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254 . Clarus 590 GC User’s Guide
5.
Single Point is the default setting. When the Single Point Calibration radio button is selected, the
Offset field is active and the GC Tune drop down field is inactive. (GC Tune is only available if it is
downloaded. A successful tune must be performed in order for GC tune to be enabled. Only
those channels for which a valid tune exists will be available on the drop down list. The selection
will be made from the external GC Tune software, but the user may override this.)
The actual temperature under the single point radio button is the time-averaged actual oven
temperature.
6.
Allow the oven temperature to equilibrate for at least 30 minutes by setting the time in the
Equilibrate
field. Press
OK
. The displayed temperature will approach 100.00
°
C (or the oven
temperature you entered in step 4), and the thermometer readout will approach a value close to
100.00
°
C.
Enter the Required Offset Value
1.
After the temperature has stabilized, subtract the thermometer reading from the actual oven
temperature shown on the previous screen.
2.
Using the plus and minus keys enter a value into the above screen, then press OK. For example,
if the the rm om e te r re a ds 101.55 C, a nd the ove n te m pe ra ture re a ds 100.10 C, type a va lue of
-
1.45 C.
Remove the Thermometer Probe
After temperature calibration is satisfactory:
1.
Open the oven door and allow the oven to cool until the fan stops.
2.
Remove the temperature probe.
3.
Fill in any hole left by the probe in the oven insulation.
4.
Replace the left-side instrument cover.
Summary of Contents for CLARUS 590 GC
Page 1: ...CLARUS 590 GC User s Guide GAS CHROMATOGRAPHY ...
Page 9: ...About This Manual 9 Flame Ionization Detector FID 270 TCD 273 Autosampler 277 Index 279 ...
Page 10: ...10 Clarus 590 GC User s Guide ...
Page 11: ...1 Introduction ...
Page 12: ...12 Clarus 590 GC User s Guide ...
Page 21: ...2 Touch Screen Navigation ...
Page 22: ...22 Clarus 590 GC User s Guide ...
Page 48: ...48 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Page 50: ...50 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Page 59: ...3 Using the Active Method ...
Page 60: ...60 Clarus 590 GC User s Guide ...
Page 109: ...4 Setting Up the Detectors ...
Page 110: ...110 Clarus 590 GC User s Guide ...
Page 197: ...5 Using the Method Editor ...
Page 198: ...198 Clarus 590 GC User s Guide ...
Page 207: ...6 Using the Tools Menu ...
Page 208: ...208 Clarus 590 GC User s Guide ...
Page 224: ...224 Clarus 590 GC User s Guide ECD PID NPD FPD ...
Page 225: ...Detectors 225 Output Configured ...
Page 262: ...262 Clarus 590 GC User s Guide ...
Page 263: ...7 Setting up a Typical Analysis ...
Page 264: ...264 Clarus 590 GC User s Guide ...
Page 279: ...Index ...
Page 280: ...280 Clarus 590 GC User s Guide ...