Dionex UltiMate 3000 Series, Руководство по эксплуатации

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UltiMate 3000 Series:
SD, RS, and BM Pumps
Page 58 Operating Instructions
4.7 Equilibrating the System
Before using the pump for sample analysis, equilibrate the UltiMate 3000 system:
1. Pump the starting solvent through the entire system until the system is free of any
other liquid composition.
2. Heat or cool all temperature-controlled devices to the temperature required for the
application.
3. Set the detector wavelengths and turn on the lamps.
4. Monitor the pump pressure. Verify that the reading is correct for the application and is
stable. The compression value should remain stable under 100%. The compression
value is displayed, for example, on the
Diagnostics menu on the pump display
(

page 76).
5. Monitor the detector signal and verify that the baseline signal is at the expected
reading for your application and is stable.
Perform system equilibration in Chromeleon or select the required commands and
parameters on the front panel menus of the instruments.
To equilibrate the system from Chromeleon

Select and perform the operating commands and parameters from the Commands dialog
box.

Create and run an equilibration program to automate the process (

page 68).

Use the SmartStartup Wizard to create and run the equilibration program (see below).
To create the equilibration program with the SmartStartup Wizard
1. To open the wizard, select SmartStartup on the Batch menu.
2. Follow the instructions as they appear on each page of the wizard. For additional
information about a page, click
Help .
3. After you finish the wizard, Chromeleon

Generates an equilibration program and sequence.

Opens the equilibration control panel for the instruments in the timebase (

Fig. 20,
page 59).

Opens the Start Batch on dialog box.
Click Start to begin equilibration.