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3700 Portable Samplers

Section 3 Programming Guidelines

3-71

3.13 Programming the

Sampler for a Storm
Routine

The extended programming mode contains two program
sequences. The first sequence contains the displays for time- and
flow-paced routines. The second sequence contains the displays
for STORM paced routines. Figures 3-10 and 3-11 show first
sequence displays; Figure 3-12 shows the STORM displays.

The storm input displays are divided into three sections. The
first section contains the displays that control the pacing and dis-
tribution to the first bottle group. The second section contains
the displays that control the pacing and distribution for the
second bottle group. The third section controls the start time for
the routine and may include calibration and manual suction
head displays.

3.13.1 First Section: First

Bottle Group Settings

The first section contains the input displays that:

• Set a delay to the first sample event of the first bottle

group.

• Set the time pacing for the first bottle group.

• Allocate the bottles for the first bottle group.

• Determine sample distribution for the first bottle group:

sequential, samples-per-bottle multiplexing,
bottles-per-sample multiplexing, or multi-bottle compos-
iting.

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Summary of Contents for 3700

Page 1: ...3700 Portable Samplers Installation and Operation Guide Part 60 3703 267 of Assembly 60 3704 101 Copyright 1994 All rights reserved Teledyne Isco Inc Revision GG August 8 2008 ...

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Page 3: ...Return Authorization Number specified Be sure to include a note describing the malfunction This will aid in the prompt repair and return of the equipment Teledyne Isco welcomes suggestions that would improve the information presented in this manual or enhance the operation of the equipment itself Teledyne Isco is continually improving its products and reserves the right to change product specifica...

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Page 5: ...ges périlleux Si vous utilisez cet instrument d une manière autre que celles qui sont specifiées dans ce manuel la protection fournie de l instrument peut être affaiblie cela augmentera votre risque de blessure Additional safety information can be found in Appendix C Hazard Severity Levels This manual applies Hazard Severity Levels to the safety alerts These three levels are described in the sampl...

Page 6: ...es de sécurité Ce symbole signale l existence d instructions importantes relatives au pro duit dans ce manuel Ce symbole signale la présence d un danger d électocution Risque de pincement Ces symboles vous avertit que les mains ou les doigts seront blessés sérieusement si vous les mettez entre les éléments en mouvement du mécanisme près de ces symboles Warnungen und Vorsichtshinweise Das Ausrufeze...

Page 7: ...s 1 8 1 5 2 Non Isco Flow Meters 1 9 1 5 3 Samplink for Sampling Data Retrieval 1 9 1 5 4 Liquid Level Actuator 1 10 1 5 5 Master Slave Cables 1 10 1 6 Technical Specifications 1 10 Section 2 Setup Procedures 2 1 Assembly and Disassembly of the Case 2 1 2 2 Preparing the Base Section 2 1 2 2 1 Standard Base Section 2 1 2 2 2 Compact Base Section 2 1 2 2 3 Bottles 2 2 2 3 Cooling the Samples 2 2 2 ...

Page 8: ... 9 2 Bottles and Sizes 3 38 3 9 3 Portable or Refrigerated Sampler 3 39 3 9 4 Suction Line 3 40 3 9 5 Liquid Detector 3 41 3 9 6 Programming Mode 3 42 3 9 7 Load Stored Program 3 44 3 9 8 Save Current Program 3 45 3 9 9 Flow Mode Sampling 3 46 3 9 10 Nonuniform Time 3 47 3 9 11 Calibrate Sampler 3 47 3 9 12 Sampling Stop Resume 3 47 3 9 13 Start Time Delay 3 47 3 9 14 Enable Pin 3 48 3 9 15 Event ...

Page 9: ...1 Isco Flow Meters and Flow Loggers 4 3 4 3 2 Non Isco Flow Meters 4 4 4 3 3 4 20 mA Flow Signals 4 5 4 3 4 1640 Liquid Level Actuator 4 5 4 3 5 Master Slave Connections 4 6 Section 5 Routine Maintenance 5 1 Cleaning the Sampler 5 1 5 2 Cleaning Protocols for Priority Pollutants 5 1 5 3 Pump Tubing 5 3 5 3 1 Inspection of Pump Tubing 5 3 5 3 2 Removing the Pump Tubing 5 4 5 3 3 Installing a New Pu...

Page 10: ...dard Weighted Polypropylene Strainer 2 4 2 3 Stainless Steel Strainer 2 5 2 4 CPVC Weighted Strainer 2 5 2 5 Placement of the Sampler Adjacent to Manhole 2 6 2 6 Locking the Sampler 2 8 2 7 Locked Sampler 2 9 3 1 Sequential Sample Distribution 3 3 3 2 Samples Per Bottle Multiplexing 3 5 3 3 Bottles Per Sample Multiplexing 3 5 3 4 Multiple Bottle Compositing 3 7 3 5 Storm Distribution Scheme 3 8 3 ...

Page 11: ...ations for the 3700 Portable Samplers 1 10 2 1 Strainers 2 5 3 1 Configure Option Functions 3 11 3 2 Bottle Volume Settings for Standard Bottle Configurations 3 40 3 3 Sampling Capabilities Through the Program Sequence 3 42 3 4 Factory Configure Option Settings 3 54 3 5 Factory Program Settings 3 55 3 6 Start Time Displays 3 64 3 7 Recommended Configurations for Storm Sampling 3 69 4 1 Flow Meter ...

Page 12: ... Start Time 3 99 Program Started Later Than Programmed 1st Switch Time 3 100 Program Started Later Than Programmed Stop Time 3 100 Reviewing the Sampling Results 3 103 Run State Displays Time Paced Sampling 3 107 Run State Displays Flow Paced Sampling 3 108 Run State Displays Composite Sampling 3 109 ...

Page 13: ...ng sections provide an overview of the standard and compact units sampling capabilities and a variety of inter facing equipment The end of this chapter provides a brief dis cussion of this interfacing equipment which includes Teledyne Isco 4200 Series Flow Meters 2100 Series Flow Modules and 4100 Series Flow Loggers collec tively called flow meters throughout this manual for flow paced sampling an...

Page 14: ...eric Liquid Crystal Display LCD and keypad is located on the top of the control box The 24 position keypad is used to enter program parameters and direct the following controls on off pump reverse pump forward stop the pump start sampling resume sampling display the operating status and move the distributor arm to the next bottle 1 1 2 3700 Compact Description The 3700 Compact is a modular system ...

Page 15: ...low pacing You can set the flow interval from 1 to 9 999 flow pulses Both samplers offer two types of time pacing uniform and non uniform You can take uniform time paced samples at regular time intervals a sample every 15 minutes for example You can set the interval between samples from 1 minute to 99 hours 59 minutes in 1 minute increments Using the extended pro gramming mode you can specify as m...

Page 16: ...ch multiplexed bottles or bottle sets after a programmed number of samples have been deposited or after a programmed period of time Both methods can be used with either time paced or flow paced rou tines By specifying the number of samples to be deposited you can control the volume of each bottle precisely By specifying that the sets be switched after specific time periods you can control the time...

Page 17: ...ine not another STORM routine The STORM variant of master slave sampling allows you to both increase the total volume of samples collected and extend the sampling time period 1 2 5 Accurate Sample Volumes You can program the sampler to take sample volumes of 10 to 9 990 milliliters Equipped with the LD90 liquid presence detector the 3700s deliver accurate repeatable sample volumes in changing head...

Page 18: ...stem by replacing relatively inexpensive lengths of tubing Pump speed is approximately 250 RPM which generates a velocity sufficient to obtain representative samples The pumping rate of 3 500 ml per minute is generated when using 3 8 inch ID suction line at 3 feet of head The line transport velocity using the same suction line and head is 2 9 feet per second Pump speed does not significantly affec...

Page 19: ...es 12 bottle base 950 ml 1 quart polypropylene with polyethylene foam lined caps requires 12 bottle base 4 Bottle Configuration 3800 ml 1 gallon glass with PTFE lined caps requires 4 bottle locating insert for 24 bottle standard base section Single Bottle Composite Configurations 9400 ml 2 5 gallon glass composite bottle with unlined cap requires locating insert for 24 bottle standard base section...

Page 20: ...ons that has not been certified as safe for such use The Teledyne Isco 2151 and 2151P Area Velocity Flow Mod ules are certified intrinsically safe for installation in Class I Division 1 Groups C and D hazardous locations A full line of accessories and interfacing equipment is available to help you adapt the sampler to your specific application some of the more common items are briefly discussed be...

Page 21: ...ion available from the sampler s results dis plays with a computer running Flowlink For more information on sampler enable control conditions and data retrieval refer to the help section provided with the Flowlink software 1 5 2 Non Isco Flow Meters You can connect certain non Isco Flow meters directly to a 3700 for flow paced sampling The flow meter must have an isolated contact closure of at lea...

Page 22: ...0 kg with polypropylene bottles Operational Temperature Range 32o to 120o F 0o to 50o C Storage Temperature Range 0o to 140o F 20o to 60o C Control Box Self Certified NEMA 4X and 6 ratings Submersible watertight dust tight and corrosion resistant Sampler Base Capacity 1 Sequential Base 24 350 ml glass or 1000 ml polypropylene bottles or 1 2 5 gallon 9500 ml glass or polyethylene container 2 Option...

Page 23: ...9 foot lengths of 1 4 inch ID vinyl 3 8 inch ID vinyl 3 8 inch ID PTFE lined Suction Lift 26 feet 7 9 m maximum Pumping Rate at 3 feet of head 1 4 inch ID suction tubing 3000 ml minute 3 8 inch ID suction tubing 3500 ml minute Line Transport Velocity at 3 feet of head 1 4 inch ID suction tubing 5 1 ft sec 3 8 inch ID suction tubing 2 5 ft sec Clock Specifications Real Time Clock Accuracy 1 minute ...

Page 24: ...locate the unit with respect to the receiver Plug the unit into a different outlet so the unit and receiver are on different branch circuits If necessary consult the manufacturer or an experienced radio television technician for additional suggestions You may find the following booklet prepared by the FCC help ful How to Identify and Resolve Radio TV Interference Prob lems This book is available f...

Page 25: ...de mouth wedge shaped polypropylene bottles with a capacity of 1 000 ml each Although sets of glass and plastic bottles are interchangeable in the base you cannot mix glass and plastic bottles in the same base The 3700 Standard is shipped from the factory with the sample bottles in place For first time use the only preparation nec essary will be to remove the bottle caps You can store these bottle...

Page 26: ... tub 2 3 Cooling the Samples You can cool the samples by placing cubed or crushed ice in the center of the base section Users can either dump ice into the center of the base section or place it in a plastic bag For the most uniform cooling it is best to let the melt water from the ice run between the sample bottles creating an ice bath The quantity of ice used is dependent upon the required sample...

Page 27: ... shortest length feasible this aids the downhill routing Avoid loops of coiled suction line which may hold residual amounts of liquid that would cross contaminate sample volumes A shorter suction line will also extend battery life and pump tube life because the sampler will require a shorter pumping cycle to deliver the sample volume 2 4 1 Attaching Vinyl Suction Line Attach vinyl suction line to ...

Page 28: ...ubing coupling on the other end Additionally Teledyne Isco offers two low flow stainless steel strainers Figure 2 3 for 1 4 inch ID and 3 8 inch ID suction lines For sampling from highly acidic flow streams a weighted CPVC plastic coated strainer is available Figure 2 4 The use of the strainer is optional When heavy suspended solids are involved and flow stream velocities are significant some fiel...

Page 29: ...t shows the maximum depths you can submerge the lines and strainers without risks of flotation At depths exceeding the safe depths anchor the line and strainer securely 2 6 Connection to Power Source The 3700 Series must use one of four 12 VDC power sources an Isco AC Power Pack an Isco Nickel Cadmium Battery Pack an Isco sealed lead acid battery or an external 12V direct current source such as an...

Page 30: ...ling the sampler be sure the head the vertical dis tance between the level of the liquid source and the pump is no greater than 26 feet The pump will not be able to deliver samples for heads of 26 feet or greater If it is necessary to enter the manhole to position the strainer and suction line observe standard safety precautions Refer to Appendix C for a discussion of safety considerations The sam...

Page 31: ...moved place caps on the bottles Using the base section as a carrying case is conve nient prevents undue warming of cooled samples and helps to prevent mix ups in bottle order An optional cover with carrying handles for the base section is available to aid in transportation Attach the cover to the base in the same manner as the center section It is good practice to attach an adhesive label detailin...

Page 32: ...tion 2 Setup Procedures 2 8 two cables and gather the ends of the cables with the small loops at the center of the top cover Then feed the padlock through the loops and lock as shown in Figure 2 7 Figure 2 6 Locking the Sampler ...

Page 33: ...3700 Portable Samplers Section 2 Setup Procedures 2 9 Figure 2 7 Locked Sampler ...

Page 34: ...3700 Portable Samplers Section 2 Setup Procedures 2 10 ...

Page 35: ... tions The Types of Samples section discusses sample types that can be taken in both basic and extended mode with the 3700 Sampler The Programming Introduction section discusses the sampler s program structure and introduces both basic and extended programming modes The Operating States section discusses the sampler s three operating states Introduction to the Programming Procedures describes the ...

Page 36: ...ume the distributor moves to the bottle that will receive the sample 3 For the pre sample purge the pump rotates in reverse The pre sample purge is an air purge of the suction line and inlet that clears the line of any accumulated debris It also purges residual liquid to avoid cross contamination of sam ples 4 The pump direction changes moving forward to fill the suction line up to the liquid dete...

Page 37: ...ibution There are two primary types of sample distribution sequential and composite sampling In a sequential sample each bottle receives one sample A sequential sample represents a snapshot of the flow stream at a particular point in time Figure 3 1 shows a diagram of sequential sample distribution In a composite sample the individual samples are combined com posited into a single container A comp...

Page 38: ...sample in several bottles at the same sample event There are two types of multiplexing samples per bottle and bottles per sample Samples per Bottle Multiplexing In samples per bottle multiplexing the 3700 deposits a number of individual samples in the same bottle Samples per bottle multiplexing is useful when you need to collect a series of small composite samples In samples per bottle multiplexin...

Page 39: ...sample purge by delaying the complete post sample purge until sample volumes have been delivered to each bottle of the set Instead the pump reverses until the pump tubing is purged just beyond the liquid detector When the purged liquid passes the detector the distributor moves to the next bottle and the pump begins pumping forward to deliver the next sample This repeats until each bottle of the se...

Page 40: ...aced sam pling When the flow rate varies predictably using nonuniform time intervals allows you to take samples at equal flow volumes As the flow rate increases you can take samples at equal flow volumes by decreasing the time interval As the flow rate decreases you can increase the time interval When you use nonuniform times the time interval between each sample event is programmable You can ente...

Page 41: ...volume composite sample than you can collect in one bottle You can use multiple bottle compositing with time paced or flow paced routines 3 3 4 Stops and Resumes The Sampling Stops and Resumes feature available in the extended programming mode allows you to create an inter mittent sampling schedule You can program the sampler to stop the routine at a specific time and then resume the routine later...

Page 42: ...igure 3 5 Storm Distribution Scheme 3 5 Programming Introduction The sampler s programming process is self prompting Prompts displayed on the LCD step you through the programming sequence in a logical order indicating the needed value or option For example the sampler will prompt you to enter settings for the interval between samples select either time paced or flow paced intervals sample volume i...

Page 43: ...to enter the interval between samples the number of samples in each bottle the sample size and the start time The configure sequence pro vides a number of setup options Some configure options provide equipment specifications bottle sizes suction line diameters and lengths and so on For example the 3700 Standard can use dif ferent sized sequential bottles 350 ml and 1000 ml You must enter the corre...

Page 44: ...s are noted in the Program Sequence section of the diagram shown in Figure 3 6 Figure 3 6 Interactive State Structure PROGRAM CONFIGURE SAMPLER Configure STANDBY 9 54 40 12 SEP 04 STANDBY 9 50 34 12 SEP 04 Program PROGRAM SEQUENCE CONFIGURE SEQUENCE Set Clock Bottles and Sizes Suction Line Liquid Detector Programming Mode Load Stored Program Save Stored Program Flow Mode Sampling Nonuniform Time C...

Page 45: ...rvals as specific clock times or in minutes Calibrate Sampler Basic Extended Enables disables the calibration sequence Sampling Stop Resume Extended Enables disables Sampling Stops and Resumes feature Start Time Delay Basic Extended Sets the start time delay from 0 to 9999 minutes If no specific start time is entered in the program sequence the program uses the entered start time delay The delay i...

Page 46: ...h Set Clock through Exit Configuration It is usually not necessary to change the configure option settings unless the sampling application changes significantly The sampler is always programmed and configured the sampler s internal battery maintains program and configure settings In fact the sampler is shipped with factory program and configure settings It is configured for the basic program mode ...

Page 47: ...he displays will report the sampler s progress The programming examples in this manual conclude with the run state displays you should see for each sampling routine When the routine is done the sampler will return to standby 6 Retrieve the filled sample bottles If you wish use the Dis play Status procedure discussed in detail later in this sec tion to examine the sampler s log of sampling results ...

Page 48: ...ontrol Keys Control keys let you turn the sampler on or off start or resume the currently entered program and control the sampler manually Control key functions are ON OFF Pressing the ON OFF key when the sampler is off will turn the sampler on reactivate the display and place the sampler in the standby state Pressing the ON OFF key when the sampler is on will halt all sampling activity and clear ...

Page 49: ...ference number START SAMPLING When in the standby state pressing the START SAMPLING key will begin the sampling program When entering a sampler ID this key will type a space RESUME SAMPLING When PROGRAM HALTED is displayed pressing the RESUME SAMPLING key will cause the sampler to continue with the current sample program at the point were it was halted When entering a sampler ID this key will type...

Page 50: ...the next step Numeric Keys The numeric keys consist of 10 digit keys a key and a key You use the digit keys to enter quantities and the arrow keys to move through the configure option list or program options Left Arrow Press the left arrow key to select one of two or more program options displayed when the sampler is in the interactive state When more than one numeric entry is displayed for exampl...

Page 51: ...s There are two types of input displays displays that prompt you to make a choice between time paced and flow paced sampling for example and displays that prompt for numeric input sample volume for example In displays that ask you to make a choice you must select one of as many as four alternatives placed in brackets The display above prompts you to select the program or configure sequence The cho...

Page 52: ... to 3 30 p m enter a time of 15 30 When the display above first appears the first two digits 12 will blink To enter a new time type in the new hour 15 Store the hour entry and advance to minutes by pressing the ENTER PROGRAM key If you do not need to change the month or year entry accept the entry by pressing the right arrow or ENTER PROGRAM key Use the left arrow key to return to a pre vious posi...

Page 53: ...amming Mode structure Figures 3 10 3 11 and 3 12 chart the structure of the Extended Programming Mode The charts are provided to act as a map to the programming process Both charts are divided into sections Sample Pacing Sample Distribution Sample Volume and Key Times which correspond to the steps listed in the procedure discussed below Each chart contains the input displays used in the sequence T...

Page 54: ...VOLUMES OF ml 1 MAX SUCTION HEAD OF FEET 1 MAX Display 70 Display 80 CALIBRATE SAMPLE VOLUME YES NO See Example Calibration Procedure Display 90 ENTER START TIME YES NO Yes Flow Time TAKE FIRST SAMPLE AT HH MM DD MMM START FLOW COUNT AT HH MM DD MMM Display 92 MULTIPLEX SAMPLES YES NO BOTTLES PER SAMPLE SAMPLES PER BOTTLE BOTTLES PER SAMPLE EVENT 1 24 SAMPLES PER BOTTLE 1 MAX Samples Per Bottle Bo...

Page 55: ...r truly representative sampling the interval in either time or flow paced sampling should be longer than the duration of the sampling cycle If the intervals are too short you will not miss any sample events although some events will occur at improper times You can determine the duration of the cycle by programming the sampler with the desired settings pressing the manual sample key and timing the ...

Page 56: ...tion to add the suction head setting to the program sequence The suction head display will appear after you enter the sample volume However when the head is unknown or variable omit the suc tion head setting by disabling that setting in the Liquid Detector configure option By disabling the setting you allow the liquid detector to determine the operating suc tion head each time a sample is taken Ca...

Page 57: ... foot length of 3 8 inch vinyl suction line enable the liquid detector and select the basic programming mode Pro cedures for reinitialization of the program settings and configure options to factory settings are placed in Steps 22 through 24 in Example Checking the Configure Option Settings Example Checking the Configure Option Settings 1 If the sampler is not already on press the ON OFF key to tu...

Page 58: ...TER PROGRAM key to accept the entry and advance to step 10 1001 ml ARE YOU SURE YES NO 10 Press the ENTER PROGRAM key at this display to access the Suction Line input displays shown in steps 11 to 13 SELECT OPTION SUCTION LINE 11 Select 1 4 if you are using 1 4 inch suction line 3 8 if you are using 3 8 inch suction line Press the ENTER PROGRAM key to accept the selection If you select 1 4 you wil...

Page 59: ...nt RETRY UP TO 0 TIMES WHEN SAMPLING 0 3 19 To verify the programming mode setting press the ENTER PROGRAM key SELECT OPTION PROGRAMMING MODE 20 Select BASIC Press the ENTER PROGRAM key to accept the selection BASIC EXTENDED PROGRAMMING MODE 21 Scroll through the remaining options with the arrow keys Use the techniques above to change or verify the settings If you want to reinitialize the configur...

Page 60: ...rn it on The standby display shown here will appear Press ENTER PROGRAM to access the interactive state STANDBY 5 34 50 19 JUN 04 2 Access the program sequence by selecting PROGRAM Because PROGRAM will already be selected blinking press the ENTER PROGRAM key to accept it and move to the next step PROGRAM CONFIGURE SAMPLER 3 To enter the interval between samples in time increments select TIME If TI...

Page 61: ...to the start time The first line reports the bottle which will receive the next sample volume The second line reports the start time at the left and the current time on the right BOTTLE 1 AT 5 44 5 42 33 When the start time arrives the sampler will take the first sample The sample event cycle begins with a pre sample purge During the purge the display indicates the number of the bottle that will r...

Page 62: ...ly returns to the standby state PROGRAMMING SEQUENCE COMPLETE 8 After you properly install the sampler press the START SAMPLING key to run the program STANDBY 10 37 23 19 JUN 04 9 To start the sampling routine with the first bottle press the ENTER PROGRAM key To start the routine with another bottle enter the starting bottle number here START SAMPLING AT BOTTLE 1 1 24 The first line of this displa...

Page 63: ...next sample event This series of displays will repeat until the last sample is taken at bottle 24 and the sampling routine is done BOTTLE 2 AFTER 5 PULSES This display informs you that the sampling routine is completed The number of sample events displays in the upper right corner The second line indicates the current time and date DONE 24 SAMPLES 22 48 32 20 JUN 04 Example Flow Paced Sequential S...

Page 64: ...tine with another bottle enter the starting bottle number here START SAMPLING AT BOTTLE 1 1 24 This is used with samples per bottle multiplexing The first line tells the number of the upcoming sample the total number of samples each bottle is to receive and the current bottle number Here the upcoming sample is the first of four samples Bottle 1 The second line indicates the scheduled time of the s...

Page 65: ...he final sample has been deposited in the first bottle the display changes to indicate the new sample bottle This display indicates that the upcoming sample event will place the first of four sample volumes in Bottle 2 at 7 00 1 OF 4 BOTTLE 2 AT 7 00 6 45 25 This display appears as the pump begins the pre sample purge for the first sample delivered to Bottle 2 1 OF 4 BOTTLE 2 1 OF 4 BOTTLE 2 PUMPI...

Page 66: ... SAMPLE VOLUMES OF 500 ml 10 1000 9 Select YES ENTER START TIME YES NO Enter the start time for the sampling routine Note that the sampler may receive flow pulses before the sampling rou tine begins Any pulses received before the start time will be disregarded START FLOW COUNT AT 5 00 20 06 JUN After this message appears briefly the sampler automatically returns to the standby state PROGRAMMING SE...

Page 67: ...ctor The suction line is not completely purged instead the liquid is pumped just past the liquid detector At the end of the pump tube purge the distributor moves to the next bottle of the set The display remains unchanged until the distributor relocates to the next bottle of the set BOTTLE 1 PUMPING 500 ml When the distributor relocates above the next bottle the bottle number reported in the displ...

Page 68: ...you must enter the number of samples required before entering the sample volumes At four samples per hour the 12 hour period would yield 48 samples The total sample volume collected at the end of the routine would be 12 000 ml 48 samples x 250 ml sample well within the capacity of the 4 gallon bottle Example Time Paced Composite Sampling 1 If the sampler is not already on press the ON OFF key to t...

Page 69: ...tions press the EXIT PROGRAM key to return to standby 13 Press the ENTER PROGRAM key to reenter the interactive state STANDBY 10 38 50 19 JUN 04 14 Access the program sequence by selecting PROGRAM PROGRAM CONFIGURE SAMPLER 15 Select TIME TIME FLOW PACED SAMPLING 16 Enter 0 to set the hours at zero Press ENTER PROGRAM to store the number 0 and move to the minutes entry SAMPLE EVERY 0 HOURS 1 MINUTE...

Page 70: ...upcoming sample event and the total number of programmed samples The second line indicates the scheduled time of the upcoming event followed by the current time SAMPLE 1 OF 48 AT 6 00 5 50 43 When the time to the next sample event has elapsed and the sampler has initiated the sample event the sampling cycle begins SAMPLE 1 OF 48 When the pump reverses for the pre sample purge the second line disap...

Page 71: ... cycle will include rinse cycles and retries if the sampler is configured to perform them This ensures that the calibration procedure includes the pump cycle used while running the sampling program Example Calibration 1 Press ENTER PROGRAM to access the interactive state STANDBY 9 34 50 19 JUN 04 2 Access the program sequence by selecting PROGRAM PROGRAM CONFIGURE SAMPLER 3 Step through the progra...

Page 72: ...ou can scroll through the list of configure options without viewing each input display If you are interested in only one or two options you can use this method to locate the option of interest quickly Each option is discussed below in the order in which it appears when configuring the sampler Individual input displays and their settings are discussed separately within the discussion of each option...

Page 73: ... 3700 Compact 1 12 and 24 bottles are the only valid choices as the 4 bottle option is not available The 3700 Standard can be programmed for continuous sampling which means that they will sample into successive sets of bottles until the last set of bottles has been sampled into and then return to the first set of bottles and continue sampling indefi nitely into successive sets Continuous sampling ...

Page 74: ...ou change the current suction line settings the CALCU LATING PUMP TABLE VALUES message will appear for a short time Because the volumetric delivery of the sample varies with the diameter type and length of the suction line the sampler must revise the internal pump tables The electronic pump count uses the tables as reference for sample delivery There are three types of suction lines available for ...

Page 75: ...am sequence If the detector is disabled the sampler uses a calcu lated number of pump counts based on the suction head entry to deliver the correct sample volume With the detector disabled the sampler operates at diminished accuracy Display 240 Rinse Cycles The Rinse Cycle setting is available only when the detector is enabled It sets the number of suction line rinses from 0 to 3 Rinses are used t...

Page 76: ...r time intervals from 1 minute to 99 hours 59 minutes Time Pacing Nonuniform Clock Time Intervals Extended Samples taken at irregular time intervals by specifying the time and date of each sample You can enter dates as far as one month in advance of the current date Time Pacing Nonuniform Intervals in Minutes Extended Samples taken at irregular time intervals by specifying the amount of time in mi...

Page 77: ... can switch bottles after a specified number of samples have been deposited Bottles per Sample Multiplexing Extended Sample volumes placed in more than one bottle at each sample event Multiple Bottle Compositing Extended More than one sample volume placed in a set of bottles You can switch bottle sets after a specified number of samples have been deposited Storm Volumes and Accuracy Sample Volume ...

Page 78: ...tine If no start time is entered the Start Time Delay will be used Maximum Flow Interval Extended You can enter maximum period of time between flow paced sam ple events If this period of time is exceeded the sampler will ter minate the routine Table 3 3 Sampling Capabilities Through the Program Sequence Continued Example Load Stored Program 1 Press ENTER PROGRAM to access the interactive state STA...

Page 79: ...rogram will replace the default program with the current settings Reinitialization of the sampler restores the default program settings shown in Tables 3 4 and 3 5 Note Saving a program will overwrite a program saved earlier under the same number You can view settings for the current program with the Display Status procedure Example Save Current Pro gram shows how to save a current sampling progra...

Page 80: ...se countdown If you select NO no samples be taken at the switch time and the pulse countdown will not be reset The switch will SELECT OPTION SET CLOCK 4 You can save the current program only when the sampler is configured for the extended programming mode To verify the programming mode setting press the ENTER PROGRAM key SELECT OPTION PROGRAMMING MODE 5 Select EXTENDED Press the ENTER PROGRAM key ...

Page 81: ...sequence You can enter as many as 24 times 12 stop times and 12 resume times For example the Stop Resume option allows you to define a sampling routine which will take samples at intervals of 15 minutes between 6 a m to 8 a m and between 4 p m to 6 p m Sampling Stops and Resumes are not available in a storm routine If you are using a time switched sampling routine that includes the use of stops an...

Page 82: ...am sequence When using a start time delay of greater than 0 take care when the sampler is being inhibited by another sampler a flow meter or a Liquid Level Actuator 3 9 14 Enable Pin The Enable Pin option allows you to program the sampler s response to a device controlling pin F of the flow meter connector for example a 4200 Series Flow Meter a 4100 Series Flow Logger or the 1640 Liquid Level Actu...

Page 83: ...s the sampler to take a sample when the pin is enabled A response of NO pre vents the sampler from taking a sample when the pin is enabled Display 322 Reset Sample Interval Reset Sample Interval controls the time or flow pulse countdown If you select YES a full sample interval begins when pin F is enabled If you select NO the interval will not be reset when the sampler is enabled the set tings ent...

Page 84: ...orward pumping only a continuous signal during the entire pump cycle a continuous signal during forward pumping only The event mark includes a signal sent on pin D which is inter preted and recorded by an Isco flow meter as the bottle number s for the sample event The bottle number signal consists of a number of 100 millisecond 12 volt pulses that equal the bottle number i e four pulses rep resent...

Page 85: ...the entire pump cycle from the beginning of the pre sample purge to the end of the post sample purge Select FWD PUMPING when you want a continuous signal transmitted while the pump is delivering a sample volume Display 331 Pulse Signal The Pulse Signal setting will appear when you select PULSE Two options are available The first option PURGE sends a pulse at the beginning of the pre sample Pre sam...

Page 86: ... failure at a pump count that differs significantly from the current setting enter that value here The factory set value of 500 000 pump counts will deliver approxi mately 500 samples of 200 ml each using a 3 8 inch by 10 foot vinyl suction line at a 5 foot suction head Display 350 351 and 352 3 9 18 Program Lock Select ENABLE to turn the lock on When the Program Lock is enabled each protected dis...

Page 87: ...the pump serviced A count near 100 is typical Distributor Test Following the pump test you can test the distributor If you elect to test the distributor the sampler will move the distributor to Position 24 then return it to Position 1 The positions are indicated on the display If the message DIS TRIBUTOR JAMMED is displayed check the routing of the pump tubing and the bottles in the tub If the tub...

Page 88: ...OW MODE SAMPLING sample at start time 270 NO sample at switch times 271 NO NONUNIFORM TIME 280 MINUTES CALIBRATE SAMPLER 290 DISABLE SAMPLING STOP RESUME 300 DISABLE sample at stop times 301 NO sample at resume times 302 NO START TIME DELAY 310 2 ENABLE PIN master slave 320 DISABLE sample upon disable 321 NO sample upon enable 322 NO reset sample interval 323 NO inhibit countdown 324 NO EVENT MARK...

Page 89: ...TERVALS 11 UNIFORM TIME FLOW STORM PACED SAMPLING 12 TIME TIME FLOW BOTTLE GROUP 14 FLOW MINUTE DELAY TO FIRST TIMED SAMPLE 15 0 MINUTES DURING AFTER TIME MODE 16 DURING _MINUTE DELAY TO SECOND GROUP SAMPLES 17 30 SAMPLE EVERY HOURS MINUTES 21 1 HOUR 0 MINUTES SAMPLE EVERY PULSES 1 9999 22 10 TAKE TIMED SAMPLE EVENTS 1 MAX 23 1 SAMPLE INTERVALS OF MINUTES 1 99 24 60 TAKE SAMPLES 1 MAX 25 10 QUANTI...

Page 90: ...nce to allow you to take advantage of the additional fea tures The Sample Pacing program section is extended to include settings for nonuniform times The Sample Distribution section is modified to let you program the sampler for multiple bottle CHANGE BOTTLES BASED ON TIME SAMPLE 40 COUNT CHANGE SETS BASED ON TIME SAMPLE 41 COUNT CHANGE BOTTLES EVERY HOURS MIN 42 2 HOURS 0 MINUTES CHANGE SETS AFTE...

Page 91: ... enter nonuniform intervals in two ways The first method allows you to define the interval between each sample event in minutes For example you can program the sampler to take sample 2 after an interval of 10 minutes sample 3 after an interval of 30 minutes sample 4 after an interval of 60 minutes and so on Sample 1 would be taken at the start time The second method allows you to enter a specific ...

Page 92: ...only when you have specified bottle or bottle set changes based on time in the Sample Distribution section If you select TIME rather than SAMPLES in the CHANGE SETS BASED ON TIME SAMPLES display you first will be asked if you want to enter a setting for the first switch time If you respond YES you will be prompted for the time of the first bottle or set change The first time switch displays are in...

Page 93: ...STORM PACED SAMPLING Display 12 Program Configure Storm To Configure Sequence Display 30 Display 44 BOTTLES PER SAMPLE EVENT 1 24 CHANGE SETS BASED ON TIME SAMPLES BTL CHANGE BOTTLES BASED ON TIME SAMPLES One Botttle Per Sample Event CHANGE SETS AFTER HOURS MINUTES CHANGE SETS AFTER SAMPLES CHANGE BOTTLES AFTER HOURS MINUTES CHANGE BOTTLES AFTER SAMPLES Time Count Time Count More Than One Bottle P...

Page 94: ...splay 46 Display 100 Display 101 Display 102 Display 47 FIRST BOTTLE CHANGE AT HH MM DD MM Flow Time TAKE FIRST SAMPLE AT HH MM DD MM START FLOW COUNT AT HH MM DD MM Display 91 Display 92 No PROGRAMMING SEQUENCE COMPLETE Change Bottles Sets Based on Time Change Bottles Sets Based on Samples ENTER FIRST SWITCH TIME YES NO Yes No Display 95 SUCTION HEAD OF FEET 1 MAX CALIBRATE SAMPLE VOLUME YES NO S...

Page 95: ...ROUP Display 50 SAMPLE VOLUMES OF ____ ml EACH 10 MAX SUCTION HEAD OF FEET 1 MAX CALIBRATE SAMPLE VOLUME YES NO Display 70 Display 80 ENTER START TIME YES NO Display 90 STORM ENABLED AFTER HH MM DD MMM Display 93 Display 17 Display 24 __ MINUTE DELAY TO SECOND GROUP SAMPLES SAMPLE INTERVAL OF ___ MINUTE 1 9999 Display 16 Display 22 DURING AFTER FIRST GROUP SAMPLE EVERY PULSES 1 9999 MAX FLOW INTER...

Page 96: ...mple will be taken at the resume time unless you have selected ENABLE in the Sample at Resume display of the Sampling Stops and Resumes option When you are using Stops and Resumes with flow paced rou tines the 3700 will not take a sample at the start time unless you have configured the sampler to do so in the Flow Mode Sam pling configure option With flow paced routines no sample will be taken at ...

Page 97: ...ns for certain sampling applications They send flow pacing signals flow pulses to the sampler for flow paced sampling The second function pro vides disable inhibit or enable signals to the sampler A sampler receiving a disable signal will suspend the sampling routine until it receives an enable signal The sampler will disregard a disable signal it receives from a flow meter during the delay to sta...

Page 98: ...d NOTE Nonuniform clock time programming is designed to replace flow pacing when a flow meter is not available at the site Before using a sampler programmed for nonuniform clock times with a flow meter be sure flow pacing is not a more appropriate application 3 11 3 Manual Sample Key and Programmed Start Times The sampler will disregard the manual sample key during the delay to start time and duri...

Page 99: ...3700 Portable Samplers Section 3 Programming Guidelines 3 65 Figure 3 14 Start Time Diagram I I I I I I ...

Page 100: ...3700 Portable Samplers Section 3 Programming Guidelines 3 66 Figure 3 15 Start Time Diagram for Nonuniform Time Routines ...

Page 101: ...t uses flow paced sampling The maximum flow interval setting affects routines that fill the second bottle group with flow paced samples The maxi mum flow interval setting limits the amount of time between flow paced sample events For example if the flow rate declines so that the amount of time between flow paced sam ple events exceeds a maximum flow interval setting of two hours the sampler will t...

Page 102: ...o flow meter cabling Isco Flow Meters can also be equipped with a modem to communicate with Flowlink over standard telephone lines Solar Panel Battery Charger Installation Checklist This checklist summarizes the four steps required to set up a storm monitoring installation 1 Program and install the flow meter Install the rain gauge if used You can program 4200 Series Flow Meters for sampler enable...

Page 103: ...flow meter s control condition The time between flow paced sample events exceeds the storm routine s maximum flow interval setting Manual Samples Manual sampling is not available during a storm routine If you press MANUAL SAMPLE during a storm routine the sampler will disregard the key Run State Displays Run state displays for storm routines are identical to displays used with conventional routine...

Page 104: ...Start Time Delay 310 Enable Pin Sample upon disable 321 Disregarded by STORM routines Sample upon enable 322 Disregarded by STORM routines Reset sample interval 323 Disregarded by STORM routines Inhibit countdown 324 Disregarded by STORM routines Event Mark Continuous pulse 330 Select preferred Event Mark Pump cycle fwd only 331 Select preferred Event Mark Purge Counts Pre sample counts 340 Enter ...

Page 105: ...rol the pacing and dis tribution to the first bottle group The second section contains the displays that control the pacing and distribution for the second bottle group The third section controls the start time for the routine and may include calibration and manual suction head displays 3 13 1 First Section First Bottle Group Settings The first section contains the input displays that Set a delay ...

Page 106: ...3700 Portable Samplers Section 3 Programming Guidelines 3 72 Figure 3 16 Storm Sampling Flow Pacing for the Second Bottle Group ...

Page 107: ...amount of time between the time the sampler is enabled and the first sample delivered to the first bottle group The sampler may be enabled at the start time The acceptable range of values for the delay to first group sample is 0 to 999 minutes If the delay is 0 the sampler will take the first sample when enabled by the flow meter Subsequent time paced samples will occur at the time interval entere...

Page 108: ...tion schemes are available for both bottle groups Because STORM programming is part of the extended programming mode the sample distribution displays used Display s 30 and 31 are identical to other extended mode programming routines Refer to Example Time Paced Multiplexed samples per bottle Sampling for samples per bottle multiplexing Example Extended Flow Paced Multiplexed bottles per sample Samp...

Page 109: ...e first group sample the delay to the second group sample determines the period between the time the sampler is enabled and the first sample is deposited in the second bottle group You can use this setting to fill the second bottle group during the same time the sampler fills the first bottle group or after the sampler fills the first bottle group Figure 3 17 shows a time diagram for a STORM routi...

Page 110: ... when it begins timing the delay to first group sample The sampler will take the first sample of the second bottle group as soon at it counts a full flow pulse interval If you select AFTER the sampler will begin counting flow pulses after the last sample event of the first bottle group Use Display 22 to enter the flow pulse interval for the second bottle group The third flow paced display allows y...

Page 111: ... start time for the routine select YES in Display 90 illustrated in Step 17 of Example Storm Sampling The sampler will prompt you to enter a start time with Display 93 step 18 If you select NO the start time will be delayed by the amount set in the Start Time Delay configure option After you ve made these entries the sampler will present the PROGRAMMING SEQUENCE COMPLETE message and return to stan...

Page 112: ...le group Your entry in Display 15 determines the Delay to First Group Delay to Second Group Samples The delay to second group sample is the period between the time the sampler is enabled not the start time and the time the first sample volume is delivered to the second bottle group This delay is determined by your entry in Display 17 You can enter a delay to second group sample only for time paced...

Page 113: ...n millimeters Samplers using French Spanish and German language displays support metric units for suction line and suction head measure ments Samplers with English displays support either English or metric units for suction line and suction head measurements Always enter sample volumes in milliliters To program the sampler for foreign language displays begin by placing the sampler in standby Then ...

Page 114: ...roughout this section demonstrate the steps used to program the sampler for several different sampling rou tines in the extended programming mode Each programming example concludes with the run state displays that appear for that routine Note Before programming a sampler in the extended programming mode the sampler must be configured for extended program ming Refer to the section Programming Mode ...

Page 115: ...UENCE COMPLETE 13 When the sampler is properly installed press the START SAMPLING key to run the program STANDBY 10 37 23 19 JUN 04 14 To start the sampling routine with the first bottle accept the blinking 1 by pressing the ENTER PROGRAM key If you want to start the routine with another bottle enter the starting bottle number here BOTTLE 1 AT 8 00 10 38 07 This display appears as the sampler coun...

Page 116: ... left The current time is displayed on the right BOTTLE 2 AT 8 30 8 01 11 The cycle of displays is repeated for each bottle until the sampling routine is done When the routine is completed this message appears It reports the status of the routine DONE the total number of sample events and the current time and date DONE 24 SAMPLES 8 10 35 21 JUN 04 Example Time Paced Sampling Uniform Intervals Cont...

Page 117: ...e is to receive It also indicates the current bottle number Thus this display indicates that the upcoming sample is the first of four samples and bottle one is to receive the next sample The second line indicates the scheduled time of the sample The current time is shown in the right corner as the sampler counts down to the next sample event time 1 OF 4 BOTTLE 1 AT 5 41 5 39 33 When the scheduled ...

Page 118: ... the upcoming sample event will place the first of four sample volumes in bottle 2 at 7 00 1 OF 4 BOTTLE 2 AT 7 00 6 45 25 This display appears as the pump delivers the first sample to bottle 2 1 OF 4 BOTTLE 2 The cycle of displays is repeated for each bottle until the sampling routine is done When the routine is completed this message appears It reports the status of the routine DONE the total nu...

Page 119: ...by pressing the ENTER PROGRAM key If you want to start the routine with another bottle enter the starting bottle number here START SAMPLING AT BOTTLE 1 1 23 This display appears after you press the start sampling key to start the routine It reports the scheduled start time on the first line The second line reports the current time and date START FLOW COUNT AT 10 37 23 20 06 JUN When the scheduled ...

Page 120: ...e delivery it reverses to purge the liquid from the pump tube past the liquid detector The suction line is not completely purged instead the liquid is pumped just past the liquid detector At the end of the pump tube purge the distributor moves to the next bottle of the set The display remains unchanged until the distributor relocates to the next bottle of the set BOTTLE 1 PUMPING 800 ml As the dis...

Page 121: ...wo hours Press the ENTER PROGRAM key to advance to the minutes entry CHANGE SETS EVERY 2 HOURS 0 MINUTES 8 Press ENTER PROGRAM to accept an entry of 0 for minutes CHANGE SETS EVERY 2 HOURS 0 MINUTES 9 Enter 100 to set the sample volume at 100 ml SAMPLE VOLUMES OF 100 ml EACH 10 330 10 Select NO ENTER START TIME YES NO 11 Select YES ENTER FIRST SWITCH TIME YES NO 12 Enter the time at which you want...

Page 122: ...iving bottle number on the first line during the pre sample purge SAMPLE 1 BOTTLE 1 When the pump begins to run forward to deliver the sample the second line appears it reports the sample volume SAMPLE 1 BOTTLE 1 PUMPING 100 ml When the sample delivery has been completed for the first bottle of the set the distributor moves to the second bottle SAMPLE 1 BOTTLE 2 PUMPING 100 ml After the bottles of...

Page 123: ...ervals or flow intervals can be used with the actuator as well SAMPLE 1 BTLS 3 4 AFTER 1000 PULSES SAMPLE 1 BTLS 3 4 AFTER 1000 PULSES The cycle of displays is repeated for each bottle until the sampling routine is done When the routine is completed this message appears It reports the status of the routine DONE the total number of sample events and the current time and date DONE 96 SAMPLES 6 10 35...

Page 124: ...S 12 Enter 1 to set the number of samples per bottle to 1 CHANGE BOTTLES EVERY 1 SAMPLES 1 50 13 Enter 500 to set the sample volume at 500 ml SAMPLE VOLUMES OF 500 ml 10 1000 14 Select NO ENTER START TIME YES NO After this message is displayed briefly the sampler will automatically return to the standby state PROGRAMMING SEQUENCE COMPLETE 15 Press the START SAMPLING key to run the program STANDBY ...

Page 125: ...During the purge the display indicates the receiving bottle number BOTTLE 1 As soon as the pump runs forward to deliver the sample volume the message on the second line appears This message remains through the post sample purge BOTTLE 1 PUMPING 500 ml This display appears when the post sample purge from the previous sample event is completed It indicates the bottle number which is to receive the s...

Page 126: ...Times 1 Enter the time and date for the first sample event Times and dates are entered on the second line of the display TAKE SAMPLES AT 1 06 00 19 JUN 2 Enter the time and date for the second sample event The controller will guess a time at the hour succeeding the previously entered time 1 06 00 19 JUN 2 07 00 19 JUN 3 Enter the time and date for the third sample event 2 06 30 19 JUN 3 07 00 19 J...

Page 127: ...ree stop times and two resume times 5 STOP or RESUME TIMES 0 24 14 Enter the time and date of the first stop time 8 00 a m STOP SAMPLING AT 1 08 00 19 JUN 15 Enter the time and date the program should resume 11 00 a m RESUME SAMPLING AT 1 11 00 19 JUN 16 Enter the time and date of the second stop time 1 30 p m or 13 30 You must enter the times in military time STOP SAMPLING AT 2 13 30 19 JUN 17 En...

Page 128: ...er here START SAMPLING BOTTLE 1 1 24 This display appears as the sampler counts down the time remaining to the start time The first line reports the bottle which will receive the next sample volume The second line reports the start time at the left and the current time on the right BOTTLE 1 AT 6 00 10 38 07 When the start time arrives the sampler will take the first sample The sample event cycle b...

Page 129: ...ween samples to five minutes SAMPLE INTERVALS OF 5 MINUTES 1 999 Display 24 7 Enter the number of bottles per sample event 3 3 BOTTLES PER SAMPLE EVENT 1 23 Display 30 8 Enter 1 to place one sample in each bottle 1 SAMPLES PER BOTTLE 1 2 Display 31 9 Enter the sample volume of 900 ml SAMPLE VOLUMES OF 900 ml 10 1000 Display 50 The sampler will display this message before automatically advancing to...

Page 130: ...omatically return to the standby state PROGRAMMING SEQUENCE COMPLETE 19 This display appears when you press START SAMPLING START STORM PROGRAM AT 6 00 5 33 07 The displays shown in step 22 alternate as the sampler s clock approaches the start time The first line reports the bottles which will receive the first sample volumes for each bottle group The second line reports the start time at the left ...

Page 131: ...NTER PROGRAM MANUAL SAMPLE NEXT BOTTLE and DISPLAY STATUS Program Halted A sampling program can be halted with either the STOP or EXIT PROGRAM key if this occurs the sampler will display the halt message shown below If you halt the program to take a manual sample or to change a setting in the program or configure sequence the sampler will return to standby If this is the case you will not be able ...

Page 132: ...ave programmed and configured the sampler use the START SAMPLING key to run the sampling program The first display you ll see after pressing the START SAMPLING key is illustrated below If you want to have the sampling program begin with a bottle other than Bottle 1 enter the first bottle number here If 1 is acceptable press the ENTER PROGRAM key to place the sampler into the run state If you do no...

Page 133: ... number of samples that will be skipped if you do not change the start time it appears only if more than one sample event time has passed 1 SAMPLES WILL BE SKIPPED 1 Select YES if you want to change the start time Select NO if missed samples are acceptable CHANGE START TIME YES NO Display 142 2 This display appears when you select YES in display 142 and a sample event is to occur at the start time...

Page 134: ...r a short time then advances to the next display PAST SWITCH TIME 1 Select YES to change the switch time Select NO to continue the routine CHANGE SWITCH TIME YES NO Display 143 2 This display appears when you select YES in display 143 and the bottles per sample event is set at 1 Enter the new switch time FIRST BOTTLE CHANGE AT 5 30 19 JUN Display 46 3 This display appears when you select YES in di...

Page 135: ... the display below to notify you that the program fin ished because the liquid level float float cage was tripped This display alternates with the DONE display at approximately 3 second intervals 3 17 2 Display Status You can access a summary of the current program settings and the results of the most recent sampling routine with the DISPLAY STATUS key This key is valid in both the run and standby...

Page 136: ...ults Review Select REVIEW to review the program settings and sampling results The sampler will present the display shown below Use this display to leave the Display Status procedure or to review the program settings or sampling results No Select NO to return to the previous operating state If you entered Display Status from standby the standby message will reappear If you entered Display Status fr...

Page 137: ... settings or results report The sampler will interrupt the reports to take a sample if necessary Select NO to return to standby The sampler will display one of two messages as it sends the data to the printer The first message informs you that the trans mission is in progress The second message is a warning informing you that the sampler is unable to detect the printer If you see the warning messa...

Page 138: ...issed only one sample will be taken PROGRAM STARTED AT 5 30 19 JUN 04 5 This display reports the nominal sample volume Press ENTER PROGRAM to advance to the next display 200 ml SAMPLES 6 This display reports the bottle number s for each sample event It also reports the source of the event in this case the sample was taken at the start time Press ENTER PROGRAM to advance to the next display SAMPLE ...

Page 139: ...Disable The sample event was initiated when the sampler became disabled by a device connected to pin F of the flow meter connector generally a 4200 Series Flow Meter a 4100 Series Flow Logger or a Liquid Level Actuator This source is also reported when the sample was taken at a programmed stop time Two different configure option settings control this event the Sample Upon Disable setting in the En...

Page 140: ...The sampler was unable to take the sample because no liquid was detected Sampler Shut Off The sampler was unable to take the sample because it was halted with the ON OFF key during the sample event 3 18 Run State A sampler in the run state is executing the sampler s instructions according to the settings you ve entered in the program and con figure sequences To start a sampling program and place t...

Page 141: ...he next sample event The bottle set consists of four bottles The sampling program requires that four samples be placed in each bottle of the set 1 OF 4 BTLS 1 4 AT 6 00 5 55 33 Indicates the sample and bottle number of the next sample event The current time appears in the lower right corner The sampling program requires that you use one bottle per sample event and that you switch the bottles on a ...

Page 142: ...nt The sampling program requires three bottles per sample event BOTTLES 5 7 AFTER 25 PULSES Indicates the number of the upcoming sample the total number of samples each bottle is to receive and the current bottle number This display indicates that four samples are to be deposited in each bottle 1 OF 4 BOTTLE 1 AFTER 10 PULSES Indicates the sample and bottle numbers of the next sample event The bot...

Page 143: ...he next sample and the total number of samples for time paced routines The current time is shown in the lower right corner SAMPLE 1 OF 12 AT 6 00 5 43 33 Indicates the sample number of the next sample and the total number of samples for flow paced routines SAMPLE 1 OF 12 AFTER 10 PULSES Indicates a sample in progress BOTTLE 1 PUMPING 200 ml ...

Page 144: ...3700 Portable Samplers Section 3 Programming Guidelines 3 110 ...

Page 145: ...a shorter pump tube and install the optional composite shut off float cage assembly With the portable com plete the preparation by the adding a composite sample con tainer and locating ring in the standard bottle base or an optional composite base With the compact remove the inner sleeve and install the proper bottle configuration for composite sampling These are the listed steps needed to convert...

Page 146: ...tainers in the standard sample bottle tub you must have the standard base composite bottle locating deck with the 3700 Standard Installing the Deck in the 3700 Standard Prepare the standard bottle base by first removing the retaining ring and sample bottles Then place the locating deck open side down in the bottom of the sample bottle tub The locating deck has two recessed areas the deeper recess ...

Page 147: ... flow meter connector located on the rear of the sampler Closed pipe flow meters are connected to the sampler s Flow Meter port using the Teledyne Isco 4 20 mA Input Interface device see Appendix B Accessories Your sampler has an additional connector labeled PRINTER used to connect the sampler to an Isco Field Printer or laptop computer Both the flow meter connector and the printer con nector use ...

Page 148: ...of the contact closure must be directly proportional to total flow Teledyne Isco offers both a connector and cable clamp to connect a non Isco Flow meter to the 3700 samplers Connect the flow meter pulse output to the A and C pins of the 6 pin Flow Meter connector on the 3700 Figure 4 2 Refer to your flow meter s instruction manual for further details A B C D E F Table 4 1 Flow Meter Connector Wir...

Page 149: ...00 Sampler can also be used with flow meters having other types of outputs for example a 4 to 20 mA output directly proportional to the flow rate However these flow meters require a special interface device to convert their output signal to one compatible with the 3700 sampler The 4 20 mA Sampler Input Interface converts 4 to 20 mA output signals from both non Isco Flow meters and closed pipe flow...

Page 150: ...tuator can be found in the discussion of the Enable Pin configure option in Section 3 9 14 4 3 5 Master Slave Connections Using samplers in master slave configuration operates samplers in pairs while one sampler performs a sampling routine the other sampler awaits a command to begin sampling Installing two samplers as master and slave near manholes allows you to double the sampling capacity thereb...

Page 151: ...e you want to sample continuously or for storm water runoff monitoring In continuous sampling applica tions service each sampler when it terminates its routine After servicing press the START SAMPLING key to start the sampler again and resume the master slave cycle The samplers can cycle continuously because each has the same role and usually iden tical sampling routines If you use a master slave ...

Page 152: ...3700 Portable Samplers Section 4 Options and Interfacing Equipment 4 8 ...

Page 153: ...n a cleaning solution and pumping this solution through the tubing system using the pump forward and pump reverse keys Follow with a clean water rinse Sample Bottles The glass sample bottles have a wide mouth to facilitate cleaning You can wash them with a brush and soapy water in a dishwasher or in an autoclave Do not autoclave the plastic lids The 1000 ml polypropylene plastic wedge shaped sampl...

Page 154: ...l 1 Do not reuse sample tubing No cleaning required Use new sample tubing for each new sampling setup 2 Use PTFE tubing where samples for organics are to be col lected Teledyne Isco Pump Tube 1 Rinse by pumping hot tap water through tubing for at least 2 minutes 2 Acid wash tubing by pumping at least a 20 solution of hydrochloric acid through tubing for at least 2 minutes 3 Rinse by pumping hot ta...

Page 155: ...er the constant mechanical strain placed on the tubing by the peristaltic action of the pump eventually causes the tubing to fatigue and fail Remove the cover periodically to inspect the pump tubing for wear inside the pump Check the tubing for cracks where the pump roller compresses the tubing Replace the worn out pump tubing with a new pump tube if necessary Note The importance of regular tubing...

Page 156: ...3 Unscrew the distributor arm retaining nut indicated in Figure 5 1 and pull the arm off the distributor shaft Do not manually rotate the distributor arm CAUTION Do not attempt to manually rotate the distributor arm Severe damage to the distributor drive mechanism may result 4 Pull the pump tube out of the distributor arm and coil spring assembly 5 Turn the center section back over and pull the tu...

Page 157: ...Portable Samplers Section 5 Routine Maintenance 5 5 Figure 5 1 Interior of 3700 Standard Center Section View of the Pump Tube Distributor Arm Located at Bottle 1 Pump Tube Port Distributor Arm Retaining Nut ...

Page 158: ... Figure 5 2 Liquid Detector and Pump Housing Figure 5 3 Interior of Liquid Detector and Pump Housing Liquid Detector Captive Thumb Screws 6 Outer Pump Housing Inner Pump Housing Pump Rotor Machine Screw Pump Shaft Locate bands here to correctly place tubing ...

Page 159: ...that its lid is tightly attached to its base Be sure to tighten the two captive thumbscrews tightly 6 Feed the free end of the tube down through the pump tube port in the center section 7 Turn the center section over again and feed the end of the tube into the coil spring 8 Pull the tube through the coil spring and carefully insert the tube into the body of the distributor arm 9 Feed the end of th...

Page 160: ...allation of the bulk tubing Remove the suction line from the pump tubing by detaching the tube coupling see Section 2 4 1 If you must use a completely new suction line strainer assembly of the standard 10 or 25 foot length install it as described in Section 2 4 1 Bulk Suction Line If you are using bulk suction line to replace the old line detach the old line from the tube coupling and remove the s...

Page 161: ...e 10 screws indicated in Figure 5 4 around the outer rim of the control box bezel and carefully lift the bezel and cover off the control box Inspect the Control Box If there is a leak repair it by referring to the previous section or by returning the control box to the factory The factory has specialized equipment to detect leaks and thoroughly test the units after repair Renewing the Desiccant If...

Page 162: ... cover coat the cover s gasket with a light film of silicone grease to seal the control box Tighten the 10 screws that hold the control box cover and bezel in place using an even cross torquing pattern Figure 5 4 Location of 10 Screws on Control Box Lid Screws 10 Humidity Indicator ...

Page 163: ...3700 Portable Samplers Section 5 Routine Maintenance 5 11 Figure 5 5 Internal Desiccant controller lid removed Grounding Strap Desiccant Bags 3 ...

Page 164: ...3700 Portable Samplers Section 5 Routine Maintenance 5 12 ...

Page 165: ... Go to Training and Support and select Product Support Click Automatic Wastewater Sam plers In the left margin click Schematics Enter the serial number of your instrument then click Get Schematics to view a list of PDF files that contain the available schematics 6 1 1 If Serious Problems Occur If you suspect an electronic problem Teledyne Isco strongly rec ommends calling the Teledyne Isco Technic...

Page 166: ...n in Figure 6 1 4 Unscrew the distributor arm retaining nut indicated in Figure 6 1 and pull the arm off the distributor shaft 5 Pull the pump tube out of the distributor arm and coil spring assembly and feed it out of the pump tube port in the center section 6 You can then remove the control box by unscrewing the six screws indicated in Figure 6 1 and lifting the center section off the control bo...

Page 167: ...rpeted floors movement of woolen or synthetic clothes over chair seats workbenches etc are high enough to destroy CMOS circuitry when you are performing repair work To gain access to the electronic components housed in the control box 1 Disconnect the power source from the sampler 2 Remove the 10 screws around the outer edge of the con trol box lid as indicated in Figure 5 4 Distributor Arm Retain...

Page 168: ... and lift off the shield This reveals the main circuit board shown in Figure 6 3 6 To remove the circuit board assembly from the control box cover unscrew the four hex threaded stand offs and the Phillips head screw shown in Figure 6 2 You can now pull the circuit board away from the control box cover 7 To disconnect the circuit board assembly from the cover disconnect the connector shown in Figur...

Page 169: ...n the Access to Electronic Components section Follow the steps below to gain access to these and other components in the lower section of the control box 1 Disconnect power from the unit 2 Remove the 2 nuts and the screw shown in Figure 6 4 Remove the ground strap by removing the remaining screw 3 Lift the plastic tray straight up out of the control box 4 The distributor gear case can be removed f...

Page 170: ...rews 3 Remove the pump tubing from the interior of the pump 4 Remove the pump rotor by loosening the machine screw and lock nut attaching the rotor to the pump shaft Figure 5 3 shows the location of the machine screw Rotate the rotor until you can reach the screw with a screwdriver inserted through the pump housing inlet sleeve 5 Slide the rotor off the pump shaft 6 Remove the inner pump housing b...

Page 171: ...es over chair seats workbenches etc are high enough to destroy CMOS circuitry when you are performing repair work Ideally all tools soldering irons etc should be grounded and you should conduct all work on a grounded metal workbench with a grounding strap worn around your wrist Obviously in field repair situations such precautions are impractical However you must avoid certain extreme hazards 1 Ne...

Page 172: ...ging Foil is satisfactory metallic plastic bags are also available and work well If you purchase replacement components that do not come in marked protective pack aging do not use them They may already be destroyed 8 Once assembled and soldered printed circuit boards are easily damaged by improper repair procedures Do not attempt to remove components particularly ICs from printed circuit boards un...

Page 173: ...re 6 7 The display module attached to the main circuit board also contains a small circuit board This module is fully assembled when pur chased It does not contain any user serviceable parts Unless the display module is being replaced do not disturb it 6 3 2 Main Board P4 supplies power to the circuitry pin 1 is ground and pin 2 is 12 volts A 5 volt switching regulator IC U11 obtains a 5 volt rail...

Page 174: ...control box produces a signal proportional to an induced strain on the pump tubing This signal is routed through P8 to IC U15 and its associated circuitry where it is massaged into a YES or NO indication of liquid presence IC U15 the main circuit component of the detection system contains a switched capacitor low pass filter and two Op Amps A collection of transistors resistors and diodes are used...

Page 175: ...3700 Portable Samplers Section 6 Servicing 6 11 Figure 6 6 Main Circuit Board Component Layout OUT OUT OUT OUT OUT OUT ...

Page 176: ...tate then starts the pump by sending a high signal through pin 3 of P7 By waiting for the relay to change state before applying power you can prevent arcing at the relay contacts The LED photo transistor device IC201 is a key element of the pump revolution count sensor Whenever the pump is running power is supplied to IC201 A rotating disk positioned between the LED and photo transistor periodical...

Page 177: ...The following section briefly describes the method by which the sample volume is determined The 3700 uses a peristaltic pump to transport the sample from the source to the sample bottle When compared with other suction lift sample gathering methods the peristaltic pump has numerous advantages sim plicity reliability no requisite metering chamber an easy to clean design etc 6 4 1 Volumetric Determi...

Page 178: ...of factors other than those dis cussed above Thus even with the sophistication of the sample volume measuring functions of the 3700 the volume of sample deposited in the sample bottle may vary from the pro grammed value The repeatability of a sample volume from sample to sample which normally is the most important consid eration is typically within the 10 ml specification ...

Page 179: ...ent parts listings including part descriptions and order numbers Replacement parts can be purchased by contacting Teledyne Isco s Customer Service Department Teledyne Isco Inc Customer Service Department P O Box 82531 Lincoln NE 68501 USA Phone 800 228 4373 402 464 0231 FAX 402 465 3022 E mail IscoInfo teledyne com ...

Page 180: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 2 ...

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Page 184: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 6 60 3703 262 REV J 3 2 ...

Page 185: ...EMBLY 9 60 9004 132 BOTTLE CARRIER 24 BOTTLE 10 60 2903 006 500ML SAMPLE BOTTLE 11 299 0334 00 CAP WITH FOAM LINER 500ML POLYPROPYLENE 12 60 3704 111 BOTTLE HOLD DOWN CORD ASSEMBLY 13 489 0002 00 CABLE CLAMP NYLON 3 8 X 14 15 291 0000 00 GLASS BOTTLE 2 5 GALLON WITH CAP BALE 16 299 0013 04 BOTTLE 2 5 GALLON WITH CAP NALGENE 17 60 3704 186 GLASS CAP ASSEMBLY TEFLON LINED 18 291 0011 10 BOTTLE 375ML...

Page 186: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 8 ...

Page 187: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 9 Screw 10 32 x 3 4 Locknut 10 32 Flat Washer 8 Lock Washer 8 Screw 8 32 x 3 4 6 For mounting controller to center section ...

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Page 194: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 16 ...

Page 195: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 17 ...

Page 196: ...3700 Portable Samplers Appendix A Replacement Parts Lists A 18 ...

Page 197: ...er locking assembly 68 6700 111 Model 3700 Sampler controller with pump tubing 68 3700 004 Extra 24 bottle base with 24 polypropylene bottles 1000 ml with caps 60 3704 033 Extra 24 bottle base with 24 glass bottles 350 ml with caps 60 3704 031 Extra 12 bottle base with 12 one quart bottles with caps liners 68 3700 019 Extra 12 bottle base with 12 one liter round polypropylene bottles with caps 68 ...

Page 198: ... quantity 500 Includes instruction sheet 68 6700 114 ProPak disposable bags 1 liter polyethylene quantity 1 000 Includes instruction sheet 68 6700 096 Holder retaining ring for 24 ProPak holders 60 9003 475 B 3 Suction Lines and Strainers 3 8 ID 10 vinyl suction line with standard weighted polypropylene strainer 60 9004 378 3 8 ID 25 vinyl suction line with standard weighted polypropylene strainer...

Page 199: ...44 028 Connect cable for external 12 VDC power source terminates in heavy duty battery clips 60 1394 023 B 5 Interfacing Equipment 1640 Liquid Level Actuator 60 1644 000 1640 Instruction Manual 60 1644 009 Connect cable 25 Teledyne Isco sampler to Isco Flow meter 60 3004 107 Connector only without cable for use with non Isco Flow meters with an isolated contact closure proportional to flow 68 1680...

Page 200: ...3700 Portable Samplers Appendix B Accessories B 4 ...

Page 201: ...ired C 1 Practical Safety Precautions The following procedures are those used by Black Veatch a respected consulting firm and are published here by permission Field personnel must keep safety uppermost in their minds at all times When working above ground rules of common sense and safety prevail However when entering manholes strict safety procedures must be observed Failure to do so could jeop ar...

Page 202: ...ng When a gasoline engine blower is used it must be located so that exhaust fumes cannot enter the manhole If testing equipment is not available the manhole should be assumed to contain an unsafe atmosphere and forced ventilation must be provided It should never be assumed that a manhole is safe just because there is no odor or the manhole has been entered previously 4 Entering Manholes Since the ...

Page 203: ... with a properly designed hook Use of a pick ax screwdriver or small pry bar may result in injury A suitable tool can be made from 3 4 inch round or hex stock Two inches of one end should be bent at a right angle and the other end should be formed into a D handle wide enough to accommodate both hands Even with this tool care must be exercised to prevent the cover from being dropped on the toes The...

Page 204: ...ts in print that do not reflect true conditions One of the most common errors is the assumption that people have died from a lack of oxygen The human body is able to function very well with substantially reduced oxygen concentra tions No one worries about going to Santa Fe New Mexico elev 2 100 meters where the partial pressure of oxygen is equal to 16 2 a normal atmosphere is about 21 oxygen When...

Page 205: ...eaths elsewhere in the world The presence of H2S in a sewer atmosphere is easily deter mined A bellows and ampoule type of tester is very satisfactory for the purpose even though it is only crudely quantitative When using a tester of this type do not bring the air to the ampoule by way of a tube as this may change the H2S concen tration Hang the ampoule in the air to be tested with a suction tube ...

Page 206: ...he top who can lift you out C 3 Hazardous Gases The following table contains information on the properties of hazardous gases Table C 1 Hazardous Gases Gas Chemical Formula Common Properties Specific Gravity or Vapor Density Air 1 Physiological Effect Max Safe 60 Min Exposure ppm Max Safe 8 Hour Exposure ppm Explosive Range by vol in air Limits lower upper Likely Location of Highest Concentration ...

Page 207: ... Irritates respi ratory tract Kills most ani mals in a very short time at 0 1 4 1 At bottom Chlorine cylinder and feed line leaks Detectable odor at low concentra tions Formal dehyde CH2O Colorless pun gent suffocating odor 1 07 Irritating to the nose 10 7 0 73 0 Near bottom Incom plete com bustion of organics Common air pollut ant fungi cide Detectable odor Gasoline C5H12 to C9H20 Volatile solven...

Page 208: ...trogen N2 Simple asphyx iant Colorless tasteless Non flammable Principal constit uent of air about 79 0 97 Physiologically inert Near top but may be found near bottom Sewer gas sludge gas Also issues from some rock strata Oxygen deficiency indicator Nitrogen Oxides NO N2O NO2 Colorless Colorless sweet odor Reddish brown Irritating odor Deadly poison 1 04 1 53 1 58 60 to 150 ppm cause irritation an...

Page 209: ...ble gas indicator Turpentine C10H16 Colorless Char acteristic odor 4 84 Eye irritation Headache diz ziness nausea irritation of the kidneys 100 At bottom Solvent used in paint 1 Detectable odor at low concentration s 2 Combustible gas indica tor Xylene C8H10 Colorless flam mable 3 66 Narcotic in high concentrations less toxic than benzene 100 1 1 7 0 At bottom Solvent Combustible gas indicator Per...

Page 210: ...3700 Portable Samplers Appendix C General Safety Procedures C 10 ...

Page 211: ...elect CONFIGURE to access the configure sequence Display 1 PROGRAM CONFIGURE SAMPLER This informational display appears when you stop the pump with the STOP key after pressing the PUMP FORWARD key It reports the number of pump counts detected while the pump was in operation Exit this display by pressing any key except STOP and ON OFF Display 3 COUNTS FORWARD This informational display appears when...

Page 212: ...rst and second bottle groups concurrently Select AFTER to collect samples for the second bottle group after the sampler has filled the first bottle group Display 16 DURING AFTER FIRST GROUP This display appears after you select STORM in Display 12 Enter the amount of time between the time the sam pler is enabled and the first sample event for the second bottle group Display 17 ___ MINUTE DELAY TO ...

Page 213: ...ppears when you have selected SAMPLES PER BOTTLE in Display 36 In the extended programming mode it appears when the sampler is configured for 2 8 or 24 bottles and there is only one bottle set Enter the number of samples you want deposited in each bottle Display 31 SAMPLES PER BOTTLE 1 MAX Select YES if you want the routine to perform bottles per sample or samples per bottle multiplexing Select NO...

Page 214: ...isplay 43 The display will also appear if you start the routine after the programmed switch time Display 47 FIRST SET CHANGE AT HH MM MM DD This display appears when the sampler is configured for 2 4 8 12 or 24 bottle configurations under uniform time flow or nonuniform time modes of sample pacing Select YES to sample continuously Select NO to stop the sam pling routine after the last set of bottl...

Page 215: ...DD MMM This display appears when you have selected YES in Display 90 Enter the start time and date for the flow pulse countdown This display will also appear if you have initiated the routine after a programmed start time so that you can reprogram the start time Display 92 START FLOW COUNT AT HH MM DD MM This display is the last display of the storm branch It appears when you select YES in Display...

Page 216: ...available for customers who still have Field Printers The printed results include data for sample events completed when you pressed the display status key Display 148 REVIEW PRINT PROGRAM INFORMATION This display appears after you select Print in Display 148 Select NO to return to standby Select Settings to print the settings report Select RESULTS to print the results report Display 149 PRINT PROG...

Page 217: ...isplay 230 Select VINYL if you are using vinyl suction line PTFE if you are using PTFE suction line Display 231 SUCTION LINE IS VINYL PTFE Suction Line configure option Enter the length of the suction line Do not include the tube coupling or the strainer in the length measurement Display 232 SUCTION LINE LENGTH IS FEET 3 99 Liquid Detector configure option Select ENABLE to turn on the Liquid Detec...

Page 218: ...iform Time configure option Select CLOCK TIME to enter the nonuniform time intervals as clock times Dis play 26 Select MINUTES to set the nonuniform intervals in minutes Display 27 Display 280 ENTER INTERVALS IN CLOCK TIME MINUTES Calibrate Sampler configure option Select ENABLE to add calibration displays to the program sequence Select DISABLE to omit the calibration displays Display 290 ENABLE D...

Page 219: ...val countdown continue while the sampler is disabled Display 324 INHIBIT COUNTDOWN YES NO Event Mark configure option Select CONTINUOUS SIGNAL to send a variable duration event mark signal from pin E of the flow meter connector Select PULSE to send a 3 second event mark signal Display 330 CONTINUOUS SIGNAL PULSE Event Mark configure option This setting appears when you select CONTINUOUS SIGNAL in ...

Page 220: ...3700 The controller will not allow you to make any changes to a program or configure sequence setting until you enter the pass number when requested Select DISABLE to turn the pro gram lock off Display 360 ENABLE DISABLE PROGRAM LOCK Sampler ID configure option Enter the sampler identification here The sampler will accept as many as 10 characters including periods press resume sampling dashes pres...

Page 221: ...lating how much flow based on the average flow rate occurs during that time interval For example assume that the average flow is 2 5 MGD and it is desired to collect a sample every 30 minutes The flow increment between samples is calculated 2 5 MGD 2 500 000 GAL DAY 2 500 000 GAL DAY X 1 DAY 24 HR X 1 HR 60 MIN 1736 GAL MIN 736 GAL MIN X 30 MIN SAMPLE 52 080 GAL SAMPLE Thus the desired flow increm...

Page 222: ... the total time over which the composite sample is to be collected The total number of samples to be collected is determined by first calculating the total flow volume over the sampling period and then dividing this by the flow increment between samples For example assume that the average flow is 2 5 MGD the flow increment between samples is 50 000 gallons and the composite sample is to be collect...

Page 223: ... be a prudent choice For critical applications cali bration of the sample volume can be used It is important to select an individual sample volume which will not result in an overfilled sample container under worst case conditions The nominal volume of the composite sample may be calculated by multiplying the programmed nominal sample volume by the total number of samples to be collected In the ex...

Page 224: ...3700 Portable Samplers Appendix E Calculating Flow Increment Between Samples E 4 ...

Page 225: ...er device a each sample event Each time the flow meter receives an event mark pulse the flow meter places a mark on the its recording chart Marking the recording chart cross references the charted flow with the sample events Multiplex sampling There are two types of multiplexing samples per bottle and bottles per sample In samples per bottle multiplexing a bottle receives samples from more than on...

Page 226: ...s crete sample volumes placed in each bottle Sampling program See sampling routine Sampling routine A sampling routine also called a sampling program is the process of taking samples according to the program settings you enter when programming and configuring the controller The program settings define the sample pacing distribution volume and key clock times Suction head Suction head is the vertic...

Page 227: ... Safety Data Sheets This appendix provides Material Safety Data sheets for the internal desiccant used in the 3700 sampler Specific questions regarding the use and handling of these products should be directed to the manufacturer listed in the MSDS ...

Page 228: ...rphous Silica 63231 67 4 99 PEL 20 RESPIRABLE TLV 5 LIMIT NONE HAZARD IRRITANT Synthetic amorphous silica is not to be confused with crystalline silica such as quartz cristobalite or tridymite or with diatomaceous earth or other naturally occurring forms of amorphous silica that frequently contain crystalline forms This product is in granular form and packed in bags for use as a desiccant Therefor...

Page 229: ...nd from venting safety device or any discoloration of the tank due to fire SECTION V HEALTH HAZARD DATA Health hazards may arise from inhalation ingestion and or contact with the skin and or eyes Ingestion may result in damage to throat and esophagus and or gastrointestinal disorders Inhalation may cause burning to the upper respiratory tract and or temporary or permanent lung damage Prolonged or ...

Page 230: ...nel need protection against inhalation of dusts or fumes Eye protection is required Vacuuming and or wet methods of cleanup are preferred Place in appropriate containers for disposal keeping airborne particulates at a minimum SECTION VIII SPECIAL PROTECTION INFORMATION Respiratory Protection Provide a NIOSH MSHA jointly approved respirator in the absence of proper environmental control Contact you...

Page 231: ...ontained herein is based upon data considered true and accurate However United Desiccants makes no warranties expressed or implied as to the accuracy or adequacy of the information contained herein or the results to be obtained from the use thereof This information is offered solely for the user s consideration investigation and verification Since the use and conditions of use of this information ...

Page 232: ...H20 1 2 1 Vapor Pressure mm Hg and Temperature N A Melting Point N A Vapor Density Air 1 N A Evaporation Rate __________ 1 N A Solubility in Water Insoluble but will adsorb moisture Water Reactive Not reactive but will adsorb moisture Appearance and Odor Purple crystals no odor Section 3 Fire and Explosion Hazard Data Flash Point and Methods Used N A Auto Ignition Temperature N A Flammability Limi...

Page 233: ... at least 2 glasses of water Section 6 Control and Protective Measures Respiratory Protection Specify Type Use NIOSH approved dust mask or respirator Protective Gloves Light cotton gloves Eye Protection Safety glasses VENTILATION Local Exhaust Mechanical General Special TO BE USED Other Specify Other Protective Clothing and Equipment None Hygienic Work Practices Avoid raising dust Avoid contact wi...

Page 234: ...3700 Portable Samplers Appendix G Material Safety Data Sheets G 8 ...

Page 235: ...d Stored Program 3 44 Master Slave 3 48 Nonuniform Time 3 47 Portable Refrigerated 3 39 Program Lock 3 52 Programming Mode 3 42 Purge Counts 3 52 Run Diagnostics 3 52 Sampler ID 3 52 Save Current Program 3 45 Set Clock 3 38 Start Time Delay 3 47 Stop Resume 3 47 Suction Line 3 40 Tubing Life 3 52 D Data Retrieval 1 9 Delay 3 47 3 64 Desiccant 5 9 Diagnostics 3 52 Disassembly 2 1 Display Index D 1 ...

Page 236: ... 3 52 Samples Cooling 2 2 Recovery 2 7 Sampling Cycle 3 2 Distribution 3 3 Event Cycle 6 13 Event Mark 3 50 Events 3 2 Flow Mode 3 46 Initiation 3 104 Intervals 1 3 Master Slave 1 5 3 48 4 6 Multiplex 1 3 Nonuniform Time 3 47 Pacing 3 3 Programming 3 42 Start Times 1 5 Stop Resume 3 47 STORM 1 4 3 7 3 67 Volume Delivery 6 13 Volumes 1 5 Samplink 1 9 Servicing CMOS Circuitry 6 7 Controller 6 1 Dist...

Page 237: ...摞尐㻑ⅴₚᇭ O Represent the concentration of the hazardous substance in this component s any homogeneous pieces is lower than the ST standard limitation X 嫷䯉年㦘㹡㦘䓸德咂年捷ↅ䤓㩟德㧟㠨䤓摞怔 ST 㪖屓䤓棟摞尐㻑ᇭ 㷳㫈㗽棔 ₙ嫷㓢 X 䤓㔏㦾扪嫛扪㷴広㢝ᇭ X Represent the concentration of the hazardous substance in this component s at least one homogeneous piece is higher than the ST standard limitation Manufacturer may give technical r...

Page 238: ......

Page 239: ...Performance Criteria EN61000 4 2 Electrostatic Discharge Level 2 4kV contact discharge Level 3 8kV air discharge A A EN61000 4 3 Radiated RF Immunity 80 MHz to 1000MHz 80 AM at 1kHz Level 1 10V m A EN61000 4 4 Electrical Fast Transient Level 2 2kV on ac lines A EN61000 4 5 Surge on AC Lines 2kV common mode 1kV differential mode A EN61000 4 6 Conducted RF on AC lines 150 kHz to 80 MHz 3V rms 80 mod...

Page 240: ......

Page 241: ... issued from Teledyne Isco The warrantor is Teledyne Isco Inc 4700 Superior Lincoln NE 68504 U S A This warranty applies to the USA and countries where Teledyne Isco Inc does not have an authorized dealer Customers in countries outside the USA where Teledyne Isco has an authorized dealer should contact their Teledyne Isco dealer for warranty service In the event of instrument problems always conta...

Page 242: ......

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