multi EA 4000
Function and setup
37
3.6.2
Manual TIC solids module setup
A 50 ml Erlenmeyer flask is used as the reactor to which a TIC head with three connec-
tions for the supply of phosphoric acid, oxygen as the carrier gas and the measuring
gas outlet is attached.
A magnetic stirrer with a heating work plate ensures the sample is mixed well with the
added acid and heats the mixture slightly to speed up the reaction.
1 Supply of phosphoric acid (hose no. 6)
2 Measuring gas outlet
3 Supply of carrier gas (oxygen)
4 Erlenmeyer flask
5 Magnetic stirring rod
6 Magnetic stirrer with heated working
plate
Figure 27 TIC reactor of the manual TIC solids module
The carrier gas flow is set via the "O
2
" needle valve with measuring glass on the sepa-
rating wall in of the manual TIC solids module.
1 Measuring glass
2 Needle valve
Figure 28 Flow regulator for the oxygen flow
TIC reaction chamber
Flow setting of the carrier
gas flow
Summary of Contents for Analytik Jena multi EA 4000
Page 1: ...Operating Manual multi EA 4000 Elementary analyzer C S and Cl solids analysis...
Page 50: ...Commissioning multi EA 4000 50 Figure 32 multi EA 4000 C S Hose diagram...
Page 52: ...Commissioning multi EA 4000 52 Figure 33 multi EA 4000 Cl Hose diagram...
Page 54: ...Commissioning multi EA 4000 54 Figure 34 multi EA C S Cl for C S measurements Hose diagrams...
Page 55: ...multi EA 4000 Commissioning 55 Figure 35 multi EA 4000 C S Cl for Cl measurements...
Page 57: ...multi EA 4000 Commissioning 57 Figure 36 Automatic TIC solids module Hose diagrams...
Page 58: ...Commissioning multi EA 4000 58 Figure 37 multi EA 4000 C S with automatic TIC solids module...
Page 61: ...multi EA 4000 Commissioning 61 Figure 39 multi EA 4000 C S Cl with man TIC solids module...
