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Agilent Technologies 5975T LTM GC/MSD, Руководство по устранению неисправностей и техническому обслуживанию

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196

Troubleshooting and Maintenance Guide

12

Vacuum System

Calibration Valve and Vent Valve

Calibration valve

A calibration valve (

Figure 28

) is an electromechanical valve 

with a vial to hold the tuning compound. When a calibration 
valve is opened, tuning compound in the vial diffuses into the 
ion source. The valve is controlled by the MSD ChemStation.

EI calibration valve

The EI calibration valve is held onto the top of the analyzer 
chamber by two screws. A small O-ring provides a face seal.

Perfluorotributylamine (PFTBA) is the most commonly used 
tuning compound for EI operation. PFTBA is required for 
automatic tuning of the MSD. Other compounds can be used for 
manual tuning.

Vent valve

The vent valve knob (

Figure 29

) screws into a threaded port in 

the front of the calibration valve. An O-ring is compressed 
between the knob and the valve to form a seal. The threaded end 
of the knob has an air passage inside it, allowing air to flow into 
the manifold when the knob is partially unscrewed. If you turn 
the knob too far, the O-ring can come out of its slot.

Figure 28

Calibration valve

EI calibration valve

EI calibration vial

Vent valve knob

EI CALIBRATION
above analyzer window

Содержание 5975T LTM GC/MSD

Страница 1: ...Agilent Technologies Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide...

Страница 2: ...y and fitness for a par ticular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing use or perfor mance of this document or of a...

Страница 3: ...l Tasks Troubleshooting Tips and Tricks 28 Rule 1 Look for what has been changed 28 Rule 2 If complex isn t working go back to simple 28 Rule 3 Divide and conquer 28 Concepts 29 How to troubleshoot us...

Страница 4: ...let operating in split mode 46 For any inlet operating in splitless mode 46 Sample Decomposition in Inlet Missing Peaks 47 Peak Fronting 48 Peaks are fronting 48 Peaks have flat tops 48 Peaks have spl...

Страница 5: ...62 Inlet will not heat up 62 LTM column module will not heat up 62 Heated guard column enclosure will not heat up 63 Analyzer Error Messages 64 Difficulty in mass filter electronics 64 Difficulty with...

Страница 6: ...Shutdown Symptoms Column Shutdowns 88 Hydrogen Shutdowns 89 Thermal Shutdowns 90 7 Instrument Power On and Communication Symptoms Instrument does not turn on 92 Foreline pump is not operating 93 MSD...

Страница 7: ...m Gauge 130 To Remove the Micro Ion Vacuum Gauge 132 To Lubricate the Side Plate O Ring 133 To Lubricate the Vent Valve O Ring 135 Maintaining the Analyzer 137 To Remove the EI Ion Source 139 To Disas...

Страница 8: ...plitless Inlet 176 To Clean the Split Splitless Inlet 179 12 Vacuum System Overview 182 Vacuum System Components 183 Common Vacuum System Problems 184 Foreline Pump 185 High Vacuum Pump 189 Turbo pump...

Страница 9: ...ies 223 Side Panel Connectors 224 Interfacing to External Devices 227 15 Parts To Order Parts 230 Electronics 231 Covers 237 Local Control Panel 238 Vacuum System 240 Analyzer 248 EI GC MSD Interface...

Страница 10: ...10 Troubleshooting and Maintenance Guide...

Страница 11: ...en Safety 19 Safety and Regulatory Certifications 23 Cleaning Recycling the Product 26 Liquid Spillage 26 Moving or Storing the GC MSD 26 This manual describes the troubleshooting and maintenance of t...

Страница 12: ...1 cm high 60 cm wide and 54 cm deep The weight is 46 5 kg for the mainframe The attached foreline roughing pump weighs an additional 15 kg standard pump for wet and 4 5 kg for dry The basic components...

Страница 13: ...features Model G3880A Feature High vacuum pump Standard turbo Optimal He column flow mL min 1 2 Maximum recommended gas flow mL min Total gas flow into the MSD column flow 2 0 Maximum gas flow mL min...

Страница 14: ...system Electron Ionization EI systems EI systems ionize sample molecules by bombarding them with electrons The ions including fragments are drawn into the quadrupole analyzer where they are separated...

Страница 15: ...P Direct insertion probe EI Electron impact ionization EM Electron multiplier detector EMV Electron multiplier voltage EPC Electronic pneumatic control eV Electron volt GC Gas chromatograph HED High e...

Страница 16: ...Troubleshooting and Maintenance Guide 1 Introduction RFPA Radio frequency power amplifier Torr Unit of pressure 1 mm Hg Turbo Turbomolecular pump Table 2 Abbreviations continued Abbreviatio n Definiti...

Страница 17: ...trostatic discharge is a threat to GC MSD electronics The printed circuit boards in the GC MSD can be damaged by electrostatic discharge Do not touch any of the boards unless it is absolutely necessar...

Страница 18: ...d similar absorbents in the oil pan could ignite and damage the pump and other parts of the MSD WARNING The insulation around the inlets detectors valve box and the insulation cups is made of refracto...

Страница 19: ...der bright light WARNING The use of hydrogen as a carrier gas is potentially dangerous WARNING When using hydrogen H2 as the carrier gas or fuel gas be aware that hydrogen gas can flow into the guard...

Страница 20: ...which hydrogen can accumulate Table 3 and know what precautions to take if they know or suspect that hydrogen has accumulated Note that these mechanisms apply to all mass spectrometers including the G...

Страница 21: ...e operator can close the shutoff valves Closing the shutoff valves does not shut off the flow of carrier gas As a result hydrogen may slowly accumulate in the mass spectrometer Table 3 Hydrogen accumu...

Страница 22: ...MSD are closed do not heat the capillary column without carrier gas flow Turn off the hydrogen at its source if a power failure occurs If a power failure occurs while the GC MSD system is unattended...

Страница 23: ...D is designed and manufactured under a quality system registered to ISO 9001 Information The Agilent Technologies 5975T LTM GC MSD meets the following IEC International Electro technical Commission cl...

Страница 24: ...intended use of the instrument Agilent Technologies assumes no liability for the customer s failure to comply with these requirements See accompanying instructions for more information Indicates a ho...

Страница 25: ...s 1 Relocate the radio or antenna 2 Move the device away from the radio or television 3 Plug the device into a different electrical outlet so that the device and the radio or television are on separat...

Страница 26: ...Spillage Do not spill liquids on the instrument Moving or Storing the GC MSD The best way to keep your GC MSD functioning properly is to keep it pumped down and hot with carrier gas flow If you plan t...

Страница 27: ...or more possible causes are listed In general the causes listed first are the most likely causes or the easiest to check and correct If the material in this chapter and in the online help proves insuf...

Страница 28: ...rrect gas If the LTM column was just replaced suspect air leaks or contaminated or bleeding column Rule 2 If complex isn t working go back to simple A complex task is not only more difficult to perfor...

Страница 29: ...evelopment of new methods Proceed with troubleshooting under the assumption that method s are working properly This manual also includes common troubleshooting tasks as well as information needed prio...

Страница 30: ...the instrument after altering a column causes incorrect flows changed or incorrect split ratios retention time changes and peak shifts Automatic Liquid Sampler configuration Keep the Automatic Liquid...

Страница 31: ...red sample supply gas type gas flow rates detectors inlets installed and so forth Any messages that appear on the display Results of any troubleshooting tests you have run Instrument details Obtain th...

Страница 32: ...32 Troubleshooting and Maintenance Guide 2 Concepts and General Tasks...

Страница 33: ...iler Peaks Present High Boiler Peaks are Missing 41 Baseline Rise During LTM Column Temperature Program 42 Poor Peak Resolution 44 Peak Tailing 45 Peak Boiling Point or Molecular Weight Discrimination...

Страница 34: ...al these symptoms do not prevent you from operating your GC MSD system They indicate however that the data you are acquiring may not be the best data obtainable These symptoms can be caused by instrum...

Страница 35: ...e Checking for Leaks on page 99 Check for sufficient carrier gas supply pressure The pressure delivered to the instrument must be at least 40 kPa 10 psi greater than the maximum inlet pressure require...

Страница 36: ...umn connection See Checking for Leaks on page 99 Check sample level in vials Run replicates of known standards to verify the problem Consider if this is the first run Has the instrument stabilized Poo...

Страница 37: ...e causes all inlet and detector combinations Check the septum type and installation Perform complete inlet maintenance Replace all consumable parts and bake out the inlet Perform column maintenance Ba...

Страница 38: ...ensions See Configurable Items to Always Keep Current on page 30 Check the autosampler injection volume Check the vial caps Check configured syringe size Some syringe sizes are specified at half capac...

Страница 39: ...tenance Check for leaks See Checking for Leaks on page 99 No peaks If an analysis shows no chromatographic peaks only a flat baseline or minor noise run one of the automated tune programs If the MSD p...

Страница 40: ...foreline or analyzer chamber pressure Very dirty ion source Calibration valve is not working correctly Bad signal cable connection Filament has failed or is not connected correctly Bad ion source wir...

Страница 41: ...romatographic Symptoms 3 Troubleshooting and Maintenance Guide 41 Low Boiler Peaks Present High Boiler Peaks are Missing Cold spot at the point where the LTM transfer line touches the LTM column toroi...

Страница 42: ...nt Check for contamination See Contamination or Carryover on page 37 Consider the effect of column film thickness on bleed Check for leaks at the column fittings See Checking for Leaks on page 99 Prep...

Страница 43: ...is not properly swept resulting in excess solvent on the column and slow solvent decay Baseline wanders Insufficient carrier gas supply pressure Malfunctioning flow or pressure regulator Intermittent...

Страница 44: ...to optimum linear velocity Install and use deactivated consumable parts in the inlet for example a liner Perform column maintenance Bake out contaminants replace the inlet guard column and reverse an...

Страница 45: ...Consider the type of adapter liner and inlet seal being used One or all of these may be contaminated or active Check adapters if installed and liner for solid particles For splitless injection consid...

Страница 46: ...method to determine expected performance For any inlet operating in split mode Check liner type Increase the inlet temperature and verify that the insulation cup is installed and contains insulation C...

Страница 47: ...onality of traps Verify that the liner is appropriate for the sample being run Perform complete inlet maintenance Replace all consumable parts and bake out the inlet Install a deactivated liner Check...

Страница 48: ...being used If using capillary splitless injection consider the compound solubility in the injection solvent Try changing the solvent Check purity of sample solvent Peaks are fronting Column film thick...

Страница 49: ...Chromatographic Symptoms 3 Troubleshooting and Maintenance Guide 49 Peaks have split tops Bad injection technique Injection is too large...

Страница 50: ...short and long are relative to the width of the chromatographic peaks Noisy baseline A noisy baseline or high detector output can indicate leaks contamination or electrical problems Some noise is inev...

Страница 51: ...the new conditions before it starts a run some baseline changes are to be expected If experiencing baseline wander check for leaks especially at the septum and at the column See Checking for Leaks on...

Страница 52: ...ing may disappear at the same time Check for a contaminated ion source Check for the correct jet Retention times for all peaks drift shorter Column has been shortened Initial column temperature was in...

Страница 53: ...terface ion source or mass filter Incorrect sample concentration Leaking GC inlet Dirty GC inlet Incorrect split ratio Purge off time in splitless mode is too short Excessive pressure in the MSD Dirty...

Страница 54: ...column type is correct Perform column maintenance Bake out contaminants replace the inlet guard column and reverse and bake out the column as needed Verify that the liner type is appropriate for the...

Страница 55: ...ity is poor also apply to mass spectra No peaks Ion source cables not connected Bad connections to or from the detector HED power supply output cable has failed Other electronics failure Isotopes are...

Страница 56: ...g may be responsible Repeller voltage is too high Peaks are too wide Incorrect DC polarity on the quadrupole mass filter Dirty quadrupole mass filter Peak widths are inconsistent MSD has not had enoug...

Страница 57: ...as a different relative abundance target 3 only applies to Autotune Not enough time for the MSD to warm up and pump down Analyzer chamber pressure is too high Ion source temperature is too high Column...

Страница 58: ...ptoms Repeller voltage is too low Not enough time for the MSD to warm up and pump down Analyzer chamber pressure is too high Column carrier gas flow is too high Poor filament operation Dirty ion sourc...

Страница 59: ...lyzer chamber pressures can only be measured if your system is equipped with the optional gauge controller Foreline pressure is too high If the pressure you observe for a given column flow has increas...

Страница 60: ...for the following Column carrier gas flow is too low Column plugged or crushed by overtightened nut Empty or insufficient carrier gas supply Bent or pinched carrier gas tubing These could create a fa...

Страница 61: ...enough time to reach temperature setpoint Ion source heater cartridge is not connected Ion source temperature sensor is not connected Ion source heater failed burned out or shorted to ground Ion sourc...

Страница 62: ...working correctly These will cause a GC error message GC error messages are described in the documentation supplied with your GC Inlet will not heat up Incorrect setpoint Setpoint entered in wrong hea...

Страница 63: ...correctly Heated guard column enclosure will not heat up Incorrect setpoint Setpoint entered in wrong heated zone Enclosure has not had enough time to reach temperature setpoint Enclosure heater not...

Страница 64: ...ilter quad contacts are shorted or otherwise not working correctly Mass filter is not working correctly MSD electronics are not working correctly Difficulty with the electron multiplier supply Large p...

Страница 65: ...ck on to remove this error message Be sure the turbo pump has slowed down before switching off the MSD The message will reappear if the underlying problem has not been corrected Turbo pump Large vacuu...

Страница 66: ...plier voltage is too low Signal cable is not connected Electrical leads to the detector are not connected correctly HED power supply output cable failed Electrical leads to the ion source are not conn...

Страница 67: ...e 5 minutes to reach 80 of its normal operating speed Turbo pump is not working correctly MSD electronics are not working correctly The system is in standby This message is triggered by a shutdown sig...

Страница 68: ...ilament has failed try the other filament MSD electronics are not working correctly There is not enough signal to begin tune Corrupted tune file Poor mass axis calibration Amu gain or offset is too hi...

Страница 69: ...and 44 or m z 14 and 16 Poor sensitivity Low relative abundance of m z 502 this varies with the tune program used Leaks can occur in either the GC or the MSD The most likely point for an air leak is...

Страница 70: ...r gas tubing Fingerprints improper handling of clean parts Contamination originating in the MSD typically comes from one of the following sources Air leak Cleaning solvents and materials Foreline pump...

Страница 71: ...ump oil or PFTBA Foreline pump oil vapor or calibration valve leak 73 147 207 221 281 295 355 429 Dimethylpolysiloxane Septum bleed or methyl silicone column bleed 149 Plasticizer phthalates Vacuum se...

Страница 72: ...72 Troubleshooting and Maintenance Guide 3 Chromatographic Symptoms...

Страница 73: ...Not Reach Setpoint Pressure or Flow 78 A Gas Exceeds Pressure Setpoint or Flow 79 The Inlet Pressure or Flow Fluctuates 80 Cannot Maintain a Pressure as Low as the Setpoint on a Split Inlet 81 The Me...

Страница 74: ...a component key for example Front inlet to see which setpoints or conditions are not ready Check for a sampler problem Check for a data system problem If performing manual injections in splitless or g...

Страница 75: ...fficient delivery pressure Check the restrictors installed in the Aux EPC module See Restrictors in the Advanced User Guide Check the configured gas type The configured gas type must match the actual...

Страница 76: ...ered ready a temperature must be at setpoint 1 C for 30 s If a temperature never becomes ready do the following Check for a missing insulation cup on an inlet Check for a very large temperature differ...

Страница 77: ...Set a Flow or Pressure If you cannot set a flow or pressure using the split splitless inlet do the following Check the column mode Check that a capillary column is configured to the correct inlet Che...

Страница 78: ...o the following Check for sufficient gas supply delivery pressure The pressure at the supply should be at least 10 psi greater than the desired setpoint Check for leaks See Chapter 8 Checking for Leak...

Страница 79: ...ce Guide 79 A Gas Exceeds Pressure Setpoint or Flow If a gas exceeds its pressure or flow setpoint do the following Decrease the split ratio Replace the split vent filter Verify that the correct liner...

Страница 80: ...s purifier or gas generator is operating at or near capacity Check the supply gas for sufficient delivery pressure Verify that the supply pressure regulator is functioning properly Check for leaks See...

Страница 81: ...tpoint on a Split Inlet If the instrument cannot maintain a pressure as low as the setpoint check for the following Consider using a liner designed for split analysis Check for a plugged liner Check f...

Страница 82: ...ch the calculated flow displayed on the GC do the following Verify that the measured flows are corrected to 25 C and 1 atmosphere Verify that the correct column dimensions are configured accurately in...

Страница 83: ...83 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 5 ALS Symptoms Plunger Errors 84 Syringe Needle Bends During Injection into Inlet 85...

Страница 84: ...4 Troubleshooting and Maintenance Guide 5 ALS Symptoms Plunger Errors If the 7693 ALS reports a plunger error see if the syringe plunger is sticking or is not securely connected to the plunger carrier...

Страница 85: ...is not too tight Check that the syringe is installed correctly into the syringe carriage Check that the needle support and guide are clean Remove any residue or septum deposits Check that you are usi...

Страница 86: ...86 Troubleshooting and Maintenance Guide 5 ALS Symptoms...

Страница 87: ...87 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 6 Shutdown Symptoms Column Shutdowns 88 Hydrogen Shutdowns 89 Thermal Shutdowns 90...

Страница 88: ...LTM column temperature setpoint Off Turns off all flows for the column When viewed their parameters flash Off For example the septum purge and column flows would turn off Turns off all other heaters W...

Страница 89: ...closes and turns off both pressure and flow controls When viewed these parameters will flash Off Opens the split vent valve in the inlet Turns off the LTM column heaters Turns off the inlet guard col...

Страница 90: ...r another heated zone is not within its allowable temperature range lower than minimum temperature or higher than maximum temperature To recover from this state 1 Fix the cause of the shutdown Check f...

Страница 91: ...wer On and Communication Symptoms Instrument does not turn on 92 Foreline pump is not operating 93 MSD turns on but then the foreline pump shuts off 94 Local control panel says No server found 95 Inst...

Страница 92: ...Nothing happens when the instrument is switched on The foreline pump does not start The cooling fan for the high vacuum pump does not turn on The local control panel is not on Disconnected power cord...

Страница 93: ...ing power the fan is operating and the local control panel is lit but the foreline pump is not operating Large air leak usually the analyzer door open has caused pumpdown failure You must power cycle...

Страница 94: ...pump and the high vacuum pump if the system fails to pump down correctly This is usually because of a large air leak either the sideplate has not sealed correctly or the vent valve is still open This...

Страница 95: ...ng and Maintenance Guide 95 Local control panel says No server found Disconnected LAN cable between MSD and the switch or the switch and the PC PC is turned off Holding the No Cancel key down for 5 se...

Страница 96: ...trument Turns On Then Stops During Startup During Self Test If the instrument turns on but the normal display does not appear 1 Turn the power switch Off Wait one minute then turn the power On 2 If th...

Страница 97: ...ng followed by an IP address For example if the IP address is 10 1 1 101 enter ping 10 1 1 101 If LAN communications are working properly you will see a successful reply For example If the ping test i...

Страница 98: ...98 Troubleshooting and Maintenance Guide 7 Instrument Power On and Communication Symptoms...

Страница 99: ...T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 8 Checking for Leaks Leak Check Tips 100 To Check for External Leaks 101 To Check for Instrument Leaks 103 Leaks in Capillary Fl...

Страница 100: ...in 9 16 in and 1 4 in wrenches for tightening Swagelok and column fittings 2 Check any potential leak points associated with any maintenance recently performed 3 Check instrument capillary fittings a...

Страница 101: ...these connections Gas supply bulkhead fittings Gas cylinder fitting Regulator fittings Traps Shut off valves T fittings Perform a pressure drop test 1 Turn off the instrument 2 Set the regulator pres...

Страница 102: ...and Maintenance Guide 8 Checking for Leaks 4 Wait 5 min If there is a measurable drop in pressure there is a leak in the external connections No drop in pressure indicates that the external connectio...

Страница 103: ...ks Check for leaks at these connections Inlet septum septum head liner split vent trap split vent trap line and purge vent fittings LTM column connections to inlets GC MSD transfer line and unions Fit...

Страница 104: ...loose do not tighten it further Instead remove the connection trim the column end and install it again See To Attach a Capillary Column Using SilTite Metal Fittings on page 114 Also inspect the plate...

Страница 105: ...105 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 9 Troubleshooting Tasks To Measure a Split Vent or Septum Purge Flow 106...

Страница 106: ...d split vent flows exit through the pneumatic module at the top rear of the instrument See Figure 4 To measure split vent or septum purge flows attach the flowmeter to the appropriate tube WARNING Hyd...

Страница 107: ...ate and use a 1 8 in tub adapter as shown above to covert the 1 8 in threaded fitting into a 1 8 tube This prevents the rubber flowmeter tubing from leaking around the threads which will result in lea...

Страница 108: ...108 Troubleshooting and Maintenance Guide 9 Troubleshooting Tasks...

Страница 109: ...alve Assembly 129 To Install a Micro Ion Vacuum Gauge 130 To Remove the Micro Ion Vacuum Gauge 132 To Lubricate the Side Plate O Ring 133 To Lubricate the Vent Valve O Ring 135 Maintaining the Analyze...

Страница 110: ...tion and to take corrective action Table 5 Maintenance schedule Task Every week Every 6 months Every year As needed Vacuum System Check the foreline pump oil level X Replace the foreline pump oil X Ch...

Страница 111: ...bles between these boards Wires and cables between these boards and the connectors on the side panel of the instrument Some connectors on the side panel for example the foreline power receptacle Norma...

Страница 112: ...il droplets It does not trap any other chemicals If you are using toxic solvents or analyzing toxic chemicals do not use this oil trap For all foreline pumps install a hose to take the exhaust from th...

Страница 113: ...n or near printed circuit boards or when you work on components with wires contacts or cables connected to printed circuit boards always use a grounded antistatic wrist strap and take other antistatic...

Страница 114: ...wrench Column cutting tool 5181 8836 Internal nut G2855 20530 Lint free gloves 2 Pass the tubing end through the internal nut and SilTite ferrule leaving approximately 1 cm of fused silica tubing pro...

Страница 115: ...of the nuts by turning 45 to 60 degrees of rotation but no more than 60 degrees one flat 4 Remove the swaging nut 5 Using a wafer column cutter trim the tubing at the small end of the ferrule leaving...

Страница 116: ...116 Troubleshooting and Maintenance Guide 10 General Maintenance 6 Insert the assembled ferrule and nut into the SilTite fitting Tighten with a wrench by only 15 to 20 degrees of rotation...

Страница 117: ...Tite Fitting Loosen and remove the internal nut If tubing and ferrule do not come free insert a pointed object pen paper clip into the ferrule release hole and press firmly You will hear a click as th...

Страница 118: ...ecking the dry foreline pump diaphragms typically every 3 years Failure to perform these tasks as scheduled can result in decreased instrument performance It can also result in damage to your instrume...

Страница 119: ...lower line follow steps 2 through 6 to add foreline pump oil If your instrument is nearing its scheduled time for replacement of the foreline pump oil replace the oil instead of adding oil If the oil...

Страница 120: ...120 Troubleshooting and Maintenance Guide 10 General Maintenance Figure 5 Foreline pump standard pump shown without safety cage Fill cap Oil level lines Drain plug Oil mist filter...

Страница 121: ...b bench next to the GC MSD 3 Place a book or other object under the pump motor to tilt it up slightly Remove the fill cap See Figure 5 4 Place a container under the drain plug 5 Remove the drain plug...

Страница 122: ...object from under the pump motor 4 Add foreline pump oil until the oil level in the window is near but not above the upper line The foreline pump requires approximately 0 28 L of oil 5 Wait a few min...

Страница 123: ...om the outboard housing and take it axially off the frame 6 Remove the worn tip seals and discard 7 If compressed air is available blow any remaining tip seal debris from the scroll parts If seal debr...

Страница 124: ...14 Reconnect the electrical connector at the front cowling 15 Replace the front cowling and the four M5 bolts that hold it in place See Figure 6 16 Reconnect the pump to electrical power 17 Repositio...

Страница 125: ...Execute menu 3 Remove the analyzer window cover 4 Loosen the calibration vial collar Figure 7 Do not remove the collar 5 Pull the calibration vial out You may feel some resistance due to residual vacu...

Страница 126: ...ight Do not use a tool to tighten the collar It does not require that much force 10 Reinstall the analyzer window cover 11 Select Purge Calibrant Valve from the Vacuum menu in the Tune and Vacuum Cont...

Страница 127: ...nd valve 1 If the vacuum gauge controller is on turn it off 2 In Tune and Vacuum Control view select Purge Calibrant Valve under the Vacuum menu This will open the CI calibration valve for several min...

Страница 128: ...nect it 3 Loosen the collar and remove the calibration vial Figure 7 Just loosen the collar do not remove it 4 Remove the two screws holding the valve assembly to the top of the analyzer chamber Do no...

Страница 129: ...s in place If it is worn or damaged replace it 3 Install the calibration and vent valve assembly and tighten the screws that hold it in place 4 Reconnect the calibration valve cable to the connector n...

Страница 130: ...the MSD See Figure 8 4 Detach the provided KF 16 clamp from the analyzer chamber flange 5 Place the KF16 O ring in the groove on the analyzer chamber flange Replace it if it is worn or damaged 6 Hold...

Страница 131: ...General Maintenance 10 Troubleshooting and Maintenance Guide 131 Figure 8 Removing MSD rear cover Rear MSD cover Captive screws...

Страница 132: ...f the Micro Ion vacuum gauge 4 Unscrew the large thumbnut on the gauge clamp 5 Remove the long screw from the clamp 6 While supporting the gauge body remove the clamp from the mounting flange 7 Remove...

Страница 133: ...hamber See the 5975T LTM GC MSD Operation Manual 3 Remove the analyzer by disconnecting the source wiring and loosening the sideboard from the hinge See the 5975T LTM GC MSD Operation Manual 4 Use a c...

Страница 134: ...134 Troubleshooting and Maintenance Guide 10 General Maintenance 6 Close the analyzer chamber 7 Pump down the MSD Figure 9 Side plate O ring Side plate O ring...

Страница 135: ...e Procedure 1 Vent the instrument 2 Completely remove the vent valve knob Figure 10 3 Inspect the O ring If the O ring appears damaged replace it 4 Use a clean lint free cloth or glove to spread a thi...

Страница 136: ...vent valve knob 7 Pump down the instrument Figure 10 Vent valve O ring Vent valve knob Vent valve O ring CAUTION Be very careful when reinstalling the vent valve knob It is possible to cross thread th...

Страница 137: ...moving parts from the analyzer During analyzer maintenance procedures take care to avoid contaminating the analyzer or interior of the analyzer chamber Wear clean gloves during all analyzer maintenanc...

Страница 138: ...tive The HED ceramic insulator must never be touched More information is available If you need more information about the locations or functions of analyzer components refer to Chapter 13 Analyzer on...

Страница 139: ...analyzer components 4 Disconnect the seven wires from the ion source Do not bend the wires any more than necessary Figure 11 and Table 7 5 Trace the wires for the ion source heater and temperature se...

Страница 140: ...aintenance WARNING The analyzer operates at high temperatures Do not touch any part until you are sure it is cool Figure 11 Removing the ion source Source feedthrough board Ion source Thumbscrews Sour...

Страница 141: ...he ion source See the To Remove the EI Ion Source on page 139 2 Remove the filaments Figure 12 3 Separate the repeller assembly from the source body The repeller assembly includes the source heater as...

Страница 142: ...gure 12 Disassembling the EI ion source Source body Filament Setscrew Interface socket Repeller Repeller insulator Source heater assembly Repeller insulator Washer Repeller nut Ion focus lens Drawout...

Страница 143: ...thylene chloride reagent grade Ultrasonic bath Preparation 1 Disassemble the ion source See page 141 2 Collect the following parts to be cleaned Figure 13 Repeller Interface socket Source body Drawout...

Страница 144: ...nalyzer seriously consider replacing the contaminated parts Figure 13 Source parts to be cleaned Source body Repeller Interface socket Drawout plate Drawout cylinder Ion focus lens Entrance lens CAUTI...

Страница 145: ...ible particles rinse again 6 Separate the parts that were abrasively cleaned from the parts that were not abrasively cleaned 7 Ultrasonically clean the parts each group separately for 15 minutes in ea...

Страница 146: ...e source body 4 Install the setscrew that holds the lenses in place 5 Reinstall the repeller repeller insulators washer and repeller nut into the source heater assembly The resulting assembly is calle...

Страница 147: ...4 Assembling the ion source Interface socket Source body Setscrew Repeller Repeller insulator Filament 1 of 2 Source heater assembly Repeller insulator Washer Repeller nut do not over tighten Ion focu...

Страница 148: ...029 Pliers long nose 8710 1094 Procedure 1 Slide the ion source into the source radiator Figure 15 2 Install and hand tighten the source thumbscrews Do not overtighten the thumbscrews 3 Connect the io...

Страница 149: ...1 5 mm 8710 1570 Procedure 1 Vent the MSD 2 Open the analyzer chamber 3 Remove the ion source See the To Remove the EI Ion Source on page 139 4 Remove the filament s to be replaced Figure 16 Figure 1...

Страница 150: ...150 Troubleshooting and Maintenance Guide 10 General Maintenance Figure 16 Replacing filaments Filament 1 Filament 2...

Страница 151: ...ce body 5 Replace the screw to the ion source body 6 After installing the filament verify that it is not grounded to source body 7 Reinstall the ion source See the To Reinstall the EI Ion Source on pa...

Страница 152: ...the MSD 2 Open the analyzer chamber 3 Remove the ion source from the source radiator See the To Remove the EI Ion Source on page 139 4 Remove the filaments 5 Remove the repeller assembly Figure 17 The...

Страница 153: ...aintenance 10 Troubleshooting and Maintenance Guide 153 Figure 17 Replacing the heater and sensor Source body Repeller Repeller insulator Filament Filament Repeller nut washer insulator Source heater...

Страница 154: ...tall the repeller repeller insulators washer and repeller nut Figure 17 The resulting assembly is called the repeller assembly 3 Connect the repeller assembly to the source body 4 Reinstall the filame...

Страница 155: ...9 Hex ball driver 1 5 mm 8710 1570 Hex ball driver 2 0 mm 8710 1804 Procedure 1 Vent the instrument 2 Open the analyzer chamber 3 Disconnect the mass filter heater and temperature sensor wires from th...

Страница 156: ...ass filter heater assembly G1099 60172 Procedure 1 Unpack the new mass filter heater assembly Figure 18 The heater temperature sensor and heater block are already assembled 2 Install the heater assemb...

Страница 157: ...General Maintenance 10 Troubleshooting and Maintenance Guide 157 Figure 18 Mass filter heater and sensor Mass filter radiator Heater sensor assembly...

Страница 158: ...he retaining clip Figure 19 Lift the arm of the clip up and then swing the clip away from the electron multiplier horn 4 Remove the electron multiplier horn 5 Install the new electron multiplier horn...

Страница 159: ...General Maintenance 10 Troubleshooting and Maintenance Guide 159 8 Pump down the MSD Figure 19 Replacing the electron multiplier horn Electron multiplier horn Retaining clip...

Страница 160: ...onduct ESD to the printed circuit boards to which they are connected This is especially true of the mass filter quadrupole contact wires which can carry ESD to sensitive components on the side board E...

Страница 161: ...he functions of electronic components refer to Chapter 14 Electronics on page 215 Most of the procedures in this chapter are illustrated with video clips CAUTION In order to be effective an antistatic...

Страница 162: ...ly affect coil adjustment 4 In the Tune and Vacuum Control view select Optimize Quadropole Frequency from the Execute menu 5 Enter an m z value of 100 6 Slowly turn the quad frequency adjustment screw...

Страница 163: ...h 7 for m z 650 The minimum voltage is typically between 300 and 340 mV 9 Exit the Set Optimize Quadrupole Frequency program 10 Select MS OFF from the Execute menu 11 Close the analyzer cover 12 Tune...

Страница 164: ...ll already be off but for safety you should switch off the instrument and unplug the power cord It is not necessary to allow air into the analyzer chamber 2 Turn one of the fuse holders Figure 21 coun...

Страница 165: ...Maintenance Guide 165 6 Repeat steps 3 through 6 for the other fuse Always replace both fuses 7 Reconnect the instrument power cord to the electrical outlet 8 Pump down the MSD Figure 21 Primary fuses...

Страница 166: ...166 Troubleshooting and Maintenance Guide 10 General Maintenance...

Страница 167: ...rts for the Split Splitless Inlet 168 Exploded Parts View of the Split Splitless Inlet 171 To Clean the Septum Seat in the Insert Assembly of the Split Splitless Inlet 172 To Replace the Gold Seal on...

Страница 168: ...800 L Yes 5181 3315 Splitless Direct inject 2 mm id quartz 250 L No 18740 80220 Splitless Direct inject 2 mm id 250 L Yes 5181 8818 Direct inject Headspace or purge and trap 1 5 mm id 140 L No 18740...

Страница 169: ...olumn blanking nut Testing use with any ferrule 5020 8294 Column nut universal Connect column to inlet or detector 5181 8830 2 pk Column cutter ceramic wafer Cutting capillary columns 5181 8836 4 pk T...

Страница 170: ...ncludes SS washer 5182 9652 Stainless steel washer 0 375 inch od 12 pk 5061 5869 Reducing nut 18740 20800 Column nut blanking plug 5020 8294 Capillary inlet preventative maintenance kit split 5188 649...

Страница 171: ...ntenance Guide 171 Exploded Parts View of the Split Splitless Inlet Column nut Ferrule Reducing nut Washer Inlet gold seal Retaining nut Septum Septum retainer nut Split splitless inlet body Liner Spl...

Страница 172: ...onal Tweezers Compressed filtered dry air or nitrogen Wrench capillary inlet optional 2 Load the maintenance method see the 5975T LTM GC MSD Operation Manual and wait for the GC to become ready 3 Slid...

Страница 173: ...ompressed air or nitrogen to blow away the pieces of steel wool and septum 8 Line up the tab on the bottom of the septum assembly with the slot on the insert assembly and push down to connect Slide th...

Страница 174: ...Replacement washer 1 4 inch wrench for column 1 2 inch wrench Lint free gloves 2 Load the maintenance method and wait for the GC to become ready 3 Open the Guard Column enclosure door 4 Remove the in...

Страница 175: ...place the new gold seal on top of it raised portion facing down 7 Replace the reducing nut and tighten securely with a wrench 8 Install the inlet guard column 9 Bakeout contaminants See the 5975T LTM...

Страница 176: ...become ready 3 Remove the pneumatics cover on the top of the instrument 4 Loosen the screws on the retaining clip WARNING Be careful The oven and or inlet may be hot enough to cause burns If either i...

Страница 177: ...eldment on the filter trap assembly Be careful not to stress the tubing between the split vent valve and the trap 7 Remove the old filter cartridge and two O rings 8 Verify the new O rings are seated...

Страница 178: ...nce Guide 11 Maintaining the Split Splitless Inlet 12 Fully tighten the split vent front weldment onto the trap 13 Check for leaks 14 Restore the analytical method 15 Reset the split vent trap counter...

Страница 179: ...aintenance method and wait for the GC to become ready 3 Remove the inlet liner 4 Disconnect the column from the inlet 5 Remove the reducing nut and gold seal See To Replace the Gold Seal on the Split...

Страница 180: ...tall the gold seal and reducing nut 11 Install the liner and O ring 12 Install the column See the 5975T LTM GC MSD Operation Manual 13 Check for leaks 14 Bakeout contaminants See 5975T LTM GC MSD Oper...

Страница 181: ...ew 182 Vacuum System Components 183 Common Vacuum System Problems 184 Foreline Pump 185 High Vacuum Pump 189 Analyzer Chamber 190 Side Plate 191 Vacuum Seals 193 Turbo Pump and Fan 195 Calibration Val...

Страница 182: ...rument uses two vacuum pumps to obtain the vacuum levels needed One of two types of foreline pumps standard or dry creates a low vacuum then a high vacuum standard turbomolecular turbo pump engages to...

Страница 183: ...door and front and rear end plates Vacuum seals Calibration valve s and vent valve Vacuum control electronics Vacuum gauges and gauge control electronics Each of these is discussed in more detail in t...

Страница 184: ...you turn on the instrument power Continue to press until the sound from the foreline pump becomes quieter Pumpdown failure shutdown The system will shut down both the high vacuum and the foreline pump...

Страница 185: ...Pump The foreline pump Figure 24 reduces the pressure in the analyzer chamber so the high vacuum pump can operate It also pumps away the gas load from the high vacuum pump The foreline pump is connect...

Страница 186: ...Hose to vacuum pump Ballast control Fill cap Exhaust outlet Oil drip tray Power switch Oil level window with oil mist filter Drain plug on front Standard pump shown without safety cage Dry pump shown...

Страница 187: ...tall an 11 mm id hose to remove the exhaust from your lab A window sight glass in the front of the standard foreline pump shows the level of the foreline pump oil There are two marks next to the windo...

Страница 188: ...r towels and similar absorbents in the oil pan could ignite and damage the pump and other parts of the MSD WARNING Combustible materials or flammable non flammable wicking material placed under over o...

Страница 189: ...ntenance Guide 189 High Vacuum Pump Turbo pump system The 5975T LTM GC MSD has a turbo pump with a screen to keep debris out of the pump but no baffle is necessary Pump speed is controlled by the turb...

Страница 190: ...ings provide the seals between the plates and the manifold Ports in the manifold and the plates provide attachment points for the Micro Ion vacuum gauge calibration valve vent valve GC MSD interface a...

Страница 191: ...oughs to analyzer components The electronic side board is mounted on the atmospheric side of the side plate Thumbscrews are located at each end of the side plate CAUTION Fasten both side plate thumbsc...

Страница 192: ...Maintenance Guide 12 Vacuum System Figure 26 Side plate feedthroughs High voltage HED Detector focus Ion source and heater Mass filter quadrupole Screws for radiator mounting brackets Signal detector...

Страница 193: ...ings into place against the side plate O ring and must be held in place when the MSD is turned on for pump down to assure a good seal The front and rear end plates are screwed onto the manifold and sh...

Страница 194: ...ar Tightening the collar presses the ferrule compressing the O ring around the part The calibration vials use compression seals High voltage feedthrough seal The high voltage HED feedthrough seal is a...

Страница 195: ...olecules that reach the outlet A controller regulates current to the pump and monitors pump motor speed and temperature A cooling fan is located between the turbo pump and the front panel of the MSD T...

Страница 196: ...eal Perfluorotributylamine PFTBA is the most commonly used tuning compound for EI operation PFTBA is required for automatic tuning of the MSD Other compounds can be used for manual tuning Vent valve T...

Страница 197: ...Vacuum System 12 Troubleshooting and Maintenance Guide 197 Figure 29 Vent valve Vent valve knob O ring Air passage Valve closed Valve open Valve open too far...

Страница 198: ...not ionize as readily as nitrogen Therefore the indicated pressure for helium is approximately six times lower than the absolute pressure For example a reading of 2 0 10 5 Torr versus an absolute pres...

Страница 199: ...d Maintenance Guide Agilent Technologies 13 Analyzer Overview 200 EI Ion Source 202 Filaments 203 Other Source Elements 205 Quadrupole Mass Filter 207 Detector 210 Analyzer Heaters and Radiators 212 T...

Страница 200: ...s selected ions to pass through the filter and strike the detector The detector generates a signal current proportional to the number of ions striking it The analyzer is attached to the vacuum side of...

Страница 201: ...bleshooting and Maintenance Guide 201 Figure 30 The analyzer Detector Mass filter contact cable Mass filter heater assembly Feedthrough board Mass filter contact Ion source inside radiator Mass filter...

Страница 202: ...where they pass through several electrostatic lenses These lenses concentrate the ions into a tight beam which is directed into the mass filter Ion source body The ion source body Figure 31 is a cylin...

Страница 203: ...ment will give better performance than the other To select the better of the two filaments run two autotunes one with each filament Use the filament that gives the best results Emission current The fi...

Страница 204: ...acquisition parameters set the solvent delay so that the analyzer will not turn on while the solvent peak is eluting When the software prompts Override solvent delay at the beginning of a run always s...

Страница 205: ...voltage too low results in poor sensitivity and poor high mass response Setting repeller voltage too high results in precursors poor mass filtering and poor low mass resolution Drawout plate and cylin...

Страница 206: ...the 4 4 volt permanent offset Entrance lens voltage 4 4 VDC offset gain mass Entrance lens offset The entrance lens offset EntOff controls the fixed voltage applied to the entrance lens It can be vari...

Страница 207: ...gments are electrically isolated One pair has positive voltages applied the other negative A combined direct current DC and radio frequency RF signal is applied to the two pairs of segments The magnit...

Страница 208: ...ged If you are tuning with a compound other than PFTBA there may not be an ion at m z 219 In that case set the 219 width to the last value found for it by Autotune or set it to 0 DC polarity The DC po...

Страница 209: ...e radiator If absolutely necessary that is if the only alternative is replacement the quadrupole can be cleaned Cleaning must be performed by Agilent Technologies service personnel CAUTION Never put t...

Страница 210: ...he HED electrons are emitted These electrons are attracted to the more positive EM horn Do not touch the insulator EM horn The EM horn carries a voltage of up to 3000 volts at its opening and 0 volts...

Страница 211: ...nstrument Control view to see the tune charts Sudden changes usually indicate a different type of problem See Also Troubleshooting in the online help for more information about symptoms that may indic...

Страница 212: ...he MSD ChemStation In selecting the temperatures to use consider the following Higher temperatures help keep the analyzer clean longer Higher ion source temperatures result in more fragmentation and t...

Страница 213: ...Analyzer 13 Troubleshooting and Maintenance Guide 213 Figure 34 Heaters and radiators Mass filter radiator Mass filter heater assembly Ion source radiator Ion source heater assembly...

Страница 214: ...214 Troubleshooting and Maintenance Guide 13 Analyzer...

Страница 215: ...27 The following assemblies make up the MSD electronics Except for the Side panel and connectors Local Control Panel and power switch and Interfacing to other devices sections most of this material is...

Страница 216: ...Maintenance Guide 14 Electronics Figure 35 MSD electronics module MSD LAN MS Log amplifier Main board for MSD Cooling fan Low voltage MSD HED power supply MSD Toroid transformer AC board power supply...

Страница 217: ...or instrument status Run autotune Run method Run sequence View and set analyzer temperatures View LTM column temperature inlet temperature and GC MSD interface temperature View inlet flows Display err...

Страница 218: ...s proportional to the mass selected Generates the DC component of the voltage applied to the quadrupole mass filter The magnitude of this voltage is proportional to the RF voltage Passes voltages gene...

Страница 219: ...ntrol card Sends digital information to the LAN MS control card Generates voltages for the ion source lenses Generates control signals for filament selection filament emission current and electron ene...

Страница 220: ...rol board It performs these functions Provides input voltage transparency for the MSD Distributes AC line power to the AC DC power supply the foreline pump and the turbo pump controller Turns the cali...

Страница 221: ...s is usually because of a large air leak either the sideplate has not sealed correctly or the vent valve is still open This feature helps prevent the foreline pump from sucking air through the system...

Страница 222: ...AN MS control card include Instrument controller Data processor Main processor Serial communication processor Network communication controller Remote start processor Random access memory RAM Status LE...

Страница 223: ...the 10 000 volts DC for the high energy dynode HED in the detector for the EI MSD The HED power supply also provides 600 VDC for the detector focus lens Due to the high impedance of this circuit measu...

Страница 224: ...wer cord brings in all electrical power for the MSD The power cord can be detached from the instrument Foreline pump power cord receptacle The foreline pump power cord receptacle provides AC power for...

Страница 225: ...are controlled by valve drivers 5 through 8 BCD connector This connector provides two control relays and a BCD input for a stream selection valve Sampler connector This connector provides an injector...

Страница 226: ...ntenance Guide 14 Electronics Figure 36 Side panel connections High vacuum power connector not shown Remote start Primary fuses Power cord Foreline pump power cord LAN GC LAN MSD Event connector BCD c...

Страница 227: ...e requests to send a system ready signal They also include Receive a start run signal from an external device Program the timing of events during a run System ready When interfacing to an external dev...

Страница 228: ...n the instrument Since remote start cables are made for most common devices this is often the simplest way A general purpose remote start cable 05890 61080 is also available which terminates in spade...

Страница 229: ...uid Sampler 258 Reusable Shipping Containers 259 Consumables and Maintenance Supplies 260 This chapter lists parts that can be ordered for use in maintaining your instrument It includes most of the pa...

Страница 230: ...cations as new parts Rebuilt assemblies can be identified by their part numbers The first two digits of the second part of the part number are 69 or 89 such as xxxxx 69xxx or xxxxx 89xxx Rebuilt assem...

Страница 231: ...35900 60800 LAN cable shielded 8121 0008 Power cord Taiwan South America C19 20A 8120 6360 Power cord US 120V C19 20 amp 8120 6894 Power cord Japan C19 20 amp 8120 6903 Power cord Australia C19 16 amp...

Страница 232: ...PS main board G1099 60427 Mass filter contact cable kit inside analyzer G3170 60130 Side board control ribbon cable main board side board G1099 60410 Signal cable signal feedthrough on side plate to s...

Страница 233: ...3 BCD EVENT harness G4360 60516 MS DC 24V harness G4360 60517 Side fan Y cable G4360 60523 Inlet Detector heater harness G4360 60535 Table 13 Internal cables continued Description Part number Table 14...

Страница 234: ...975T ALS controller assembly G4360 67529 5975T Power module assembly G4360 67200 5975T AP board PCA G4360 65100 5975T Connector board PCA G4360 65003 5975T LTM logic PCA G4360 65101 non orderable Fast...

Страница 235: ...e 38 Electronics module Main board Signal amplifier board LAN MS control card AC board HED power supply Cooling fan Cooling fan Low voltage power supply Toriod transformer Table 16 Fuses and power swi...

Страница 236: ...236 Troubleshooting and Maintenance Guide 15 Parts Power button 5041 1203 Power switch extender rod G3170 40007 Table 16 Fuses and power switches continued Description Part number...

Страница 237: ...escription Part number Side panel lower assembly G3880 60070 PANEL SUB REAR G3880 00030 Front panel grill assembly G3880 60060 Side panel upper assembly G3880 60080 PANEL REAR G3880 00026 GC Module si...

Страница 238: ...e 15 Parts Local Control Panel This section lists replaceable parts for the LCP and related covers See Table 18 Table 18 LCP and related parts Figure 39 Item Description Part number 1 LCP fascia G3880...

Страница 239: ...Parts 15 Troubleshooting and Maintenance Guide 239 Figure 39 LCP replacement parts LCP assembly and fascia...

Страница 240: ...for front and rear end plates 0905 1441 GC MSD interface O ring 0905 1405 HED feedthrough G1099 80012 HED feedthrough O ring 0905 0490 KF10 16 seal foreline pump inlet 0905 1463 KF25 O ring assembly t...

Страница 241: ...eline inlet Micro Ion vacuum gauge 0100 1397 Foreline Hose packaging cap flange G3170 40132 KF16 Hose adapter G1099 20531 KF25 Clamp tp end of hose not shown 0100 0549 KF25 Hose adapter tp end of hose...

Страница 242: ...242 Troubleshooting and Maintenance Guide 15 Parts Figure 40 Foreline pump and related parts 1 Safety cage removed for clarity 4 3 2 6 5 7 3...

Страница 243: ...terchangeable but give an optimum fit if they are matched 1400 3241 Dry foreline pump G3170 80028 Dry foreline pump exchange G3170 89028 Foreline pump inlet seal KF10 16 0905 1463 KF10 16 Clamp foreli...

Страница 244: ...Series EXSLRIDP3 Replacement filter element for IDP Series silencer REPLSLRFILTER2 Vibration isolation kit for IDP Series IDP3VIBISOKIT Isolation valve retrofit kit for IDP Series 115 VAC VPI16IDP115...

Страница 245: ...05 1463 KF10 16 clamp Foreline inlet 0100 1397 KF16 hose adapter G1099 20531 KF25 clamp tp end of hose not shown 0100 0549 KF25 hose adapter tp end of hose not shown G1099 20532 Exhaust oil mist trap...

Страница 246: ...MSD vacuum system components Figure 43 Item Description Part number Claw clamps for baffle adapter standard turbo G3170 60590 Clamp for vacuum gauging 0100 1397 1 Fan for high vacuum pump G1099 60564...

Страница 247: ...600 Turbo separate power supply control wiring harness G3170 60835 5 Analyzer chamber manifold G3170 20560 Manifold EMC gasket G3170 80031 Table 23 Turbo pump MSD vacuum system components Figure 43 co...

Страница 248: ...2 TX T10 PN SQ Cone SS qty 2 0515 0664 2 EI Calibration valve assembly Turbo pump MSDs G3170 60204 3 Calibration vial G3170 80002 4 End plate front glass G3170 20552 4 End plate front acrylic G3170 20...

Страница 249: ...4 EI 350 ion source new Turbo inert G3170 65760 4 EI 350 ion source rebuilt Turbo inert G3170 69760 6 Magnet assembly 05971 60160 Low gauss magnet assembly G3163 60560 Mass filter cable kit G3170 601...

Страница 250: ...ting and Maintenance Guide 15 Parts RFPA fan assembly G3170 60023 Quad Stops need 2 G3170 20023 Table 25 Analyzer parts Figure 45 continued Item Description Part number Figure 45 Analyzer parts 7 unde...

Страница 251: ...humbscrew G1099 20138 Magnet mounting screws 0515 1046 Screw magnet bracket to source radiator 0515 1602 Screws source radiator and detector to quad radiator G3170 20123 Screws mass filter contact ass...

Страница 252: ...el Standard 05971 20134 12 Drawout plate 6 mm Inert Used in G2860A and G2860B extended linearity kits G2589 20045 12 Drawout plate 6 mm Stainless Steel G3163 20530 9 Entrance lens G3170 20126 3 EI fil...

Страница 253: ...e 46 EI source 1 9 10 12 11 4 8 5 3 3 7 7 2 Table 28 Repeller assembly Description Part number EI 350 Anodized Repeller assembly G3170 60172 Inert EI 350 Anodized Repeller assembly G3170 60171 Insulat...

Страница 254: ...29 Heater sensor block assembly Description Part number EI 350 Anodized Source Heater Assembly G3170 60180 Inert EI 350 Anodized Source Heater Assembly G3170 60177 EI 350 Anodized Source Heater Assemb...

Страница 255: ...n G1099 20301 Setscrew for heater sensor assembly 0515 0236 Screws M4x0 7 panhead for heater sleeve 0515 0383 Welded interface assembly G1099 60301 RTGA Welded interface assembly G2589 60060 GC MSD in...

Страница 256: ...assembly G4360 67320 Table 33 GC module mainframe Description Part number 5975T Latching block G4360 67020 5975T Cooling fan G4360 67049 5975T Door latch G4360 67391 5975T Oven door latch spring G4360...

Страница 257: ...Parts 15 Troubleshooting and Maintenance Guide 257 Table 35 LTM module parts Description Part number CPM union Inert G3182 60580 5975T Column module fan assembly G3900 60019...

Страница 258: ...ber ALS tower G4513 64000 Syringe 10 L 23 26 ga GT FN Taper 5181 3354 Spot Hi Density turret G4513 40532 ALS main cable assembly G4514 60610 ALS consumables and supplies Vial kit 07673 80090 Diffusion...

Страница 259: ...nce Guide 259 Reusable Shipping Containers Table 37 Reusable shipping container parts Description Part number 5975T Metal strap kit 2 pk G3880 80018 5975T Reusable container package base G3880 80019 F...

Страница 260: ...Small 8650 0029 Grease Apiezon L high vacuum 6040 0289 Table 39 GC consumables Description Part number Column nut fitting 05988 20066 Ferrules 0 4 mm 200 250 m 10 pk 5062 3508 1 16 Ferrule no hole gra...

Страница 261: ...61 RP Wrench angled 19251 00100 Table 41 Tools Description Part number Column cutter 5181 7487 Column installation tool G1099 20030 Ferrule pre swage tool capillary flow G2855 20530 Funnel 9301 6461 H...

Страница 262: ...llary inlet G3452 20512 Column cutter wafer 4 pk 5181 8836 Driver nut 1 4 inch 8710 1561 T 20 Torx key or screwdriver 8710 1807 T 10 Torx key or screwdriver 8710 2140 3 mm hex key wrench 8710 2411 Ele...

Страница 263: ...0 inch Small ultrasonic cleaning bath with aqueous detergent for cleaning inlet parts Gloves clean lint free nylon for handling contamination sensitive parts 8650 0030 large 8650 0029 small Steel wool...

Страница 264: ...0 63011 221 3822LTM DB 17ms 20m 18mm 18 m G3900 63012 221 4722LTM DB 5ms 20m 0 18mm 0 18 m G3900 63013 221 5522LTM DB 5msUI 20m 18mm 18 m G3900 63014 221 5522UILTM DB 608 20m 0 18mm 0 18 m G3900 63015...

Страница 265: ...0 25mm 0 50 m G3900 63035 222 7033LTM INNOWax 20m 18mm 18 m G3900 63036 29091N 577LTM HP VOC 30m 0 20mm 1 12 m G3900 63037 29091R 303LTM HP 5msUI 15m 25mm 25 m G3900 63038 29091S 431UILTM HP 5msUI 20m...

Страница 266: ...ferrules for 0 4 mm id columns 5184 3569 SilTite metal ferrules for 0 5 mm id columns 5184 3570 Table 44 Nuts ferrules and hardware for capillary columns to inlet Column id mm Description Typical use...

Страница 267: ...pk Column cutter ceramic wafer Cutting capillary columns 5181 8836 4 pk Table 44 Nuts ferrules and hardware for capillary columns to inlet continued Column id mm Description Typical use Part number q...

Страница 268: ...10 gram 8500 0656 PFTBA sample kit 05971 60571 Foreline pump tray G1099 00015 Eval A hydrocarbons 05971 60045 Micro Ion gauge electronics G3170 89001 Methane isobutane gas purifier G1999 80410 J20 1...

Страница 269: ...x 6x paddle plastic G2855 40001 Column storage fitting G2855 20590 Table 48 5975T GC module shipping kit G3880 60585 Description Part number Button syringe plunger 19245 40030 Syringe 10 L straight FN...

Страница 270: ...270 Troubleshooting and Maintenance Guide 15 Parts Tool wrench 1 4 inch to 5 16 inch 8710 0510 Wrench G3452 20512 Table 48 5975T GC module shipping kit G3880 60585 continued Description Part number...

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