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Take the electrospray probe and connect its gas line to
Nebuliser
on the front
panel.
Connect the liquid flow of a LC system or syringe pump to the probe.
Insert the probe into the source and tighten the two thumb nuts to secure the
probe firmly.
Plug the probe lead into
Capillary / Corona
on the front panel.
On the MassLynx top-level window, click on
to launch the tune page.
The top line of the tune page indicates the current ionisation mode.
If necessary, change the ionisation mode using the
Ion Mode
command.
Set
Source Temp
to 100°C and
Desolvation Temp
to 20°C.
Warning:
Operating the source without the source enclosure results
in solvent vapour escape and the exposure of hot surfaces and high
voltages.
Warning:
The ion source block can be heated to temperatures of 150°C, and is
maintained at the set temperature when the source enclosure is removed.
Touching the ion block when hot may cause burns to the operator.
Routine Procedures
Page 39
Quattro Ultima
User's Guide
Blanking
Plug
Corona
Discharge
Pin
Mounting
Contact
Exhaust
Liner
High Voltage
Socket
Cleanable
Baffle
Summary of Contents for Quattro Ultima
Page 2: ...Quattro Ultima User s Guide...
Page 68: ......
Page 100: ...Data Acquisition Page 100 Quattro Ultima User s Guide...
Page 117: ...Mass Calibration Page 117 Quattro Ultima User s Guide...
Page 140: ...Mass Calibration Page 140 Quattro Ultima User s Guide...
Page 212: ...Maintenance and Fault Finding Page 212 Quattro Ultima User s Guide...
Page 222: ...Reference Information Page 222 Quattro Ultima User s Guide...