238
MD 610_2d 11/2019
Phosphonates
Persulfate UV oxidation method
with Vario Powder Pack
0 – 125 mg/l (seeTable 1)
1.
Choose the appropriate sample volume from table 1
(seefollowing pages).
2.
Pipette the chosen sample volume into a clean 50 ml
graduated cylinder. If necessaryfill up with deionised
water to the 50 ml mark and mix well.
3.
Fill a clean vial (24 mm Ø) with
10 ml of the prepared
water sample
(this is the blank).
4.
Transfer
25 ml of the prepared water sample
into
the digestion vial.
5.
Add the contents of
one Vario PotassiumPersulfate
F10 Powder Pack
straight from the foil to the digestion
vial.
6.
Close the digestion vial tightly with the cap and swirl
until the reagent is dissolved completely.
7.
Insert the UV lamp into the digestion vial (Note 3, 4, 5).
CAUTION: Wear UV safety goggles!
8.
Switch the UV lamp on and wait for a
reaction period
of 10 minutes
.
9.
After the reaction period isfinished switch the UV lamp
off and remove the lamp from the vial.
10. Filla secondvial (24 mm Ø) with
10 ml of the digested
sample
(this is the sample).
11. Add the contents of
one Vario Phosphate Rgt. F10
Powder Pack
straight from the foil into eachvial (blank
and sample).
12. Close the vials tightly with the cap and swirl gently
several times (30 sec.).
(Note 6)
3
1
6
Countdown 1
10:00
start:
1
2
3
4
Содержание Lovibond MD 610
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Страница 279: ...273 MD 610_2d 11 2019 Notes 1 SO3 Na2 SO3 Reagent Formof reagent Quantity Order No SULFITE LR Tablet 100 518020BT...
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