Agilent Technologies 5975T LTM GC/MSD, Troubleshooting And Maintenance Manual

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Agilent 5975T LTM GC/MSD
Troubleshooting and Maintenance Guide
Agilent Technologies
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Chromatographic Symptoms
Chromatographic Symptoms 34
Retention Times Not Repeatable 35
Peak Areas Not Repeatable 36
Contamination or Carryover 37
Larger Peaks Than Expected 38
Peaks Not Displayed/No Peaks 39
Low Boiler Peaks Present/High Boiler Peaks are Missing 41
Baseline Rise During LTM Column Temperature Program 42
Poor Peak Resolution 44
Peak Tailing 45
Peak Boiling Point or Molecular Weight Discrimination Poor 46
Sample Decomposition in Inlet/Missing Peaks 47
Peak Fronting 48
Noisy Signal, Including Wander, Drift, and Baseline Spikes 50
Low Peak Area or Height (Low Sensitivity) 54
Mass Spectral Symptoms 55
Pressure Symptoms 59
Temperature Symptoms 61
Analyzer Error Messages 64
Air Leaks 69
Contamination 70