211
Cleaning the Burner Chamber
4. Clean the burner chamber and flow spoiler with a soft brush and a mild
laboratory detergent solution.
5. Clean the inside of the burner end cap with a soft wireless brush and a mild
laboratory detergent solution.
6. After cleaning, rinse thoroughly with deionized water.
7. Reassemble the burner system.
Cleaning the Burner Chamber After Use With Organic Solvents
If you aspirate aqueous samples immediately after organic samples (e.g. oils or
MIBK extracts), the absorption signals can be noisy and erratic. After aspirating
organic samples, perform the procedure below to prevent contamination of
subsequent aqueous samples.
1. Aspirate for 5 minutes an organic solvent that is miscible with the samples that
have just been aspirated.
2. Aspirate methanol or another solvent miscible with both the organic solvent
and water, for 5 minutes.
3. Aspirate 1% nitric acid solution for five minutes.
4. Flush the drain tube thoroughly with water. Empty the collection vessel and
refill with water. Dispose of hazardous or corrosive solutions properly and
observe local codes concerning the effect of the waste on the environment.
Note
If the solid deposits cannot be removed with a soft brush and a mild
laboratory detergent solution, the internal cavity of the chamber may be
soaked overnight with the 0.5% Triton X-100 + 5% HNO
3
acid when the
opening for the burner head is closed. Thoroughly rinse the internal cavity
with de-ionized water before use. If solid deposits still remain, you will
need to replace the spray chamber.
Содержание PINAACLE 900 Series
Страница 1: ...PINAACLE 900 SERIES Customer Hardware and Service Guide ATOMIC SPECTROSCOPY...
Страница 2: ......
Страница 3: ...PinAAcle 900 Series Customer Hardware and Service Guide...
Страница 26: ...10 Safety Practices Burner Locking Mechanism Label Item Description 1 Press button to unlock the lever 1...
Страница 52: ...36 Safety Practices...
Страница 55: ...39 Lab Space Requirements Dimensions and Weights Figure 2 1 Instrument dimenstions...
Страница 84: ...68 Preparing Your Laboratory...
Страница 91: ...75 The PinAAcle 900 Series Spectrometer System Figure 3 2 Optical System for the PinAAcle 900H...
Страница 92: ...76 System Description Figure 3 3 Optical System for the PinAAcle 900T...
Страница 93: ...77 The PinAAcle 900 Series Spectrometer System Figure 3 4 Optical System for the PinAAcle 900Z...
Страница 101: ...85 Burner Assembly System Figure 3 8 Block diagram of the burner system...
Страница 210: ...194 Preparing the System...
Страница 278: ...262 Maintenance Figure 6 31 Insertion removal tools Item Description 1 Graphite tube holder insertion removal tool 1...
Страница 310: ...294 Maintenance Figure 6 54 Window key Item Description 1 Window key 1...
Страница 354: ...338 Maintenance...
Страница 388: ...I 6 Index W WEEE Instructions 34 Weights 39 Windows cleaning 321 refitting 320 removing 318...
Страница 389: ......