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Distillation Process Analyzer DPA-4.5

Safety

WARNING
Hazard for unauthorized persons

Unauthorized persons who do not fulfill the
requirements described here are not aware of the
hazards posed in the work area.

For this reason:

– Keep unauthorized persons out of the work area.

– In case of doubt, address these persons and

instruct them to leave the work area.

– Interrupt work as long as unauthorized persons

are within the work area.

December 2013

Содержание DPA-4.5

Страница 1: ...DA00EN MDH 10 A December 2013 Distillation Process Analyzer DPA 4 5 Operating Manual...

Страница 2: ...BARTEC BENKE GmbH Borsigstra e 10 D 21456 Reinbek Germany Tel 49 0 40 72703 0 Fax 49 0 40 72703 363 E mail service bartec benke de Internet www bartec benke de...

Страница 3: ...26 2 4 2 Control box Ex p 27 2 4 3 Measuring unit box Ex d 29 2 4 4 Junction boxes Ex e 31 2 4 5 Potential equalization 31 2 4 6 Main switch and emergency off device 32 2 4 7 Signs and safety warning...

Страница 4: ...Safety instructions for transport 75 5 2 Symbols on the packaging 77 5 3 Transport inspection 78 5 4 Packaging 78 5 5 Center of gravity and suspension eyebolt 79 5 6 Transport 80 5 7 Storage 81 6 Inst...

Страница 5: ...k 129 10 5 1 General visual inspection 129 10 5 2 Checking the safety equipment 129 10 5 3 Checking the pressure monitor 131 10 5 4 Checking the residual current device 131 10 5 5 Maintenance on the d...

Страница 6: ...Distillation Process Analyzer DPA 4 5 Contents 12 Index 157 6 December 2013...

Страница 7: ......

Страница 8: ...cessible for operating personnel at all times If the device is handed over to a third party the operating manual must also be handed over For the purposes of clarity the figures in this operating manu...

Страница 9: ...amage to property DANGER indicates an imminent hazard which if not avoided will result in serious injury or death WARNING indicates a potential hazard which if not avoided can result in serious injury...

Страница 10: ...Warning about flammable substances Warning about potentially explosive atmospheres Warning about dangerous electrical current Warning about potential hand injuries Warning about hot surfaces Examples...

Страница 11: ...eding other liquids vapors or gases into the device in particular this applies to an external vent drain system Adding oxygen or hydrogen can result in the risk of explosions Rinsing with steam High t...

Страница 12: ...and environmental protection regulations applicable in the area of application must be observed In addition to this the operator is responsible for ensuring that the device is always in a technically...

Страница 13: ...nges Otherwise the obligations agreed upon in the delivery contract the general terms and conditions and the delivery terms of the manufacturer apply as well as any legal regulations valid at the time...

Страница 14: ...page 14 The replacement parts list can be found in the customer folder 1 8 Customer service Should you require any technical information our customer service department will be happy to help you You...

Страница 15: ...ducting parts poses an immediate life threatening hazard Damage to the insulation or to individual components can cause fatal injury For this reason If the insulation is damaged immediately disconnect...

Страница 16: ...ng operation and cause burns upon contact For this reason Before handling operating materials check whether they are hot Allow them to cool down if necessary Hot surfaces WARNING Danger of burns due t...

Страница 17: ...jects left lying around Dirt deposits and objects left lying around constitute slipping and stumbling hazards and can cause injuries For this reason Always maintain a clean and orderly work area Remov...

Страница 18: ...other substances requiring further safety measures may also be in use at the location of the device It is the responsibility of the operator to ensure compliance with the pertinent regulations and leg...

Страница 19: ...t be obtained for all work with flames or hot materials Keep a fire extinguisher at close hand Stop work at once in the event of fire Leave the danger area until the all clear signal is given Toxic su...

Страница 20: ...event pollutants from entering water bodies the sewage system or the ground Drinking water can be contaminated by small quantities of pollutants entering the ground and or bodies of water Environmenta...

Страница 21: ...or use in zone 1 Pressurization in the box ensures that the atmosphere inside is not explosive ia ib ia Intrinsically safe electrical circuits lead out of the box They cannot result in a potentially e...

Страница 22: ...osive atmospheres arise In division 2 hazardous concentrations of combustible gases vapors and mist do not usually occur under normal operating conditions The device may be used in such areas Groups B...

Страница 23: ...ed by a potentially explosive atmosphere are kept inside a box The box is designed in such a way that in the event of an explosion in the interior the pressure is maintained and thereby prevents the s...

Страница 24: ...at the control box in intrinsically safe electrical circuits NOTE The list with the explosion protected components or subassemblies used and the corresponding certificates can be found in the custome...

Страница 25: ...e intact For this reason Before starting work check whether the safety devices are correctly installed and fully functional Never disable safety devices Make sure that the safety devices such as emerg...

Страница 26: ...4 1 Overview of safety devices on the analyzer 1 2 3 4 5 6 Figure 2 1 Locations of the safety equipment 1 Locking screw for measuring unit box cover 2 Key switch 3 Lock on power supply box 4 Ground 5...

Страница 27: ...till have electrical charges or high temperatures which represent potential ignition sources Figure 2 1 Control box key switch The key switch is used to turn the pressure monitor of the control box on...

Страница 28: ...ervice work close the control box carefully with the aid of the two catches and switch on the pressure monitor again using the key switch The pressure monitor can be switched off for servicing or main...

Страница 29: ...ecked and all flame arresters replaced If the temperature on the surface of the flame arrester is more than 60 C explosion protection is compromised Temperature class For distillation the product is h...

Страница 30: ...ff the power supply before opening and wait for 25 minutes Unscrew the locking screw 1 in Figure 2 3 in the box cover NOTE The box cover is equipped with a hinge to prevent it from falling down Turn t...

Страница 31: ...the pressurization of the control box The control unit controls and monitors the flow rate of the protective gas and the inner box pressure during rinsing During operation only the inner box pressure...

Страница 32: ...t must be possible to secure the main switch with a lock to prevent it from being switched on without authorization The emergency off device must be connected in such a way that once the power supply...

Страница 33: ...elivered and must be clearly legible WARNING Danger of injury resulting from illegible symbols Over the course of time stickers and signs can become dirty or otherwise unrecognizable For this reason A...

Страница 34: ...1 Warning Danger of explosion due to ignition sources inside wait 25 minutes 2 Warning Danger of explosions due to electrostatic discharge 3 Warning Do not touch parts that are not intrinsically safe...

Страница 35: ...rnings inside the measuring unit box 5 Warning Danger of injury from fluids under pressure 6 Warning about hot surfaces 7 Warning about dangerous electrical current 8 Sign for wearing safety gloves 9...

Страница 36: ...stic surfaces with a dry cloth can result in static discharge Any sparks could ignite a potentially explosive atmosphere For this reason Always clean plastic surfaces with a damp cloth Sticker 4 see p...

Страница 37: ...under pressure Sticker 5 see p 35 WARNING Danger of injury from fluids under pressure Lines inside the measuring unit box are still under pressure even if the device is switched off In case of defect...

Страница 38: ...system Do not direct drawn off air back into the work room Install washing facilities and eye baths in the workplace Install solvent resistant flooring Creeping vapors can constitute an ignition sour...

Страница 39: ...ed product by thorough rinsing and bleeding for example Make sure that the product properties correspond to the given specifications Vent and drain WARNING Danger of explosions due to uncontrolled che...

Страница 40: ...d control lines must also be free of voltage When work has been concluded close the box firmly and switch on the pressure monitor again with the Explosion protection key switch Flame arresters for Ex...

Страница 41: ...re trained for the special locations in which they work and are aware of the relevant standards and regulations They are also acquainted with the relevant standards and regulations for explosion prote...

Страница 42: ...fill the requirements described here are not aware of the hazards posed in the work area For this reason Keep unauthorized persons out of the work area In case of doubt address these persons and instr...

Страница 43: ...g The following minimum requirements must be met when performing maintenance on the analyzer Antistatic Fire retardant Tight fitting and closed No rings necklaces or other jewelry Safety boots The fol...

Страница 44: ...imit value is exceeded by a factor of 100 self contained respiratory protection apparatus must be used Respiratory protection may only be used when there is an oxygen content of at least 17 in the air...

Страница 45: ...ock may only be removed by once it has been ascertained that there are no persons in the danger area Securing against being switched on again Switch off the power supply If possible secure the switch...

Страница 46: ...d kit blankets etc and fire extinguishers ABC powder within immediate reach Should something happen act correctly Trigger the emergency off device immediately Interrupt connected substance supplies wi...

Страница 47: ...ic pressure Measuring range 20 420 C resolution 0 1 C at 0 100 condensed sample in the receiver Method SAM Standard Analysis Mode RAM Rapid Analysis Mode ASTM D 86 DIN EN ISO 3405 IP 123 Similar to Co...

Страница 48: ...plosion protection Marking according to ATEX 94 9 EC II 2 G IIC T4 Gb see type plate 3 3 Product flows Possible product flows Up to three product flows for measurement in the process Up to three valid...

Страница 49: ...1 to 3 ASTM D 86 Group 4 ASTM D 86 For the definition of the groups see page 60 18 C 23 C or 9 21 K above the pour point but max 50 C Cloud point maximum with trace heating option 25 C Viscosity at in...

Страница 50: ...Consumption rinsing phase 8 Nm 3 h for DPA 4 5 LowP minimum 16 5 Nm h Consumption with vortex cooler 5 50 Nm 3 h depending on cooling capacity Quality class according to ISO 8573 1 Class 2 Purging gas...

Страница 51: ...Inlet temperature General Groups 1 to 3 ASTM D 86 Group 4 ASTM D 86 10 70 C 0 4 C At least 5 K below desired cooling pipe temperature Prefiltered with mesh width 50 m 3 6 Electrical data Voltage suppl...

Страница 52: ...inputs Voltage High Low 15 28 V DC 0 4 V DC Reference potential 0 V ground Analog outputs Signal 4 20 mA Apparent ohmic resistance maximum 1000 Reference potential 0 V ground Digital outputs Voltage 2...

Страница 53: ...tection marking Serial number Year of construction Rated voltage Rated current pre fuse Measuring range Inlet pressure Inlet temperature Consumption Measuring unit The type plate for the measuring uni...

Страница 54: ...ificate number Serial number Year of construction Protective gas Supply pressure Cut off pressure Purging flow rate Purging duration Leakage rate Junction boxes The type plate for the junction boxes i...

Страница 55: ...Distillation Process Analyzer DPA 4 5 Technical data 3 9 Operating and storage conditions Ambient temperature Operation 5 40 C Storage 20 60 C Humidity Operation 5 80 Storage 5 85 December 2013 55...

Страница 56: ...Liquid Petrochemical product discharged via drain Gaseous Petrochemical product purging gas and bubble gas discharged via vent and drain Vent Pressure Atmospheric pressure Back pressure on request Fo...

Страница 57: ...Process Analyzer DPA 4 5 Technical data 3 12 General specifications Weight Device without optional features 250 kg Chiller optional 100 kg Dimensions Width 1 140 mm Height 1 900 mm Depth 710 mm Decem...

Страница 58: ...Design and function 4 Design and function 4 1 Overview Figure 4 1 Analyzer with chiller 1 Measuring unit box 2 Touchscreen 3 Control box 4 Power supply box 5 Signal junction box 6 Chiller optional 7...

Страница 59: ...cess analyzer can be used to monitor both the production process and the defined specifications for mineral oil products Three product flows each with a calibration flow can be connected to the proces...

Страница 60: ...lowered according to ASTM D 86 the FBP may not exceed 400 C Nitrogen is added to the sample in the receiver Along with the nitrogen the fill level in the receiver is measured via a differential press...

Страница 61: ...s on the composition and expected volatility properties of the product The assignment to a group determines the product s inlet temperature and the cooling medium temperature for the condenser among o...

Страница 62: ...w 1 Outlet filter 2 Cooling pipe 3 Flame arrester for instrument air 4 Flame arrester for bubble gas 5 Receiver 6 Inlet flame arrester for product 7 Metering pump 8 Vent flame arrester 9 Outlet flame...

Страница 63: ...e receiver 5 The collected quantity of product can be measured with a differential pressure measuring device by bubbling in nitrogen To fill the distillation flask 12 fresh product is fed into the rec...

Страница 64: ...e 4 3 Outside of the control box 1 Stylus for touchscreen 2 Touchscreen 3 Pressure monitor display 4 Explosion protection switch The pressurized enclosure of the control box also contains all electric...

Страница 65: ...PC that provides the user interface controls and monitors all processes and performs external communications IO card for processing internal and external digital and analog inputs and outputs Power s...

Страница 66: ...ing the cooling medium If the optional receiver tempering is installed there will normally be a needle valve for adjusting the flow of cooling medium through the receiver It can only be omitted if coo...

Страница 67: ...n Fluid technology DPA 4 5 LowP Figure 4 6 Fluid technology for DPA 4 5 LowP 1 Vacuum ejector pressure regulator 2 Bubble gas pressure regulator 3 Pressure monitor pressure regulator 4 Pressure regula...

Страница 68: ...ressurization of the control box The control unit controls and monitors the flow rate of the protective gas and the inner box pressure during rinsing During operation only the inner box pressure is mo...

Страница 69: ...11 Drain Design The optional sample conditioning system is upstream of the product supply system The components are arranged as follows in the sample flow direction Connection for product inlet Inlet...

Страница 70: ...e receiver optional and any other applications For more information on the chiller please refer to the accompanying handbook Receiver tempering Depending on the product in addition to the cooling of t...

Страница 71: ...h temperatures can occur on the inside of the control box To prevent this the box can be equipped with a vortex cooler Serial interface Serial interface for data exchange Measured values are output us...

Страница 72: ...igure 4 9 Connections 1 Product outlet drain 6 Cooling medium outlet 2 Vent DPA 4 5 LowP second separate vent 7 Instrument air inlet 3 Validation product inlet 8 Cooling medium inlet 4 Product inlet 9...

Страница 73: ...ure monitor is switched off The control box contains ignition sources Operating the device when the pressure monitor of the control box is deactivated can result in explosions in potentially explosive...

Страница 74: ...ith coalescer and filter unit for setting the primary pressure of instrument air and nitrogen The pressure regulator protects against particles and moisture entering the instrument air or nitrogen in...

Страница 75: ...ly immediately prior to assembly Suspended loads WARNING Danger of death due to suspended loads When loads are being lifted falling or uncontrollably swinging components pose a danger to life and limb...

Страница 76: ...r material damage if adequate space to maneuver is not provided For this reason Make sure that neither persons nor obstacles are in the swing range WARNING Danger of injury from transport item tipping...

Страница 77: ...wise the content can be damaged Protect against moisture Protect the packaged items against moisture and store in a dry place Lift here Lifting equipment chains lifting belts should only be attached t...

Страница 78: ...for the expected transport conditions Only environmentally sound materials have been used for the packaging The packaging is designed to protect the individual components from transport damage corros...

Страница 79: ...r DPA 4 5 Transport packaging and storage 5 5 Center of gravity and suspension eyebolt L T H 1 2 Figure 5 1 Center of gravity 1 Suspension eyebolt 2 Center of gravity with chiller HxLxD approx 900 x 5...

Страница 80: ...the packaged item and commence transport Transport with a crane device without packaging The device can be transported with a crane under the following conditions The crane and lifting equipment must...

Страница 81: ...rature 20 to 60 C The storage room may not be subject to large temperature fluctuations Risk of condensation forming Relative humidity 5 to 85 non corrosive If the device is to be stored for longer th...

Страница 82: ...ith ATEX Directive 94 9 EC Written permission hot work permit must be obtained for all work with flames or hot materials Keep a fire extinguisher at close hand Stop work at once in the event of fire L...

Страница 83: ...certain tasks this will be mentioned in the warnings in this chapter Fundamental principles WARNING Danger of injury due to improper installation and commissioning Improper installation and commission...

Страница 84: ...otherwise result in a short circuit Securing against being switched on again DANGER Danger of death due to unauthorized restarting During installation work there is the danger that the power supply c...

Страница 85: ...ork room is sufficiently ventilated Adhere to emission limit values If necessary install an exhaust air treatment system Do not direct drawn off air back into the work room Install washing facilities...

Страница 86: ...in use for the control box make sure that at the very most dripping water can hit the device in compliance with EN 60529 Make sure that the hot air discharge of the vortex cooler is not hindered 6 3 F...

Страница 87: ...fications can pose a danger to persons and property Unauthorized modifications to the device of any kind constitute a high safety risk for personnel and the device itself For this reason Do not instal...

Страница 88: ...ith skin or eyes can lead to serious permanent health damage or death For this reason Avoid direct exposure Do not inhale vapors If unknown concentrations or concentrations above the limit values for...

Страница 89: ...e before beginning any work General instructions Before establishing the pipe connections equip the supply lines to the device for the product instrument air nitrogen and cooling medium each with a ma...

Страница 90: ...pressure Greater variations affect the results of measurements Connect the analyzer to a separate vent if necessary A Vent drain system The analyzer is equipped with a combined vent drain system as s...

Страница 91: ...tion is installed connect the supply and return lines to the correspondingly labeled connections on the sample conditioning system Cooling with cooling medium NOTE The pipe connected to the cooling me...

Страница 92: ...ical current DANGER Danger of death due to electrical current Touching voltage conducting parts poses an immediate life threatening hazard Damage to the insulation or to individual components can caus...

Страница 93: ...rrupted no situations can arise that endanger persons or property Install the main switch and emergency off device in an easily accessible location close to the device Label the main switch and emerge...

Страница 94: ...escribed in the terminal plan 8 Tighten the cable ducts 9 Close unused cable ducts and drill holes for cable ducts professionally 10 Attach the contact protection to the terminals again 11 Lock the po...

Страница 95: ...at first when no more air escapes open it completely 3 Open the system side shut off valve in the instrument air supply line carefully 4 Rinse the supply line for at least 2 minutes If dirt is still...

Страница 96: ...e corresponding operational data plates on the analyzer A pressure regulator may be installed for the vortex cooler as an option The analyzer is now supplied with instrument air Additionally set the v...

Страница 97: ...2 Open the screw connection of the cooling medium inlet supply line see page 72 slightly at first when no more cooling medium escapes open it completely 3 Place a collection container with a capacity...

Страница 98: ...o not require any external cooling medium see page 97 NOTE Fill the chiller with cooling medium on commissioning Filling the chiller 4 3 1 2 Figure 6 1 Filling the chiller Open and remove the cover of...

Страница 99: ...cooling medium supply lines are clean see page 97 Procedure Open the system side shut off valve of the cooling medium supply line Check whether the screw connection is sealed tightly Cooling medium f...

Страница 100: ...ids could cause serious injuries For this reason Before performing any work disconnect the supply lines and depressurize them Wear suitable protective goggles and gloves Hazardous substances WARNING D...

Страница 101: ...ne NOTE The analyzer can be fitted with an optional sample conditioning system see page 69 The product inlet is then located on the product conditioning system 2 Open the screw connection of the produ...

Страница 102: ...ion and preparation for commissioning 9 Dispose of the product in the collection container professionally Rinse all product and validation product supply lines as described above Check the connections...

Страница 103: ...med NOTE Installing the analyzer and the necessary preparations for commissioning are described in Chapter 6 7 1 Safety Personnel Commissioning is only to be performed by specialists for potentially e...

Страница 104: ...can lead to serious permanent health damage or death For this reason Avoid direct exposure Do not inhale vapors If unknown concentrations or concentrations above the limit values for the particular su...

Страница 105: ...with the specifications in the installation plan and technical data The product is sufficiently filtered in accordance with the technical data The product supply line is clean see page 100 for detail...

Страница 106: ...th instrument air This results in considerable noises emissions The pressure monitor displays the remaining rinsing time During the purging phase all electrical operating equipment without its own ign...

Страница 107: ...system side flow meter If necessary re adjust the flow meter If necessary repeat the adjustments to the pressure regulator and flow meter until the target values are attained Operation In normal oper...

Страница 108: ...of accidents Explosion protection WARNING Explosion protection is no longer provided when the pressure monitor is switched off The control box contains ignition sources Operating the device when the...

Страница 109: ...missioning chapter Procedure Open the shut off valve in the product supply line Switch on the power supply with the main switch The control box is purged with instrument air This results in considerab...

Страница 110: ...works fully automatically The analysis process can be followed on the analyzer s touchscreen The analyzer can be operated with the touchscreen stylus NOTE For more detailed information on operating c...

Страница 111: ...chscreen Click Exit Click Shutdown in the operating system Wait until the control computer has shut down Switch off with the analyzer main switch The petrochemical product continues to flow through th...

Страница 112: ...in the device For this reason Only use the emergency off function in genuine emergencies During normal operation always shut the device down first using the software function After the emergency Depe...

Страница 113: ...anufacturer Service address BARTEC BENKE GmbH Borsigstra e 10 D 21456 Reinbek Germany Tel 49 0 40 72703 0 Fax 49 0 40 72703 363 E mail service bartec benke de 9 1 Safety Personnel The work described i...

Страница 114: ...screw tightening torques Electrical current DANGER Danger of death due to electrical current Touching voltage conducting parts poses an immediate life threatening hazard Damage to the insulation or to...

Страница 115: ...ver deactivate the explosion protection during normal operation Leave the key switch in the Explosion protection On position Deactivation of the explosion protection Explosion protection Off position...

Страница 116: ...lead to serious permanent health damage or death For this reason Avoid direct contact Do not inhale vapors If unknown concentrations or concentrations above the limit values for the particular substa...

Страница 117: ...principle If faults arise that pose a direct danger to personnel or property switch the analyzer off immediately with the emergency off device Investigate the cause of the fault Depending on the type...

Страница 118: ...No display on the pressure monitor The power supply of the device has been interrupted e g defective tripped fuse Check the power supply and restore it The pre fuse of the pressure monitor only presen...

Страница 119: ...low see display on flow controller Product supply line shut off valve is closed primary pressure too low leakage product has run out filter is blocked Analyzer product has run out leakage Drain blocke...

Страница 120: ...emperature of the cooling medium is too high Make sure that the cooling medium is treated in accordance with the technical data specifications The temperature of the cooling pipe is too low The temper...

Страница 121: ...a fault conduct the following steps for restarting Reset the emergency off device If necessary acknowledge the alarms issued by the process software PACS see software handbook Make sure that nobody c...

Страница 122: ...rk Safety goggles Safety gloves NOTE If other safety equipment is to be worn for certain tasks this will be mentioned in the warnings in this chapter Fundamental principles WARNING Danger of injury du...

Страница 123: ...ng fuses check that they are of the correct type Keep moisture away from voltage conducting parts This could otherwise result in a short circuit Securing against being switched on again DANGER Danger...

Страница 124: ...an lead to serious permanent health damage or death For this reason Avoid direct exposure Do not inhale vapors If unknown concentrations or concentrations above the limit values for the particular sub...

Страница 125: ...ources of ignition The control box contains ignition sources Opening in potentially explosive atmospheres can cause explosions Before opening ensure that no potentially explosive atmosphere is present...

Страница 126: ...tentially explosive atmospheres Depending on application Monthly to every 2 years Clean replace the distillation flask Every 6 months Check the safety equipment Check that all electrical terminals are...

Страница 127: ...10 1 Toolbox Figure 10 2 Toolbox with tools and spare hoses 1 Spare pneumatic hose 6 4 mm 2 3 9 mm cotter pin driver for heating cartridges and flame arresters 3 Handle for opening measuring unit box...

Страница 128: ...and must not be damaged To clean the touchscreen only use water and detergent or monitor cleaning foam Cleaning the touchscreen Switch off the device When touching the touchscreen functions can be ina...

Страница 129: ...5 2 Checking the safety equipment Procedure The external safety markings can be checked while the device is operating The signs and positioning of the warning labels and stickers are on page 33 To ch...

Страница 130: ...the housing or installations No open drill holes No assembly notches Door closed catch secured with screw Measuring unit box Cover fastened with locking screw No damage to the housing or built in comp...

Страница 131: ...age free at the output terminals of the pressure monitor and other contactors if applicable To do this open the power supply box using a double bit key If no voltage is present then the pressure monit...

Страница 132: ...The distillation flask can also be cleaned by the manufacturer To do this send the distillation flask to BARTEC BENKE You can find contact details on page 14 Personal protective equipment Safety gogg...

Страница 133: ...Process Analyzer DPA 4 5 Maintenance Removing the distillation flask and expansion tank Open the plug connections 1 3 Figure 10 1 Unplugging the distillation flask heater and temperature sensor Decem...

Страница 134: ...with a felt tip pen to ensure that they are reassembled correctly Use another wrench to hold the other side of the bolt connections Loosen the hose connection 1 and the bolt connection on the bubble...

Страница 135: ...k the bolt connections with a felt tip pen to ensure that they are reassembled correctly Use another wrench to hold the other side of the bolt connections Remove bolts 1 5 in order Carefully remove th...

Страница 136: ...the opening at the top Remove coking on the bottom of the flask by blasting it with nutshell granulate To do this guide the angled pipe down into the distillation flask Remove all residue of blasting...

Страница 137: ...bubble pipe and turn the bit while pushing it back and forth Repeat this until all the coking has been detached and the pipe is largely free Installing the distillation flask and expansion tank Assem...

Страница 138: ...e lined up and the cables are laid correctly Only hand tighten the bolts 1 to 6 at first It should be possible to put in the distillation flask without any major strain Using another wrench as a count...

Страница 139: ...ansion tank back in the correct position see the illustration below Only hand tighten the bolt 1 at first Using another wrench as a counterhold tighten the bolts until the markings line up This is rou...

Страница 140: ...connections Plug the connectors 1 3 back together Figure 10 10 Plugging in the distillation flask heater and temperature sensor Close the measuring unit box Restarting operation For the steps to be ta...

Страница 141: ...Figure 4 2 on page 62 through which the petrochemical product flows need to be cleaned on a regular basis In case of clean products e g gasoline annual cleaning is normally sufficient Product impuriti...

Страница 142: ...lters 2 are equipped with gaps with a left hand angular offset Personal protective equipment Safety goggles Safety gloves hazardous substances Required tools Open end wrenches of the following sizes 1...

Страница 143: ...of the inner box A kind of punch made of plastic is best suited to prevent damage to the flame filters Checks Check that the O ring 6 is in perfect condition Replace it if necessary Replacement parts...

Страница 144: ...become loose and the strips of the filter disc can be moved easily New flame filters can be obtained from BARTEC BENKE To order them information on the filter gap width the material and the angular o...

Страница 145: ...embly paste penetrates the interior If the outer box has been removed from the Ex d box e g for complete replacement of the flame arrester Before screwing the outer box into the Ex d box make sure the...

Страница 146: ...this is also defective you can replace it at the same time Required tools 2 5 mm Allen key Plastic mallet Supplied 3 9 mm cotter pin driver see page 127 To remove the heating cartridges carry out the...

Страница 147: ...Figure 10 12 Loosening the flask bottom temperature sensor holder Undo the screw 1 of the flask bottom temperature sensor holder 2 3 Figure 10 13 Removing the flask bottom temperature sensor Carefully...

Страница 148: ...able In some cases the heating rods may be stuck so tight in their holes that they cannot be pulled out In this case proceed as follows 2 Figure 10 15 Removing the heating cartridges Use the supplied...

Страница 149: ...taken after maintenance work please refer to page 151 10 5 8 Replacing the battery of the industry PC The analyzer is controlled using an industry PC It is located in the control box see page 64 The i...

Страница 150: ...sive atmospheres Therefore Always only use replacement batteries from BARTEC BENKE CAUTION Unsuitable batteries can damage the industry PC Therefore Always only use replacement batteries from BARTEC B...

Страница 151: ...covers have been properly reinstalled Make sure that all tools materials and other equipment used have been removed again from the work area Clean the work area and remove any substances that have le...

Страница 152: ...rgy components with sharp edges points and corners in and around the device or on the required tools can cause injuries For this reason Before starting work ensure there is adequate space for the dism...

Страница 153: ...hould only be performed by a qualified electrician Special tools required Electrician s equipment Electrical current DANGER Danger of death due to electrical current Touching voltage conducting parts...

Страница 154: ...ally explosive atmospheres Personal protective equipment Safety goggles Safety gloves Hazardous substances WARNING Danger of injury from toxic substances Swallowing inhaling or contact with skin or ey...

Страница 155: ...Disconnecting pipe connections Check that the pressure has been fully released Collect any residual materials that may emerge separately Disconnect the pipe connections in accordance with the installa...

Страница 156: ...crap material and components lubricants and other auxiliary media must be treated as hazardous waste and may only be disposed of by approved specialist companies Your local authorities or specialist d...

Страница 157: ...tillation 60 Distillation flask 62 Distillation group 61 Distillation process 60 E Electrical current 15 Emergency off 112 Emissions 56 F Fault table 118 Faults 113 FBP 47 60 61 Fill level 60 Final bo...

Страница 158: ...g 66 70 Recovery system 70 Replacement parts 14 Respiratory protection depending on air recirculation 44 S Safety 15 Safety boots 43 Safety devices 25 Safety equipment commissioning 103 faults 113 gen...

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