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Knauer BlueShadow 80P, Инструкция по эксплуатации

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BlueShadow Pump 80P Instructions V7685 

4. Installation

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4.1 Preparations   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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4.1.1 

Operating location   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

12

4.1.2 

Power supply   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

13

4.1.3 

Unpacking the device  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

13

4.2 

Connecting the piston backflushing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

14

4.3 

Eluent inlet   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

15

4.3.1 

Connecting the eluent inlet to the pump head   . . . . . . . . . . . . . . . . . . . . . . . . . . .

16

4.3.2 

Connecting the eluent line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

17

4.4 

Changing the setup to LPG  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

18

4.4.1 

Valve block types  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

18

4.4.2 

Connecting the LPG module  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

18

4.4.3 

Controlling the LPG module   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

19

4.5 Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

19

4.5.1 

Pin header connectors   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

20

4.5.2 

Events connector  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

22

4.5.3 

Connecting cables to the pin header . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

23

4.5.4 

Connecting the device to a computer  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

24

4.5.5 

Configuring the LAN settings   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

25

4.5.6 

Connect devices to LAN  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

25

4.5.7 

Configuring the router  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

26

4.5.8 

Integrating the LAN into the company network  . . . . . . . . . . . . . . . . . . . . . . . . . . .

26

4.5.9 

Controlling several systems separately in the LAN   . . . . . . . . . . . . . . . . . . . . . . . .

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4.5.10  Analog control  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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5. Operation

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5.1 

Switching on the pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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5.2 

Configuring the LPG module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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5.3 

Purging the pump  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

28

5.3.1 

Piston backflushing  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

29

5.4 

Switch on and self test. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

30

5.5 

Operating with LC display and keypad   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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5.5.1 

LED status  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

31

5.5.2 

RFID icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

31

5.5.3 

Operating with the keypad   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

32

5.6 

Menu structure  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

33

5.6.1 

Main menu   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

33

5.6.2 

Menu structure: overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

34

5.6.3 

Device setting parameters  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

35

5.7 

GLP menu  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

39

5.8 

Program menu  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

39

5.8.1 

Create program  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

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Содержание BlueShadow 80P

Страница 1: ...Pump 80P Instructions Document no V7685 HPLC HPLC ...

Страница 2: ...h CET Fax 49 30 8015010 Email support knauer net KNAUER Wissenschaftliche Geräte GmbH Hegauer Weg 38 14163 Berlin Germany Phone 49 30 809727 0 Fax 49 30 8015010 Internet www knauer net E Mail info knauer net Document number V7685 Version number 1 1 Release date 2020 11 17 Translation of the original edition The information in this document is subject to change without prior notice For the latest v...

Страница 3: ... Foreseeable misuse 3 2 2 User qualification 3 2 3 Operator responsibility 4 2 4 Personal safety equipment 4 2 5 Working with solvents 5 2 5 1 General requirements 5 2 5 2 Contamination by health threatening solvents 5 2 5 3 Avoiding leakage 5 2 6 Specific environments 6 2 6 1 Earthqake endangered areas 6 2 6 2 Explosive environment 6 2 6 3 Cooling room 6 2 6 4 Wet room 6 2 7 Maintenance care and ...

Страница 4: ...in header 23 4 5 4 Connecting the device to a computer 24 4 5 5 Configuring the LAN settings 25 4 5 6 Connect devices to LAN 25 4 5 7 Configuring the router 26 4 5 8 Integrating the LAN into the company network 26 4 5 9 Controlling several systems separately in the LAN 26 4 5 10 Analog control 27 5 Operation 28 5 1 Switching on the pump 28 5 2 Configuring the LPG module 28 5 3 Purging the pump 28 ...

Страница 5: ...utions 45 7 3 System messages 46 8 Maintenance and care 50 8 1 Maintenance contract 50 8 2 Cleaning and caring for the device 50 8 3 Checking the fittings 51 8 3 1 Torque values 51 8 3 2 Tighten fittings 51 8 4 Flushing the pump 51 8 5 Pump head 52 8 5 1 Dismounting the pump head 52 8 5 2 Installing the pump head 53 8 6 Check valves 54 8 6 1 Removing the check valves 54 8 6 2 Cleaning the check va...

Страница 6: ...mber 58 10 3 Eluents and other operating materials 58 11 Technical data 59 11 1 Solvent delivery 59 11 2 Communication 60 11 3 General 60 12 Chemical compatibility of wetted materials 62 12 1 General 62 12 2 Plastics 62 12 3 Non metals 64 12 4 Metals 65 13 Repeat orders 66 13 1 Devices 66 13 2 Spare parts 66 ...

Страница 7: ...nd other instructions from the KNAUER web site www knauer net library 1 2 Signal words Possible dangers related to the device are distinguished in personal and material damages Symbol Meaning DANGER red indicates a highly hazardous situa tion If not avoided it will result in death or serious injury WARNING orange indicates a hazardous situa tion If not avoided it could result in death or serious i...

Страница 8: ...case you notice any damage inform the Technical Support and the shipping company within three workdays 1 4 3 Warranty conditions For information on warranty please refer to our general terms and condi tions on the website www knauer net terms 1 4 4 Warranty seal A blue or orange warranty seal is affixed to some devices A blue seal is used by KNAUER s Manufacturing or Customer Support for devices t...

Страница 9: ...e functionality and safety of the device Operation in potentially explosive areas without special and additio nal explosion protection Contact the KNAUER Customer Support for more information 2 2 User qualification The user is qualified to handle the device if all of the following points apply He has at least a basic knowledge of liquid chromatography He has knowledge about the properties of the u...

Страница 10: ...early regulate and specify responsibilities for installation operation troubleshooting maintenance and cleaning and set clear rules Ensure that all personnel who work with the device have read and un derstood these operating instructions Train the personnel who work with the device at regular intervals and inform them about the dangers Provide the necessary safety equipment to the employees workin...

Страница 11: ... onto hot surfaces in the interior Degas solvents before use and observe their purity 2 5 2 Contamination by health threatening solvents Contamination with toxic infectious or radioactive substances poses a hazard for all persons involved during operation repair sale and dis posal of a device All contaminated devices must be properly decontaminated by a spe cialist company or the operating company...

Страница 12: ...in wet rooms 2 7 Maintenance care and repair Avoiding electric shock Before performing any maintenance and ser vice work disconnect the device from the power supply Tools Use only tools recommended or prescribed by the manufacturer Spare parts and accessories Only use original parts and accessories made by KNAUER or a company authorized by KNAUER PEEK fittings Use PEEK fittings only for a single p...

Страница 13: ...uest form and decontamination report Devices which are shipped without the completed document Service request form and decontamination report will not be repaired If you would like to return a device to KNAUER make sure to enclose the com pleted document www knauer net servicerequest ...

Страница 14: ...dient is formed on the high pressure side of the pump 3 1 Intended use The device or device system is suitable for high pressure liquid chroma tography It is suitable for laboratory use for separating substance mix tures that can be dissolved in a solvent or solvent mixture Dosing pump Separation of substances Filtration of substances 3 2 Performance features Dual piston technology Liquid transpor...

Страница 15: ...ad 5 Tube connections for the piston backflushing 6 Pump head Fig 1 Front view Legend 1 Socket for the LPG valve block 2 Events connector 3 Opening of the fan 4 Warranty seal 5 Power switch 6 Power supply 7 CE mark 8 Remote connector 9 Interface RS 232 bl LAN connection bmSerial number Fig 2 Rear view 1 2 3 5 5 6 4 1 2 bm 3 4 bl 9 8 5 6 7 ...

Страница 16: ... 3 Pump head 500 ml stainless steel The pump head is equipped with an RFID chip It is used to monitor and save all important parameters and settings of the pump and pump head The RFID technology offers the following advantages Automatic detection of all important pump head parameters by means of radio signals radio frequency identification by the pump software or the chromatography software Pump h...

Страница 17: ...claration of Conformity Testing seals in Canada and the USA at nationally recognized testing centers NRTL The certified device or system has successfully passed the qual ity and security tests A warranty seal is affixed to some devices For more information see chap 1 4 4 on p 2 3 6 Scope of delivery Note Only use original parts and accessories made by KNAUER or a company authorized by KNAUER Power...

Страница 18: ... strip is always accessible so that the device can be disconnect ed from the power supply Position the device on a level surface Protect the device against direct exposure to sunlight Set up the device at a location not exposed to air drafts such as air conditioning systems Do not set up the device near to other machines that cause floor vibrations Keep the the devices away from high frequency sou...

Страница 19: ... must be free from ripple residual current voltage peaks and electromagnetic interference The connectors for the mains voltage are grounded accordingly The device receives sufficient power with reserve capacity The device is intended for use with AC power networks of 100 240 V Make sure that the power plug on the power supply wall socket or power strip is always accessible so that the device can b...

Страница 20: ...In case any parts are missing contact the Technical Support 7 Set up the device at the operation site Lift the foam padding Store packaging and keep the included packing list for repeat orders 4 2 Connecting the piston backflushing The pump is equipped with automatic piston backflushing It increases the service life of the seals and pistons and removes contaminants from the area behind the seals T...

Страница 21: ...tlet 2 and lead to the waste bottle Fig 4 Connectors 12 34 for piston backflushing 4 3 Eluent inlet Note The acessory Kit includes PTFE tubing and PETP bushing sealing ring which can be used for standard HPLC applications For applications with aggressive solvents PEEK or stainless steel parts are available The eluent lines are connected by the eluent inlet to the pump head Legend 1 Knurled head sc...

Страница 22: ...pump head Process Figure 1 With the knurled head screw 2 screw the eluent inlet into the inlet screw fitting 1 of the pump head 2 Turn the eluent inlet until the intake manifold input 3 points forward 3 Tighten the knurled head screw Fig 6 Eluent inlet variant 1 Fig 7 Eluent inlet variant 2 1 2 3 ...

Страница 23: ...00 ml 1 Push the Teflon hose 1 through the fastening screw 2 and the cutting ring 3 2 Insert the hose end as far as possible into the eluent inlet fitting 4 of the pump head 3 Tighten the fastening screw by hand Fig 8 Connecting the eluent line to the pump head Pump head Process Figure 1000 ml 1 Push the Teflon hose directly on the olive type tube fitting 1 2 Fasten the Teflon hose with hose clamp...

Страница 24: ...ws with sealing ring 3 Plug Fig 10 Ternary LPG valve block 4 4 2 Connecting the LPG module Note Always place seals in pairs on both fastening screws Process Figure 1 In the Setup menu select Gradient type LPG ternary or otherwise LPG binary 2 Switch off the pump and pull the power plug 3 Unscrew the eluent inlets from the inlet screw fittings 3 of the pump head 1 4 Screw tight LPG valve block 2 wi...

Страница 25: ...trolling the LPG module Manual control of the pump via keypad PC control with chromatography software 4 5 Control There are 3 ways to operate the pump Via the pin head As part of a LAN via the LAN connector of the router Operation on display All connectors are located on the rear side of the detector Legend 1 Socket for the LPG valve block 2 Events connector 3 Remote connector 4 Interface RS 232 5...

Страница 26: ...TTL TTL compatible output Levels passive 0 V active 5 V Pulse 5 V for at least 1000 ms 3OC TTL Output Levels passive 0 V active 5 V Pulse 5 V for at least 1000 ms GND Reference point of the voltage at the signal inputs 4TTL TTL compatible output Levels passive 0 V active 5 V Pulse 5 V for at least 1000 ms 5TTL TTL compatible output Levels passive 0 V active 5 V Pulse 5 V for at least 1000 ms ...

Страница 27: ... load of the relay contact 1 A 24 V DC Relay Contact The contact is on a floating basis Its setting depends on the settings in the Control Unit or software Steady rate signal passive open relay contact active closed relay contact Pulse Closed relay contact for at least 1000 ms Permissible load of the relay contact 1 A 24 V DC Analog GND Reference point of the voltage at the signal inputs Analog ou...

Страница 28: ...eiving a signal short circuit to ground from an external device an error message appears and the device stops The error is acknowledged via the keypad Error GND Reference point of the voltage at the signal inputs 24V Event controlled switching of 24 V against GND Protection 24 V 200 mA 5V Provides a voltage of 5 V with respect to GND This makes it possible to supply a consumer that is switched by ...

Страница 29: ... are used to exchange control signals The device is switched off The power plug has been disassembled from the device Operating tool Prerequisites Tools Electronic defect Connecting cables to the multi pin connector of a switched on device causes a short circuit Turn off the device before connecting cables Pull the power plug Electronic defect Electrostatic discharge can destroy the electronics We...

Страница 30: ...which have been assigned by IPv4 IPv6 is not supported This chapter describes how to set up a chromatography system in a local area network LAN and how a network administrator can integrate this LAN into your company network The description applies to the operating system Windows and all conventional routers To set up a LAN we recommend to use a router That means the following steps are required 1...

Страница 31: ...rsion 4 TCP IPv4 5 Click on the button Properties 6 Check the settings in the tab General The correct settings for the DHCP client are a Obtain an IP address automatically Obtain DNS server address automatically 7 Click on the button OK 4 5 6 Connect devices to LAN A router 3 has several LAN ports 2 and one WAN port 4 that can be used to integrate the LAN into a wide area network WAN e g a com pan...

Страница 32: ...e router There is a patch cable for the connection 1 Check that the IP address range of the router and of the company network do not overlap 2 In case of an overlap change the IP address range of the router 3 Use the patch cable to connect the router WAN port to the company network 4 Restart all devices including the computer 4 5 9 Controlling several systems separately in the LAN Devices connecte...

Страница 33: ...lueShadow Pump 80P Instructions V7685 4 5 10 Analog control Analog ports serve for exchanging analog control signals Reference point for the signals is the connector GND OUT Device sends signal IN Device receives signal ...

Страница 34: ...to three channels can be activated for the solvents used Process 1 Press to go to the Main menu 2 Press to open the device settings 3 Use the arrow keys to select the Gradient mode submenu 4 Use the arrow keys up and down to choose LPG 2 for binary or LPG 3 for ternary gradient Confirm with or press any horizon tal key 5 3 Purging the pump Before the pump can be used it must be purged to remove ex...

Страница 35: ... the venting screw 1of the pressure sensor 2 Connect the syringe with the silicone tubing to the outlet 2 3 Press the purging button to open the purging mode and select respective gra dient and flow 4 With the syringe extract fluid through the purge port 2 5 If the extracted fluid flows continuously stop suc tion and close the venting screw 1 Fig 16 Venting screw of the pres sure sensor The purgin...

Страница 36: ...opropanol Legend 1 Inlet from the solvent bottle to the flush pump 2 Outlet from the flush pump to the pump head Fig 17 Connectors for piston backflushing 5 4 Switch on and self test 1 Switch on the pump 2 The display shows Initialization The device runs a self test 3 Wait until the self test has been completed 4 After the test has been successfully completed the most recently ac tive program will...

Страница 37: ... an LED on the front side The co lor of the LED shows the current status LED Status Green Pump is ready idle status Green flashing Pump is running Yellow Firmware upload in progress Yellow flashing Device initialization Red A serious error occured Red flashing An acknowledgeable error occured Blue Device in standby 5 5 2 RFID icon The status of a RFID valve is shown on the display in the main disp...

Страница 38: ...Navigation button Navigation through menu with horizontal keys Adjustment of values at input fields with verti cal keys Menu button Select main menu Return to one menu further up in the menu structure Confirmation button Confirm selection Entering sub menu Activation of numeric pad usage at input value Start and stop button Starts or stops the pump with set values Purge button Opens purge option S...

Страница 39: ...Press to access the submenus Setup GLP Program and Link Note If the status PLAY is displayed on the screen the pump is not running By pushing the pump starts running If STOP is displayed the pump is running Press to stop the pump Navigate through main menu 1 Press to access the menu 2 Navigate between menu points by using horizontal arrow keys 3 Enter submenus using Note With the vertical keys you...

Страница 40: ...34 Operation BlueShadow Pump 80P Instructions V7685 5 6 2 Menu structure overview Fig 19 Menu structure overview ...

Страница 41: ... device should be restarted Pr limits Settings for the minimum and maximum pressure The pump stops automatically if the pres sure drops below the minimum value or exceeds the maximum value The minimum pressure value is used to ensure that the pump does not run dry If the minimum is set to 0 the min imum system pressure is not monitored Pump head Pump head selection automatic detection 100 ml 250 m...

Страница 42: ...ethanol 90 10 0 34 Start input After receiving a signal from an external device the device or a program start an automatic run Software sends a trigger signal via LAN There are four possible settings Enabled Program starts Disabled No program starts Start pump Pump starts to run Stop pump Running pump stops Grad mode Setting of type and channel for high pressure gradient HPG low pressure gradient ...

Страница 43: ...age range opti ons 1 V 2 V 5 V Signal source Pressure preset for the output of the currently measured pressure for the purpose of external recordings or control Slave B for the output of a signal for controlling a second pump Disabled Time constant OUT Set the time constant for analog output to be used for signal smoothing The larger the value of the selected time constant the stronger the applied...

Страница 44: ...e control voltage is applied a resulting flow rate is displayed at actu al interpreted flow based on the basic setting 10 ml corresponds to 1 V for the 100 ml pump head 50 ml corresponds to 1 V for the 500 ml pump head This flow rate value can be changed Thus a se cond calibration point is generated which modi fies the scaling Time constant Set the time constant for analog input to be used for sig...

Страница 45: ... change the value by the numeric pad 4 Move the cursor to the double arrow on the lower left line to navi gate to the next line or create a new line 5 8 1 Create program The use of the display is demonstrated using the example of a program to be created Program 01 is used to create a solvent gradient channels A and B with constant flow of 100 ml min The percentage of solvent A is to be conti nuous...

Страница 46: ...into the status end E 6 Press to stop the pump 5 8 3 Change program When new values for the different program lines are entered the old values are overwritten 1 Select the menu Program 2 Select a program number 3 Navigate to the desired line and value 4 Activate the numeric pad by pressing and enter a new value 5 8 4 Delete program lines 1 Select the menu Program 2 Select the desired program numbe...

Страница 47: ...reated and saved Navigate Link menu 1 Open the desired link number 2 Use the horizontal arrow keys to navigate through the two lines of the display 3 To change a value use the vertical arrow keys or press and change the value by the numeric pad 4 Move the cursor to the double arrow on the lower left line to navigate to the next line or create a new line 5 9 1 Create link Process Figure 1 Select th...

Страница 48: ...us hold H and starts pumping with the initial flow rate of the program 5 Navigate to the pump status and press the up arrow key to set the pump into a run status R 6 The link will start running the programs 7 Use the down arrow key with the cursor on the pump status to pau se the execution of the link Status H 8 Press the up arrow key to resume the run Status R 5 9 3 Delete link Process Figure 1 S...

Страница 49: ...ion OQ The Operation Qualification includes an extensive functionality test accor ding to KNAUER standard OQ documents The Operation Qualification is a standardized document and free of charge It is not part of the delivery Please contact the technical support in case of request The Operation Qualification includes the following Definition of customer requirements and acceptance terms Documentatio...

Страница 50: ...ter set to DCHP server Is the IP address range sufficient for all the connected devices 3 Check all connections Are the patch cable connected to the LAN ports and not the WAN port Are all cable connections between devices and router correct Are the cables plugged in tightly 4 If the router is integrated into a company network pull out the patch cable from the WAN port Can the devices communicate w...

Страница 51: ...the check valves Changing the check valves If the pump head seals are defective solvent enters the piston backflushing inform the technical support Pressure or flow rate fluctuations Check the following options Cleaning the check valves Changing the check valves Purge the pump head so as to remove the air bubbles Tighten the capillary screw fittings on to the inlet and outlet screw fittings of the...

Страница 52: ...hardware Pump head without RFID detection If necessary replace pump head Auto pump head Read failed Switch the device off and on Repeat the automatic configuration step in the chromatography software Remove pump head clean it and install it again Note Inform the technical support in case the system message repeats itself Auto pump head write failed Switch the device off and on Repeat the automatic...

Страница 53: ...ailed Switch the device off and on Inform the techni cal support in case the system message repeats itself E Error input activated Device error change device settings G GUI communication failed internal Switch the device off and on Inform the techni cal support in case the system message repeats itself I Instrument in error state Switch the device off and on Inform the techni cal support in case t...

Страница 54: ...pressure or adjust the lower pressure limit Restart the system Motor failure Switch the device off and on Inform the techni cal support in case the system message repeats itself N No link available Create a link and edit it No link available pls edit link first Create a link and edit it No time table to start Edit the data by means of the chromatography software Non existing com ponent is set to n...

Страница 55: ...edit or delete data by means of the chromatography software this program is used in WAKEUP First quit or delete wakeup program WakeUp and then edit or delete the data by means of the chromatography software Time already exists Correct the time entry Time table line is empty Edit the program line Too many lines in program Check the number of program lines A maxi mum of 100 program lines are possibl...

Страница 56: ...ce will ensure successful analyses and reproducible results 8 1 Maintenance contract The following maintenance work on the device may only be performed by the manufacturer or a company authorized by the manufacturer and is covered by a separate maintenance contract Opening the device or removing housing parts 8 2 Cleaning and caring for the device Device defect Intruding liquids can cause damage t...

Страница 57: ...nd alternately to prevent the pump pistons on the inside from jamming 4 Tighten the knurled head screw 5 on the eluent inlet Fig 20 Screw fittings 2 3 1 4 5 on the pump head 8 4 Flushing the pump Generally the pump and all its components valves degasser should be flushed after each operation Also flush the pump to clean the tubing be fore changing the solvent and to remove air bubbles in the capil...

Страница 58: ...Depending on the requirements of the user different pump heads are used 8 5 1 Dismounting the pump head The pump head has been flushed Allen screwdriver Note Loosen the opposite pairs of fastening screws of the pump head evenly and alternately to prevent the pump pistons on the inside from jamming Materials Next step Prerequisites Tools Life threatening injuries Health danger if getting in contact...

Страница 59: ...ff the pump head Fig 22 Removing the pump head Maintain the check valves see next section or install a new pump head 8 5 2 Installing the pump head Allen screwdriver Tweezers may be necessary for removal Process 1 Using an Allen key tighten the opposite pairs of fastening screws evenly and alternately to prevent the pump pistons on the inside from jamming 2 Tighten all fastening screws evenly 3 Sc...

Страница 60: ...steel Torques for Inlet and Outlet Fittings 100 ml 15 Nm 250 ml 15 Nm 500 ml 12 Nm 1000 ml 12 Nm 8 6 1 Removing the check valves The pump head has been flushed The capillaries have been removed The pump head has been dismounted Open end wrench torque sizes 10 17 Procedure Process Figure 1 Unscrew the outlet fittings 1 2 Remove the check valve 2 3 Unscrew the inlet fittings 3 4 Remove the check val...

Страница 61: ...capillaries have been removed The pump head has been dismounted Open end wrench torque sizes 10 17 Note PEEK fittings can withstand pressures up to 400 bar for 1 16 and 200 bar for 1 8 Note The ball and position of the valves have been harmonized to each other Insert the valves in the direction of flow Procedure Process Figure 1 Insert the check valves 1 so that the notch of the check valve 2 poin...

Страница 62: ...Transporting the device Carefully prepare the device for transport or storage If you want to return your device to KNAUER for repairs enclose the Service Request Form which can be downloaded from our website For a secure transport note the weight and dimensions of the device see chapter 11 on page 59 Bruising danger Damage to the device by carrying or lifting it on protruding housing parts The dev...

Страница 63: ... 4 2 Storing the pump head If you want to store pump heads separately proceed as follows The pump head has been dismounted see chapter 8 5 1 on page 52 Syringe Flushing solution Procedure Process 1 Fill the flushing solution into a syringe and inject into the capillary at the pump head inlet Leave it for 5 minutes 2 Flush with suitable purging solution 3 Fill the pump head with isopropanol 4 Seal ...

Страница 64: ...umber classifies to category 8 and 9 which among others comprises laboratory equipment All distributors and importers are responsible for the disposal of old devices as defined by the WEEE directive End users can send their old devices manufactured by KNAUER back to the distributor the importer or the company free of charge but would be charged for the disposal 10 3 Eluents and other operating mat...

Страница 65: ...nded 5 200 ml min continous working 1000 ml pump head 1 1000 ml min 10 800 ml min recommended 10 400 ml min continous working Maximum pressure 100 ml pump head 400 bar to 100 ml min 250 ml pump head 225 bar to 100 ml min Linear reduction 225 200 bar of 100 150 ml min 200 bar of 150 250 ml min 500 ml pump head 100 bar to 500 ml min 1000 ml pump head 75 bar to 350 ml min Linear reduction 75 50 bar o...

Страница 66: ... via RFID Programming 19 programs 10 program links Links 1 WAKE UP program Program 20 11 3 General Power supply Pump 100 240 V 50 60 Hz Binary LPG valve block 24 V Ternary LPG valve block 12 V Supply frequency 50 60 Hz Power consumption Pump maximum 320 W Binary or ternary valve block 5 W Protection type IP 20 Dimensions W H D 407 x 242 x 191 mm Depth x Width x Height Weight 13 2 kg Area of use Fo...

Страница 67: ...61 Technical data BlueShadow Pump 80P Instructions V7685 Air humidity below 90 non condensing Operating height max 2000 meters above sea level ...

Страница 68: ...0 C unless stated otherwise Please note that higher temperatures can signifi cantly affect the stability of different materials 12 2 Plastics Polyetheretherketone PEEK PEEK is a durable and resistant plastic and next to stainless steel the standard material in HPLC It can be used at temperatures up to 100 C and is highly chemical resistant against almost all commonly used sol vents in a pH range o...

Страница 69: ...ene POM POM HTF POM is a semi crystalline high molecular thermoplastic material which stands out due to its high stiffness low friction value and thermic stability It can even substitute metal in many cases POM H TF is a combination of PTFE fibres and acetal resin and is softer and has better slip properties as POM The material is resistant against diluted acids pH 4 as well as diluted lyes alipha...

Страница 70: ...erized by a high hardness a low coefficient of fric tion and thus low wear In addition it is highly biocompatible DLC is inert against all acids alkalis and solvents commonly used in HPLC Ceramic Ceramic is resistant against corrosion and wear and is fully biocompati ble An incompatibility against acids alkalis and solvents commonly used in HPLC is not known Alumina Al2O3 Due to their high resista...

Страница 71: ... are used or with a mixture of higher compatibility They are inert against almost all solvents Exceptions are biological appli cations which are metal ion sensible and applications with extreme cor rosive conditions These steels in comparison to commonly used steels are increasingly resistant against hydrochloric acid cyanides and other halogen acids chlorides and chlorinated solvents The use in i...

Страница 72: ...ories APD60MC Pump with 1000 ml pump head stainless steel with accessories APD30NA Pump with 1000 ml pump head titanium with accessories APD60NB 13 2 Spare parts Article Order Number 100 ml pump head stainless steel accessories A4029 1 100 ml pump head titanium accessories A4029V2 250 ml pump head stainless steel accessories A4021 1 250 ml pump head titanium accessories A4021V2 500 ml pump head st...

Страница 73: ...rk cable A5255 Set of connector strips 2 x connector strip 12 pos stylus A1420V12 2 x flat ribbon cable 1 5 m 10 pos A1467 RS 232 connection cable A0895 Instruction kit 80P F4020V1 0 Accessory kit for 100 ml 250 ml and 500 ml pump head F4021 Accessory kit for 1000 ml pump head F4022 ...

Страница 74: ...AUER instructions online www knauer net library KNAUER Wissenschaftliche Geräte GmbH Hegauer Weg 38 14163 Berlin Phone Fax E Mail Internet 49 30 809727 0 49 30 8015010 info knauer net www knauer net KNAUER 2020 ...

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