134 . Clarus 590 GC User’s Guide
The make-up gas control valve consists of an outer ring (used to turn the make-up gas completely off or
on), a protective cap, and an inner needle valve (used to adjust the flow of make-up gas). Removing the
cap exposes the needle valve adjustment screw. To set flow, use a small thin screwdriver (P/N 09907273),
supplied in the shipping kit) to turn the adjustment screw. Turn the screwdriver counterclockwise to
increase the flow or clockwise to decrease the flow.
You should only adjust make-up gas flow after a column has been installed and the carrier gas flow or
pressure has been set to the value required for the analysis.
Make-up gas need not be added when using packed columns, where the carrier gas flow is 30 mL/min or
higher.
To adjust the make-up gas:
1.
Turn the outer ring of the make-up valve fully clockwise.
2.
From the System Status window touch
Tools
. From the Tools drop down menu touch
Utilities
.
3.
In the Utilities screen touch
Stopwatch
icon.
4.
Measure the flow rate. For best accuracy, use a soap bubble flowmeter volume that gives a reading
of at least 30 seconds.
Summary of Contents for CLARUS 590 GC
Page 1: ...CLARUS 590 GC User s Guide GAS CHROMATOGRAPHY ...
Page 9: ...About This Manual 9 Flame Ionization Detector FID 270 TCD 273 Autosampler 277 Index 279 ...
Page 10: ...10 Clarus 590 GC User s Guide ...
Page 11: ...1 Introduction ...
Page 12: ...12 Clarus 590 GC User s Guide ...
Page 21: ...2 Touch Screen Navigation ...
Page 22: ...22 Clarus 590 GC User s Guide ...
Page 48: ...48 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Page 50: ...50 Clarus 590 GC User s Guide PPC Active Method Configuration Screen Manual Pneumatics ...
Page 59: ...3 Using the Active Method ...
Page 60: ...60 Clarus 590 GC User s Guide ...
Page 109: ...4 Setting Up the Detectors ...
Page 110: ...110 Clarus 590 GC User s Guide ...
Page 197: ...5 Using the Method Editor ...
Page 198: ...198 Clarus 590 GC User s Guide ...
Page 207: ...6 Using the Tools Menu ...
Page 208: ...208 Clarus 590 GC User s Guide ...
Page 224: ...224 Clarus 590 GC User s Guide ECD PID NPD FPD ...
Page 225: ...Detectors 225 Output Configured ...
Page 262: ...262 Clarus 590 GC User s Guide ...
Page 263: ...7 Setting up a Typical Analysis ...
Page 264: ...264 Clarus 590 GC User s Guide ...
Page 279: ...Index ...
Page 280: ...280 Clarus 590 GC User s Guide ...