Operation
multi EA 4000
92
Enter the calculated factor in the method on the tab C
ALIBRATION
in the input
field D
AY FACTOR
. Accept the value with [A
CCEPT
] for the subsequent measure-
ments.
For the calculation of a new split factor the day factor must be set to a value of 1 n the
method on the tab C
ALIBRATION
.
6.4.7
Burning off quartz boats
Quartz boats must be burned off
before first use,
after cleaning heavy contamination.
To do so perform the measurement routine with empty quartz boats.
6.5
TIC/TOC determination with the automatic TIC solids module
6.5.1
Preparing the automatic TIC solids module for the analysis
WARNING
Risk of electric short circuit! In the combustion furnace HTS1500 very high electrical
currents occur in spite of a low voltage (max. 14 V). The combustion tube is part of the
cover of live components.
Only switch on the analyzer with the combustion tube inserted! Always switch off the
analyzer from the mains switch at the rear of the device for conversions and mainte-
nance to the combustion tube or combustion furnace.
CAUTION
There is a risk of burns at the hot the combustion furnace! Allow the basic device to
cool down sufficiently before conversion!
The TIC reactor of the automatic TIC solids module consists of a quartz tube with inlets
for acid and oxygen and a measuring gas outlet. The quartz tube is attached to the ce-
ramic combustion tube with a coupling. The following components are required to
connect the two tubes:
Base element of the gas sluice for C/S measurements (with sealing rings)
Pressure ring
2 sealing rings
Knurled ring
Summary of Contents for Analytik Jena multi EA 4000
Page 1: ...Operating Manual multi EA 4000 Elementary analyzer C S and Cl solids analysis...
Page 50: ...Commissioning multi EA 4000 50 Figure 32 multi EA 4000 C S Hose diagram...
Page 52: ...Commissioning multi EA 4000 52 Figure 33 multi EA 4000 Cl Hose diagram...
Page 54: ...Commissioning multi EA 4000 54 Figure 34 multi EA C S Cl for C S measurements Hose diagrams...
Page 55: ...multi EA 4000 Commissioning 55 Figure 35 multi EA 4000 C S Cl for Cl measurements...
Page 57: ...multi EA 4000 Commissioning 57 Figure 36 Automatic TIC solids module Hose diagrams...
Page 58: ...Commissioning multi EA 4000 58 Figure 37 multi EA 4000 C S with automatic TIC solids module...
Page 61: ...multi EA 4000 Commissioning 61 Figure 39 multi EA 4000 C S Cl with man TIC solids module...
