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EVEL

CCURACY

& P

RECISION

ERIFICATION

ROTOCOL

.............................

Sievers M500e TOC Analyzer

Operation and Maintenance Manual

DLM 78510-02 EN Rev. B

226

Low Level Accuracy & Precision Verification Protocol

1.0 I

NTRODUCTION

Perform the following Accuracy & Precision Protocol to verify accuracy and precision

methods of a Sievers M500e TOC Analyzer.

2.0 S

COPE

This procedure applies to the Sievers M500e TOC Analyzer.

3.0 M

ATERIALS

NOTE:

Use

only

Sievers standards purchased from SUEZ.

3.1 Sievers M500e TOC Analyzer

3.2

Accuracy & Precision Verification Worksheet

3.3

Low Level Accuracy/Precision Verification Standard Set:

3.3.1 One vial — Rw Blank
3.3.2 One vial — 100 ppb TOC

4.0 D

EFINITIONS

4.1 None

5.0 P

ROCEDURE

5.1 If the Analyzer is taking measurements, click

Stop Analysis

5.2 On the

System Protocols

screen, select the

Verification

tab.

Summary of Contents for Sievers M500e

Page 1: ...DLM 78510 02 EN REV B Total Organic Carbon TOC Analyzer Sievers M500e 1 05firmwareorlater Sievers M500e operation and maintenance manual ...

Page 2: ...tact Customer Care at 1 800 255 6964 or your local service provider For a copy of the Declaration of Conformity and ISO 9001 Registration Visit our website Customer Support Sievers Analyzers Instruments Sievers Accreditations Certificates ISO Certifications and Accreditations or Declarations of Conformity Electronic versions of the Analyzer s Operation and Maintenance Manual and the M500 Qualifica...

Page 3: ...02 EN Rev B 3 SUEZ 2022 IDENTIFICATION RECORDS Analyzer serial number _____________ This is located on the side of the Analyzer Date of receipt and installation of Analyzer _____________ This is the warranty start date Default Administrative User ID ADMIN Default Administrative Password SIEVERS ...

Page 4: ...s 18 Chapter 1 Introduction 52 Chapter 2 System Description 53 System Specifications 53 System Overview 54 Sample Flow Path 55 Additional System Components 57 Microprocessor Controller and Electronics 57 Data Outputs 57 Chapter 3 Installation 58 Overview 58 Step 1 Unpack and Inspect the Analyzer 59 Packing List 60 Additional Installation Equipment 61 Step 2 Complete the Identification Records 62 S...

Page 5: ...Installing a USB Connection for Data Transfer Optional 88 Installing a Serial Connection Optional 88 Installing an Ethernet Connection Optional 89 Step 9 Configure Basic Analyzer Settings 90 Enabling Analyzer Security Optional 90 Enabling Password Protection Optional 90 Configuring Local Settings 92 Setting the Measurement Mode 94 Configuring an Ethernet Connection 98 Enabling a PDF Printer 100 Se...

Page 6: ...s Data Tab 132 The Settings Screen 133 Settings Screen System Setup Tab 133 Configuring Local Settings 133 Configuring Result Preferences 136 Setting Trend Graph Display Options 137 Configuring Export Preferences 138 Settings Screen Instrument Settings Tab 140 Viewing System Constants 140 Saving System Constants 140 Printing and Exporting or System Constants 140 Importing System Constants 142 Sett...

Page 7: ... Settings Screen Errors Tab 166 Settings Screen Backup Restore Tab 167 Backing Up the Database 167 Scheduling Automatic Database Backups 169 Archiving the Database 171 Restoring a Backup 175 Restoring System Constants 176 The Data Screen 177 Reviewing Data History 177 The Password Protection Screen 182 The Help Screen 182 Chapter 5 Password Protection 183 Overview 183 Password Protection 183 Using...

Page 8: ...fication Protocol 226 Reviewing Calibration and Verification History 229 Protocol and Calibration Worksheets 231 4 20 mA Output Operation Verification Optional Worksheet 232 TOC Single Point Calibration Worksheet 233 Low Level TOC Single Point Calibration Worksheet 234 TOC Multi Point Calibration Worksheet 235 TC IC Conductivity Autozero Worksheet 236 TOC Autozero Worksheet 237 Accuracy Precision ...

Page 9: ...lems with The DI Water Pump 253 Using the Diagnostics Menu 253 System Tests 255 Alarms 255 Analog Outputs 257 Modbus 258 Network Folder 259 Printer 260 Sample Flow Rate 260 IC Power Relay 261 Internet Connection 261 USB Serial Loopback 262 Serial Loopback 263 WiFi 263 Export Diagnostics 264 Service Diagnostics 265 Level 1 Diagnostics 266 Step 4 Contact Technical Support 266 Step 5 Return the Analy...

Page 10: ...h Standard iOS 291 Analyzer Configured with Sample Inlet Block 294 Appendix B Streaming Data 297 Data Streaming Methods 297 To stream data via a serial RS 232 port 297 To stream data via Ethernet 298 Determining Your Communications Port Number 299 Appendix C Warning and Error Descriptions 300 Appendix D DI Water Installation Details 308 Additional DI Water Installation Details 308 Installing the r...

Page 11: ...O Panel 9 Pin Male D Connector 89 Table 4 1 The Analyzer s Standard Toolbar 119 Table 6 1 Standards Required for TOC Single Point Calibration 192 Table 6 2 Standards Required for TOC Multi Point Calibration 192 Table 6 3 Standards Required for Accuracy Precision Verification 192 Table 8 1 Replacement Schedule for Consumables 272 Table 8 2 Sievers M500e TOC Analyzer 3 Year Maintenance Worksheet 285...

Page 12: ...en when Password Protection is not enabled 113 Figure 4 2 Home screen when Password Protection is enabled 114 Figure 4 3 The Standard iOS System 116 Figure 4 4 The Sample Inlet Block 116 Figure 4 5 Standard Toolbar 119 Figure 4 6 The Home Screen 123 Figure 4 7 Online Data Graphical View 131 Figure 4 8 Online Data Table View 132 Figure 4 9 Online Data Details 132 Figure 4 10 System Protocols and Gr...

Page 13: ...istered trademark of E I du Pont de Nemours Windows and Excel are registered trademarks of the Microsoft Corporation The Analyzer described in this manual is covered by one or more patents issued to and owned or pending by SUEZ including the following US 6723565 and any of its non US counterparts US 8101417 and any of its non US counterparts US 8003048 and any of its non US counterparts US 9116099...

Page 14: ...interventions are to be reviewed and authorized as correct and complete at the completion of the service by a customer representative or designate SUEZ warrants these services for 30 days after the authorization and will correct any qualifying deficiency in labor provided that the labor service deficiency is exactly related to the originating event No other remedy other than the provision of labor...

Page 15: ...f merchantability and fitness for a particular purpose LIMITACIÓN DE REMEDIOS Y RESPONSABILIDAD La garantía anterior no se aplicará a los defectos que resulten de la realización incorrecta o inadecuada de la instalación el mantenimiento el ajuste la calibración o el manejo por parte del cliente La instalación el mantenimiento el ajuste la calibración o el manejo deberán llevarse a cabo de acuerdo ...

Page 16: ...e à une autre partie sans l autorisation expresse écrite du groupe SUEZ SUEZ exclut tout particulièrement les garanties implicites de commercialisation et d adaptabilité dans un but spécifique BESCHRÄNKTE ANSPRÜCHE UND HAFTUNG Die vorangehende Garantie gilt nicht für Schäden die aus unsachgemäßer oder unzureichender Installation Wartung Anpassung Kalibrierung oder Betrieb durch den Kunden resultie...

Page 17: ...relato La garanzia è valida solo per l acquirente originale La presente garanzia limitata non è trasferibile dall acquirente originale a terzi senza l espresso consenso scritto da parte di SUEZ SUEZ declina espressamente le garanzie implicite di commerciabilità e idoneità a un particolare scopo 限定責任および救済前述の保証はお客様による不適切または不十分な取り付け保守調整校正あるいは操作によって生じた不具合には適用されないものとします取り付け保守調整校正または操作は Oper...

Page 18: ...ive earth terminal ground for the Analyzer This symbol indicates the European Union Directive 2012 19 EU for waste electrical and electronic equipment WEEE requires disposing the Analyzer separately from standard waste To avoid potentially dangerous shock before opening the Analyzer stop any analysis and power off the operating system Click the Power Off P button in the Analyzer s firmware then tu...

Page 19: ...y be impaired To avoid injury and to ensure accurate analysis results ensure that the Analyzer door is closed and latched during normal operation This symbol on the instrument indicates that the product does contain restricted substances included in China RoHS II Please refer to the following table Please Note This product contains a UV Lamp with Hg which meets the exemption defined in Annex III 4...

Page 20: ... or local government regulations In the case of any broken or damaged UV lamp handle the remains in accordance with your organization s toxic waste handling procedure and dispose of them in accordance with federal state or local government regulations The WEEE Directive 2012 19 EU applies to batteries and requires their removal and separate collection Once removed the used batteries are governed b...

Page 21: ... always apply liquid to the cloth directly and do not spray liquids directly on the Analyzer Do not use water or cleaners on the touchscreen as water can damage or discolor the polarizer Refer to the next section for recommendations on cleaning the touchscreen Wipe away any condensation immediately Operating the Analyzer in Online mode with no sample flow and with the Flow Sensor off can result in...

Page 22: ...nalizador Este símbolo indica que para cumplir con la Directriz de la Unión Europea 2012 19 EU relacionada con el desecho de equipos eléctricos y electrónicos WEEE el Analizador deberá desecharse por separado de los residuos comunes Para evitar posibles descargas eléctricas antes de abrir el analizador detener todo análisis en marcha y apagar el sistema operativo Pulsar el botón OFF P en el Firmwa...

Page 23: ...ner el análisis antes de apagar el analizador Este es un producto con seguridad de Clase I Se debe instalar a un suministro de alimentación con descarga a tierra Para evitar daños al analizador y la posibilidad de sufrir lesiones asegurarse de que el instrumento esté conectado a una línea de alimentación de la tensión correcta Este es un producto de Clase A En un entorno residencial este producto ...

Page 24: ...á la garantía Para evitar los daños al Analizador instale el filtro y reemplace el elemento filtrante según sea necesario Asegúrese de que el reservorio de agua DI pizeta esté lleno en especial cuando se analizan muestras con TOC elevado o altas concentraciones de sal Después de analizar muestras con TOC elevado o alto contenido de sal siempre enjuague el Analizador haciendo correr agua DI de bajo...

Page 25: ... táctil Seque toda condensación de inmediato Cuando se haga funcionar el analizador en modo En línea sin que haya caudal de muestras y con el sensor de flujo apagado se pueden obtener mediciones erróneas Los estándares para el Analizador de TOC Sievers M500 En línea son acidificados Si se preparan estándares propios y se utilizan viales de cristal asegurarse de acidificar dichos estándares a un pH...

Page 26: ...à terre de l analyseur Ce symbole indique que pour la conformité avec la directive 2012 19 EU de l Union Européenne concernant les matériels électroniques et électriques mis au rebut l analyseur doit être éliminé séparément des déchets standards Pour éviter tout choc potentiellement dangereux avant d ouvrir l analyseur arrêtez toute analyse et mettez le système de fonctionnement hors tension Appuy...

Page 27: ...l doit être raccordé à une source d alimentation électrique mise à la terre Pour éviter tout dommage à l analyseur et tout risque de blessure assurez vous que l analyseur est connecté à une ligne d alimentation électrique de la tension appropriée Cet équipement correspond à la classe A de la FCC Dans un environnement domestique cet équipement risque de causer des interférences électromagnétiques P...

Page 28: ...analyseur installer le filtre et remplacer l élément filtrant quand nécessaire Vérifier que le réservoir d eau DI soit plein notamment lorsque l analyse d échantillons à forte teneur en COT ou de sel est réalisée Après l analyse d un échantillon à concentration élévée en COT ou en sels toujours rincer l analyseur en exécutant un cycle d analyse avec un échantillon contenant de l eau ultrapure Cons...

Page 29: ...e de l écran tactile Essuyez immédiatement toute condensation Faire fonctionner l analyseur en mode en ligne sans aucun débit d échantillon et avec le capteur de débit éteint peut entraîner des mesures erronées Les standards de l analyseur COT en ligne Sievers M500 sont acidifiés Si vous préparez vos propres standards et utilisez des fioles en verre assurez vous d acidifier les étalons à un pH de ...

Page 30: ...e des Analysators an Dieses Symbol zeigt an dass der Analysator gemäß der EU Richtlinie 2012 19 EU zur Entsorgung von Elektro und Elektronik Altgeräten getrennt vom Normalmüll zu entsorgen is Um einen potenziell gefährlichen Schock zu vermeiden stoppen Sie vor dem Öffnen des Analysegeräts jegliche Analyse und schalten Sie das Betriebssystem aus Drücken Sie die Ausschalttaste in der Firmware des An...

Page 31: ...odukt der Schutzklasse I Es muss an eine geerdete Stromquelle angeschlossen werden Um Schäden am Analysator und die Gefahr von Verletzungen zu vermeiden stellen Sie sicher dass der Analysator an eine Stromversorgung mit der richtigen Spannung angeschlossen ist Dies ist ein Klasse A Produkt In einer häuslichen Umgebung kann dieses Produkt elektromagnetische Störungen verursachen Ergreifen Sie geeig...

Page 32: ...lysator den Inline Filter und tauschen Sie das Filterelement nach Bedarf aus Stellen Sie sicher dass der DI Wassertank gefüllt ist insbesondere bei Probenläufen mit hohem TOC Gehalt oder hohen Salzkonzentrationen Spülen Sie den Analysator nach dem Lauf von Proben mit hohem TOC oder Salzgehalt immer mit DI Wasser mit niedrigem TOC Gehalt über einen Probenzyklus Anweisungen zum Befüllen des DI Wasse...

Page 33: ... Kondensate sofort ab Der Betrieb des Analysators im Online Modus ohne Probenfluss und mit ausgeschaltetem Durchflusssensor kann zu fehlerhaften Messungen führen Die Standards für den TOC Analysator Sievers M500 sind angesäuert Wenn Sie Ihre eigenen Standards vorbereiten und Glasfläschchen verwenden stellen Sie sicher dass die Standards auf einen pH Wert von 3 angesäuert werden da die Systemprotok...

Page 34: ...ure elettriche ed elettroniche WEEE prevede lo smaltimento separato dell Analizzatore rispetto ai rifiuti standard Per evitare shock potenzialmente pericolosi prima di aprire l Analizzatore interrompere l analisi e spegnere il sistema operativo Premere il pulsante Power Off P spegnimento nel firmware dell Analizzatore quindi spegnere l interruttore e scollegarlo dall alimentazione Le operazioni ch...

Page 35: ...certarsi che l Analizzatore sia collegato a una linea elettrica con tensione adeguata Questo è un prodotto di Classe A In un ambiente domestico questo prodotto può causare interferenza elettromagnetica Prendere le misure adeguate per eliminare l interferenza Consultare l MSDS allegata a ogni set di standard per identificare tecniche di smaltimento adeguate Per evitare scosse potenzialmente pericol...

Page 36: ...campionamento Fare riferimento al manuale di manutenzione e funzionamento dell Analizzatore per istruzioni sul riempimento del serbatoio di acqua DI Per evitare danni alla pompa di acqua deionizzata accertarsi che il serbatoio di acqua deionizzata sia pieno prima di accendere l Analizzatore Per evitare false letture del TOC e possibili danni all Analizzatore accertarsi sempre che l ingresso del ca...

Page 37: ...sono acidificati Se l utente prepara i propri standard e utilizza fiale di vetro gli standard devono essere acidificati a un pH di 3 o i protocolli del sistema daranno risultati scarsi Accertarsi di centrare il tubo di sfiato all interno dei raccordi dei tubi per evitare schiacciamenti sotto il tubo di sfiato ed evitare che il campione fluisca Avvertenze ...

Page 38: ...クは分析装置の保護アース端子接地を示していますこの記号は廃電気電子機器 WEEE に関する EU 指令 2012 19 EU に関するものであり分析装置を適切に処分することが求めていることを示します潜在的に危険な感電を避けるため分析装置を開ける前に分析を停止してオペレーティングシステムの電源を切ります分析装置のファームウェアの電源オフ Power Off P ボタンを押し次に電源スイッチを切り電源から切り離します保守品目の取り付けを含む電源を切らずに分析装置内部にアクセスするいかなる操作も人身傷害につながる可能性があります紫外線への偶発的な曝露から身を守るために保護筐体の外で UV ランプを作動させないでください UV ランプハウジングは高温になる可能性があります UV ランプハウジングに触れる時はいつでも特に注意してくださいリ...

Page 39: ...てください潜在的に危険な感電を避けるため目視検査中にサンプルポンプを観察している間は分析装置内部のどこにも触れてはいけませんこの手順を行う際電気部品が濡れないように特に注意してください UV ランプには水銀が含まれておりお住まいの地域では有害物質に指定されている可能性がありますこれらの部品は国や地方自治体の規制に従って処分してください UV ランプが破損または損傷した場合は社内の有害廃棄物取扱手順に従って残留物を取り扱い国都道府県または地方自治体の規則に従って処分してください WEEE 指令 2012 19 EU がバッテリーに適用されその取り外しと分別回収を必要とします取り外し次第使用済み電池はバッテリー指令 2006 66 EC とその改正指令によって管理されますメーカーの指示と現地の廃棄回収要件に従って使用済みバッテリーを廃棄し...

Page 40: ...リングを行っていない時は iOS システムのドアを常に閉めてください分析装置を損傷から守るために必ず輸送前に分析装置から水を排出してください分析装置を洗浄する場合必ず液体は布に直接付けてくださいそして分析装置には液体を直接噴霧しないでください水が偏光板に損傷を与えたり変色させる可能性があるためタッチスクリーンに水またはクリーナーを使用しないでくださいタッチスクリーンの洗浄に関する推奨事項については次のセクションを参照してください凝縮物は直ちに拭き取ってくださいサンプルの流れがなく流量センサーがオフの状態でオンラインモードで分析装置を操作すると謝った測定につながる可能性があります Sievers M500 オンライン TOC 分析装置用の標準液は酸性化されています独自の標準液を調製してガラスバイアルを使用する場合標準液を必ず pH 3 ...

Page 41: ... 이 기호는 분석기를 위한 보호 접지 단자 접지 를나타냅니다 이 기호는 유럽연합 전기전자장비 폐기물 WEEE 지침 2012 19 EU 에 따라 분석기를 일반 폐기물과분리하여 폐기해야 함을 나타냅니다 위험해질 가능성이 있는 쇼크 상황을 방지하려면 분석기를 열기 전 에 모든 분석을 중지하고 운영 체계를 끄십시오 분석기 펌웨어의 전원 끄기 버튼을 누른 다음 전원 스위치를 끄고 전원 공급 장치에 서 분리하십시오 유지보수 품목 설치를 포함하여 전원을 끄지 않고 분석기 내부에 접근해야 하는 작업은 부상을 초래할 수 있습니다 우발적인 자외선 복사 노출을 방지하기 위해 보호 하우징 외부에서 는 자외선 램프를 작동하지 마십시오 자외선 램프 하우징은 뜨거울 수 있습니다 자외선 램프 하우징을 만질 때마다 각별히 주의하십시 오 ...

Page 42: ...적절한 장해제거 조치를 실행하십시오 적절한 폐기 방법을 확인하기 위해 각 표준에 동반된 MSDS 를 참조하 십시오 위험한 쇼크를 방지하기 위해 육안 검사 시 시료 펌프를 관찰하는 동안 분석기 내부에서 아무것도 만지지 마십시오 이 절차를 수행할 때 전기 부품이 젖지 않도록 각별히주의하십시오 자외선 램프는 수은을 포함하고 있으며 사용 지역에서위험물로 간주 될 수 있습니다 연방 주 지방 정부 규정에따라 이 항목들을 폐기 하십시오 자외선 램프 파손 또는 손상 시에는 기관별 유독성 폐기물 취급 절 차에 따라 남은 부분을 처리하고 연방 주 지방 정부 규정에 따라 폐기하십시오 배터리의 분리 및 별도 수거를 요구하는 WEEE 지침 2012 19 EU 가 배 터리에 적용됩니다 사용된 배터리가 분리된 후에는 배터리 지침 20...

Page 43: ...전에 항상 시료 입구가 열려 있고 탈이온수 탱크가 채워져 있는지 확인하 십시오 바이얼에서 시료를 채취하지 않을 때는 항상 iOS 시스템의 도어를 닫으십시오 분석기를 손상으로부터 보호하기 위해 운송하기 전에 항상 분석기에 서 물을 배출하십시오 분석기를 청소할 때는 항상 액체를 천에 직접 묻히고 분석기에 직접 분무하지 마십시오 물로 인해 편광자가 손상되거나 변색될 수 있기 때문에 터치스크린 에 물 또는 세제를 사용하지 마십시오 터치스크린 청소에 관한 지 침은 다음 섹션을 참조하십시오 물방울은 즉시 닦아내십시오 시료 흐름이 없고 유량 센서가 꺼진 상태에서 분석기를 온라인 모드 로 작동하면 측정 오류를 초래할 수 있습니다 Sievers M500 온라인 TOC 분석기를 위한 표준 용액은 산성화됩니다 자신만의 표준 용...

Page 44: ...os de equipamentos elétricos e eletrônicos REEE requer que o analisador seja descartado separadamente do lixo comum Para evitar choque potencialmente perigoso antes de abrir o analisador interrompa toda a análise e desligue o sistema operacional Pressione o botão Power Off P no firmware do analisador desligue o interruptor e desconecte o da fonte de alimentação Realizar qualquer operação que exija...

Page 45: ...lho está conectado a uma linha de energia com voltagem adequada Este é um produto Classe A Em ambiente doméstico o produto pode causar interferência eletromagnética Tome as medidas adequadas para corrigir o problema Consulte a MSDS Ficha Técnica de Segurança de Materiais que acompanha cada conjunto de padrões para identificar as técnicas de descarte adequada Para evitar choque potencialmente perig...

Page 46: ...a com TOC baixo Consulte o Manual de operação e manutenção do analisador para obter instruções para encher o reservatório de água deionizada Para evitar danos à bomba de água deionizada verifique se o reservatório de água deionizada está cheio antes de ligar o analisador Para evitar leituras de TOC falsas e possíveis danos ao analisador verifique sempre se a entrada de amostras está aberta e se o ...

Page 47: ...são acidificados Se preparar os seus próprios padrões e usar frascos de vidro garanta acidificar os padrões com pH igual a 3 ou os protocolos do sistema produzirão resultados ineficientes Tenha certeza de centralizar o tubo de ventilação nos encaixes da tubulação para evitar pinçamento abaixo do tubo de ventilação que impeça o fluxo de amostras Avisos ...

Page 48: ...系统向上喷出此符号表示分析仪的保护性接地端地线此符号表示符合有关废弃电气和电子设备 WEEE 的欧盟指令 2012 19 EU 分析仪应与标准废物分开单独处置为避免潜在的危险电击在打开分析仪机箱之前请先停止分析关闭操作系统的电源开关请按下分析仪固件中的关闭电源 Power Off P 键然后关闭电源开关断开电源线连接如果在不切断电源的情况下在分析仪内部进行操作包括安装维护部件都可能导致人员受伤为了防止人员意外接触紫外线辐射请勿在保护罩之外操作紫外灯紫外灯罩可能很热在碰触紫外灯罩时请格外小心第 3 组风险警告本产品释放紫外线请避免眼睛和皮肤接触无紫外线屏蔽的产品紫外反应器的玻璃窗会显示紫外灯正常工作观察时请勿靠得太近小于 6 英寸距离或时间太长多于 1 分钟观察时建议佩戴防护眼镜如果仪器未以 SUEZ 公司规定的方法使用...

Page 49: ...标样组随附的化学品安全技术说明书 MSDS 确定正确的标样处置方法为避免潜在的危险电击在目视检查过程中观察样品泵时请勿触碰分析仪内部的任何部件执行此程序时请格外小心不可弄湿电气组件紫外灯中含有汞可能在您所在地区被认为是有害物质请按照联邦州或地方管理机构的规定来处置这些物品如果紫外灯破损应根据您所在组织机构的有毒废料处理程序以及国家州省或地方政府的相关规定进行处理 WEEE 指令 2012 19 EU 适用于电池要求将电池取出并单独收集取出废旧电池后请按照电池指令 2006 66 EC 及其修正文件的规定来处理请按照制造商的说明和您所在地对废旧电池的处置和收集要求来操作在操作分析仪时如果进样管上没有装管内过滤器将会损坏分析仪并使仪器的保修失效为避免损坏分析仪请安装过滤器并按需要及时更换滤芯确保去离子水容器已灌满水尤其是在运...

Page 50: ...SUEZ 2022 请按照分析仪的操作和维护手册中的指导来加注去离子水容器为了避免损坏去离子水泵在启动分析仪之前先确保去离子水容器已灌满水为避免 TOC 读数出错和损坏分析仪在打开分析仪的电源开关之前请确保打开样品进口并注满水去离子水容器如果不从样品瓶取样请始终关闭 iOS 系统的门为了避免损坏分析仪请务必在运输前将分析仪中的水排干仪器上的此符号表示本产品含有中国 RoHS II 管理办法中限制的物质请参考下表请注意本产品含有紫外线灯含汞符合 RoHS 指令 2011 65 EC 的附件 III 4 a 规定的豁免条件警告 ...

Page 51: ...51 SUEZ 2022 在清洁分析仪时应将清洁液放在抹布上不可将清洁液直接喷洒在分析仪上不可在触摸屏上使用水或清洁剂水可以使偏振片损坏或褪色请参阅后面的章节了解触摸屏的清洁方法应立即擦去触摸屏上的冷凝水在没有样品流量且流量传感器关闭的情况下如果以在线模式运行分析仪就会导致错误的测量结果 Sievers M500 在线型 TOC 分析仪的标样已被酸化如果您自行制备标样并使用玻璃瓶请确保将标样酸化至 pH 值为 3 否则系统任务会产生不准确的分析结果请确保使排气管处于管接头内的中间位置以防止夹住排气管下部并阻碍样品流动警告 ...

Page 52: ...erally referred to simply as inorganic carbon IC TOC TC IC The Analyzer can be used to monitor water samples ranging from high purity water containing 0 03 parts per billion ppb TOC to water samples containing up to 2 5 parts per million ppm TOC The Analyzer is easy to operate with extremely low maintenance and no special training or chemical knowledge is required The Analyzer is calibrated at the...

Page 53: ...Insensitive to organic heteroatoms 12 months 3 significant digits Linear Range Accuracy Precision Analysis Modes Analysis Time Ozone Compatibility Internal Sample Flow Rate nominal External Flow Rate Sample Temperature Sample Pressure Interferences TOC Calibration Stability Display Readout instrument 100 240 VAC 70 W 50 60 Hz No user replaceable fuses Intended for indoor use only 5 40 C 41 104 F U...

Page 54: ...sists of five major subsystems 1 Sample inlet system and sample pump including the Standard iOS System 2 Oxidation reactor 3 Measurement module comprising CO2 transfer manifold 4 Fluidics module comprising DI Deionized water reservoir including resin cartridge DI water pump 5 Electronics subsystems comprising Microprocessors and circuit boards Data outputs ...

Page 55: ...easured by the Sievers M500e TOC Analyzer by inserting a filled 40 mL sample vial into the iOS System Continuous monitoring is accomplished by plumbing a sample line to the inlet of the iOS System or the Sample Inlet Block The stream splitter divides the sample stream into two equal but separate flows One stream is processed for the measurement of IC The other is processed for TC measurement The T...

Page 56: ...d loop and consists of two conductivity cells one for the TC stream and one for the IC stream a DI water pump a DI water reservoir and an ion exchange resin cartridge CO2 from the sample passes through the membrane into the DI water supplied by the integrated DI Loop while interfering compounds and other oxidation by products are blocked by the membrane and remain on the sample side The CO2 forms ...

Page 57: ...20 mA outputs LED capacitive touch panel display and interface Analog to digital conversion boards 2 with integrated signal conditioning circuits for cell conductivity and temperature measurements Data Outputs The Sievers M500e TOC Analyzer offers three 4 20 mA outputs four alarm outputs and two isolated binary start stop inputs The Analyzer also includes one serial RS 232 one USB and one Ethernet...

Page 58: ...tentially dangerous shock BEFORE opening the Analyzer stop any analysis and power off the operating system Click the on screen Power On Off P button then turn off the power switch and disconnect the Analyzer from the power supply Any operation requiring access to the inside of the Analyzer without turning off power including installation of maintenance items could result in injury The exceptions i...

Page 59: ...ing List section NOTE Always save original packing materials If for any reason the Analyzer needs to be returned it must be packed in the original carton to ensure that no damage occurs during shipment For cases when the original packaging is no longer available SUEZ replacement packaging is required for a return shipments and a charge is assessed for this new packaging Insure the Analyzer for the...

Page 60: ...t tubing 1 4 with in line filter 60 micron PFA tubing assembly 1 16 OD x 04 ID x 30 L Worm drive hose clamp 25 32 Connector male metric conversion for use with 1 4 to 6 mm tubing PVC tubing 1 2 ID 3 4 OD clear for waste line Polypropylene tubing 1 4 OD x 1 8 ID Open end wrench 9 16 Screwdriver four blades Water bottle 250 ml 8 5 ou with nozzle for filling DI water reservoir Grounding strap Termina...

Page 61: ... support the Analyzer See Step 3 Select a Location for the Analyzer on page 62 Insulated wire 18 12 AWG rated to 300 Volts for AC power conduit See Installing the AC Conduit on page 73 An external circuit breaker or switch that disconnects both poles of the supply voltage rated 2 5A Optional Insulated wire 16 22 AWG rated to 300 Volts for wiring I O terminal blocks See Installing I O Wiring on pag...

Page 62: ...onally this clearance provides proper circulation for temperature and humidity control When selecting the location mount the Analyzer so that the display screen is approximately at eye level Diagrams showing Analyzer dimensions and clearances are provided in Appendix A Analyzer Dimensions Select and procure hardware for mounting the Analyzer on a wall or instrument rack based on site specific circ...

Page 63: ...t make any connections to this terminal block J4 4 20 mA Analog Current Loop This section includes step by step instructions for Installing I O Wiring on page 63 Additional information to assist in the installation is also provided Working with Alarm Outputs J1 on page 68 Working with 4 20 mA Analog J4 Outputs on page 69 Working with Binary Inputs Remote Start Stop J2 on page 71 After installing I...

Page 64: ...ngth for each pin should be 8 9 mm 0 33 in 1 Ensure to exercise ESD protection while working inside the Analyzer 2 Unlock and push the release button to unlatch and open the door to the Analyzer 3 Remove the following covers Turn the fasteners 1 4 turn to release AC Power cover A located on the left side of the Analyzer I O Control wiring cover B located at the top of the Analyzer A B ...

Page 65: ...Analyzer 5 Route the I O wires into the instrument through the wire glands from the outside I O panel located on the left side of the Analyzer A view of the I O panel is provided identifying typical wire gland use at E and F D C E Wire Glands typically used for various types of I O cables no conduit F Wire Gland typically used for multiple I O cables and external conduit Antenna jack ...

Page 66: ...minal header on the board 8 Identify the correct pin position for each wire to install according to Table 3 2 4 20 mAAnalog Outputs J4 on page 69 or Table 3 1 Alarm Relay Outputs J1 on page 68 or Table 3 3 Isolated State Inputs J2 on page 71 9 To attach each wire use the small flat blade of the screwdriver to depress the orange tab example shown at the arrow while inserting the stripped wire into ...

Page 67: ...nal block into the terminal header on the instrument controller board 13 Repeat steps 6 12 for each I O Output or Input installation 14 If planning to install the power now leave the covers off and go to step Step 5 Install Power on page 73 Or if continuing the installation process at a later time replace the following covers push and turn the fasteners 1 4 turn to secure Electrical cover A locate...

Page 68: ...t and coil 1 000 Vrms for 1 min Detection current 10 mA Between contact sets 1 000 Vrms for 1 min Detection current 10 mA Figure 3 2 Alarm Relay Output Detail Table 3 1 Alarm Relay Outputs J1 Pin Number Signal Function 1 ALARM_1_NC Relay 1 Normally Closed contact 2 ALARM_1_COM Relay 1 Common contact 3 ALARM_1_NO Relay 1 Normally Open contact 4 ALARM_2_NC Relay 2 Normally Closed contact 5 ALARM_2_C...

Page 69: ...Instrument Powered Loop Output Nominal Operating Range 4 20 mA Current Calibration Adjustment Range 0 24 mA Alarm Indication option 22 mA Maximum Loop Resistance 600 Ohms ISOLATION LEVELS This interface does not provide safety barrier isolation The isolation is low voltage and intended to isolate the instrument DC power from the customer s power supplies only 1000 V for 1 second Operation rating S...

Page 70: ...INSTALLATION Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 70 SUEZ 2022 Figure 3 3 Typical 4 20 mA Circuit Applications ...

Page 71: ...firmware later in Step 9 Configure Basic Analyzer Settings on page 90 To avoid unexpectedly starting or stopping analysis it is important to confirm the correct signal strength before configuring binary settings For more information on activating binary input see To set the binary input on page 109 BININ to BININ Voltage Range 12 to 28 VDC Inputs are reverse polarity protected to 40 V ISOLATION LE...

Page 72: ...0e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 72 SUEZ 2022 Figure 3 5 Instrument Powered Isolated State Input Circuit Application Figure 3 6 Externally Powered Isolated State Input Circuit Application ...

Page 73: ...ice for the Analyzer To wire the AC conduit Provide the following for this procedure Insulated wire for AC power conduit 18 12 AWG rated to 300 Volts Strip length should be 8 9 mm 0 33 in Optional Metallic AC power conduit1 Alternatively a PVC conduit connector strain relief hub and sealing washer is provided in the Accessories Kit Terminal ring M4 8 for AC conduit ground wire 18 12 AWG provided i...

Page 74: ...2 4 Pull the AC line cable through the AC mains wire gland on the enclosure 5 Strip back the cable sheath on the individual wires by about 3 inches and crimp a ring terminal lug for M4 or 8 stud onto the earth lead ground conductor Rotary AC Power Switch Earth Ground Lug AC Mains Wire Gland Wiring terminals ...

Page 75: ...ower switch as follows Connect the Line brown or black wire typically wire to the front of the Terminal block in terminal 5 Connect the Neutral blue or white wire typically in terminal 4 When connecting each wire to the terminal block loosen the screws at the location shown with the arrows and insert the wires as designated Tighten the screws to secure the wires 8 After connecting the wires pull o...

Page 76: ...d wire 11 Secure both wires to grounding lug with an M4 nut 12 Replace the electrical cover and turn the fasteners 1 4 turn to secure 13 Close and latch the door to the Analyzer Lock the latch if required for the user s location Warning To assure safe operation of the instrument the AC Mains Earth Ground must be securely connected to the enclosure ...

Page 77: ... by sliding the tubing over the barb fitting 3 Place the hose clamp over the waste line and tighten to secure the connection to the waste outlet 4 Route the waste tubing to an appropriate waste outlet The waste is gravity drained and thus the waste tubing cannot be routed above the level of the waste from the waste line to between 50 300 mL min The flow rate is controlled by a needle valve which i...

Page 78: ...e Using the Instrument Startup Wizard To run the Instrument Startup Wizard This wizard guides the user with step by step instructions and photos through the process of filling the DI Water reservoir priming the DI Loop and rinsing down the measurement module For additional details about the individual steps refer to Appendix D DI Water Installation Details 1 Turn the rotary power switch located on...

Page 79: ...eration and Maintenance Manual DLM 78510 02 EN Rev B 79 SUEZ 2022 2 Navigate to the Settings s screen and select the Hardware tab 3 On the scrolling menu select Instrument Startup Wizard and click Run The Analyzer Startup Wizard screen appears ...

Page 80: ...nsing bottle from the Analyzer s Accessories kit with low TOC DI water and remove the check valve on the DI Water reservoir Click Next to go to display the next wizard screen 5 Use the dispensing bottle to fill the reservoir until the level reaches the Full indicator marking Click Next to go to display the next wizard screen ...

Page 81: ...B 81 SUEZ 2022 6 Confirm that the level of the DI water in the reservoir is at the Full indicator marking and re install the check valve Click Next to display the next wizard screen 7 Manipulate the pump tubing to move any bubbles into the reservoir Click Next to display the next wizard screen ...

Page 82: ...Z 2022 8 Install the resin cartridge in the Prime position and click Next to display the next wizard screen The Analyzer automatically starts priming the DI Loop 9 Wait three hours for the priming process to complete After completion the Instrument Startup Wizard displays a Priming is complete message ...

Page 83: ...e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 83 SUEZ 2022 10 Click Next to display the next wizard screen 11 Move the resin cartridge to the Run position and click Next to display the next wizard screen ...

Page 84: ... 12 Add more DI water to reach the Full line if needed It is not necessary to re prime the DI Loop Click Next to display a dialog box and the next wizard screen 13 On the Final Rinse Down dialog box do one of the following To start online analysis at the completion of the Instrument Startup Wizard Click Yes ...

Page 85: ...completion of the Instrument Startup Wizard Click No The dialog box clears 14 On the Analyzer Startup Wizard screen click Next to proceed to the next wizard screen 15 Confirm sample flow is established to the sample inlet system of the Analyzer and click Next to start the final rinse down and priming of the sample side The Analyzer displays the next wizard screen ...

Page 86: ...Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 86 SUEZ 2022 16 After completion of the final rinse down and priming of the sample side the final wizard screen appears with the message Analyzer is ready for operation ...

Page 87: ...nection is available to transfer data via a USB memory device Figure 3 7 Input and Output Connections The I O panel also includes three I O wire glands for connecting 4 20 mA and alarm wiring The rotary power switch and an AC Mains wire gland for installing power to the Analyzer are located below these connections on the Analyzer s enclosure panel Wiring and power installation are described in pre...

Page 88: ...s provided as an optional means of capturing data from the Analyzer Serial cables are available at many computer and office supply retail stores Refer to Figure 3 7 Input and Output Connections on page 87 and Figure 3 8 Asynchronous Serial Port RS 232 on page 89 as needed To install a serial connection 1 Connect the male end of the serial cable to the port on the Analyzer labeled RS 232 and tighte...

Page 89: ...n page 157 To set up the printer for use with the Analyzer see Enabling a PDF Printer on page 100 To assist in using the Modbus communications with the Analyzer refer to Appendix E Modbus with the Analyzer To install an Ethernet cable Provide either a cross over Ethernet cable for connecting directly to a computer or printer or a straight through Ethernet cable for connecting to a network 1 Attach...

Page 90: ...vers M500e TOC Analyzer offers one level of security Password Protection The Password Protection feature is included with all Analyzers and provides a basic level of security This section includes step by step instructions for enabling Password Protection For additional information about Password Protection refer to Chapter 5 Password Protection Enabling Password Protection Optional To enable Pass...

Page 91: ...efore Alarm 2 10 Inactivity Timeout hours and minutes The minimum timeout is one 1 minute 4 Click the Password field and use the alphanumeric keypad to enter a password 5 Confirm the Password 6 Click Save Settings 7 Record the new password in a secure location ALL users will be required to enter this login information to access the Analyzer s menus ...

Page 92: ...Also use this instruction to set the system clock 1 On the Settings s screen select the System Setup tab 2 On the Local Settings panel in the Environment section click inside any of the following fields to use the alphanumeric keypad to specify an identifier and click OK Analyzer Name Location Optional Service Provider 3 Click the Date field and use the calendar to enter the current month day and ...

Page 93: ...me with the operating system s network time protocol NTP server 8 Continue to the To configure the display format settings on page 93 To configure the display format settings Configure the settings for the date format the clock format and number format for display 1 On the Settings s screen select the System Setup tab 2 On the Local Settings panel under Display Formats select one of the following ...

Page 94: ...00 123 456 789 00 Setting the Measurement Mode Before starting normal Analyzer operation verify the default measurement mode setting for your application s configuration needs The measurement mode is set using the Protocols p screen The Analyzer uses this measurement mode setting for analysis started from the Home h screen which also displays the active measurement mode in the Protocols field To r...

Page 95: ...pecific time interval The selected method appears as the measurement mode in the Measurement Mode field on the Measurement Mode panel If an Online method is selected skip to step Grab Method The Analyzer performs analyses by drawing samples from a vial placed in the designated vial port in the Analyzer s iOS System Grab mode is not available for configurations with the Sample Inlet Block NOTE When...

Page 96: ...ad to enter the number of seconds for a normal flush 300 1500 8 Complete the following for each vial position Sample Name Click inside the field and use the alphanumeric keypad to enter a name Vial Type Select one of the following Sample Vial Blank Vial Standard Vial Rinse Vial Number of Repetitions Click inside the field and use the numeric keypad to enter the number of replicate TOC measurements...

Page 97: ...10 02 EN Rev B 97 SUEZ 2022 9 Setting the measurement mode is complete and this measurement mode now appears in the Protocols field on the Home h screen Figure 3 9 The Analyzer automatically uses this measurement mode for analysis Figure 3 9 Measurement Mode shown in Protocol field ...

Page 98: ... use a third party data acquisition software or a SCADA system with Modbus TCP IP to support the collection of real time instrument data and status information For more information refer to Appendix E Modbus with the Analyzer To collect serial data strings refer to Streaming Data on page 297 To print to a PDF printer configure the printer connection For more information refer to Enabling a PDF Pri...

Page 99: ...EN Rev B 99 SUEZ 2022 3 Select the Enable Ethernet Connection option 4 Do one of the following Select the Automatic option for a dynamic IP address Select the Manual option to enter the IP Address and Net Mask numbers You can also enter a Gateway IP and up to two DNS Servers 5 Click Save ...

Page 100: ...9 and Configuring an Ethernet Connection on page 98 the PDF printer must be enabled in the firmware To enable a PDF printer 1 Ensure the PDF printer is connected to the Analyzer directly or over an Ethernet network 2 On the Settings s screen click the Hardware tab 3 On the scrolling menu select Printer Setup and click Run The Printer Setup dialog box appears The Analyzer checks for all PDF printer...

Page 101: ...e Analyzer 5 Click Save 6 To send a test page to the printer navigate to the scrolling menu for System Tests Settings s screen Diagnostics tab 7 Select Printer and click Run The Analyzer sends a test page to the printer 8 Check the printer to ensure that it printed the test page Consult the printer manufacturer s instructions for additional help as needed ...

Page 102: ...onnection To configure a Wireless connection Use this instruction to enable a wireless connection when the WiFi option has been purchased NOTE This feature is only available in select countries 1 On the Settings s screen click the Hardware tab 2 On the scrolling menu select WiFi Setup and click Run The WiFi Setup dialog box appears ...

Page 103: ...ollowing Select the Automatic option for a dynamic IP address Select the Manual option for a fixed address and enter the IP Address and Net Mask numbers You can also enter a Gateway IP and up to two DNS Servers 5 Select the Access Point field Select the access point 6 If the WiFi network requires a password select the Password field and enter the password 7 Click Save ...

Page 104: ...ithout restoring the historical data For more information see Backing Up the Database on page 167 and Restoring System Constants on page 176 To print and export system constants 1 On the Settings s screen select the Instrument Settings tab 2 Optional To print the system constants Ensure a PDF printer is connected to the Ethernet port either directly or over a network and the PDF printer is enabled...

Page 105: ...nces panel See Configuring Export Preferences on page 138 enc encrypted 6 Leave the default destination or add a folder to it by clicking Create Folder Use the alphanumeric keypad to type a folder name and click OK The Analyzer adds the folder to the export path configured on the Export Preferences panel and displays the folder in the Path field and in the Name area NOTE The export path represents...

Page 106: ...exported Settings file Technical Support or your local service provider might need to reference the system settings for Calibration constants and other key parameters Configuring the Data I O If alarm outputs 4 20 mA outputs and or binary inputs were installed configure the connections with the appropriate values for those features now NOTE You may need to consult with your remote operations cente...

Page 107: ...tup screen appears 3 In the Select Alarm area select one of the following options to configure Alarm 1 Alarm 2 Alarm 3 or Alarm 4 4 Click the Threshold field and use the numeric keypad to set a value for the alarm threshold 1 3000 ppb and click OK 5 In the table area select an assignment option for applying the alarm such as TOC Threshold Error or Warning or Temperature Threshold ...

Page 108: ... for each alarm to configure 7 Click Save To set up 4 20 mA analog outputs 1 On the Settings s screen select the Hardware tab 2 On the scrolling menu select Analog Outputs Setup and click Run The Analog Outputs Setup screen appears 3 In the Analog Outputs Standby Error Warning Values area select values for each of the following ...

Page 109: ...sues a warning 1 mA 2 5 mA 4 mA 20 mA 22 mA or Hold Last 4 In the area for the analog output to configure 1 2 or 3 specify the calibration values Value Select the analog output value TOC TC IC Min Value Enter the lowest value ppb for output Max Value Enter the highest value ppb for output System Protocols Select one of the following for running system protocols Go To Standby to output the Standby ...

Page 110: ...ry Inputs Setup and click Run The Binary Inputs Setup screen appears 3 In the area for the Binary input to configure select the Enable Binary Input 1 or Enable the Binary Input 2 option 4 Select the Run analysis when input is high or the Run analysis when input is low option 5 Repeat steps 3 4 for the other binary input connection 6 Click Save ...

Page 111: ...ring On and Off the Analyzer This section includes instructions for turning on the Analyzer power and if Password Protection is enabled logging into the Analyzer Instructions for closing the Analyzer files and turning off power to the instrument are also included as well as references to shutting down the mains power supply for some installation and maintenance activities To power on the Analyzer ...

Page 112: ...022 When initialization is complete the Home h screen appears If Password Protection is enabled a Login button appears in the lower right corner of the Home h screen and logging into the Analyzer is required before starting analysis or proceeding to other screens Figure 4 1 Home screen when Password Protection is not enabled ...

Page 113: ...rotection on page 183 To power off the Analyzer The Sievers M500e TOC Analyzer has a Power Off P button on the Analyzer s Home screen to close all the files and an On Off rotary power switch located on the left outside panel of the Analyzer For some maintenance activities as described in applicable procedures inside the Analyzer SUEZ also recommends shutting down the mains power supply 1 On the An...

Page 114: ...n increase in the standard deviation values THE IOS SYSTEM SUEZ offers two inlet systems for use with the Sievers M500e TOC Analyzer a sample inlet block for dedicated Online analysis and a Standard Integrated Online Sampling iOS System with one vial port The iOS System provides a convenient sample inlet for Online sample sources and standards in vials Switching between Online mode analysis and gr...

Page 115: ...thod analysis Always stop analysis before opening the standard iOS System door to avoid generating erroneous measurement data 1 Using the Sample Inlet Block Figure 4 4 The Sample Inlet Block 1 If the flow sensor is On opening the iOS System door while analysis is taking place causes the flow sensor to activate and halt analysis If the flow sensor is Off opening the iOS System door while analysis i...

Page 116: ...OS is rated at IP 55 and can withstand short term steam exposure of up to 40 psi steam for 30 minutes When exposed to steam the Analyzer should be powered off or in standby mode and not in analysis mode After exposure to steam allow the Analyzer to cool before returning to Analysis mode Observe the following cool down intervals before starting analysis after steam exposure Warning The Sample Inlet...

Page 117: ...tatic Standard toolbar located on the top of the screen THE STANDARD TOOLBAR Use the Standard toolbar located at the top of the Analyzer display to select and display a new screen Simply clicking one of the corresponding icons as described in Table 4 1 The Analyzer s Standard Toolbar on page 118 The toolbar remains static as each screen is displayed providing the ability to easily switch between o...

Page 118: ...sis Most Recent Analysis Results Trend Graph or Details Error and Warning Indicators Instrument Power Off to close files Active Measurement Mode Protocol Measurement Status Active I O Consumables Status After closing files turn the rotary power switch to turn off instrument power PROTOCOLS For more screen details go to page 130 System Protocols tab Calibration Verification Validation if activated ...

Page 119: ...tridge Diagnostics tab System Tests Alarm Test Analog Output Test Modbus Test Network Folder Test Printer Test Sample Flow Rate Test IC Power Relay Test Internet Connection USB Serial Loopback Test Serial Loopback Test WiFi Test Export Diagnostics Clean Screen Service Diagnostics Sample Pump IC Cell Diagnostic Data DI Loop UV Lamp TC Cell Diagnostic Data Sample Cell Diagnostic Data Level 1 Diagnos...

Page 120: ...erify that the screen includes a Print or Print All or Print Settings or Print Table button 2 Ensure a PDF printer is connected to the Ethernet port either directly or over a network and the PDF printer is enabled in the firmware For information see Enabling a PDF Printer on page 162 3 Do one of the following If there is more than one item available to print such as a table of records or panel of ...

Page 121: ...ee Configuring Export Preferences on page 138 enc encrypted 6 Leave the default destination or add a folder to it by clicking the Create Folder button Use the alphanumeric keypad to type a folder name and click OK The Analyzer adds the folder to the export path configured on the Export Preferences panel and displays the folder in the Path field and in the Name area NOTE The export path represents ...

Page 122: ...o Start Analysis and Stop Analysis as well as monitor real time results data in a Trend Graph or Details Table format To change the trend graph settings including which values are displayed Carbon TOC IC TC the time range on the X axis and the minimum and maximum values on the Y axis see Setting Trend Graph Display Options on page 137 To change the time range on the X axis the background color and...

Page 123: ...he size of the data points on the trend graph The changes to the trend graph appear on both the Home h screen and the Online Data tab of the Data D screen You can also change the time range on the X axis of the trend graph on the Home h screen The trend graph on the Online Data tab of the Data D screen has its own options for setting the time range on the X axis 1 Click anywhere on the trend graph...

Page 124: ...e background and point size The example shows a trend graph with a time range of 1 hour a blue background and 9 pixel data points Setting the Measurement Mode The Sievers M500e TOC Analyzer provides three different Online modes for running the Analyzer with a continuous water source A Grab mode is also available for sampling from a vial in the Analyzer s Standard iOS System Select one of these mod...

Page 125: ...ged value of TOC over a specific time interval The selected method appears as the measurement mode in the Measurement Mode field on the Measurement Mode panel Go to step 9 Grab Method Grab Method The Analyzer performs analyses by drawing samples from a vial placed in the designated vial port in the Analyzer s iOS System Grab mode is not available for configurations with the Sample Inlet Block NOTE...

Page 126: ...lush 300 1500 8 Complete the following for each vial position Sample Name Click inside the field and use the alphanumeric keypad to enter a name Vial Type Select one of the following Sample Vial Blank Vial Standard Vial Rinse Vial Number of Repetitions Click inside the field and use the numeric keypad to enter the number of replicate TOC measurements for the Analyzer to perform on the sample Numbe...

Page 127: ...s for a vial have been run The Trend Graph is not available for system protocols and Grab methods See To run a grab sample on page 128 Running Online Analysis Use the Home h screen to start and stop online analysis using a continuous water source Simply click Start Analysis and Stop Analysis The Analyzer automatically uses the active online measurement mode appearing in the Protocol field For more...

Page 128: ...g in Grab mode and using glass vials the sample water must be acidified to a pH of three 3 If you are using plastic vials no acidification is required To run a grab sample 1 On the Home h screen verify that a Grab method measurement mode appears in the Protocol field 2 Insert the sampling vial into the vial port 3 Click Start Analysis NOTE A grab sample can also be started on the User Defined Meth...

Page 129: ...ntenance Manual DLM 78510 02 EN Rev B 129 SUEZ 2022 4 To view complete details review the data history Data D screen System Protocols and Grab Methods Data tab For additional information refer to To review data history for System Protocols and Grab Methods on page 179 ...

Page 130: ... of the screen to switch between views Figure 4 7 Online Data Graphical View 1 To search for protocols within a specific date range click Start Time date to display and select from an interactive calendar to set the beginning date Click the End Time date to display and select from an interactive calendar set the ending date 2 Leave the default time or click Start Time time to display a keypad Ente...

Page 131: ...ance Manual DLM 78510 02 EN Rev B 131 SUEZ 2022 Figure 4 8 Online Data Table View Select a protocol from the list and click Details to see the Online Record Details for the analysis Figure 4 9 Online Data Details You can also Print or Export the results using the appropriate button ...

Page 132: ...for protocols within a specific date range click Start Time date to display and select from an interactive calendar to set the beginning date Click the End Time date to display and select from an interactive calendar set the ending date 2 Leave the default time or click Start Time time to display a keypad Enter the numbers for hh mm ss and click OK Click End Time time to display a keypad Enter the...

Page 133: ...ttons along the bottom of the screen to Print or Export the results You can also Print All or Export All results in the Protocol Record section THE SETTINGS SCREEN SETTINGS SCREEN SYSTEM SETUP TAB Configuring Local Settings This section includes instructions for configuring settings for the local environment and display formats To configure the environment settings Define the Analyzer name and loc...

Page 134: ...Sync Automatically synchronizes the local computer time with the operating system s network time protocol NTP server 8 Continue to the To configure the display format settings on page 135 To select a new display language Optional The Analyzer is shipped from the factory with English as the default language on the Analyzer screens Use this instruction to change the display language to Chinese Simpl...

Page 135: ...ased DD MM YYYY 16 Jan 2019 Month First MM DD YYYY 01 15 2019 Day First DD MM YYYY 15 01 2019 Year First YYYY MM DD 2019 01 16 3 Select the 12 hour am pm or 24 hour 24 hour clock format such as 13 22 option to designate the time format 4 Select one of the following format options from the Numbers list 123 456 789 00 123 456 789 00 To enable screen features 1 Navigate to the Local Settings panel Se...

Page 136: ...l occur Disable All Warnings and Errors Select this option to disable all warnings and error notifications including Error History records alarms and analog outputs Configuring Result Preferences Use the Result Preferences panel to select the results data from online analysis and grab sampling to appear on the Home h screen and Data D screen data history The panel also includes Trend Graph Display...

Page 137: ...and Data D screen Rejected Repetitions can also be set whether to appear in printed and exported results To set trend graph display options 1 Navigate to the Result Preferences panel Settings s screen System Setup tab 2 In the Trend Graph Display Options area configure the following X Axis Time Range list Select one of the following options from the list 1 hour 4 hours 8 hours 12 hours 1 day 3 day...

Page 138: ...stem Setup tab 2 To enable a daily export of results data from online analysis Select the Enable Daily Export Of Online Results option Click inside the Export Time field and use the numeric keypad to enter a time 24 hour format for the daily export Continue with the remaining steps in this procedure to create default settings for use in exporting data In addition to displaying the default settings...

Page 139: ...nside the Path field and use the alphanumeric keypad to enter the network path For example mnt net server 2 online_data Click inside the User Name and Network Password fields and use the alphanumeric keypad to enter the required network security information 6 Optional Click inside the File Prefix field and use the alphanumeric keypad to enter a user assigned prefix for all exported files 7 In the ...

Page 140: ... asked to provide the serial number of the Analyzer It is located on the System Constants panel Settings s screen Instrument Settings tab Saving System Constants Backing up the Analyzer s database saves system constants calibration and user configurable settings along with history data If there is a need to return to previous settings the system constants can be restored from any backup file For m...

Page 141: ...ly or over a network and the PDF printer is enabled in the firmware For information see Enabling a PDF Printer on page 162 On the System Constants panel click Print The Analyzer prints a copy of the system constants Save the printout Technical Support or your local service provider might need to reference the system settings for Calibration constants and other key parameters 3 To export the system...

Page 142: ... memory device was used remove it for safe keeping 7 Save the exported Settings file Technical Support or your local service provider might need to reference the system settings for Calibration constants and other key parameters Importing System Constants To import System Constants 1 Navigate to the System Constants panel Settings s screen Instrument Settings tab 2 Click Import Constants The Name ...

Page 143: ... will automatically restart SETTINGS SCREEN ANALYZER SETTINGS PANEL The Analyzer Settings panel includes a scrolling table of each Analyzer setting and its value The panel can also be used to export print and import settings Also included is the configurable TOC Offset field and Analyzer options such as the 3 Minute Analysis Reviewing Analyzer Settings To review Analyzer settings 1 Navigate to the...

Page 144: ... Settings feature to support importing such a file To print and export Analyzer settings 1 Navigate to the Analyzer Settings panel Settings s screen Instrument Settings tab Print and export options are shown in the Settings section in the middle of the screen 2 Optional To print the Analyzer settings ensure a PDF printer is connected to the Ethernet port either directly or over a network and the P...

Page 145: ...ormation refer to To export from an Analyzer screen on page 120 6 Click OK to confirm and close the message Importing Analyzer Settings To import Analyzer settings 1 Navigate to the Analyzer Settings panel Settings s screen Instrument Settings tab 2 Click Import Settings The Name import dialog box appears 3 Select a source file location option USB or Network If Network is selected click Network Cr...

Page 146: ... small changes in water system conditions may make it difficult to use the TOC Autozero procedure for the purposes of achieving instrument to instrument agreement consistent with the stated analyzer specifications If the TOC Autozero procedure does not yield acceptable agreement between multiple instruments use this manual User TOC zero offset adjustment to adjust the TOC reading to match a known ...

Page 147: ...510 02 EN Rev B 147 SUEZ 2022 Activating Options To activate an Analyzer option 1 Locate the Activation Code previously e mailed from SUEZ 2 Navigate to the Analyzer Settings panel Settings s screen Instrument Settings tab 3 Click Activations The Enter Activation Code dialog box appears ...

Page 148: ...rading Firmware IMPORTANT System constants Analyzer settings and a Database Backup must be saved before upgrading Analyzer firmware See Saving System Constants on page 140 Saving Analyzer Settings on page 144 and Backing Up the Database on page 167 for instructions Use these instructions to install firmware updates To upgrade firmware using a USB memory device on page 148 To upgrade firmware throu...

Page 149: ...tenance Manual DLM 78510 02 EN Rev B 149 SUEZ 2022 3 On the Analyzer Settings panel click Upgrade Firmware The Name Firmware Upgrade screen appears NOTE All files contained on the USB memory device will appear on the this screen Select only the firmware upgrade file ...

Page 150: ...estart to complete the upgrade process The Home h screen appears 6 Remove the USB memory device from the Analyzer USB port To upgrade firmware through a network connection 1 Navigate to the Analyzer Settings panel Settings s screen Instrument Settings tab 2 On the Analyzer Settings panel click Upgrade Firmware The dialog box for upgrading the firmware appears 3 Select the Network option and click ...

Page 151: ...r includes wizard screens to guide the user with step by step instructions and photos or a settings screen For each settings screen accompanying instructions are included in this section For each menu item select the Hardware feature in the scrolling table and click Run The corresponding wizard or settings screen appears The menu includes the following Accelerated Rinse wizard Follow the screen in...

Page 152: ...on For instructions on filling the DI Water Reservoir priming the DI Loop and rinsing down the measurement module after the initial installation process refer to Chapter 8 Maintenance Level Sensor Setup Use the Level Setup screen to enable the DI Reservoir Level Sensor Refer to Configuring the Flow Sensor on page 158 for step by step instructions UV Lamp Setup Use the UV Lamp Setup screen to tempo...

Page 153: ...Setup screen appears 3 In the Select Alarm area select one of the following options to configure Alarm 1 Alarm 2 Alarm 3 or Alarm 4 4 Click the Threshold field and use the numeric keypad to set a value for the alarm threshold 1 3000 ppb and click OK 5 In the table area select an assignment option for applying the alarm such as TOC Threshold Error or Warning or Temperature Threshold 6 Repeat steps ...

Page 154: ...led configure the connections with the appropriate values for those features now The Sievers M500e TOC Analyzer has three 4 20 mA outputs Select the output range for the 4 20 mA analog outputs by following these steps Instructions for wiring the 4 20mA output can be found in Chapter 3 Installation on page 58 1 On the Settings s screen select the Hardware tab 2 On the scrolling menu select Analog O...

Page 155: ...alibration values Value Select the analog output value TOC TC or IC Min Value Enter the lowest value ppb for output Max Value Enter the highest value ppb for output System Protocols Select one of the following for running system protocols Go To Standby to output the Standby value entered in step 3 or Output Values to output actual values from protocol analyses 5 Click Save 6 To verify the operatio...

Page 156: ... select Binary Inputs Setup and click Run The Binary Inputs Setup screen appears 3 In the area for the binary input to configure select the Enable Binary Input 1 or Enable the Binary Input 2 option 4 Select the Run analysis when input is high or the Run analysis when input is low option 5 Repeat steps 3 4 for the other binary input connection 6 Click Save ...

Page 157: ...net connection To collect data use a third party data acquisition software or a SCADA system with Modbus TCP IP to support the collection of real time instrument data and status information For more information refer to Appendix E Modbus with the Analyzer and Streaming Data on page 297 To print to a PDF printer configure the printer connection For more information refer to Enabling a PDF Printer o...

Page 158: ...IP Address and Net Mask numbers You can also enter a Gateway IP and up to two DNS Servers 5 Click Save Configuring the Flow Sensor When the water flow is interrupted during Online analysis the Analyzer stops analysis after a pre determined amount of time A No Flow alarm can also be enabled to issue an error when the Analyzer detects no flow The settings can also be configured to automatically rest...

Page 159: ...Sensor Setup dialog box appears 3 Select the Enable Flow Sensor option 4 Click inside the Minutes field and use the numeric keypad to enter the number of minutes 0 90 to keep the analysis running 5 Optional Select the Enable No Flow Alarm option to instruct the Analyzer to record the warning when the flow is interrupted 6 Optional Select the Restart Analysis When Flow Returns option 7 Click Save ...

Page 160: ...el in the DI Reservoir and the Analyzer issues a warning message if the level of water falls below the Add line To enable the Level Sensor 1 On the Settings s screen click the Hardware tab 2 On the scrolling menu select Level Sensor Setup and click Run The Level Sensor Setup dialog box appears Cautions Operating the Analyzer in Online mode with no sample flow and with the Flow Sensor off can resul...

Page 161: ...he Enable DI Reservoir Level Sensor option 4 Click Save Enabling the UV Lamp An option to disable the UV lamp is available for troubleshooting purposes if needed To enable the UV Lamp 1 On the Settings s screen click the Hardware tab 2 On the scrolling menu select UV Lamp Setup and click Run The UV Lamp Setup dialog box appears ...

Page 162: ...select the option Enabling a PDF Printer After a direct or network Ethernet connection to a PDF printer has been set up and configured refer to Installing an Ethernet Connection Optional on page 89 and Configuring an Ethernet Connection on page 157 the PDF printer must be enabled in the firmware To enable a PDF printer 1 Ensure the PDF printer is connected to the Analyzer directly or over an Ether...

Page 163: ...box appears The Analyzer checks for all PDF printers that are available over the Ethernet connection and lists the printers in a dialog box 4 Select the printer to enable for use with the Analyzer 5 Click Save 6 To send a test page to the printer navigate to the scrolling menu for System Tests Settings s screen Diagnostics tab 7 Select Printer and click Run The Analyzer sends a test page to the pr...

Page 164: ...manufacturer s instructions for additional help as needed Configuring a WiFi Connection Optional To configure a WiFi connection Use this instruction to enable a wireless connection when the WiFi option has been purchased NOTE This feature is only available in select countries 1 On the Settings s screen click the Hardware tab 2 On the scrolling menu select WiFi Setup and click Run The WiFi Setup di...

Page 165: ... 6 If the WiFi network requires a password select the Password field and enter the password 7 Click Save SETTINGS SCREEN CONSUMABLES TAB Entering and Reviewing Consumables Status The Consumables tab includes installation and expiration dates as well as a real time status for the days remaining of the Analyzer s consumables UV lamp pump heads and resin cartridge This tab also includes buttons for i...

Page 166: ...consumable replaced SETTINGS SCREEN ERRORS TAB The Errors tab displays the Warning and Error History of the Analyzer The Analyzer issues two levels of messages Warnings Warnings do not stop TOC measurements but may indicate that corrective action is required to prevent eventual Analyzer shutdown or loss of data Errors Errors are serious alerts and all errors stop TOC measurements to prevent the co...

Page 167: ...m the database after creating a backup file See Archiving the Database on page 171 Manually restore the Analyzer s database See Restoring a Backup on page 175 Manually restore system constants See Restoring System Constants on page 176 For information about backing up system constants see Saving System Constants on page 140 Backing Up the Database Use this instruction to make a copy of the databas...

Page 168: ...ting a directory path or creating a folder appears Select a directory path or click the Create Folder button to create a sub folder at the end of the selected directory path If you click the Create Folder button an alphanumeric keypad appears Type the name of the new folder and click OK The folder appears as a sub folder at the end of the selected directory path For Network a dialog box for specif...

Page 169: ...he backup was successfully created appears 7 Click OK 8 If backing up to a USB memory device remove it from the USB port Scheduling Automatic Database Backups The Analyzer can automatically back up the database at a specified frequency and time starting at a specified date When running a system protocol during the time when a scheduled backup will be run disable the backup temporarily to prevent a...

Page 170: ...e USB port 5 Use the default directory path for example mnt usb or mnt net or click the Path button to specify a different directory path A dialog box for selecting a directory path or creating a folder appears 6 Select a directory path or click the Create Folder button to create a sub folder at the end of the selected directory path If you click the Create Folder button an alphanumeric keypad app...

Page 171: ...c 2020 22 00 and 7 The first automatic backup will start on 11 December 2020 at 10 00 pm To disable automatic database backups If a system protocol is performed during the time frame of an automatically scheduled backup first temporarily disable the backup to prevent any interruption to the system protocol 1 On the Settings s screen click the Backup Restore tab 2 De select Enabled in the Scheduled...

Page 172: ...anual Backup Restore section select either USB or Network as the destination of the backup file created during the Archive process 3 For USB insert a USB memory device into the USB port 4 Use the default directory path for example mnt usb or mnt net or click the Path button to specify a different directory path If you click the Path button For USB a dialog box for selecting a directory path or cre...

Page 173: ...ick within the Network Path Username and Password fields and use the alphanumeric keypad to specify those values When you finish click OK A dialog box with the specified network path appears Select the network path 5 Click Save 6 Click Create Archive A dialog box for specifying the months of history data to retain appears ...

Page 174: ...rough 15 December 2020 History data older than 15 October 2020 is removed from the Analyzer s database All history data including history data older than 15 October 2020 is included in the backup file 8 Click OK A progress bar appears When the archive is complete the backup file appears in the Available Backups to Restore section A message appears stating that the database was successfully archive...

Page 175: ... Click Restore Backup A progress bar appears and the current database is backed up prior to restoring the selected backup When the process is complete a message appears stating that the database was successfully restored and the Analyzer s firmware must be restarted 4 Click OK to restart the Analyzer s firmware When the initialization process is complete the Home h screen appears The Available Bac...

Page 176: ...ts option To restore system constants 1 On the Settings s screen click the Backup Restore tab 2 In the Available Backups to Restore section select the backup file containing the system constants to restore 3 Click Restore Constants A progress bar appears while the system constants are restored 4 When the process is complete a message appears stating that the system constants were successfully rest...

Page 177: ...nd exporting data history records To review data history for Online Methods on page 177 To review data history for System Protocols and Grab Methods on page 179 To review data history for Online Methods 1 On the Data D screen select the Online Data tab A trend graph for the specified data appears er 2 To change the color of the background and or the size of the data points see To change the displa...

Page 178: ...3 To display the online data in table view click the Table View icon tab To return to the view of the data as a trend graph click the Trend Graph icon 4 Enter filter parameters for data to view Start Time Date Click in the Start Time field on the left and use the calendar to enter the beginning date of data history to include ...

Page 179: ...Click Apply The online data meeting the applied filter parameters appears on the graph or in the table 7 To view details of the analysis select a line in the table and click Details 8 To print or export data history for a record in the table select a line and click the appropriate button Print or Export NOTE For more information about printing and exporting from an Analyzer screen refer to Printin...

Page 180: ...ter a beginning time of data history End Time Time of Day Click in the End Time field on the right and use the numeric keypad to enter an ending time of data history 3 Do one or more of the following To search by protocol name click inside the Protocol Name Filter field and use the alphanumeric keypad to enter all or part of a protocol record which includes the name and time stamp Select one or mo...

Page 181: ... the appropriate button Print or Export NOTE For more information about printing and exporting from an Analyzer screen refer to Printing and Exporting from the Analyzer Screens on page 120 7 To print or export all the system protocol and grab data history click Print All or Export All 8 To conduct a new search click Reset Filter to clear the current search parameters and data and then repeat steps...

Page 182: ...To enable Password Protection refer to Chapter 5 Password Protection THE HELP SCREEN The Help screen provides reference information about the Analyzer s system including application and system board firmware versions any IOS system and operating system The Analyzer s IP address and unique key are also included This key number may be requested by Technical Support or your local service provider whe...

Page 183: ...g Password Protection To ensure that only authorized personnel access the Analyzer assign one password that all users must enter before starting and stopping analysis or gaining access to menu screens Enabling Password Protection The same password will be required of all users Any user using this password can change the password as needed to comply with internal security policies This section prov...

Page 184: ...Click the Password field and use the alphanumeric keypad to enter a password 5 Confirm the Password 6 Click Save Settings 7 Record the new password in a secure location ALL users will be required to enter this log in information to access the Analyzer s menus To log in using Password Protection 1 Power on the Analyzer The touchscreen illuminates and displays the splash screen during the system ini...

Page 185: ... Login To change the password 1 Go to the Password Protection L screen 2 Click the Password field and use the alphanumeric keypad to enter a new password 3 Confirm the Password 4 Click Save Settings The password you entered will overwrite the previous password To disable Password Protection 1 Go to the Password Protection L screen 2 De select the Enable Security Password option 3 Click Save Settin...

Page 186: ...o methods single point calibration at 1 5 ppm or multi point calibration at 500 ppb 1 0 ppm and 1 5 ppm SUEZ recommends single point calibration for most applications Multi point calibration is available as an alternative procedure for customers A Single Point Calibration requires approximately one hour to complete and the Multi Point Calibration requires approximately two hours For the Sievers M5...

Page 187: ... also determines the background conductivity curves for each channel The Analyzer can be set to automatically perform a TOC Autozero at a specific interval The TOC Autozero is recommended only if the TOC concentration in the sample stream is 50 ppb or less To program the TOC Autozero 1 If the Analyzer is taking measurements click Stop Analysis 2 On the System Protocols p screen select the Calibrat...

Page 188: ...ments 0 03 ppb select the appropriate check box Doing so will allow you to select the number of consecutive TOC measurements 0 03 ppb that will trigger the autozero process 8 Click Save to apply the changes There is also an option to Reset TOC Autozero The Enable Adaptive Autozero check box enables the Analyzer to change the frequency of the scheduled TOC autozero based on the magnitude of the cha...

Page 189: ...ets The Analyzer can be set to automatically perform a TC IC Conductivity Autozero at a specific interval or the user can run the protocol manually 1 If the Analyzer is taking measurements click Stop Analysis 2 On the System Protocols p screen select the Calibration tab 3 Select TC IC Conductivity Autozero then click Setup 4 The Setup TC IC Conductivity Autozero dialog box appears 5 If it is not a...

Page 190: ... point calibration should require approximately one hour to complete and multi point calibration should require approximately two hours to complete NOTE For all calibration and verification procedures use only Sievers standards purchased from SUEZ To purchase standards contact Customer Care or your local service provider Standards sets for calibration and verification can be purchased individually...

Page 191: ...RDS REQUIRED FOR TOC MULTI POINT CALIBRATION Calibration Blank Reagent Water Blank Rw 2 vials 1 5 ppm TOC as KHP 1 ppm TOC as KHP 500 ppb TOC as KHP TABLE 6 3 STANDARDS REQUIRED FOR ACCURACY PRECISION VERIFICATION Reagent Water Blank Rw 500 ppb TOC or 100 ppb TOC as IPA solution for low level verification Warning Consult the MSDS that accompanies each standards set to identify proper disposal tech...

Page 192: ...he settings for future reference To save the system settings 1 On the Instrument Settings s screen Instrument Settings tab select Analyzer Settings 2 Click Export Settings 3 The next screen shows file type file name and path options for the system settings export file 4 Select the Export File Type from the list of options on the right side of the screen 5 The export file path chosen during system ...

Page 193: ...export You can change this filename by selecting the File Name field and using the on screen keyboard to type a file name 7 Click Save to export the system settings To back up the database and settings 1 On the Instrument Settings s screen Backup Restore tab in the Manual Backup Restore section select either USB or Network as the file destination then click the Path button ...

Page 194: ...78510 02 EN Rev B 194 SUEZ 2022 For USB Insert a USB memory device into the USB port select a path or create a new folder and click Save For Network Click Network Credentials to specify the network path username and password then click OK Select a path or create a new folder and click Save ...

Page 195: ...CALIBRATION PREPARATIONS Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 195 SUEZ 2022 2 Click Create Backup ...

Page 196: ...e In particular if the calibration coincides with the Analyzer s annual maintenance first replace the resin cartridge before proceeding for more information see Replacing the Resin Cartridge on page 282 Handling Standards Because of the prevalence of organic carbon contaminants sample preparation and control is extremely delicate Special handling of the standard solutions is required Store standar...

Page 197: ... If performing a Calibration or other system protocols during the time frame of an automatically scheduled data history backup first temporarily disable the backup to prevent any interruption to the system protocol To disable automatic backup On the Instrument Settings s screen Backup Restore tab de select the Scheduled Backup Enabled check box ...

Page 198: ...LM 78510 02 EN Rev B 198 SUEZ 2022 Protocol and Calibration Instructions NOTE Options to Apply passing calibration and start running online or Run accelerated rinse after protocol can be activated by clicking the appropriate check box before starting the protocol ...

Page 199: ...ch as a digital multimeter NOTE The accuracy of the multimeter can affect the results of this protocol 3 0 MATERIALS 3 1 Sievers M500 TOC Analyzer 3 2 Digital multimeter or other device capable of measuring current from 0 20 mA 3 3 4 20 mA Output Verification Worksheet 3 4 ESD wrist strap 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 Optional If DataGuard is enabled log in to the Analyzer with a User...

Page 200: ...anual DLM 78510 02 EN Rev B 200 SUEZ 2022 5 7 Remove the cover by turning the fasteners 1 4 turn to release 5 8 Locate the 4 20 mA Analog Current Loop Output J4 terminal block and attach the multimeter probes to the pins corresponding to the Analog Output 1 2 or 3 to be tested 5 9 Turn on power to the Analyzer ...

Page 201: ...11 In the Analog Output area corresponding to the output 1 2 or 3 to be tested select the Enable Analog Output x check box to activate it 5 12 Click the Set Output button for the selected output An on screen keyboard appears 5 13 Use the on screen keyboard to define the output current as 4 mA then click OK to close the keyboard 5 14 The reading on the multimeter should match the Analyzer s display...

Page 202: ...or 3 to be tested 5 20 In the Analog Outputs Standby Error Warning Values section make sure the values for each selection are different By default the value for Standby is 1 mA the value for Error is 2 5 mA and the value for Warning is 2 5 mA 5 21 Select the Value dropdown for the Analog Output to be tested Configure the output for TOC and set the Max and Min values to encompass the expected range...

Page 203: ...splayed by the multimeter can be confirmed as matching the Analyzer s measurement as follows 5 26 Calculate the error between the Analyzer TOC value and the value displayed by the multimeter as follows Acceptance criterion Error 3 5 27 Repeat steps 5 19 5 26 for the remaining Analog Outputs 5 28 Record the results of the verification s in the 4 20 mA Output Operation Verification Worksheet Optiona...

Page 204: ...point Calibration Protocol on page 212 3 0 MATERIALS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 TOC Single Point Calibration Worksheet 3 3 Calibration Set A TOC Only 3 3 1 One vial Cal Blank 1 3 3 2 One vial Rw Blank 3 3 3 One vial 1 5 ppm TOC 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Analyzer is taking measurements click Stop Analysis 5 2 Export...

Page 205: ... Open the door to the iOS System and wait 30 seconds for water to drain 5 5 3 Insert the Cal Blank 1 vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 4 When analysis of the Cal Blank 1 vial is complete a Please insert Rw Blank dialog box appears 5 5 5 Remove the Cal Blank 1 vial then insert the Rw Blank vial into the iOS System and click Vial read...

Page 206: ...ialog box appears 5 5 7 Remove the Rw Blank vial then insert the 1 5 ppm TOC vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 8 When analysis of the vial is complete remove it from the iOS and click Vial removed Continue 5 6 The TOC Single Point Calibration Protocol Complete screen appears with the Summary tab active and multiple tabs available fo...

Page 207: ...ta on the TOC Single Point Calibration Worksheet 5 8 Do one of the following 5 8 1 If the calibration passed click Apply to accept the calibration A confirmation message appears Click Apply Calibration then Close 5 8 2 If the calibration failed leave the screen as is and contact Technical Support or your local service provider Before calling e mail the backup and system settings files created in a...

Page 208: ...LS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 Low Level TOC Single Point Calibration Worksheet 3 3 Low Level Calibration Set 3 3 1 One vial Cal Blank 1 3 3 2 One vial Rw Blank 3 3 3 One vial 250 ppb TOC Standard 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Analyzer is taking measurements click Stop Analysis 5 2 Export the current system settings for...

Page 209: ...nsert Cal Blank 1 dialog box appears 5 5 2 Open the door to the iOS System and wait 30 seconds for water to drain 5 5 3 Insert the Cal Blank 1 vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 4 When analysis of the Cal Blank 1 vial is complete a Please insert Rw Blank dialog box appears 5 5 5 Remove the Cal Blank 1 vial then insert the Rw Blank vi...

Page 210: ...When analysis of the Rw Blank vial is complete a Please insert the 250 ppb TOC dialog box appears 5 5 7 Remove the Rw Blank vial then insert the 250 ppb TOC vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 8 When analysis of the vial is complete remove it from the iOS and click Vial removed Continue ...

Page 211: ...t Print and Export buttons 5 7 Referencing the Summary tab record the results data on the Low Level TOC Single Point Calibration Worksheet 5 8 Do one of the following 5 8 1 If the calibration passed click Apply to accept the calibration A confirmation message appears Click Apply Calibration then Close 5 8 2 If the calibration failed leave the screen as is and contact Technical Support or your loca...

Page 212: ...nalyzer NOTE Choose either a single point or multi point calibration for validation purposes not both For single point instructions See TOC Single Point Calibration Protocol on page 204 3 0 MATERIALS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 TOC Multi point Calibration Worksheet 3 3 Calibration Set A TOC Only 3 3 1 One vial Cal Blank 1 3 3 2 Two vials R...

Page 213: ...the database and settings by following the steps in To back up the database and settings on page 193 5 4 On the System Protocols p screen select the Calibration tab 5 5 Select TOC Multi point Calibration then click Start 5 5 1 A Please insert dialog box appears 5 5 2 Open the door to the iOS System and wait 30 seconds for water to drain 5 5 3 Insert the Cal Blank 1 vial into the iOS System and cli...

Page 214: ...ert the 1 5 ppm TOC dialog box appears 5 5 7 Remove the Rw Blank vial then insert the 1 5 ppm TOC vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 8 When analysis of the 1 5 ppm TOC vial is complete a Please insert the Rw Blank dialog box appears 5 5 9 Remove the 1 5 ppm TOC vial then insert the Rw Blank vial into the iOS System and click Vial rea...

Page 215: ...analysis of the 1 ppm TOC vial is complete a Please insert the 500 ppb TOC dialog box appears 5 5 13 Remove the 1 ppm TOC vial then insert the 500 ppb TOC vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 5 14 When analysis of the vial is complete remove it from the iOS and click Vial removed Continue 5 6 The TOC Multi point Calibration Protocol Comp...

Page 216: ...ta on the TOC Multi point Calibration Worksheet 5 8 Do one of the following 5 8 1 If the calibration passed click Apply to accept the calibration A confirmation message appears Click Apply calibration then Close 5 8 2 If the calibration failed leave the screen as is and contact Technical Support or your local service provider Before calling e mail the backup and system settings files created in ad...

Page 217: ... Analyzer 2 0 SCOPE This procedure applies to the Sievers M500e TOC Analyzer 3 0 MATERIALS 3 1 Sievers M500e TOC Analyzer 3 2 TC IC Conductivity Autozero Worksheet 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Analyzer is taking measurements click Stop Analysis 5 2 Export the current system settings for future reference or reloading by following the steps in To save the system settings on page...

Page 218: ...the System Protocols p screen select the Calibration tab 5 5 Select TC IC Conductivity Autozero and click Start 5 6 The TC IC Conductivity Autozero Results screen appears as follows Results The summary of calibration including the old and new offset values It also contains the Apply and Reject buttons as well as the Print and Export buttons ...

Page 219: ...ta on the TC IC Conductivity Autozero Worksheet 5 8 Do one of the following 5 8 1 If the calibration passed click Apply to accept the calibration A confirmation message appears Click Apply calibration then Close 5 8 2 Click Reject to reject the new offset A confirmation message appears Click Reject calibration then Close 5 9 To print or export the results click the corresponding button ...

Page 220: ...lyzer 3 0 MATERIALS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 TOC Autozero Calibration Worksheet 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Analyzer is taking measurements click Stop Analysis 5 2 Export the current system settings for future reference or reloading by following the steps in To save the system settings on page 192 5 3 Back up the d...

Page 221: ...UEZ 2022 5 5 Select TOC Autozero and click Start 5 6 After analysis is complete the Results screen appears with the summary of analysis It also contains the Apply and Reject buttons as well as the Print and Export buttons 5 7 Referencing the Results screen record the results data on the TOC Autozero Calibration Worksheet ...

Page 222: ...UEZ 2022 5 8 Do one of the following 5 8 1 Click Apply to accept the new offset A confirmation message appears Click Apply calibration then Close 5 8 2 Click Reject to reject the new offset A confirmation message appears Click Reject calibration then Close 5 9 To print or export the results click the corresponding button ...

Page 223: ...rs M500e TOC Analyzer 2 0 SCOPE This procedure applies to the Sievers M500e TOC Analyzer 3 0 MATERIALS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 Accuracy Precision Verification Worksheet 3 3 Accuracy Precision Verification Standard Set 3 3 1 One vial Rw Blank 3 3 2 One vial 500 ppb TOC 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Analyzer is taking...

Page 224: ...5 3 2 Open the door to the iOS System and wait 30 seconds for water to drain 5 3 3 Insert the Rw Blank vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 3 4 When analysis of the Rw Blank vial is complete a Please insert the 500 ppb dialog box appears 5 3 5 Remove the Rw Blank vial then insert the 500 ppb TOC vial into the iOS System and click Vial re...

Page 225: ...s for each standard Summary Select this tab to view the summary of analysis including a passed or failed result It also contains the Print Export and Close buttons 5 5 Referencing the Summary tab record the results data on the Accuracy Precision Verification Worksheet 5 6 If the verification failed leave the screen as is and contact Technical Support or your local service provider Before calling e...

Page 226: ...Sievers M500e TOC Analyzer 2 0 SCOPE This procedure applies to the Sievers M500e TOC Analyzer 3 0 MATERIALS NOTE Use only Sievers standards purchased from SUEZ 3 1 Sievers M500e TOC Analyzer 3 2 Accuracy Precision Verification Worksheet 3 3 Low Level Accuracy Precision Verification Standard Set 3 3 1 One vial Rw Blank 3 3 2 One vial 100 ppb TOC 4 0 DEFINITIONS 4 1 None 5 0 PROCEDURE 5 1 If the Ana...

Page 227: ...x appears 5 3 2 Open the door to the iOS System and wait 30 seconds for water to drain 5 3 3 Insert the Rw Blank vial into the iOS System and click Vial ready Continue The Analyzer begins analysis of the vial 5 3 4 When analysis of the Rw Blank vial is complete a Please insert the 100 ppb dialog box appears 5 3 5 Remove the Rw Blank vial then insert the 100 ppb TOC vial into the iOS System and cli...

Page 228: ...dard Summary Select this tab to view the summary of analysis including a passed or failed result It also contains Print Export and Close buttons 5 5 Referencing the Summary tab record the results data on the Accuracy Precision Verification Worksheet 5 6 If the verification failed leave the screen as is and contact Technical Support or your local service provider Before calling e mail the backup an...

Page 229: ...d Grab Methods Data tab 2 at 1 Select the date and time range in which to search for results 3 at 2 Select and de select the check boxes to filter the results to be displayed and click Apply or click Reset Filter to return to the default Calibration Verification Grab Method TOC Select the Protocol Name Filter field to enter all or part of a protocol record name to search for 4 at 3 Select a Protoc...

Page 230: ... a USB storage device or a network location Click Export All to output all Protocol Records 6 1 The next screen shows file type file name and path options for the system settings export file 6 2 Select the Export File Type from the list of options on the right side of the screen 6 3 The filename appears as the date time stamp of the export You can change this filename by selecting the File Name fi...

Page 231: ... Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 231 SUEZ 2022 Protocol and Calibration Worksheets ...

Page 232: ... 3 4 Analog Output 3 J4 pins 5 6 Max value Max value Max value Min value Min value Min value Standby current multimeter Standby current multimeter Standby current multimeter Measurement current multimeter Measurement current multimeter Measurement current multimeter TOC value Analyzer TOC value Analyzer TOC value Analyzer Value of current converted to TOC ppb Value of current converted to TOC ppb ...

Page 233: ...heet Company Name Analyzer Serial Number Firmware Version Analyzer Location Sample Lot and Expiration PASS FAIL CRITERIA Cal Blank 1 IC RSD 3 00 Cal Blank 1 TC RSD 3 0 1 5 ppm TOC RSD 3 0 Change in IC Slope 20 0 Change in TC Slope 20 0 The attached data will indicate a Passed or Failed condition Results Passed Failed Performed by Date Reviewed by Date Verified by Date ...

Page 234: ...ion Worksheet Company Name Analyzer Serial Number Firmware Version Analyzer Location Standard Lot and Expiration PASS FAIL CRITERIA Cal Blank 1 IC RSD 3 00 Cal Blank 1 TC RSD 3 0 250 ppb TOC RSD 3 0 Change in IC Slope 20 0 Change in TC Slope 20 0 The attached data will indicate a Passed or Failed condition Results Passed Failed Performed by Date Reviewed by Date Verified by Date ...

Page 235: ...al Number Firmware Version Analyzer Location Standard Lot and Expiration PASS FAIL CRITERIA Cal Blank 1 IC RSD 3 00 Cal Blank 1 TC RSD 3 00 1 5 ppm TOC RSD 3 00 1 ppm TOC RSD 3 00 500 ppb TOC RSD 3 00 Change in IC Slope 20 0 Change in TC Slope 20 0 R squared 0 988 The attached data will indicate a Passed or Failed condition Results Passed Failed Performed by Date Reviewed by Date Verified by Date ...

Page 236: ...C IC Conductivity Autozero Worksheet Company Name Analyzer Serial Number Firmware Version Analyzer Location TC Cell New Offset __________________ TC Cell Old Offset __________________ IC Cell New Offset __________________ IC Cell Old Offset __________________ Results Applied Rejected Performed by Date Reviewed by Date Verified by Date ...

Page 237: ...nual DLM 78510 02 EN Rev B 237 SUEZ 2022 TOC Autozero Worksheet Company Name Analyzer Serial Number Firmware Version Analyzer Location New TOC Offset __________________ Old TOC Offset __________________ Results Applied Rejected Performed by Date Reviewed by Date Verified by Date ...

Page 238: ...EZ 2022 Accuracy Precision Verification Worksheet Company Name Analyzer Serial Number Firmware Version Analyzer Location Standard Lot and Expiration Pass Fail Criteria TOC Difference 7 TOC RSD 3 00 The attached data will indicate a Passed or Failed condition Results Passed Failed Performed by Date Reviewed by Date Verified by Date ...

Page 239: ...EZ 2022 Low Level Accuracy Precision Verification Worksheet Company Name Analyzer Serial Number Firmware Version Analyzer Location Standard Lot and Expiration Pass Fail Criteria TOC Difference 7 TOC RSD 3 00 The attached data will indicate a Passed or Failed condition Results Passed Failed Performed by Date Reviewed by Date Verified by Date ...

Page 240: ...l inspection of the Analyzer to identify any obvious physical problems or symptoms Begin with an external visual inspection and proceed to an internal visual inspection If possible perform the inspection with the Analyzer in analysis mode to verify that relevant modules are performing as intended NOTE Be sure to fully inspect the Analyzer visually before proceeding with more in depth troubleshooti...

Page 241: ...lyzer front panel and do the following Check for leaks throughout the Analyzer there should not be moisture on the inside floor of the Analyzer case Confirm that the sample pump is turning Check to make sure there are no leaks from tubing in the DI water system Confirm that the DI water reservoir is full If necessary add water up to the Full line ...

Page 242: ...irm that all electronics cables are securely attached Make sure there are no air bubbles present in any of the DI Loop tubing Make sure tubing is not kinked or obstructed Make sure the UV lamp is working During analysis the window on the UV reactor will illuminate when the lamp is functioning properly NOTE If tubing has become bent kinked or otherwise damaged a tubing replacement kit is available ...

Page 243: ... list return to the full list of errors and warnings by clicking Reset 1 On the Settings s screen select the Errors tab 2 Review the list of messages listed most recent to earliest Use the scroll bar on the right to view any additional lines and pages of messages 3 To sort messages by time range type click one of the following options Occurrence Time Range Acknowledge Time Range 4 To search for me...

Page 244: ...al details of a message select the message line and click Details The Details dialog box appears This dialog box displays the time the error occurred a description of the error and the Error Status whether or not the error has been acknowledged by the user 9 To acknowledge a warning or error appearing in the list select a message line and click Acknowledge Error 10 To acknowledge all the warning a...

Page 245: ...owing export file types from the list of options on the right side of the screen csv xlsx pdf pdf encrypted enc encrypted 16 The filename appears as the date time stamp of the export You can change this filename by selecting the File Name field and using the on screen keyboard to type a file name 17 Click Save to export the Error History ...

Page 246: ...h the FULL mark on the outside of the reservoir 2 If the water level is low add water by following the instructions in Basic Analyzer Operation on page 111 3 If the DI reservoir is full when this error occurs power cycle the Analyzer Stop any analysis and click the Power Off P button in the Analyzer s firmware then turn off the power switch Wait 30 seconds then turn on the power switch 4 If the er...

Page 247: ...NG THE SAMPLE PUMP While the Analyzer is operating open the Analyzer front panel and make sure the sample pump is turning If the pump is not turning and the Analyzer is operating the display screen indicates that analysis is taking place contact Technical Support or your local service provider for instructions Warning To avoid potentially dangerous shock Before opening the Analyzer stop any analys...

Page 248: ... SUEZ 2022 NO SAMPLE FLOW THROUGH THE ANALYZER To troubleshoot a lack of flow through the Analyzer follow these steps 1 Perform a backflush procedure 1 1 Navigate to the Settings screen Hardware tab Select Backflush 1 2 Click Run and follow the on screen instructions to complete the backflush procedure ...

Page 249: ...le Place the Analyzer in Standby mode to open valves To check flow of water through the conductivity cells 1 Locate the restrictor tube on the DI side of the fluidics module It is a narrow looped plastic tube 2 Disconnect the PEEK fittings on each end of the restrictor tube 3 Flush the tube with water then reconnect it 4 If the restrictor tube is clear check the flow through the T fitting that the...

Page 250: ...ng unusually high IC or TC values or returning negative IC TC or conductivity values a TC IC Conductivity Autozero might be necessary See TC IC Conductivity Autozero Protocol on page 217 for instructions TOC AUTOZERO The TOC Autozero corrects for minor differences in the response of the two CO2 sensors This adjustment may help when the Analyzer is reading very high or negative values After running...

Page 251: ...on and autozero have failed to allow multiple instruments to match within the stated accuracy specifications of the Analyzer To set the TOC Offset see Setting a User TOC Offset on page 146 for instructions PROBLEMS CHANGING THE PROGRAM LANGUAGE If the program language is changed by mistake and or for help navigating back to your preferred language follow these steps These steps are designed to hel...

Page 252: ...UBLESHOOTING Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 252 SUEZ 2022 2 Count down four fields to the Language field and click the arrow to display the drop down menu ...

Page 253: ...k the air bubbles out 5 If simple manipulation of the tubing does not free the air bubbles disconnect the fitting that connects to the DI water reservoir Raise the tubing so that it is higher than the cartridge and remove the rubber vent cover Move the tubing lower than the DI water reservoir to force any air bubbles out of the tubing Be prepared to raise the tubing quickly as soon as all air is f...

Page 254: ...TROUBLESHOOTING Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 254 SUEZ 2022 ...

Page 255: ...he following procedures Alarms Use this test to verify the functionality of the Analyzer s four alarms From the Diagnostics tab select Alarms and click Run to display each alarm s current status and volume Alarms Analog Outputs Modbus Network Folder Printer Sample Flow Rate Super iOS IC Power Relay Internet Connection USB Serial Loopback Serial Loopback WiFi ...

Page 256: ...arm check box for an alarm to test its functionality 2 To test another alarm deselect the active alarm and select another Activate Alarm check box 3 When you are done testing deselect the last active alarm and click Close Test to exit the screen NOTE To change alarm settings follow the instructions at To set up alarm output on page 106 ...

Page 257: ...lay the Analog Output Test 1 Select an Enable Analog Output check box to test its functionality The Set Output button becomes available for that output 2 Use a multimeter to measure the output 3 Click the Set Output button 0 00 mA to display a numeric keypad Enter the measured output and click OK 4 To test additional analog outputs deselect the current Enable Analog Output check box and repeat ste...

Page 258: ...ructing you to connect your Modbus client to the Analyzer at the displayed IP address 1 Connect the Modbus client as instructed and click OK to continue 2 The Modbus Test screen displays a list of input statuses activations and other information Sort this data by clicking the column headings at the top of each column Register Name Address Bit and Value Scroll down using the scroll bar to see addit...

Page 259: ...tab select Network Folder and click Run to display the Network Folder Test 1 Select the User Name Network Password and Network Folder Path fields to display an alphanumeric keypad for entering the information in each field 2 When all network information has been entered click Write File to Folder to send a test file to the location If the test was successful the following dialog box will appear 3 ...

Page 260: ... print a Print Test message to the printer Sample Flow Rate Use this test to verify functionality of the Sample Pump From the Diagnostics tab select Sample Flow Rate and click Run to display the Sample Flow Rate Test 1 Follow the on screen instructions then click Start to begin the test The status of the test is displayed 2 When the test completes follow the on screen instructions to reconnect the...

Page 261: ...e Diagnostics tab select IC Power Relay and click Run to display a dialog box with further test instructions Follow the on screen instructions When the test is complete click Ok to exit the screen Internet Connection Use this test to verify connectivity from the Analyzer to the Internet From the Diagnostics tab select Internet Connection and click Run to test connectivity The results of the test a...

Page 262: ...22 USB Serial Loopback Use this test to verify the functionality of the USB ports with serial loopback From the Diagnostics tab select USB Serial Loopback and click Run to display a dialog box with further test instructions Follow the on screen instructions When the test is complete click OK to exit the screen ...

Page 263: ...gnostics tab select Serial Loopback and click Run to display a dialog box with further test instructions Follow the on screen instructions When the test is complete click OK to exit the screen WiFi Use this test to verify functionality of the Analyzer s WiFi connectivity and PCIE adapter From the Diagnostics tab select WiFi and click Run to test connectivity The results of the test are displayed C...

Page 264: ... next to each data type to be included or select Export All 2 Choose the destination for the export file Select USB or Network Folder then click Set Path to display an alphanumeric keypad to enter the destination directory 3 Click OK to accept the destination 4 Click Start Export to export the data A progress bar shows the status of the export 5 When exporting is complete you can now share this in...

Page 265: ...plays diagnostic data and or tests functionality of the Sample Pump IC TC Cells Sample Cell DI Loop UV Lamp iOS Flow Sensor Measurement Module Temperature and Door State 1 Select a Sample Pump speed 2 Select DI Loop options Disable Level Sensor DI Pump IC TC Valve 3 Select UV Lamp on off 4 Click Start Analysis 5 Click Stop Analysis when you are ready to end the test ...

Page 266: ...gathered during normal Analyzer operation Filter the graph data by selecting and de selecting the IC Cond TC Cond IC Temp and TC Temp filters STEP 4 CONTACT TECHNICAL SUPPORT After completing Step 1 Visual Inspection on page 240 through Step 3 Review Solutions for Basic Problems on page 247 contact Technical Support or your local service provider When calling please have basic Analyzer information...

Page 267: ...orization RA number Several precautions must be followed to ensure that the Analyzer is not damaged during shipment If the original shipping container has not been retained contact Technical Support or your local service provider to order shipping supplies Under no circumstances should the Analyzer be packed in anything other than the original shipping container Before repackaging water must be dr...

Page 268: ...alyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 268 SUEZ 2022 2 1 Select Drain Sample Side do not select Drain DI Loop at this time 2 2 Click Next 2 3 Ensure that the sample flow to the instrument is shut off and click Next ...

Page 269: ...enance Manual DLM 78510 02 EN Rev B 269 SUEZ 2022 2 4 Wait for the drain process to complete approximately 3 minutes 2 5 When the screen says Draining the sample side is complete click Next then Close 2 6 In the Hardware tab select Flow Sensor Setup 2 7 Click Next ...

Page 270: ...disabled unchecked and click Save 2 9 On the Protocols p screen select the User Defined Methods tab 2 10 Verify that the Measurement Mode is set to Online if not select Online Method from the list of user defined methods 2 11 Click Start to begin analysis When the waste tubing is full of air click Stop Analysis In the dialog box that appears confirm this action ...

Page 271: ...oes black turn the Analyzer power switch left to the Off position 2 14 Unplug the Analyzer from its power source DRAINING THE DI LOOP 1 Confirm that the Analyzer is powered off and unplugged and no other cables are attached 2 Detach the resin cartridge by declicking the release buttons on the DI Loop fittings then drain the resin cartridge by removing the C clips and fittings from both ends NOTE T...

Page 272: ...m inside the Analyzer door and attach it to the RUN position fitting 4 Squeeze and release the bulb several times to pump the excess water from the measurement module 5 Retrieve the drain tube from inside the Analyzer door place the free end into a waste container 1 e g a 500 mL beaker then attach the fitting to the resin cartridge inlet 2 ...

Page 273: ...waste tubing and sample inlet tubing from the Analyzer 9 Disconnect any printer alarm analog output or computer cables 10 Disconnect the power connection to the Analyzer see note below 11 Disconnect any alarm or 4 20 mA connections to the Analyzer s terminal block NOTE A qualified electrician may be needed to help detach the wiring both power and accessories from the terminal block inside the Anal...

Page 274: ...h as the UV lamp resin cartridge or pump heads perform a verification of the calibration Only re calibrate if verification indicates that a new calibration is necessary For additional assistance contact SUEZ Technical Support or your local service provider Training is also available from SUEZ This chapter covers replacement instructions for all routine maintenance items that are replaced on a regu...

Page 275: ...es Description Typical Operating Life DI Water Level 6 months Also check when replacing other items and refill as needed UV Lamp 6 months Fan Filter 6 months Sample Pump Heads 12 months Resin Cartridge Typically 24 Months depending on water quality In line Filter Replace as Needed depending on water quality Resin Cartridge DI Water Reservoir Sample Pump Heads UV Reactor UV Lamp Holder Fan Filter ...

Page 276: ...er to the Off position to complete the power off cycle 4 Open the door to the Analyzer 5 Locate the DI water reservoir See Figure 8 1 on page 275 6 If the water level is below the Full line add DI water to the reservoir as instructed in the next section To fill the DI water reservoir 1 Locate the dispensing bottle in the Analyzer s Accessories Kit 2 Have a paper towel nearby in case of any leakage...

Page 277: ...ole and squeeze the bottle to fill the DI reservoir until the water line reaches the FULL line indicated on the outside of the reservoir 6 Re insert the rubber stopper into the top of the DI reservoir 7 Close and latch the door to the Analyzer case 8 Re establish power to the Analyzer It is not necessary to prime the DI water pump for this procedure ...

Page 278: ... of the Analyzer to the Off position to complete the power off cycle 4 Open the Analyzer s door to access the inside of the Analyzer Hazardous Material Disposal The UV lamp contains mercury and may be considered hazardous material in your local area Dispose of these items in accordance with federal state or local government regulations In the case of any broken or damaged UV lamp handle the remain...

Page 279: ...he new lamp from the packet 10 Carefully slide the lamp assembly into the enclosure Stop if feeling any resistance and realign the lamp in the reactor NOTE This photo is for illustration only The Holder is removed from its installed position Insert the UV Lamp into the Holder on the UV Reactor 11 Connect the power connector to the bulkhead connector by aligning yellow lines and pushing firmly unti...

Page 280: ...s button 2 Shut off the water to the sample inlet system 3 On the Analyzer s Home screen click the Power Off button to close all the files 4 Turn the rotary power switch located on the left outside panel of the Analyzer to the Off position to complete the power off cycle 5 Open the door to access the inside of the Analyzer 6 Locate the sample pump heads see Figure on page 275 7 Remove the tubing l...

Page 281: ...e body of the pump head and attempt to move it a few degrees clockwise and counterclockwise The body of the pump head should still be able to move a slightly If the pump head body is immobile then the screws are overtightened NOTE When securing the pump head screws ensure that the body of the pump head can shift independently from the bridge to allow proper alignment between the screws and the sha...

Page 282: ... installing the resin cartridge into the RUN position To replace the resin cartridge 1 If the Analyzer is taking measurements click the Stop Analysis button 2 On the Analyzer s Home screen click the Power Off button to close all the files 3 Turn the rotary power switch located on the left outside panel of the Analyzer to the Off position to complete the power off cycle 4 Open the door to access th...

Page 283: ...ains power to the Analyzer and turn the power switch to the ON position This will turn on the DI water pump Let the Analyzer run for 30 minutes to allow the DI pump to circulate water in the DI Loop 9 Turn off the Analyzer and open the door to the Analyzer 10 Check the level of water in the DI water reservoir If the water level has dropped below the Full line remove the rubber inlet cover from the...

Page 284: ...ore moving to the next step 14 Restore power to the Analyzer 15 Enter the installation date for the resin cartridge in the firmware as described in Entering New Consumables Installation Dates on page 287 16 Let the Analyzer run for an additional 30 minutes to circulate water in the DI loop 17 Turn off the Analyzer and open the door to check and troubleshoot any leaks 18 Restore power to the Analyz...

Page 285: ...ase and can even stop A simple way to determine if the filter element needs to be changed is to periodically measure the flow rate of water out the waste line from the iOS System and replace the filter element when the flow rate starts to decrease Replace the filter element on a routine basis to prevent clogging To replace the filter element 1 If the Analyzer is taking measurements click the Stop ...

Page 286: ... 13 Reconnect the 1 4 Teflon tubing from the sampling port adapter to the inlet of the in line filter The in line filter has arrows on the body of the filter that indicate the direction of flow through the filter Tighten the nut one quarter turn past finger tight 14 Reconnect the 1 4 Teflon tubing to the outlet of the filter and tighten the nut one quarter turn past finger tight 15 Turn on the wat...

Page 287: ...llation Dates When replacing a consumable enter the date of installation on the Consumables screen to enable the Analyzer to keep an accurate record of usage and issue reminders 1 On the Settings screen select the Consumables tab 2 In the applicable area UV Lamp Pump Tubing Resin Cartridge click one of the following buttons to use the calendar for entering the date the consumable was installed The...

Page 288: ...ion to complete the power off cycle 4 Turn off power to the Analyzer with the main power switch 5 Wipe the external housing with a clean cloth dampened with water or a non abrasive cleaner 6 Wipe dry with another clean and dry soft cloth To clean the touchscreen 1 Obtain a clean soft and dry cloth or cotton pad 2 Navigate to the System Tests panel Settings screen Diagnostics tab 3 On the scrolling...

Page 289: ...mpassed by this worksheet from __________ to __________ Fan Filter 12 months UV Lamp 18 months DI Water Level 18 months Fan Filter 18 months Pump Heads 24 months UV Lamp 24 months Resin Cartridge 24 months DI Water Level 24 months Fan Filter 24 months UV Lamp 30 months DI Water Level 30 months Fan Filter 30 months Pump Heads 36 months UV Lamp 36 months DI Water Level 36 months Fan Filter 36 months...

Page 290: ...OC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 290 SUEZ 2022 Appendix A Analyzer Dimensions ANALYZER DIMENSIONS Diagrams show Analyzer dimensions and required clearances as follows inches millimeters ...

Page 291: ...IGURED WITH STANDARD IOS Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 291 SUEZ 2022 Analyzer Configured with Standard iOS Figure A 1 Analyzer Dimensions with Standard iOS System ...

Page 292: ...ANALYZER CONFIGURED WITH STANDARD IOS Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 292 SUEZ 2022 Figure A 2 Right Side Analyzer Dimensions with Standard iOS System ...

Page 293: ...ANALYZER CONFIGURED WITH STANDARD IOS Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 293 SUEZ 2022 Figure A 3 Left Side Analyzer Dimensions with Standard iOS System ...

Page 294: ...D WITH SAMPLE INLET BLOCK Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 294 SUEZ 2022 Analyzer Configured with Sample Inlet Block Figure A 4 Analyzer Dimensions with Sample Inlet Block ...

Page 295: ...ALYZER CONFIGURED WITH SAMPLE INLET BLOCK Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 295 SUEZ 2022 Figure A 5 Right Side Analyzer Dimensions with Sample Inlet Block ...

Page 296: ...NALYZER CONFIGURED WITH SAMPLE INLET BLOCK Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 296 SUEZ 2022 Figure A 6 Left Side Analyzer Dimensions with Sample Inlet Block ...

Page 297: ...345 25 4 3 123 If the Analyzer is showing resistance instead of conductivity see Setting Trend Graph Display Options on page 137 the data stream has these values mode date time TOC IC TC Temperature Resistance There are no units in the stream TOC IC TC are output as ppb The rCond and tCond values are output as µS cm and temperature is output in C Resistance is output as M cm The TOC value field ma...

Page 298: ...e the Analyzer takes a measurement the measurement is streamed to the computer and appears in the terminal window TO STREAM DATA VIA ETHERNET 1 Connect an Ethernet cable to the Analyzer as described in Installing an Ethernet Connection Optional on page 89 2 Enable the Ethernet network on the Analyzer as described in Configuring an Ethernet Connection on page 98 3 Make sure the Analyzer is powered ...

Page 299: ...mmunication port is in use To try to determine which communication port is being used to connect to the Analyzer follow these steps 1 On the computer display the Windows Device Manager For example on Windows 10 click the Start button and type Device Manager 2 In the Device Manager window scroll down to Ports Com and LPT and show the selections For example on Windows 10 click the right arrow 3 The ...

Page 300: ...hen measuring sample conductivity and insufficient readings are taken to be able to calculate the sample conductivity 802 Warning Sample Cell The Analyzer door is open Occurs during the Resistance Verification protocol when the instrument door is open 2500 Warning Flash Memory Flash Memory Error invalid value was obtained Occurs when the following constants are below 0 1 TC IC or sample cell const...

Page 301: ...s on and the current 500 mA The DI pump is off and the current 120 mA 5804 Error IC TC Valve No current was detected in the IC TC Valve Occurs when the IC TC valve is actuated and the Analyzer detects a current 5 mA 5805 Error IC TC Valve The current detected in the IC TC Valve is unexpectedly high Occurs when the Analyzer detects 200 mA when valve is actuated 5 mA when valve is not actuated 5807 ...

Page 302: ...than 15 days are left on the UV Lamp 10003 Warning Pump Tubing Pump heads should be replaced soon When updating Consumables status on startup every hour when updated remotely via T C when installing Pump Tubing if less than 15 days are left on Pump Tubing 10004 Warning Resin Cartridge Resin bed should be replaced soon Occurs when updating Consumables status on startup every hour when updated remot...

Page 303: ...aved or read because data directory does not exist or the datastore file path is invalid Also if during data export the export file path is invalid directory does not exist or does not allow writing 11401 Error Datastore Datastore error could not open file for read write Occurs when records cannot be saved because a datastore file cannot be created or opened for read write 11402 Error Datastore Da...

Page 304: ...records is invalid e g for error history if end date is prior to start date 11412 Error Datastore Datastore error when saving system setting Occurs if an error occurs while saving a system setting or system constant to database e g cannot write to datastore when editing or updating with value from Instrument Controller when receiving an unexpected response from Instrument Controller instead of con...

Page 305: ...If an error occurred while converting older version SDBS Suitability data from datastore to the latest version 11422 Error Datastore Datastore error upgrading Error History data Occurs if an error occurred while converting older version Error History data from datastore to the latest version 11423 Error Datastore Datastore error upgrading Audit Trail data Occurs if an error occurred while converti...

Page 306: ... 11508 Error Analysis Could not read protocol configuration file Occurs when system protocols cannot be read from the configuration file 11513 Error Data Parsing Level1 data parsing error could not log it Occurs while running a protocol if invalid formatted Level1 data is received 11599 Error GUI Did not receive ACK response from Instrument Controller Occurs if no confirmation was received from th...

Page 307: ...Occurs when the logging system cannot be initialized because file appenders cannot be created 11800 Error Diagnostics Failed setting Super iOS valve position Occurs during Sample Flow Rate Test if the Super iOS valve positions cannot be set 11801 Error Diagnostics Failed getting Super iOS valve position Occurs if Super iOS vial positions cannot be read from the hardware during Diagnostics 11802 Er...

Page 308: ...LS Installing the resin cartridge To install the resin cartridge 1 Locate the resin cartridge in the Analyzer s Accessories Kit Holding the cartridge with the indicated end up simultaneously insert one elbow fitting end of the resin cartridge into the Run port and the other elbow fitting end into the DI pump outlet Verify that the ends are secure before moving to the next step ...

Page 309: ...avoid damaging the cartridge 2 Continue to the next section To fill the DI water reservoir To fill the DI water reservoir 1 Continue from the previous section To install the resin cartridge on page 308 2 Locate the dispensing bottle in the Analyzer s Accessories kit 3 Have a paper towel nearby in case of any leakage during the installation process 4 Unscrew the lid of the dispensing bottle and fil...

Page 310: ... SUEZ 2022 6 Insert the tip of the bottle into the hole and squeeze the bottle to fill the DI reservoir until the water line reaches the FULL line indicated on the outside of the reservoir 7 Re insert the check valve into the top of the DI reservoir 8 Manipulate the pump tubing to move any bubbles into the reservoir ...

Page 311: ...e priming process takes approximately 180 minutes plus minimal setup and reset time 1 Continue from the previous section To fill the DI water reservoir 2 Move the resin cartridge from the Run position to the Prime position Press the top latch of the resin cartridge to release it and gently rotate the top of cartridge to the Prime position Push to insert the elbow fitting into the Prime port while ...

Page 312: ...the top of cartridge to the Run position Push to insert the elbow fitting into the Run port while leaving the lower elbow fitting end in the DI pump outlet Verify that the ends are secure before moving to the next step 6 View the water level in the DI reservoir and verify that the water level reaches the FULL line as indicated on the outside of the reservoir The water level may now be lower as wat...

Page 313: ...rvice rinse the Analyzer using the automated Accelerated Rinse feature This feature takes approximately one hour to complete To rinse the Analyzer 1 With a water flow established to the sample inlet system of the Analyzer on the Settings screen select the Hardware tab 2 Select the Accelerated Rinse in the scroll list and click RUN The Accelerated Rinse dialog box appears ...

Page 314: ... 6 Click CLOSE 7 Open the Analyzer door and inspect for any leaks especially around the DI water reservoir 8 If a leak is detected verify all fittings are tight and secure Also confirm the water level in the DI water reservoir is full If necessary turn the Analyzer power switch to Off and add more water using the water bottle with filling nozzle from the Analyzer s Accessories kit 9 Close and latc...

Page 315: ...ition software by internal Process Engineering departments It is difficult to provide all details as the bulk of the configuration and programming is completed within the third party device Various vendor SCADA systems are programmed differently As noted in the following steps some systems require memory addresses to be formatted in a unique way while others label Modbus functions differently Enab...

Page 316: ...isters referenced in this section need to be combined to create one 32 bit floating point TOC value This is necessary as Modbus only supports 16 bit registers The SCADA software will have an option for combining these values The input register at memory address 3302 can be read to display the TOC units a value of 1 ppt 2 ppb 3 ppm even though the unit of measure is fixed for the M500e TOC Analyzer...

Page 317: ...t Discrete Inputs read Status 2 1000 New Data 0 Error 1 Standby 2 Alarm 1 3 Alarm 2 4 Alarm 3 5 Alarm 4 6 Activations 2 1002 Feature 1 0 Feature 2 1 Feature 3 2 Feature 4 3 Feature 5 4 Coils read State 1 2000 Run 0 Stop 1 Coils write Run 5 2000 Stop 5 2001 Input Registers read Instrument Family 4 3010 Instrument Model 4 3011 Serial Number 4 3012 Firmware Version Major 4 3015 Firmware Version Minor...

Page 318: ...03 Reading Time Minute 4 3104 Reading Time Second 4 3105 Error Type 4 3200 Error Time Year 4 3201 Error Time Month 4 3202 Error Time Day 4 3203 Error Time Hour 4 3204 Error Time Minute 4 3205 Error Time Second 4 3206 TOC Value Low Word 4 3300 TOC Value High Word 4 3301 TOC Units 4 3302 TC Value Low Word 4 3310 TC Value High Word 4 3311 TC Units 4 3312 IC Value Low Word 4 3320 IC Value High Word 4 ...

Page 319: ...Low Word 4 3500 Sample Temp Cond Value High Word 4 3501 Sample Temp Conductivity Units 4 3502 Raw Sample Cond Value Low Word 4 3510 Raw Sample Cond Value High Word 4 3511 Raw Sample Conductivity Units 4 3512 Sample Temp Value Low Word 4 3700 Sample Temp Value High Word 4 3701 Sample Temperature Units 4 3702 Holding Registers read write not used Table E 1 Modbus Register Table Register Type Descrip...

Page 320: ...s are 0 Disabled 1 Enabled Reject units are 0 Not Rejected 1 Rejected Stream units are 20 Check Standard 10 Vial Port 1 Stream 1 2 Stream 2 3 Stream 3 4 Stream 4 5 Stream 5 Firmware Minor is yy in xx yy zzz Firmware Engineering is zzz in xx yy zzz Measurement Mode IC 10 TC 20 TOC 30 NPOC 40 Current Mode ON_LINE_MODE 0 ON_LINE_TIMED_MODE 1 ON_LINE_AVERAGED_MODE 2 GRAB_MODE 3 SAMPLE_CELL_SP_CALIBRAT...

Page 321: ...ND_MODE 19 SAMPLE_COND_LINEARITY_MODE 20 ONLINE_TOC_LOD_LOQ_MODE 21 IC_TC_CONDUCTIVITY_ZERO_MODE 22 TOC_ZERO_MODE 23 SAMPLE_CELL_ZERO_MODE 24 UPW_SAMPLE_COND_AUTOZERO_MODE 25 SUPERIOS_RINSE_MODE 26 CELL_DIAGNOSTICS_MODE 27 ACCELERATED_RINSE_MODE 28 DRAIN_SAMPLE_SIDE_MODE 29 STARTUP_MODE 30 BACKFLUSH_MODE 31 DRAIN_DI_LOOP_MODE 32 DRAIN_SUPERIOS_MODE 33 ...

Page 322: ...86 232 Conduit power 73 Constants see System Constants Consumables replacing 274 resin cartridge 282 sample pump tubing and pump heads 280 UV lamp 278 D Data streaming 297 Data History setting up 136 138 Data outputs system components 57 Database automatic backup 169 manual archive 171 manual backup 167 manual restore 175 DI Water pump prime 311 DI water reservoir 309 filling 276 filling instructi...

Page 323: ...Microprocessor controller and electronics 57 Modbus configuring 316 enabling 315 Enabling and Configuring 165 Ethernet connection 315 testing 316 Modbus Register table 316 O Online analysis running 127 P Packing list 60 Password for Password Protection 91 184 Password Protection 90 182 183 defining password 91 184 Power installing 73 Power conduit 73 Power off 113 Prime the DI Water pump 311 Print...

Page 324: ...tings restoring 176 System Specifications 53 T Terminal Blocks connecting to 63 Theory of Operation 52 Timeout user inactivity 91 184 TOC Autozero programming 187 TOC Measurements starting and stopping analysis 127 Toolbar using 117 Troubleshooting 240 preparing the Analyzer for shipping 267 visual inspection 240 U Upgrade firmware 148 USB memory device installing 88 User inactivity timeout 91 UV ...

Page 325: ...NOTES Sievers M500e TOC Analyzer Operation and Maintenance Manual DLM 78510 02 EN Rev B 325 SUEZ 2022 ...

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