Agilent Technologies 5975T LTM GC/MSD Troubleshooting And Maintenance Manual Download Page 101

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Checking for Leaks

Troubleshooting and Maintenance Guide

101

To Check for External Leaks

Check for leaks at these connections:

•

Gas supply bulkhead fittings

•

Gas cylinder fitting

•

Regulator fittings

•

Traps

•

Shut-off valves

•

T-fittings

Perform a pressure drop test.

Turn off the instrument.

Set the regulator pressure to 415 kPa (60 psi).

Fully turn the regulator pressure adjustment knob
counterclockwise to shut the valve.

Summary of Contents for 5975T LTM GC/MSD

Page 1: ...Agilent Technologies Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide...

Page 2: ...y and fitness for a par ticular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing use or perfor mance of this document or of a...

Page 3: ...l Tasks Troubleshooting Tips and Tricks 28 Rule 1 Look for what has been changed 28 Rule 2 If complex isn t working go back to simple 28 Rule 3 Divide and conquer 28 Concepts 29 How to troubleshoot us...

Page 4: ...let operating in split mode 46 For any inlet operating in splitless mode 46 Sample Decomposition in Inlet Missing Peaks 47 Peak Fronting 48 Peaks are fronting 48 Peaks have flat tops 48 Peaks have spl...

Page 5: ...62 Inlet will not heat up 62 LTM column module will not heat up 62 Heated guard column enclosure will not heat up 63 Analyzer Error Messages 64 Difficulty in mass filter electronics 64 Difficulty with...

Page 6: ...Shutdown Symptoms Column Shutdowns 88 Hydrogen Shutdowns 89 Thermal Shutdowns 90 7 Instrument Power On and Communication Symptoms Instrument does not turn on 92 Foreline pump is not operating 93 MSD...

Page 7: ...m Gauge 130 To Remove the Micro Ion Vacuum Gauge 132 To Lubricate the Side Plate O Ring 133 To Lubricate the Vent Valve O Ring 135 Maintaining the Analyzer 137 To Remove the EI Ion Source 139 To Disas...

Page 8: ...plitless Inlet 176 To Clean the Split Splitless Inlet 179 12 Vacuum System Overview 182 Vacuum System Components 183 Common Vacuum System Problems 184 Foreline Pump 185 High Vacuum Pump 189 Turbo pump...

Page 9: ...ies 223 Side Panel Connectors 224 Interfacing to External Devices 227 15 Parts To Order Parts 230 Electronics 231 Covers 237 Local Control Panel 238 Vacuum System 240 Analyzer 248 EI GC MSD Interface...

Page 10: ...10 Troubleshooting and Maintenance Guide...

Page 11: ...en Safety 19 Safety and Regulatory Certifications 23 Cleaning Recycling the Product 26 Liquid Spillage 26 Moving or Storing the GC MSD 26 This manual describes the troubleshooting and maintenance of t...

Page 12: ...1 cm high 60 cm wide and 54 cm deep The weight is 46 5 kg for the mainframe The attached foreline roughing pump weighs an additional 15 kg standard pump for wet and 4 5 kg for dry The basic components...

Page 13: ...features Model G3880A Feature High vacuum pump Standard turbo Optimal He column flow mL min 1 2 Maximum recommended gas flow mL min Total gas flow into the MSD column flow 2 0 Maximum gas flow mL min...

Page 14: ...system Electron Ionization EI systems EI systems ionize sample molecules by bombarding them with electrons The ions including fragments are drawn into the quadrupole analyzer where they are separated...

Page 15: ...P Direct insertion probe EI Electron impact ionization EM Electron multiplier detector EMV Electron multiplier voltage EPC Electronic pneumatic control eV Electron volt GC Gas chromatograph HED High e...

Page 16: ...Troubleshooting and Maintenance Guide 1 Introduction RFPA Radio frequency power amplifier Torr Unit of pressure 1 mm Hg Turbo Turbomolecular pump Table 2 Abbreviations continued Abbreviatio n Definiti...

Page 17: ...trostatic discharge is a threat to GC MSD electronics The printed circuit boards in the GC MSD can be damaged by electrostatic discharge Do not touch any of the boards unless it is absolutely necessar...

Page 18: ...d similar absorbents in the oil pan could ignite and damage the pump and other parts of the MSD WARNING The insulation around the inlets detectors valve box and the insulation cups is made of refracto...

Page 19: ...der bright light WARNING The use of hydrogen as a carrier gas is potentially dangerous WARNING When using hydrogen H2 as the carrier gas or fuel gas be aware that hydrogen gas can flow into the guard...

Page 20: ...which hydrogen can accumulate Table 3 and know what precautions to take if they know or suspect that hydrogen has accumulated Note that these mechanisms apply to all mass spectrometers including the G...

Page 21: ...e operator can close the shutoff valves Closing the shutoff valves does not shut off the flow of carrier gas As a result hydrogen may slowly accumulate in the mass spectrometer Table 3 Hydrogen accumu...

Page 22: ...MSD are closed do not heat the capillary column without carrier gas flow Turn off the hydrogen at its source if a power failure occurs If a power failure occurs while the GC MSD system is unattended...

Page 23: ...D is designed and manufactured under a quality system registered to ISO 9001 Information The Agilent Technologies 5975T LTM GC MSD meets the following IEC International Electro technical Commission cl...

Page 24: ...intended use of the instrument Agilent Technologies assumes no liability for the customer s failure to comply with these requirements See accompanying instructions for more information Indicates a ho...

Page 25: ...s 1 Relocate the radio or antenna 2 Move the device away from the radio or television 3 Plug the device into a different electrical outlet so that the device and the radio or television are on separat...

Page 26: ...Spillage Do not spill liquids on the instrument Moving or Storing the GC MSD The best way to keep your GC MSD functioning properly is to keep it pumped down and hot with carrier gas flow If you plan t...

Page 27: ...or more possible causes are listed In general the causes listed first are the most likely causes or the easiest to check and correct If the material in this chapter and in the online help proves insuf...

Page 28: ...rrect gas If the LTM column was just replaced suspect air leaks or contaminated or bleeding column Rule 2 If complex isn t working go back to simple A complex task is not only more difficult to perfor...

Page 29: ...evelopment of new methods Proceed with troubleshooting under the assumption that method s are working properly This manual also includes common troubleshooting tasks as well as information needed prio...

Page 30: ...the instrument after altering a column causes incorrect flows changed or incorrect split ratios retention time changes and peak shifts Automatic Liquid Sampler configuration Keep the Automatic Liquid...

Page 31: ...red sample supply gas type gas flow rates detectors inlets installed and so forth Any messages that appear on the display Results of any troubleshooting tests you have run Instrument details Obtain th...

Page 32: ...32 Troubleshooting and Maintenance Guide 2 Concepts and General Tasks...

Page 33: ...iler Peaks Present High Boiler Peaks are Missing 41 Baseline Rise During LTM Column Temperature Program 42 Poor Peak Resolution 44 Peak Tailing 45 Peak Boiling Point or Molecular Weight Discrimination...

Page 34: ...al these symptoms do not prevent you from operating your GC MSD system They indicate however that the data you are acquiring may not be the best data obtainable These symptoms can be caused by instrum...

Page 35: ...e Checking for Leaks on page 99 Check for sufficient carrier gas supply pressure The pressure delivered to the instrument must be at least 40 kPa 10 psi greater than the maximum inlet pressure require...

Page 36: ...umn connection See Checking for Leaks on page 99 Check sample level in vials Run replicates of known standards to verify the problem Consider if this is the first run Has the instrument stabilized Poo...

Page 37: ...e causes all inlet and detector combinations Check the septum type and installation Perform complete inlet maintenance Replace all consumable parts and bake out the inlet Perform column maintenance Ba...

Page 38: ...ensions See Configurable Items to Always Keep Current on page 30 Check the autosampler injection volume Check the vial caps Check configured syringe size Some syringe sizes are specified at half capac...

Page 39: ...tenance Check for leaks See Checking for Leaks on page 99 No peaks If an analysis shows no chromatographic peaks only a flat baseline or minor noise run one of the automated tune programs If the MSD p...

Page 40: ...foreline or analyzer chamber pressure Very dirty ion source Calibration valve is not working correctly Bad signal cable connection Filament has failed or is not connected correctly Bad ion source wir...

Page 41: ...romatographic Symptoms 3 Troubleshooting and Maintenance Guide 41 Low Boiler Peaks Present High Boiler Peaks are Missing Cold spot at the point where the LTM transfer line touches the LTM column toroi...

Page 42: ...nt Check for contamination See Contamination or Carryover on page 37 Consider the effect of column film thickness on bleed Check for leaks at the column fittings See Checking for Leaks on page 99 Prep...

Page 43: ...is not properly swept resulting in excess solvent on the column and slow solvent decay Baseline wanders Insufficient carrier gas supply pressure Malfunctioning flow or pressure regulator Intermittent...

Page 44: ...to optimum linear velocity Install and use deactivated consumable parts in the inlet for example a liner Perform column maintenance Bake out contaminants replace the inlet guard column and reverse an...

Page 45: ...Consider the type of adapter liner and inlet seal being used One or all of these may be contaminated or active Check adapters if installed and liner for solid particles For splitless injection consid...

Page 46: ...method to determine expected performance For any inlet operating in split mode Check liner type Increase the inlet temperature and verify that the insulation cup is installed and contains insulation C...

Page 47: ...onality of traps Verify that the liner is appropriate for the sample being run Perform complete inlet maintenance Replace all consumable parts and bake out the inlet Install a deactivated liner Check...

Page 48: ...being used If using capillary splitless injection consider the compound solubility in the injection solvent Try changing the solvent Check purity of sample solvent Peaks are fronting Column film thick...

Page 49: ...Chromatographic Symptoms 3 Troubleshooting and Maintenance Guide 49 Peaks have split tops Bad injection technique Injection is too large...

Page 50: ...short and long are relative to the width of the chromatographic peaks Noisy baseline A noisy baseline or high detector output can indicate leaks contamination or electrical problems Some noise is inev...

Page 51: ...the new conditions before it starts a run some baseline changes are to be expected If experiencing baseline wander check for leaks especially at the septum and at the column See Checking for Leaks on...

Page 52: ...ing may disappear at the same time Check for a contaminated ion source Check for the correct jet Retention times for all peaks drift shorter Column has been shortened Initial column temperature was in...

Page 53: ...terface ion source or mass filter Incorrect sample concentration Leaking GC inlet Dirty GC inlet Incorrect split ratio Purge off time in splitless mode is too short Excessive pressure in the MSD Dirty...

Page 54: ...column type is correct Perform column maintenance Bake out contaminants replace the inlet guard column and reverse and bake out the column as needed Verify that the liner type is appropriate for the...

Page 55: ...ity is poor also apply to mass spectra No peaks Ion source cables not connected Bad connections to or from the detector HED power supply output cable has failed Other electronics failure Isotopes are...

Page 56: ...g may be responsible Repeller voltage is too high Peaks are too wide Incorrect DC polarity on the quadrupole mass filter Dirty quadrupole mass filter Peak widths are inconsistent MSD has not had enoug...

Page 57: ...as a different relative abundance target 3 only applies to Autotune Not enough time for the MSD to warm up and pump down Analyzer chamber pressure is too high Ion source temperature is too high Column...

Page 58: ...ptoms Repeller voltage is too low Not enough time for the MSD to warm up and pump down Analyzer chamber pressure is too high Column carrier gas flow is too high Poor filament operation Dirty ion sourc...

Page 59: ...lyzer chamber pressures can only be measured if your system is equipped with the optional gauge controller Foreline pressure is too high If the pressure you observe for a given column flow has increas...

Page 60: ...for the following Column carrier gas flow is too low Column plugged or crushed by overtightened nut Empty or insufficient carrier gas supply Bent or pinched carrier gas tubing These could create a fa...

Page 61: ...enough time to reach temperature setpoint Ion source heater cartridge is not connected Ion source temperature sensor is not connected Ion source heater failed burned out or shorted to ground Ion sourc...

Page 62: ...working correctly These will cause a GC error message GC error messages are described in the documentation supplied with your GC Inlet will not heat up Incorrect setpoint Setpoint entered in wrong hea...

Page 63: ...correctly Heated guard column enclosure will not heat up Incorrect setpoint Setpoint entered in wrong heated zone Enclosure has not had enough time to reach temperature setpoint Enclosure heater not...

Page 64: ...ilter quad contacts are shorted or otherwise not working correctly Mass filter is not working correctly MSD electronics are not working correctly Difficulty with the electron multiplier supply Large p...

Page 65: ...ck on to remove this error message Be sure the turbo pump has slowed down before switching off the MSD The message will reappear if the underlying problem has not been corrected Turbo pump Large vacuu...

Page 66: ...plier voltage is too low Signal cable is not connected Electrical leads to the detector are not connected correctly HED power supply output cable failed Electrical leads to the ion source are not conn...

Page 67: ...e 5 minutes to reach 80 of its normal operating speed Turbo pump is not working correctly MSD electronics are not working correctly The system is in standby This message is triggered by a shutdown sig...

Page 68: ...ilament has failed try the other filament MSD electronics are not working correctly There is not enough signal to begin tune Corrupted tune file Poor mass axis calibration Amu gain or offset is too hi...

Page 69: ...and 44 or m z 14 and 16 Poor sensitivity Low relative abundance of m z 502 this varies with the tune program used Leaks can occur in either the GC or the MSD The most likely point for an air leak is...

Page 70: ...r gas tubing Fingerprints improper handling of clean parts Contamination originating in the MSD typically comes from one of the following sources Air leak Cleaning solvents and materials Foreline pump...

Page 71: ...ump oil or PFTBA Foreline pump oil vapor or calibration valve leak 73 147 207 221 281 295 355 429 Dimethylpolysiloxane Septum bleed or methyl silicone column bleed 149 Plasticizer phthalates Vacuum se...

Page 72: ...72 Troubleshooting and Maintenance Guide 3 Chromatographic Symptoms...

Page 73: ...Not Reach Setpoint Pressure or Flow 78 A Gas Exceeds Pressure Setpoint or Flow 79 The Inlet Pressure or Flow Fluctuates 80 Cannot Maintain a Pressure as Low as the Setpoint on a Split Inlet 81 The Me...

Page 74: ...a component key for example Front inlet to see which setpoints or conditions are not ready Check for a sampler problem Check for a data system problem If performing manual injections in splitless or g...

Page 75: ...fficient delivery pressure Check the restrictors installed in the Aux EPC module See Restrictors in the Advanced User Guide Check the configured gas type The configured gas type must match the actual...

Page 76: ...ered ready a temperature must be at setpoint 1 C for 30 s If a temperature never becomes ready do the following Check for a missing insulation cup on an inlet Check for a very large temperature differ...

Page 77: ...Set a Flow or Pressure If you cannot set a flow or pressure using the split splitless inlet do the following Check the column mode Check that a capillary column is configured to the correct inlet Che...

Page 78: ...o the following Check for sufficient gas supply delivery pressure The pressure at the supply should be at least 10 psi greater than the desired setpoint Check for leaks See Chapter 8 Checking for Leak...

Page 79: ...ce Guide 79 A Gas Exceeds Pressure Setpoint or Flow If a gas exceeds its pressure or flow setpoint do the following Decrease the split ratio Replace the split vent filter Verify that the correct liner...

Page 80: ...s purifier or gas generator is operating at or near capacity Check the supply gas for sufficient delivery pressure Verify that the supply pressure regulator is functioning properly Check for leaks See...

Page 81: ...tpoint on a Split Inlet If the instrument cannot maintain a pressure as low as the setpoint check for the following Consider using a liner designed for split analysis Check for a plugged liner Check f...

Page 82: ...ch the calculated flow displayed on the GC do the following Verify that the measured flows are corrected to 25 C and 1 atmosphere Verify that the correct column dimensions are configured accurately in...

Page 83: ...83 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 5 ALS Symptoms Plunger Errors 84 Syringe Needle Bends During Injection into Inlet 85...

Page 84: ...4 Troubleshooting and Maintenance Guide 5 ALS Symptoms Plunger Errors If the 7693 ALS reports a plunger error see if the syringe plunger is sticking or is not securely connected to the plunger carrier...

Page 85: ...is not too tight Check that the syringe is installed correctly into the syringe carriage Check that the needle support and guide are clean Remove any residue or septum deposits Check that you are usi...

Page 86: ...86 Troubleshooting and Maintenance Guide 5 ALS Symptoms...

Page 87: ...87 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 6 Shutdown Symptoms Column Shutdowns 88 Hydrogen Shutdowns 89 Thermal Shutdowns 90...

Page 88: ...LTM column temperature setpoint Off Turns off all flows for the column When viewed their parameters flash Off For example the septum purge and column flows would turn off Turns off all other heaters W...

Page 89: ...closes and turns off both pressure and flow controls When viewed these parameters will flash Off Opens the split vent valve in the inlet Turns off the LTM column heaters Turns off the inlet guard col...

Page 90: ...r another heated zone is not within its allowable temperature range lower than minimum temperature or higher than maximum temperature To recover from this state 1 Fix the cause of the shutdown Check f...

Page 91: ...wer On and Communication Symptoms Instrument does not turn on 92 Foreline pump is not operating 93 MSD turns on but then the foreline pump shuts off 94 Local control panel says No server found 95 Inst...

Page 92: ...Nothing happens when the instrument is switched on The foreline pump does not start The cooling fan for the high vacuum pump does not turn on The local control panel is not on Disconnected power cord...

Page 93: ...ing power the fan is operating and the local control panel is lit but the foreline pump is not operating Large air leak usually the analyzer door open has caused pumpdown failure You must power cycle...

Page 94: ...pump and the high vacuum pump if the system fails to pump down correctly This is usually because of a large air leak either the sideplate has not sealed correctly or the vent valve is still open This...

Page 95: ...ng and Maintenance Guide 95 Local control panel says No server found Disconnected LAN cable between MSD and the switch or the switch and the PC PC is turned off Holding the No Cancel key down for 5 se...

Page 96: ...trument Turns On Then Stops During Startup During Self Test If the instrument turns on but the normal display does not appear 1 Turn the power switch Off Wait one minute then turn the power On 2 If th...

Page 97: ...ng followed by an IP address For example if the IP address is 10 1 1 101 enter ping 10 1 1 101 If LAN communications are working properly you will see a successful reply For example If the ping test i...

Page 98: ...98 Troubleshooting and Maintenance Guide 7 Instrument Power On and Communication Symptoms...

Page 99: ...T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 8 Checking for Leaks Leak Check Tips 100 To Check for External Leaks 101 To Check for Instrument Leaks 103 Leaks in Capillary Fl...

Page 100: ...in 9 16 in and 1 4 in wrenches for tightening Swagelok and column fittings 2 Check any potential leak points associated with any maintenance recently performed 3 Check instrument capillary fittings a...

Page 101: ...these connections Gas supply bulkhead fittings Gas cylinder fitting Regulator fittings Traps Shut off valves T fittings Perform a pressure drop test 1 Turn off the instrument 2 Set the regulator pres...

Page 102: ...and Maintenance Guide 8 Checking for Leaks 4 Wait 5 min If there is a measurable drop in pressure there is a leak in the external connections No drop in pressure indicates that the external connectio...

Page 103: ...ks Check for leaks at these connections Inlet septum septum head liner split vent trap split vent trap line and purge vent fittings LTM column connections to inlets GC MSD transfer line and unions Fit...

Page 104: ...loose do not tighten it further Instead remove the connection trim the column end and install it again See To Attach a Capillary Column Using SilTite Metal Fittings on page 114 Also inspect the plate...

Page 105: ...105 Agilent 5975T LTM GC MSD Troubleshooting and Maintenance Guide Agilent Technologies 9 Troubleshooting Tasks To Measure a Split Vent or Septum Purge Flow 106...

Page 106: ...d split vent flows exit through the pneumatic module at the top rear of the instrument See Figure 4 To measure split vent or septum purge flows attach the flowmeter to the appropriate tube WARNING Hyd...

Page 107: ...ate and use a 1 8 in tub adapter as shown above to covert the 1 8 in threaded fitting into a 1 8 tube This prevents the rubber flowmeter tubing from leaking around the threads which will result in lea...

Page 108: ...108 Troubleshooting and Maintenance Guide 9 Troubleshooting Tasks...

Page 109: ...alve Assembly 129 To Install a Micro Ion Vacuum Gauge 130 To Remove the Micro Ion Vacuum Gauge 132 To Lubricate the Side Plate O Ring 133 To Lubricate the Vent Valve O Ring 135 Maintaining the Analyze...

Page 110: ...tion and to take corrective action Table 5 Maintenance schedule Task Every week Every 6 months Every year As needed Vacuum System Check the foreline pump oil level X Replace the foreline pump oil X Ch...

Page 111: ...bles between these boards Wires and cables between these boards and the connectors on the side panel of the instrument Some connectors on the side panel for example the foreline power receptacle Norma...

Page 112: ...il droplets It does not trap any other chemicals If you are using toxic solvents or analyzing toxic chemicals do not use this oil trap For all foreline pumps install a hose to take the exhaust from th...

Page 113: ...n or near printed circuit boards or when you work on components with wires contacts or cables connected to printed circuit boards always use a grounded antistatic wrist strap and take other antistatic...

Page 114: ...wrench Column cutting tool 5181 8836 Internal nut G2855 20530 Lint free gloves 2 Pass the tubing end through the internal nut and SilTite ferrule leaving approximately 1 cm of fused silica tubing pro...

Page 115: ...of the nuts by turning 45 to 60 degrees of rotation but no more than 60 degrees one flat 4 Remove the swaging nut 5 Using a wafer column cutter trim the tubing at the small end of the ferrule leaving...

Page 116: ...116 Troubleshooting and Maintenance Guide 10 General Maintenance 6 Insert the assembled ferrule and nut into the SilTite fitting Tighten with a wrench by only 15 to 20 degrees of rotation...

Page 117: ...Tite Fitting Loosen and remove the internal nut If tubing and ferrule do not come free insert a pointed object pen paper clip into the ferrule release hole and press firmly You will hear a click as th...

Page 118: ...ecking the dry foreline pump diaphragms typically every 3 years Failure to perform these tasks as scheduled can result in decreased instrument performance It can also result in damage to your instrume...

Page 119: ...lower line follow steps 2 through 6 to add foreline pump oil If your instrument is nearing its scheduled time for replacement of the foreline pump oil replace the oil instead of adding oil If the oil...

Page 120: ...120 Troubleshooting and Maintenance Guide 10 General Maintenance Figure 5 Foreline pump standard pump shown without safety cage Fill cap Oil level lines Drain plug Oil mist filter...

Page 121: ...b bench next to the GC MSD 3 Place a book or other object under the pump motor to tilt it up slightly Remove the fill cap See Figure 5 4 Place a container under the drain plug 5 Remove the drain plug...

Page 122: ...object from under the pump motor 4 Add foreline pump oil until the oil level in the window is near but not above the upper line The foreline pump requires approximately 0 28 L of oil 5 Wait a few min...

Page 123: ...om the outboard housing and take it axially off the frame 6 Remove the worn tip seals and discard 7 If compressed air is available blow any remaining tip seal debris from the scroll parts If seal debr...

Page 124: ...14 Reconnect the electrical connector at the front cowling 15 Replace the front cowling and the four M5 bolts that hold it in place See Figure 6 16 Reconnect the pump to electrical power 17 Repositio...

Page 125: ...Execute menu 3 Remove the analyzer window cover 4 Loosen the calibration vial collar Figure 7 Do not remove the collar 5 Pull the calibration vial out You may feel some resistance due to residual vacu...

Page 126: ...ight Do not use a tool to tighten the collar It does not require that much force 10 Reinstall the analyzer window cover 11 Select Purge Calibrant Valve from the Vacuum menu in the Tune and Vacuum Cont...

Page 127: ...nd valve 1 If the vacuum gauge controller is on turn it off 2 In Tune and Vacuum Control view select Purge Calibrant Valve under the Vacuum menu This will open the CI calibration valve for several min...

Page 128: ...nect it 3 Loosen the collar and remove the calibration vial Figure 7 Just loosen the collar do not remove it 4 Remove the two screws holding the valve assembly to the top of the analyzer chamber Do no...

Page 129: ...s in place If it is worn or damaged replace it 3 Install the calibration and vent valve assembly and tighten the screws that hold it in place 4 Reconnect the calibration valve cable to the connector n...

Page 130: ...the MSD See Figure 8 4 Detach the provided KF 16 clamp from the analyzer chamber flange 5 Place the KF16 O ring in the groove on the analyzer chamber flange Replace it if it is worn or damaged 6 Hold...

Page 131: ...General Maintenance 10 Troubleshooting and Maintenance Guide 131 Figure 8 Removing MSD rear cover Rear MSD cover Captive screws...

Page 132: ...f the Micro Ion vacuum gauge 4 Unscrew the large thumbnut on the gauge clamp 5 Remove the long screw from the clamp 6 While supporting the gauge body remove the clamp from the mounting flange 7 Remove...

Page 133: ...hamber See the 5975T LTM GC MSD Operation Manual 3 Remove the analyzer by disconnecting the source wiring and loosening the sideboard from the hinge See the 5975T LTM GC MSD Operation Manual 4 Use a c...

Page 134: ...134 Troubleshooting and Maintenance Guide 10 General Maintenance 6 Close the analyzer chamber 7 Pump down the MSD Figure 9 Side plate O ring Side plate O ring...

Page 135: ...e Procedure 1 Vent the instrument 2 Completely remove the vent valve knob Figure 10 3 Inspect the O ring If the O ring appears damaged replace it 4 Use a clean lint free cloth or glove to spread a thi...

Page 136: ...vent valve knob 7 Pump down the instrument Figure 10 Vent valve O ring Vent valve knob Vent valve O ring CAUTION Be very careful when reinstalling the vent valve knob It is possible to cross thread th...

Page 137: ...moving parts from the analyzer During analyzer maintenance procedures take care to avoid contaminating the analyzer or interior of the analyzer chamber Wear clean gloves during all analyzer maintenanc...

Page 138: ...tive The HED ceramic insulator must never be touched More information is available If you need more information about the locations or functions of analyzer components refer to Chapter 13 Analyzer on...

Page 139: ...analyzer components 4 Disconnect the seven wires from the ion source Do not bend the wires any more than necessary Figure 11 and Table 7 5 Trace the wires for the ion source heater and temperature se...

Page 140: ...aintenance WARNING The analyzer operates at high temperatures Do not touch any part until you are sure it is cool Figure 11 Removing the ion source Source feedthrough board Ion source Thumbscrews Sour...

Page 141: ...he ion source See the To Remove the EI Ion Source on page 139 2 Remove the filaments Figure 12 3 Separate the repeller assembly from the source body The repeller assembly includes the source heater as...

Page 142: ...gure 12 Disassembling the EI ion source Source body Filament Setscrew Interface socket Repeller Repeller insulator Source heater assembly Repeller insulator Washer Repeller nut Ion focus lens Drawout...

Page 143: ...thylene chloride reagent grade Ultrasonic bath Preparation 1 Disassemble the ion source See page 141 2 Collect the following parts to be cleaned Figure 13 Repeller Interface socket Source body Drawout...

Page 144: ...nalyzer seriously consider replacing the contaminated parts Figure 13 Source parts to be cleaned Source body Repeller Interface socket Drawout plate Drawout cylinder Ion focus lens Entrance lens CAUTI...

Page 145: ...ible particles rinse again 6 Separate the parts that were abrasively cleaned from the parts that were not abrasively cleaned 7 Ultrasonically clean the parts each group separately for 15 minutes in ea...

Page 146: ...e source body 4 Install the setscrew that holds the lenses in place 5 Reinstall the repeller repeller insulators washer and repeller nut into the source heater assembly The resulting assembly is calle...

Page 147: ...4 Assembling the ion source Interface socket Source body Setscrew Repeller Repeller insulator Filament 1 of 2 Source heater assembly Repeller insulator Washer Repeller nut do not over tighten Ion focu...

Page 148: ...029 Pliers long nose 8710 1094 Procedure 1 Slide the ion source into the source radiator Figure 15 2 Install and hand tighten the source thumbscrews Do not overtighten the thumbscrews 3 Connect the io...

Page 149: ...1 5 mm 8710 1570 Procedure 1 Vent the MSD 2 Open the analyzer chamber 3 Remove the ion source See the To Remove the EI Ion Source on page 139 4 Remove the filament s to be replaced Figure 16 Figure 1...

Page 150: ...150 Troubleshooting and Maintenance Guide 10 General Maintenance Figure 16 Replacing filaments Filament 1 Filament 2...

Page 151: ...ce body 5 Replace the screw to the ion source body 6 After installing the filament verify that it is not grounded to source body 7 Reinstall the ion source See the To Reinstall the EI Ion Source on pa...

Page 152: ...the MSD 2 Open the analyzer chamber 3 Remove the ion source from the source radiator See the To Remove the EI Ion Source on page 139 4 Remove the filaments 5 Remove the repeller assembly Figure 17 The...

Page 153: ...aintenance 10 Troubleshooting and Maintenance Guide 153 Figure 17 Replacing the heater and sensor Source body Repeller Repeller insulator Filament Filament Repeller nut washer insulator Source heater...

Page 154: ...tall the repeller repeller insulators washer and repeller nut Figure 17 The resulting assembly is called the repeller assembly 3 Connect the repeller assembly to the source body 4 Reinstall the filame...

Page 155: ...9 Hex ball driver 1 5 mm 8710 1570 Hex ball driver 2 0 mm 8710 1804 Procedure 1 Vent the instrument 2 Open the analyzer chamber 3 Disconnect the mass filter heater and temperature sensor wires from th...

Page 156: ...ass filter heater assembly G1099 60172 Procedure 1 Unpack the new mass filter heater assembly Figure 18 The heater temperature sensor and heater block are already assembled 2 Install the heater assemb...

Page 157: ...General Maintenance 10 Troubleshooting and Maintenance Guide 157 Figure 18 Mass filter heater and sensor Mass filter radiator Heater sensor assembly...

Page 158: ...he retaining clip Figure 19 Lift the arm of the clip up and then swing the clip away from the electron multiplier horn 4 Remove the electron multiplier horn 5 Install the new electron multiplier horn...

Page 159: ...General Maintenance 10 Troubleshooting and Maintenance Guide 159 8 Pump down the MSD Figure 19 Replacing the electron multiplier horn Electron multiplier horn Retaining clip...

Page 160: ...onduct ESD to the printed circuit boards to which they are connected This is especially true of the mass filter quadrupole contact wires which can carry ESD to sensitive components on the side board E...

Page 161: ...he functions of electronic components refer to Chapter 14 Electronics on page 215 Most of the procedures in this chapter are illustrated with video clips CAUTION In order to be effective an antistatic...

Page 162: ...ly affect coil adjustment 4 In the Tune and Vacuum Control view select Optimize Quadropole Frequency from the Execute menu 5 Enter an m z value of 100 6 Slowly turn the quad frequency adjustment screw...

Page 163: ...h 7 for m z 650 The minimum voltage is typically between 300 and 340 mV 9 Exit the Set Optimize Quadrupole Frequency program 10 Select MS OFF from the Execute menu 11 Close the analyzer cover 12 Tune...

Page 164: ...ll already be off but for safety you should switch off the instrument and unplug the power cord It is not necessary to allow air into the analyzer chamber 2 Turn one of the fuse holders Figure 21 coun...

Page 165: ...Maintenance Guide 165 6 Repeat steps 3 through 6 for the other fuse Always replace both fuses 7 Reconnect the instrument power cord to the electrical outlet 8 Pump down the MSD Figure 21 Primary fuses...

Page 166: ...166 Troubleshooting and Maintenance Guide 10 General Maintenance...

Page 167: ...rts for the Split Splitless Inlet 168 Exploded Parts View of the Split Splitless Inlet 171 To Clean the Septum Seat in the Insert Assembly of the Split Splitless Inlet 172 To Replace the Gold Seal on...

Page 168: ...800 L Yes 5181 3315 Splitless Direct inject 2 mm id quartz 250 L No 18740 80220 Splitless Direct inject 2 mm id 250 L Yes 5181 8818 Direct inject Headspace or purge and trap 1 5 mm id 140 L No 18740...

Page 169: ...olumn blanking nut Testing use with any ferrule 5020 8294 Column nut universal Connect column to inlet or detector 5181 8830 2 pk Column cutter ceramic wafer Cutting capillary columns 5181 8836 4 pk T...

Page 170: ...ncludes SS washer 5182 9652 Stainless steel washer 0 375 inch od 12 pk 5061 5869 Reducing nut 18740 20800 Column nut blanking plug 5020 8294 Capillary inlet preventative maintenance kit split 5188 649...

Page 171: ...ntenance Guide 171 Exploded Parts View of the Split Splitless Inlet Column nut Ferrule Reducing nut Washer Inlet gold seal Retaining nut Septum Septum retainer nut Split splitless inlet body Liner Spl...

Page 172: ...onal Tweezers Compressed filtered dry air or nitrogen Wrench capillary inlet optional 2 Load the maintenance method see the 5975T LTM GC MSD Operation Manual and wait for the GC to become ready 3 Slid...

Page 173: ...ompressed air or nitrogen to blow away the pieces of steel wool and septum 8 Line up the tab on the bottom of the septum assembly with the slot on the insert assembly and push down to connect Slide th...

Page 174: ...Replacement washer 1 4 inch wrench for column 1 2 inch wrench Lint free gloves 2 Load the maintenance method and wait for the GC to become ready 3 Open the Guard Column enclosure door 4 Remove the in...

Page 175: ...place the new gold seal on top of it raised portion facing down 7 Replace the reducing nut and tighten securely with a wrench 8 Install the inlet guard column 9 Bakeout contaminants See the 5975T LTM...

Page 176: ...become ready 3 Remove the pneumatics cover on the top of the instrument 4 Loosen the screws on the retaining clip WARNING Be careful The oven and or inlet may be hot enough to cause burns If either i...

Page 177: ...eldment on the filter trap assembly Be careful not to stress the tubing between the split vent valve and the trap 7 Remove the old filter cartridge and two O rings 8 Verify the new O rings are seated...

Page 178: ...nce Guide 11 Maintaining the Split Splitless Inlet 12 Fully tighten the split vent front weldment onto the trap 13 Check for leaks 14 Restore the analytical method 15 Reset the split vent trap counter...

Page 179: ...aintenance method and wait for the GC to become ready 3 Remove the inlet liner 4 Disconnect the column from the inlet 5 Remove the reducing nut and gold seal See To Replace the Gold Seal on the Split...

Page 180: ...tall the gold seal and reducing nut 11 Install the liner and O ring 12 Install the column See the 5975T LTM GC MSD Operation Manual 13 Check for leaks 14 Bakeout contaminants See 5975T LTM GC MSD Oper...

Page 181: ...ew 182 Vacuum System Components 183 Common Vacuum System Problems 184 Foreline Pump 185 High Vacuum Pump 189 Analyzer Chamber 190 Side Plate 191 Vacuum Seals 193 Turbo Pump and Fan 195 Calibration Val...

Page 182: ...rument uses two vacuum pumps to obtain the vacuum levels needed One of two types of foreline pumps standard or dry creates a low vacuum then a high vacuum standard turbomolecular turbo pump engages to...

Page 183: ...door and front and rear end plates Vacuum seals Calibration valve s and vent valve Vacuum control electronics Vacuum gauges and gauge control electronics Each of these is discussed in more detail in t...

Page 184: ...you turn on the instrument power Continue to press until the sound from the foreline pump becomes quieter Pumpdown failure shutdown The system will shut down both the high vacuum and the foreline pump...

Page 185: ...Pump The foreline pump Figure 24 reduces the pressure in the analyzer chamber so the high vacuum pump can operate It also pumps away the gas load from the high vacuum pump The foreline pump is connect...

Page 186: ...Hose to vacuum pump Ballast control Fill cap Exhaust outlet Oil drip tray Power switch Oil level window with oil mist filter Drain plug on front Standard pump shown without safety cage Dry pump shown...

Page 187: ...tall an 11 mm id hose to remove the exhaust from your lab A window sight glass in the front of the standard foreline pump shows the level of the foreline pump oil There are two marks next to the windo...

Page 188: ...r towels and similar absorbents in the oil pan could ignite and damage the pump and other parts of the MSD WARNING Combustible materials or flammable non flammable wicking material placed under over o...

Page 189: ...ntenance Guide 189 High Vacuum Pump Turbo pump system The 5975T LTM GC MSD has a turbo pump with a screen to keep debris out of the pump but no baffle is necessary Pump speed is controlled by the turb...

Page 190: ...ings provide the seals between the plates and the manifold Ports in the manifold and the plates provide attachment points for the Micro Ion vacuum gauge calibration valve vent valve GC MSD interface a...

Page 191: ...oughs to analyzer components The electronic side board is mounted on the atmospheric side of the side plate Thumbscrews are located at each end of the side plate CAUTION Fasten both side plate thumbsc...

Page 192: ...Maintenance Guide 12 Vacuum System Figure 26 Side plate feedthroughs High voltage HED Detector focus Ion source and heater Mass filter quadrupole Screws for radiator mounting brackets Signal detector...

Page 193: ...ings into place against the side plate O ring and must be held in place when the MSD is turned on for pump down to assure a good seal The front and rear end plates are screwed onto the manifold and sh...

Page 194: ...ar Tightening the collar presses the ferrule compressing the O ring around the part The calibration vials use compression seals High voltage feedthrough seal The high voltage HED feedthrough seal is a...

Page 195: ...olecules that reach the outlet A controller regulates current to the pump and monitors pump motor speed and temperature A cooling fan is located between the turbo pump and the front panel of the MSD T...

Page 196: ...eal Perfluorotributylamine PFTBA is the most commonly used tuning compound for EI operation PFTBA is required for automatic tuning of the MSD Other compounds can be used for manual tuning Vent valve T...

Page 197: ...Vacuum System 12 Troubleshooting and Maintenance Guide 197 Figure 29 Vent valve Vent valve knob O ring Air passage Valve closed Valve open Valve open too far...

Page 198: ...not ionize as readily as nitrogen Therefore the indicated pressure for helium is approximately six times lower than the absolute pressure For example a reading of 2 0 10 5 Torr versus an absolute pres...

Page 199: ...d Maintenance Guide Agilent Technologies 13 Analyzer Overview 200 EI Ion Source 202 Filaments 203 Other Source Elements 205 Quadrupole Mass Filter 207 Detector 210 Analyzer Heaters and Radiators 212 T...

Page 200: ...s selected ions to pass through the filter and strike the detector The detector generates a signal current proportional to the number of ions striking it The analyzer is attached to the vacuum side of...

Page 201: ...bleshooting and Maintenance Guide 201 Figure 30 The analyzer Detector Mass filter contact cable Mass filter heater assembly Feedthrough board Mass filter contact Ion source inside radiator Mass filter...

Page 202: ...where they pass through several electrostatic lenses These lenses concentrate the ions into a tight beam which is directed into the mass filter Ion source body The ion source body Figure 31 is a cylin...

Page 203: ...ment will give better performance than the other To select the better of the two filaments run two autotunes one with each filament Use the filament that gives the best results Emission current The fi...

Page 204: ...acquisition parameters set the solvent delay so that the analyzer will not turn on while the solvent peak is eluting When the software prompts Override solvent delay at the beginning of a run always s...

Page 205: ...voltage too low results in poor sensitivity and poor high mass response Setting repeller voltage too high results in precursors poor mass filtering and poor low mass resolution Drawout plate and cylin...

Page 206: ...the 4 4 volt permanent offset Entrance lens voltage 4 4 VDC offset gain mass Entrance lens offset The entrance lens offset EntOff controls the fixed voltage applied to the entrance lens It can be vari...

Page 207: ...gments are electrically isolated One pair has positive voltages applied the other negative A combined direct current DC and radio frequency RF signal is applied to the two pairs of segments The magnit...

Page 208: ...ged If you are tuning with a compound other than PFTBA there may not be an ion at m z 219 In that case set the 219 width to the last value found for it by Autotune or set it to 0 DC polarity The DC po...

Page 209: ...e radiator If absolutely necessary that is if the only alternative is replacement the quadrupole can be cleaned Cleaning must be performed by Agilent Technologies service personnel CAUTION Never put t...

Page 210: ...he HED electrons are emitted These electrons are attracted to the more positive EM horn Do not touch the insulator EM horn The EM horn carries a voltage of up to 3000 volts at its opening and 0 volts...

Page 211: ...nstrument Control view to see the tune charts Sudden changes usually indicate a different type of problem See Also Troubleshooting in the online help for more information about symptoms that may indic...

Page 212: ...he MSD ChemStation In selecting the temperatures to use consider the following Higher temperatures help keep the analyzer clean longer Higher ion source temperatures result in more fragmentation and t...

Page 213: ...Analyzer 13 Troubleshooting and Maintenance Guide 213 Figure 34 Heaters and radiators Mass filter radiator Mass filter heater assembly Ion source radiator Ion source heater assembly...

Page 214: ...214 Troubleshooting and Maintenance Guide 13 Analyzer...

Page 215: ...27 The following assemblies make up the MSD electronics Except for the Side panel and connectors Local Control Panel and power switch and Interfacing to other devices sections most of this material is...

Page 216: ...Maintenance Guide 14 Electronics Figure 35 MSD electronics module MSD LAN MS Log amplifier Main board for MSD Cooling fan Low voltage MSD HED power supply MSD Toroid transformer AC board power supply...

Page 217: ...or instrument status Run autotune Run method Run sequence View and set analyzer temperatures View LTM column temperature inlet temperature and GC MSD interface temperature View inlet flows Display err...

Page 218: ...s proportional to the mass selected Generates the DC component of the voltage applied to the quadrupole mass filter The magnitude of this voltage is proportional to the RF voltage Passes voltages gene...

Page 219: ...ntrol card Sends digital information to the LAN MS control card Generates voltages for the ion source lenses Generates control signals for filament selection filament emission current and electron ene...

Page 220: ...rol board It performs these functions Provides input voltage transparency for the MSD Distributes AC line power to the AC DC power supply the foreline pump and the turbo pump controller Turns the cali...

Page 221: ...s is usually because of a large air leak either the sideplate has not sealed correctly or the vent valve is still open This feature helps prevent the foreline pump from sucking air through the system...

Page 222: ...AN MS control card include Instrument controller Data processor Main processor Serial communication processor Network communication controller Remote start processor Random access memory RAM Status LE...

Page 223: ...the 10 000 volts DC for the high energy dynode HED in the detector for the EI MSD The HED power supply also provides 600 VDC for the detector focus lens Due to the high impedance of this circuit measu...

Page 224: ...wer cord brings in all electrical power for the MSD The power cord can be detached from the instrument Foreline pump power cord receptacle The foreline pump power cord receptacle provides AC power for...

Page 225: ...are controlled by valve drivers 5 through 8 BCD connector This connector provides two control relays and a BCD input for a stream selection valve Sampler connector This connector provides an injector...

Page 226: ...ntenance Guide 14 Electronics Figure 36 Side panel connections High vacuum power connector not shown Remote start Primary fuses Power cord Foreline pump power cord LAN GC LAN MSD Event connector BCD c...

Page 227: ...e requests to send a system ready signal They also include Receive a start run signal from an external device Program the timing of events during a run System ready When interfacing to an external dev...

Page 228: ...n the instrument Since remote start cables are made for most common devices this is often the simplest way A general purpose remote start cable 05890 61080 is also available which terminates in spade...

Page 229: ...uid Sampler 258 Reusable Shipping Containers 259 Consumables and Maintenance Supplies 260 This chapter lists parts that can be ordered for use in maintaining your instrument It includes most of the pa...

Page 230: ...cations as new parts Rebuilt assemblies can be identified by their part numbers The first two digits of the second part of the part number are 69 or 89 such as xxxxx 69xxx or xxxxx 89xxx Rebuilt assem...

Page 231: ...35900 60800 LAN cable shielded 8121 0008 Power cord Taiwan South America C19 20A 8120 6360 Power cord US 120V C19 20 amp 8120 6894 Power cord Japan C19 20 amp 8120 6903 Power cord Australia C19 16 amp...

Page 232: ...PS main board G1099 60427 Mass filter contact cable kit inside analyzer G3170 60130 Side board control ribbon cable main board side board G1099 60410 Signal cable signal feedthrough on side plate to s...

Page 233: ...3 BCD EVENT harness G4360 60516 MS DC 24V harness G4360 60517 Side fan Y cable G4360 60523 Inlet Detector heater harness G4360 60535 Table 13 Internal cables continued Description Part number Table 14...

Page 234: ...975T ALS controller assembly G4360 67529 5975T Power module assembly G4360 67200 5975T AP board PCA G4360 65100 5975T Connector board PCA G4360 65003 5975T LTM logic PCA G4360 65101 non orderable Fast...

Page 235: ...e 38 Electronics module Main board Signal amplifier board LAN MS control card AC board HED power supply Cooling fan Cooling fan Low voltage power supply Toriod transformer Table 16 Fuses and power swi...

Page 236: ...236 Troubleshooting and Maintenance Guide 15 Parts Power button 5041 1203 Power switch extender rod G3170 40007 Table 16 Fuses and power switches continued Description Part number...

Page 237: ...escription Part number Side panel lower assembly G3880 60070 PANEL SUB REAR G3880 00030 Front panel grill assembly G3880 60060 Side panel upper assembly G3880 60080 PANEL REAR G3880 00026 GC Module si...

Page 238: ...e 15 Parts Local Control Panel This section lists replaceable parts for the LCP and related covers See Table 18 Table 18 LCP and related parts Figure 39 Item Description Part number 1 LCP fascia G3880...

Page 239: ...Parts 15 Troubleshooting and Maintenance Guide 239 Figure 39 LCP replacement parts LCP assembly and fascia...

Page 240: ...for front and rear end plates 0905 1441 GC MSD interface O ring 0905 1405 HED feedthrough G1099 80012 HED feedthrough O ring 0905 0490 KF10 16 seal foreline pump inlet 0905 1463 KF25 O ring assembly t...

Page 241: ...eline inlet Micro Ion vacuum gauge 0100 1397 Foreline Hose packaging cap flange G3170 40132 KF16 Hose adapter G1099 20531 KF25 Clamp tp end of hose not shown 0100 0549 KF25 Hose adapter tp end of hose...

Page 242: ...242 Troubleshooting and Maintenance Guide 15 Parts Figure 40 Foreline pump and related parts 1 Safety cage removed for clarity 4 3 2 6 5 7 3...

Page 243: ...terchangeable but give an optimum fit if they are matched 1400 3241 Dry foreline pump G3170 80028 Dry foreline pump exchange G3170 89028 Foreline pump inlet seal KF10 16 0905 1463 KF10 16 Clamp foreli...

Page 244: ...Series EXSLRIDP3 Replacement filter element for IDP Series silencer REPLSLRFILTER2 Vibration isolation kit for IDP Series IDP3VIBISOKIT Isolation valve retrofit kit for IDP Series 115 VAC VPI16IDP115...

Page 245: ...05 1463 KF10 16 clamp Foreline inlet 0100 1397 KF16 hose adapter G1099 20531 KF25 clamp tp end of hose not shown 0100 0549 KF25 hose adapter tp end of hose not shown G1099 20532 Exhaust oil mist trap...

Page 246: ...MSD vacuum system components Figure 43 Item Description Part number Claw clamps for baffle adapter standard turbo G3170 60590 Clamp for vacuum gauging 0100 1397 1 Fan for high vacuum pump G1099 60564...

Page 247: ...600 Turbo separate power supply control wiring harness G3170 60835 5 Analyzer chamber manifold G3170 20560 Manifold EMC gasket G3170 80031 Table 23 Turbo pump MSD vacuum system components Figure 43 co...

Page 248: ...2 TX T10 PN SQ Cone SS qty 2 0515 0664 2 EI Calibration valve assembly Turbo pump MSDs G3170 60204 3 Calibration vial G3170 80002 4 End plate front glass G3170 20552 4 End plate front acrylic G3170 20...

Page 249: ...4 EI 350 ion source new Turbo inert G3170 65760 4 EI 350 ion source rebuilt Turbo inert G3170 69760 6 Magnet assembly 05971 60160 Low gauss magnet assembly G3163 60560 Mass filter cable kit G3170 601...

Page 250: ...ting and Maintenance Guide 15 Parts RFPA fan assembly G3170 60023 Quad Stops need 2 G3170 20023 Table 25 Analyzer parts Figure 45 continued Item Description Part number Figure 45 Analyzer parts 7 unde...

Page 251: ...humbscrew G1099 20138 Magnet mounting screws 0515 1046 Screw magnet bracket to source radiator 0515 1602 Screws source radiator and detector to quad radiator G3170 20123 Screws mass filter contact ass...

Page 252: ...el Standard 05971 20134 12 Drawout plate 6 mm Inert Used in G2860A and G2860B extended linearity kits G2589 20045 12 Drawout plate 6 mm Stainless Steel G3163 20530 9 Entrance lens G3170 20126 3 EI fil...

Page 253: ...e 46 EI source 1 9 10 12 11 4 8 5 3 3 7 7 2 Table 28 Repeller assembly Description Part number EI 350 Anodized Repeller assembly G3170 60172 Inert EI 350 Anodized Repeller assembly G3170 60171 Insulat...

Page 254: ...29 Heater sensor block assembly Description Part number EI 350 Anodized Source Heater Assembly G3170 60180 Inert EI 350 Anodized Source Heater Assembly G3170 60177 EI 350 Anodized Source Heater Assemb...

Page 255: ...n G1099 20301 Setscrew for heater sensor assembly 0515 0236 Screws M4x0 7 panhead for heater sleeve 0515 0383 Welded interface assembly G1099 60301 RTGA Welded interface assembly G2589 60060 GC MSD in...

Page 256: ...assembly G4360 67320 Table 33 GC module mainframe Description Part number 5975T Latching block G4360 67020 5975T Cooling fan G4360 67049 5975T Door latch G4360 67391 5975T Oven door latch spring G4360...

Page 257: ...Parts 15 Troubleshooting and Maintenance Guide 257 Table 35 LTM module parts Description Part number CPM union Inert G3182 60580 5975T Column module fan assembly G3900 60019...

Page 258: ...ber ALS tower G4513 64000 Syringe 10 L 23 26 ga GT FN Taper 5181 3354 Spot Hi Density turret G4513 40532 ALS main cable assembly G4514 60610 ALS consumables and supplies Vial kit 07673 80090 Diffusion...

Page 259: ...nce Guide 259 Reusable Shipping Containers Table 37 Reusable shipping container parts Description Part number 5975T Metal strap kit 2 pk G3880 80018 5975T Reusable container package base G3880 80019 F...

Page 260: ...Small 8650 0029 Grease Apiezon L high vacuum 6040 0289 Table 39 GC consumables Description Part number Column nut fitting 05988 20066 Ferrules 0 4 mm 200 250 m 10 pk 5062 3508 1 16 Ferrule no hole gra...

Page 261: ...61 RP Wrench angled 19251 00100 Table 41 Tools Description Part number Column cutter 5181 7487 Column installation tool G1099 20030 Ferrule pre swage tool capillary flow G2855 20530 Funnel 9301 6461 H...

Page 262: ...llary inlet G3452 20512 Column cutter wafer 4 pk 5181 8836 Driver nut 1 4 inch 8710 1561 T 20 Torx key or screwdriver 8710 1807 T 10 Torx key or screwdriver 8710 2140 3 mm hex key wrench 8710 2411 Ele...

Page 263: ...0 inch Small ultrasonic cleaning bath with aqueous detergent for cleaning inlet parts Gloves clean lint free nylon for handling contamination sensitive parts 8650 0030 large 8650 0029 small Steel wool...

Page 264: ...0 63011 221 3822LTM DB 17ms 20m 18mm 18 m G3900 63012 221 4722LTM DB 5ms 20m 0 18mm 0 18 m G3900 63013 221 5522LTM DB 5msUI 20m 18mm 18 m G3900 63014 221 5522UILTM DB 608 20m 0 18mm 0 18 m G3900 63015...

Page 265: ...0 25mm 0 50 m G3900 63035 222 7033LTM INNOWax 20m 18mm 18 m G3900 63036 29091N 577LTM HP VOC 30m 0 20mm 1 12 m G3900 63037 29091R 303LTM HP 5msUI 15m 25mm 25 m G3900 63038 29091S 431UILTM HP 5msUI 20m...

Page 266: ...ferrules for 0 4 mm id columns 5184 3569 SilTite metal ferrules for 0 5 mm id columns 5184 3570 Table 44 Nuts ferrules and hardware for capillary columns to inlet Column id mm Description Typical use...

Page 267: ...pk Column cutter ceramic wafer Cutting capillary columns 5181 8836 4 pk Table 44 Nuts ferrules and hardware for capillary columns to inlet continued Column id mm Description Typical use Part number q...

Page 268: ...10 gram 8500 0656 PFTBA sample kit 05971 60571 Foreline pump tray G1099 00015 Eval A hydrocarbons 05971 60045 Micro Ion gauge electronics G3170 89001 Methane isobutane gas purifier G1999 80410 J20 1...

Page 269: ...x 6x paddle plastic G2855 40001 Column storage fitting G2855 20590 Table 48 5975T GC module shipping kit G3880 60585 Description Part number Button syringe plunger 19245 40030 Syringe 10 L straight FN...

Page 270: ...270 Troubleshooting and Maintenance Guide 15 Parts Tool wrench 1 4 inch to 5 16 inch 8710 0510 Wrench G3452 20512 Table 48 5975T GC module shipping kit G3880 60585 continued Description Part number...

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