Installation and commissioning
multi N/C pharma HT
60
CAUTION
Risk of poisoning due to ozone
The ozone generator contained in the device produces ozone (O
3
). When used in accor-
dance with the intended use, the downstream ozone decomposer decomposes the poi-
sonous gas. Various safety measures result in the automatic shut-down of the ozone
generator. The following nevertheless applies:
¡
If there is a sharp smell of ozone, switch the device off immediately and inform cus-
tomer service.
¡
To guarantee perfect and safe operation, Analytik Jena recommends annual inspec-
tion and maintenance by customer service.
Installation on the analyzer
}
Set up the detector next to the analyzer.
}
Connect the carrier gas to the gas connection with quick-release coupling.
}
Set up the gas connection between the detector and the analyzer:
– "sample in" connection on the detector
– "CLD" connection on the analyzer
}
Connect the "CLD" interface on the rear of the analyzer with the RS 232 interface on
the detector via the supplied serial data cable.
}
Switch on the detector. The status LED indicates operational readiness.
Checking and changing the
configuration
}
Switch on the analyzer and the detector. Start the multiWin program and initialize
the analysis system.
}
Check the device configuration with the Instrument | System-Information menu op-
tion in the multiWin set-up info window.
}
If necessary, change the configuration:
– Exit the multiWin program.
– Start the setup tool in the Windows interface with Start | Program files | multi-
Win | multiWin setup tool.
– Select the detector (CLD-TOC) in the N-measurement list.
– Exit the multiWin set-up tool window with [Create].
– Start the multiWin program and initialize the analysis system.
– Open the Options window with menu option Configuration | Edit options. Go to
the Analyzer components tab.
}
In the Sensors group, activate nitrogen measurement with the N-measurement ak-
tive option.
}
Exit the window with [OK].
4.3.5
Integrated solids module
An integrated solids module, the Swab Test module, can be added to the combustion
system of the analyzer. Small amounts of solid samples can be examined with the solids
module, e.g., during cleaning validation.
The module achieves digestion temperatures of up to 950 °C. Sample digestion is per-
formed by catalysts.
