclusive and range is set according to Table B 11 The example below sets current output channel 4 to the 0 20 mA range This command responds with feature not enabled if the I O expansion board is not detected Send set analog iout ...

Страница 322: ...ow sets channel 2 to the 0 10 V range Send set analog vout range 2 3 Receive set analog vout range 2 3 ok Table B 12 Analog Voltage Output Range Values Range Output Range 1 0 1 V 2 0 100 mV 3 0 10 V 4 0 5 V 0 cannot be set to this but may report Undefined dig in This command reports the status of the digital inputs as a 4 digit hexadecimal string with the most significant bit MSB being input 16 Se...

Страница 323: ...dout channel index state This command assigns digital output channel to be assigned to the action associated with index and assigns it an active state of state open or closed Send set dout 2 2 open Receive set dout 2 2 open ok dtoa channel This reports the outputs of the 6 or 12 Digital to Analog converters according to Table B 13 The example below shows that the D A 1 is 97 7 full scale Send dtoa...

Страница 324: ...lable for selection in the current mode determined by single dual auto gas mode for analog output digital output and digital inputs The index number is used to insert the variable in a field location in a list using set sp field index The example below reports the list of analog output index numbers and variables Send list var aout Receive list var aout index variable 0 none 1 conc 2 tgflo 3 agflo...

Страница 325: ... 16 The example below sets the relay no 1 logic to normally open Note If the command is sent without an appended relay number then all the relays are assigned the set logic of normally open closed 5 Send set relay open 1 Receive set relay open 1 ok The Erec Lrec Srec layouts contain the following A format specifier for parsing ASCII responses A format specifier for parsing binary responses In addi...

Страница 326: ...the fields from a binary response Parameters MUST be separated by spaces and the line is terminated by a n Valid fields are t parse a time specifier 2 bytes D parse a date specifier 3 bytes i ignore one 8 bit character 1 byte e parse a 24 bit floating point number 3 bytes n x E parse a 24 bit floating point number 3 bytes N x f parse a 32 bit floating point number 4 bytes c parse an 8 bit signed n...

Страница 327: ... by a possible string enclosed in quotes that is used to place a string into the value field The value source which is the item or word number in the DATA ERec response appears next This is followed by an optional bitfield designator The datum identified by the value source can be printed as a string s hexadecimal x decimal d or floating point f or binary b number Typically bitfield extractions ar...

Страница 328: ...anslation table entries which the user may select from when setting the parameter This is not necessarily the same as the entries which may be displayed Then there appears an optional button designator This will be one of B I L T or N B Indicates a button which pops up an input dialog prompting the user for a new value using the designated input format The input format is specified from the B thro...

Страница 329: ...d is NO the value is taken from the third element of the data response and interpreted as a string NO 18sBd ddd set no coef s n This is a line which also appears slightly indented The next field is also NO but the value is taken from the eighteenth element of the data response again interpreted as a string A button appears on this line which when pressed pops up an input dialog which will state Pl...

Страница 330: ...e words which correspond to each input value the zeroth value appearing first 0 local 1 remote etc The selection list shows that only the first two values in this case are to be shown to the user when the button is pressed The T button indicates full translation input code to string and user selection number to output string xC This is a line that starts a new column the xC or L Comp 6 11x off on ...

Страница 331: ...instrument This is achieved by using the supported MODBUS commands listed below For details of the Model 146i MODBUS Protocol specification see the following topics Serial Communication Parameters on page C 1 TCP Communication Parameters on page C 2 Application Data Unit Definition on page C 2 Function Codes on page C 3 MODBUS Commands Supported on page C 8 Additional information on the MODBUS pro...

Страница 332: ...over serial connections Note Device ID 0 used for broadcast MODBUS commands is not supported Device IDs 128 through 247 i e 0x80 hex to 0xF7 hex are not supported because of limitations imposed by C Link In MODBUS over TCP IP a MODBUS Application Protocol Header MBAP is used to identify the message This header consists of the following components Transaction Identifier 2 Bytes 0x0000 to 0xFFFF Pas...

Страница 333: ...ensure error free transmission The error check is a two byte 16 bit CRC value This section describes the various function codes that are supported by the Model 146i Read Coils Inputs read the status of the digital outputs relays in the instrument Issuing either of these function codes will generate the same response These requests specify the starting address i e the address of the first output sp...

Страница 334: ...code 1 Byte 0x01 or 0x02 Starting Address 2 Bytes 0x0000 to maximum allowed by instrument Quantity of outputs 2 Bytes 1 to maximum allowed by instrument Unit Identifier 1 Byte 0x00 to 0xFF Passed back in response Response Function code 1 Byte 0x01 or 0x02 Byte count 1 Byte N Output Status n Byte N N or N 1 N Quantity of Outputs 8 if the remainder not equal to zero then N N 1 Error Response Functio...

Страница 335: ...strument Issuing either of these function codes will generate the same response These functions read the contents of one or more contiguous registers These registers are 16 bits each and are organized as shown below All of the values are reported as 32 bit IEEE standard 754 floating point format This uses 2 sequential registers least significant 16 bits first The request specifies the starting reg...

Страница 336: ...Illegal Address 03 Illegal Data 04 Slave Device Failure Here is an example of a request and response to read registers 10 13 Request Field Name Hex Function 0x03 Starting Address Hi 0x00 Starting Address Lo 0x09 No of Registers Hi 0x00 No of Registers Lo 0x04 Response Field Name Hex Function 0x03 Byte Count 0x06 Register value Hi 10 0x02 Register value Lo 10 0x2B Register value Hi 11 0x00 Register...

Страница 337: ...ant in the request data field A value of 0xFF00 requests the action to be ON A value of 0x0000 requests it to be OFF All other values are illegal and will not affect the output The normal response is an echo of the request returned after the state has been written Request Function code 1 Byte 0x05 Starting Address 2 Bytes 0x0000 to maximum allowed by instrument Output Value 2 Bytes 0x0000 or 0xFF0...

Страница 338: ...Hi FF Output Value Lo 00 The following Table C 1 through Table C 3 lists the MODBUS commands supported for the Model 146i Table C 1 Read Coils for 146i Coil Number Status 1 GAS BIT 1 2 GAS BIT 2 3 GAS BIT 3 4 SPAN BIT 1 5 SPAN BIT 2 6 SPAN BIT 3 7 O3 PERM BIT 1 8 O3 PERM BIT 2 9 O3 PERM BIT 3 10 O3 PERM BIT 4 11 PHOTO BIT 1 12 PHOTO BIT 2 13 GAS A 14 GAS B 15 GAS C 16 GAS D 17 GAS E 18 GAS F 19 OZ...

Страница 339: ...O3 LAMP TEMP 32 PERM GAS TEMP 33 PRESSURE 34 PHOT BENCH TEMP 35 PHOT LAMP TEMP 36 PHOT INTENSITY 37 O3 LEVEL Table C 2 Read Registers for 146i Register Number Variable 40001 40002 GAS CONC 40003 40004 TARGET GFLOW 40005 40006 ACTUAL GFLOW 40007 40008 TARGET ZFLOW 40009 40010 ACTUAL ZFLOW 40011 40012 TARGET TFLOW 40013 40014 ACTUAL TFLOW 40015 40016 O3 CONC 40017 40018 PERM CONC 40019 40020 PRESSUR...

Страница 340: ...33 40034 ANALOG 2 40035 40036 ANALOG 3 40037 40038 ANALOG 4 40039 40040 ANALOG 5 40041 40042 ANALOG 6 40043 40044 ANALOG 7 40045 40046 ANALOG 8 Table C 3 Write Coils for 146i Coil Number Action 101 GAS BIT 1 102 GAS BIT 2 103 GAS BIT 3 104 SPAN BIT 1 105 SPAN BIT 2 106 SPAN BIT 3 107 O3 PERM BIT 1 108 O3 PERM BIT 2 109 O3 PERM BIT 3 110 O3 PERM BIT 4 111 PHOTO BIT 1 112 PHOTO BIT 2 113 AOUTS TO ZE...

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