Installation
Varian, Inc.
User Manual 450-GC
Page: 29
Method to Analyze a Varian Test Sample on a Varian Test Column
Test Sample
Part Number
Concentrati ons of Test Compoun ds
TCD
82-005048-01
3.00
μ
g/
μ
L of C
14
, C
15
and C
16
in iso-octane.
ECD
82-005048-02
33.0 pg/
μ
L of lindane and aldrin in iso-octane.
PFPD
82-005048-03
20.0 ng/
μ
L of n-dodecanethiol, tributylphosphate, methyl
parathion; 4000 ng/
μ
L of n-pentadecane in iso-octane.
TSD
82-005048-04
2.00 ng/
μ
L of azobenzene, methyl parathion; 4.00 ng/
μ
L
malathion and 4.00
μ
g/
μ
L C
17
in iso-octane.
FID (Capillary Column)
82-005048-07
30 ng/
μ
L of C
14
, C
15
and C
16
in iso-octane.
FID (Packed Column)
82-005048-00
3 ng/
μ
L of C
14
, C
15
and C
16
in iso-octane.
Note:
If the FID test sample is not available, the TCD test sample can be used if first diluted 100:1.
Table 12: Varian Test Samples
Note:
These conditions may not conform to the requirements of your analytical column. Do not exceed your
column’s T
max
. See Column Manufacturer’s specifications for your column.
For 1041 and 1061 Injectors
ECD
FID
TCD
a
TSD
PFPD
Initial column oven temp (°C)
80
80
80
80
80
Initial column oven hold time (min)
1
1
1
1
1
Program 1 ramp rate (°C/min)
20
20
20
20
20
Final column oven temp (
°
C)
200
200
200
200
200
Final column hold time (min)
5
5
5
5
5
Initial column oven temp (°C)
(Isothermal operation)
190
140
140
175
175
Initial column oven hold time (min)
(Isothermal operation)
15
15
15
15
15
Injector temp (
°
C)
220
220
220
220
220
Detector temp (
°
C)
300
300
220
300
300
b
Range
1
12
0.05
12
10
c
Initial Autozero
On
On
On
On
On
TSD bead current (amps)
3.0
±
0.3
Table 13: Varian Test Sample 1041 and 1061 Conditions
a
a
T
TC
CD
D R
Re
ef
f e
er
r e
en
nc
ce
e F
Fllo
ow
w –
– R
Ra
atte
e f
f o
or
r c
ca
ar
r r
r iie
er
r g
ga
as
s f
f llo
ow
w tth
hr
r o
ou
ug
gh
h tth
he
e r
r e
ef
f e
er
r e
en
nc
ce
e c
ce
ellll iis
s 2
20
0
±±
1
1 m
mL
L//m
miin
n..
b
b
D
De
ep
pe
en
nd
ds
s o
on
n a
ap
pp
plliic
ca
attiio
on
n:: S
S--m
mo
od
de
e 2
20
00
0°°C
C,, P
P--m
mo
od
de
e 3
30
00
0°°C
C a
an
nd
d N
N--m
mo
od
de
e 2
25
50
0°°C
C..
c
c
N
No
or
r m
ma
all r
r a
an
ng
ge
e:: 1
10
0 iif
f V
Va
ar
r iia
an
n tte
es
sttm
miix
x iis
s b
be
eiin
ng
g u
us
se
ed
d..
Summary of Contents for 450-GC
Page 92: ...AutoSamplers Page 152 User Manual 450 GC Varian Inc...
Page 144: ...Detectors Flame Ionization Detector FID Page 294 User Manual 450 GC Varian Inc...
Page 177: ...Maintenance Page 438 User Manual 450 GC Varian Inc...
Page 179: ...Shipping Cleaning and Disposal Instructions Page 440 User Manual 450 GC Varian Inc...
Page 201: ......
