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Maintenance & Troubleshooting

Replacing the Pyrolyzer Heater

Thermo Fisher Scientific

SOLA II User Guide 10-5

Warning

The pyrolyzer can be extremely hot, even after power is turned off.

Use extreme care to prevent burns!

The pyrolyzer heater is enclosed in the pyrolyzer housing, which is shown in
the figure below.

Figure 10–2. Pyrolyzer housing

The following table lists the part numbers for the parts referenced in this
procedure. With the exception of the heater being replaced, the existing parts
can be reused if in good condition. The part numbers are provided here for
convenience.

Replacing the

Pyrolyzer Heater

Summary of Contents for SOLA II

Page 1: ...SOLA II Sulfur Online Analyzer User Guide P N 90 1307 0 Revision AB Part of Thermo Fisher Scientific...

Page 2: ...SOLA II Sulfur Online Analyzer User Guide P N 90 1307 0 Revision AB...

Page 3: ...rning is a registered trademark of Dow Corning Corporation All other trademarks are the property of Thermo Fisher Scientific Inc and its subsidiaries Thermo Fisher Scientific Thermo Fisher makes every...

Page 4: ......

Page 5: ...O 5625 F 08 2007 Revised per ECO 5921 G 10 2007 Revised per ECO 6018 H 03 2008 Revised per ECO 6230 J 04 2008 Revised per ECO 6320 K 06 2008 Revised per ECO 6419 M 04 2009 Revised per ECO 6903 N 05 20...

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Page 7: ...6 Injection Valve 2 7 Specifications 2 8 Parts List 2 10 Spare Parts 2 15 Storage 2 21 Installation 3 1 Requirements 3 1 Sample Line Installation 3 2 Sample Tubing Preparation 3 2 Electrical Connecti...

Page 8: ...ng a High Calibration 6 20 The Calibrate High Function 6 20 The Recalibrate High Function 6 20 Adjusting the Reading 6 21 Calibration Setup Menu Items 6 22 Density Compensation Setup 6 25 Viewing Alar...

Page 9: ...n A 3 Pyrolyzer Settings A 3 Oven Settings A 11 The Lockout Menu A 18 Rotary Valve Service B 1 Initial Precautions B 1 Valve Disassembly B 2 Cleaning the Valve Body B 3 Cleaning the Rotor B 4 Rotor As...

Page 10: ...idation History F 5 Stream Plot F 5 Detector Status F 6 Alarms Status F 6 Remote Controls F 7 Analyzer Status F 8 Configuration F 8 The X Purge System G 1 Description G 1 X Purge Specifications G 3 In...

Page 11: ...allation J 4 Toxic Hazardous Substances Tables K 1 Connecting to a Sarasota FD910 Density Meter L 1 Purpose L 1 Connections L 1 Connecting One Density Meter to a Dual Stream System L 3 Related Technic...

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Page 13: ...safely install operate and maintain the system described however personnel are still responsible for considering all actions and procedures for potential hazards or conditions that may not have been...

Page 14: ...ytical systems which must be understood by all persons installing using or maintaining the analyzer system This information is designed to aid personnel in the safe installation operation and service...

Page 15: ...els Appropriate precautions must be taken to prevent sparks present in the analyzer environment that may ignite combustible materials Precautions must also be taken to prevent electrical shock if the...

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Page 17: ...transfers a small amount of sample approximately 1 0 L into an air carrier gas The air sample mixture passes through the mixing chamber to ensure complete mixing and then flows to the pyrolyzer The py...

Page 18: ...such as H2S COS methyl mercaptan benzothiophenes dibenzothiophenes sulfides disulfides and thiols Consider the measurement of a sample of diesel gasoline or another common petroleum fraction such as n...

Page 19: ...ure that only light from SO2 is measured Once the proper wavelength of light is selected its intensity is measure by a photomultiplier tube PMT The PMT converts light energy to electrical energy throu...

Page 20: ...UV light onto a mirror assembly The mirror assembly contains four selective mirrors that reflect only the wavelengths that excite SO2 molecules As the excited SO2 molecules decay to lower energy state...

Page 21: ...thing of measurement signal using moving average Measuring total sulfur with the PUVF detection method requires the conversion of all sulfur compounds in the sample to SO2 This is typically accomplish...

Page 22: ...g consists of multiple small tubes encased in a large outer tube Air circulates through the outer tube with sample passing through the inner tube Moisture passes from the sample through the tubing whe...

Page 23: ...asured quantities of the sample stream into a controlled carrier airflow An auxiliary airflow is added to this sample and air mixture The sample then passes to the mixing chamber where it vaporizes if...

Page 24: ...T4 optional with back up purge system standard SOLA II IECEx G Ex pz IIC T Gc T3 and T4 with back up purge system Zone 1 G Ex px IIC T Gb X Purge system T3 and T4 with back up purge system Table 2 2 A...

Page 25: ...ser interface 4 buttons with context sensitive functions Streams Dual streams optional with autostream select or DCS control of stream selection Alarms Standard I O board time out oven pyrolyzer tempe...

Page 26: ...others application dependent Kalrez Viton The following table lists the SOLA II SOLA II Trace parts Note Unless otherwise specified the parts listed below are for the SOLA II and the SOLA II Trace un...

Page 27: ...to mixer TE 8852 Filter detector HA 100153 Filter disposable PUVF inlet not used with Perm A Pure 47 1362 0 Filter inlet 2 micron used for sample and air inlet HA 101291 Filter Perm A Pure Dryer 25 1...

Page 28: ...One year spare parts kit Valco valve gas phase applications 97 1590 0 One year spare parts kit Valco valve liquid phase applications TE 4811 O ring TE 4808 O ring between reaction chamber 63 1150 0 O...

Page 29: ...Socket assembly PMT 97 1646 0 Quick repair kit 97 1644 0 N2 addition field installation 97 1651 0 Solenoid manifold adapter kit 31 0030 Solenoid 24 Vdc 5 port 4 way 2 position manifold mount 31 1367 0...

Page 30: ...nylon 1 4 OD x 0 035 wall 40 0609 Tubing FEP 0 125 OD x 0 062 ID high temperature 40 0600 Tubing 1 8 OD x 0 085 ID 0 020 304SS 97 1591 1 Two year spare parts kit Dinfa valve liquid phase applications...

Page 31: ...8 ID x 5 7 8 OD 1 8 width 1 Thermocouple pyrolyzer S type 4 Rotor liquid sample valve 1 0 l 4 port or 6 port 1 O ring kit for liquid injection valve actuator 1 Filter inline 2 micron 1 8 tube 1 Filter...

Page 32: ...4 Ferrules for pyrolyzer tube fittings graphite 2 Pyrolyzer tube looped 2 Pyrolyzer O ring 5 5 8 ID x 5 7 8 OD 1 8 width 2 Rotor 10 port gas 97 1591 2 Two year spare parts kit Valco valve gas phase a...

Page 33: ...1589 1 Startup spare parts kit Dinfa valve liquid phase applications Qty Includes 4 Ferrules for pyrolyzer tube fittings graphite 2 Pyrolyzer tube looped 2 Pyrolyzer O ring 5 5 8 ID x 5 7 8 OD 1 8 wid...

Page 34: ...8 width 1 Filter inline 2 micron 1 8 tube connections 1 Thermocouple pyrolyzer S type 97 1591 1 Two year spare parts kit Dinfa valve liquid phase applications 1 Slider block 1 2 l 1 UV flash lamp 2 F...

Page 35: ...ort 1 16 150 psi 175 C 1 Optical bench assembly 1 Trigger pak for SO2 bench 1 Pyrolyzer assembly 1 Board power supply for SO2 bench 1 Board flasher supply for SO2 bench 1 PCA SOLA II I O circuit PCBA...

Page 36: ...ve replacement parts P N Description 89 2803 0 Solenoid relay PCB 29 1230 0 Heater for pyrolyzer assembly HA 101812 Ferrules for pyrolyzer tube fittings graphite 30 1025 0 Pyrolyzer tube looped 63 113...

Page 37: ...Guide 2 21 P N Description TE 8666 PUVF flash lamp 89 2897 0 CPU 89 2898 0 I O PCB 85 1164 0 Power supply 24 Vdc DIN rail mount If storing the instrument the storage environment should be protected an...

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Page 39: ...ications Mounting requirements The mounting site must be as close as possible to the sampling point The analyzer must be sheltered from extreme weather conditions Avoid mounting the analyzer in high v...

Page 40: ...n on contact When using isopropyl alcohol avoid breathing the vapors and contact with the skin Appropriate measures must be taken to prevent ignition of the isopropyl alcohol vapors Use isopropyl alco...

Page 41: ...wire copper or tin plated copper power wire rated for at least 600 Vac and 20 A at the required length Warning This apparatus must be earth grounded Warning Installation of this instrument requires an...

Page 42: ...ers Chapter 6 Open Open Analyzer operation for streams is performed as specified in the Stream Setup parameters Chapter 6 Close Shorted to associated ground terminal Remote Measurement Range Control T...

Page 43: ...concentration in the sample Full scale 20 mA DC represents the measured concentration specified in High Range or Low Range depending on range selected Analog Output 2 This 4 20 mA DC signal represent...

Page 44: ...ponse time System gases meet quality and quantity pressure and flow specifications according to Chapter 2 PUVF vent is vented to atmospheric pressure PUVF vent is NOT connected to headers with varying...

Page 45: ...b Ensure the power voltage and frequency matches the instrument requirements c Ensure a suitable circuit breaker and power switch is installed d Ensure the instrument is properly grounded e Inspect al...

Page 46: ...ecified in the application notes shipped with the instrument or as recorded in the system logbook Note that the pyrolyzer and oven do not begin heating immediately due to the safety interlocks Note Th...

Page 47: ...le when the instrument temperatures reach operating levels 8 Allow the analyzer system to stabilize Monitor the measured values on the front panel for consistent analysis readings to determine when th...

Page 48: ...id manifold regulator to 0 psig Doing so blocks sample flow to the injection valve and purges sample from the injection valve 2 Observe reported sulfur value 3 Do not interrupt power instrument air ca...

Page 49: ...ed in an ATEX hazardous area with a T4 rating do not open the oven door for 140 minutes Caution Failure to allow adequate cooling time before opening the oven can lead to equipment damage or injury to...

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Page 51: ...er the passcode as seen in Figure 5 1 2 Press the button below Ent Enter and Figure 5 2 appears 3 To increase the first digit s value press the button below the up arrow Decrease the value by pressing...

Page 52: ...sample flow to the analyzer 4 Apply power to the instrument 5 Analysis begins automatically when the pyrolyzer reaches operating temperature If you need to change the configuration press any button an...

Page 53: ...ght The PUVF includes a system to monitor and compensate for decreases in the UV light output as the bulb ages However in the case of injection valve failure the PUVF system begins rapidly increasing...

Page 54: ...Operation Injection Valve Failure Alarm 5 4 SOLA II User Guide Thermo Fisher Scientific Figure 5 4 Sample diverter valves Figure 5 5 Sample diverter valves functional diagram...

Page 55: ...tream Setup Clock Setup Modbus Setup Dual Range Setup Inject Setup Autocal Setup Alarms Setup Calibration Setup and Density Compensation Setup Figure 6 1 Top level configuration menu 1 Access the subm...

Page 56: ...re 6 4 4 The Average Time submenu allows you to set the averaging time The average time is a period 1 240 seconds during which the analyzer takes SO2 measurements used to determine a moving average of...

Page 57: ...l it reaches the programmed average time Figure 6 6 6 The fast average time provides the ability to respond to changes faster without sacrificing stability achieved using a longer average time Note Bo...

Page 58: ...2 The Stream Mode submenu allows you to configure the analyzer to continuously monitor stream 1 Stream 1 continuously monitor stream 2 Stream 2 or to alternate between the streams Timed Stream Figure...

Page 59: ...o reduce the flow in order to conserve calibration validation standards You can program each stream for high or low flows If equipped with the second stream option the analyzer has NO and NC pneumatic...

Page 60: ...e Thermo Fisher Scientific Figure 6 13 1 Access the Clock Setup menu to change the time and date Figure 6 14 2 Enter the time in hh mm ss 24 hour format and the date in the following screen in mm dd y...

Page 61: ...COM 3 and COM 4 Figure 6 17 2 Select one of the baud rates available for RS485 Com 3 38400 19200 9600 4800 2400 and 1200 bps or select Disable Figure 6 18 3 Set the ID network address for Com 3 The a...

Page 62: ...full scale value When the signal drops below 90 of the low range full scale value the system switches back to low range When Remote Range Select is enabled output scaling is controlled by a remote co...

Page 63: ...on the 4 20 mA signal Figure 6 23 Set the 20 mA scaling for the high and low ranges for stream 2 using the submenus for stream 2 1 Enter the Inject Setup menu to set injection parameters Figure 6 24...

Page 64: ...een 2 and 9999 seconds A 6 port valve injects at each actuator move in both positions Thus if a 6 port valve is used set the rate to twice the desired injection interval Figure 6 26 1 Enter this menu...

Page 65: ...hen an automatic calibration is performed the analyzer calculates the percentage the new calibration factor deviates from the previous calibration factor If the percentage deviation is less than the a...

Page 66: ...e manually initiated adjust reading function Setting both deviations to the same value disables the autocal making it a validation only function The autocal validation functions can be used with a pro...

Page 67: ...Sample Flow alarm is available if the flow meter option is present The set point for the low sample flow alarm is a percentage of the 4 20 mA signal from the flow meter Figure 6 35 3 To set up a Cham...

Page 68: ...ld activate The value can be from 0 to 1200 V Figure 6 37 5 Set up a Lamp Voltage Rate of Change alarm by entering the rate of change in lamp voltage at which the alarm should activate The value can b...

Page 69: ...ect latching the alarm must be acknowledged before it will clear Figure 6 40 8 Set the High Alarm for stream 1 by entering the first level of high concentration for stream 1 at which the alarm should...

Page 70: ...SOLA II calibration Figure 6 43 Prior to calibrating the instrument the sulfur concentration expected at the two points must be entered in the calibration setup menus Configuration Calibration Setup...

Page 71: ...w cal value 0 00 ppm Low cal 555 600 kHz High cal value 100 00 ppm High cal 15000 000 kHz Figure 6 44 Typical SOLA II calibration The high and low calibration can be performed independently Changing e...

Page 72: ...he Calibration Setup menu can be used to correct the calibration by moving the line without changing the slope see Figure 6 47 Enabling the Autocal function will cause the software to perform this cor...

Page 73: ...low calibration value to zero 2 Exit the Calibration Setup menu 3 Reduce the pressure at the solenoid manifold air regulator to zero this is the bottom regulator located in the pneumatic cabinet Lower...

Page 74: ...e concentration of the standard used 2 Step down to the Average Cal Readings screen It is recommended that you set this value to the maximum 240 3 Exit the Calibration Setup menu and go to Configurati...

Page 75: ...through the injection valve 3 Let the reported concentration reach a new value and stabilize 4 Go to Configuration Calibration Setup Recalibrate High Press YES to accept the new high calibration At t...

Page 76: ...structions on the various calibration functions are discussed in the previous sections Figure 6 48 Main menu heading 1 Select the engineering unit related to the concentration entered for the calibrat...

Page 77: ...ne calibration standard and no injections to calibrate the background enter zero See Performing a Low Calibration at Zero for more Figure 6 51 4 Set the number of readings the analyzer should average...

Page 78: ...standard See Performing a High Calibration for more You can do the same for the low concentration standard by accessing the Recalibrate Low menu item not shown See Performing a Low Calibration at Zer...

Page 79: ...ter inputs the densities that correspond to 4 mA and 20 mA must be entered The analyzer maintains a moving average of the 4 20 mA readings and converts the readings to g cc using a linear interpolatio...

Page 80: ...er Guide Thermo Fisher Scientific 1 Enter the Density Compensation Setup menu Figure 6 59 2 Select Live If you are using stream 2 be sure the menu item is for stream 2 Figure 6 60 3 Enter the density...

Page 81: ...he densitometer used Figure 6 62 In the following screen Figure 6 63 enter the density that corresponds to the 20 mA output of the densitometer Figure 6 62 Figure 6 63 The following provides instructi...

Page 82: ...ensation Setup 6 28 SOLA II User Guide Thermo Fisher Scientific 2 Enter the correction factor The value may be from 0 to 9 999 Figure 6 65 Note that when using a correction factor you do not need to e...

Page 83: ...Chapter 7 Viewing Alarms The second top level menu is the View Ack Alarm menu Figure 7 1 Access this menu to review all active alarms Use the up and down arrows to scroll through the alarms individual...

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Page 85: ...TX Pulse UV Control Figure 8 1 The Input Output Test menu consists of four groups of submenus Set Outputs Menu View Mux Analogs 4 20 mA Inputs and View Digital Inputs Figure 8 2 In the Set Outputs gr...

Page 86: ...ream 1 to 4 8 12 16 or 20 mA Stream 2 4 20 mA Press Enter to change the 4 20 mA output for stream 2 to 4 8 12 16 or 20 mA Sample Solenoid Controls the sample diverter Stream 1 Solenoid Controls the va...

Page 87: ...s menu Note that all signals are displayed as raw frequencies Figure 8 4 Following are the analogs in the order they appear within menu 1 ADC 0 Lamp V 2 ADC 1 Chamber Flow 3 ADC 7 Pressure 4 ADC 9 PMT...

Page 88: ...he Watlow alarm input1 I O Board Displays the status of all eight inputs simultaneously Zero 0 denotes open One 1 denotes closed CPU Digital In Dip Switches Displays the positions of dip switches loca...

Page 89: ...g are the menu items within the View Parameters menu Table 8 3 Menu Item Description At line sample Access this item to view the latest at line sample results Sample AVG The Average Concentration of t...

Page 90: ...so displays the gain currently selected PMT Signal kHz The actual frequency proportional to the PMT output also displays the gain currently selected PMT Voltage The input voltage to the PMT Internal T...

Page 91: ...Signal Gain Select the amplifier gain 1 2 5 10 20 50 100 Note The selection is only valid when auto gain is turned OFF Test Gains Place the gain selection under manual control to verify the functional...

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Page 93: ...rom a source other than the regular process input The sample to be analyzed is introduced into the instrument in the same manner that a calibration standard is There are three parameters to configure...

Page 94: ...omputed as a percentage of the computed average If it is less than or equal to the programmed value the analyzer reports a successful sample If it is greater than the programmed value an error is repo...

Page 95: ...st strap is not available be sure to touch a grounded metal object before touching any internal components Handle all printed circuit boards by the edges Carefully observe the instructions in each pro...

Page 96: ...pressure compressed air Use a soft paintbrush or cloth to remove stubborn dirt Use the following leak test procedure to verify that there are no system leaks 1 Set the sample and air regulators for ze...

Page 97: ...ument logbook 10 Allow the analyzer to warm up until it stabilizes Figure 10 1 Three way valve for measuring flow rates 1 Obtain a precision flow measurement instrument such as a bubble meter 2 Ensure...

Page 98: ...2 port and adjust the CLEAN AIR 2 regulator to obtain the required flow 10 Turn the MEAS CLEAN AIR 2 3 way valves to point up for normal operation 11 Restart the analyzer according to Chapter 5 For d...

Page 99: ...event burns The pyrolyzer heater is enclosed in the pyrolyzer housing which is shown in the figure below Figure 10 2 Pyrolyzer housing The following table lists the part numbers for the parts referenc...

Page 100: ...t down the analyzer system Allow the system to cool completely 2 Carefully remove the two sample tubes from the top of the pyrolyzer housing using a backup wrench to keep the stainless steel fittings...

Page 101: ...ion will be attached to the lid Figure 10 4 Carefully lift all of it out to avoid damaging the pyrolyzer tube Figure 10 4 Housing lid with insulation and pyrolyzer tube attached 9 As shown in Figure 1...

Page 102: ...nd the heater wires and remove the wire sleeves Set the sleeves and fittings aside 11 Loosen the thermocouple fitting and remove the thermocouple from the housing Set it aside for re installation late...

Page 103: ...er Scientific SOLA II User Guide 10 9 Figure 10 7 Insert replacement heater into housing Figure 10 8 Heater wires fed through fittings 14 Slide the wire sleeves onto the heater wires Tighten the stain...

Page 104: ...the hole Remove the bit and then carefully feed the thermocouple tube through the stainless steel fitting on the housing Figure 10 10 Tighten the thermocouple fitting to secure it to the housing Figur...

Page 105: ...11 around it Figure 10 13 Figure 10 13 Pyrolyzer housing O ring 19 Gently slide the lid into the housing Note The pyrolyzer tube insulation and Kaowool insulation should still be attached to the lid S...

Page 106: ...ng to the oven enclosure using the screws removed earlier two mounting screws on top of housing two on bottom 23 If necessary reconnect the wires from the oven temperature switches 24 Reconnect the he...

Page 107: ...n will be attached to the lid Figure 10 15 Carefully lift all of it out of the housing Figure 10 15 Housing lid with insulation and pyrolyzer tube attached 3 To remove the existing pyrolyzer tube unsc...

Page 108: ...0 17 Apply the Kaowool insulation 6 Holding the insulation and pyrolyzer tube gently attach the housing lid against the insulation allowing both ends of the tube to come out of the lid approximately 1...

Page 109: ...zer Heater to re install the housing and complete this procedure Coking carbon buildup can occur in the pyrolyzer reaction tube when sample or calibration flow is too high or when there is no airflow...

Page 110: ...the troubleshooting guidelines presented in Table 10 4 may be helpful in isolating the fault Additional information can be obtained from the following sources System drawings Application notes for the...

Page 111: ...2 Sample diverter valve may be inhibiting sample flow Remove the analyzer from suspend mode correct any alarm conditions and or ensure solenoid air manifold is set at 60 psig ALARM displayed Sample Fl...

Page 112: ...e flasher lamp trigger pak or lamp intensity control electronics Replace valve rotor In extreme cases replace entire valve head Check filtration system to ensure particulate is not getting to the inje...

Page 113: ...locations 12320 Cardinal Meadow Drive Sugar Land TX 77478 USA 1 800 437 7979 Unit 702 715 7 F Tower West Yonghe Plaza No 28 Andingmen East Street Beijing 100007 CHINA 86 10 8419 3588 86 10 8419 3580 f...

Page 114: ...ment shall be Buyer s exclusive remedy against Thermo Fisher Thermo Fisher shall not be liable for labor charges or other losses or damages of any kind or description including but not limited to inci...

Page 115: ...ange This appendix provides basic operating instructions and default configuration settings For complete operating information and troubleshooting refer to the EZ ZONE PM PID Controller user s manual...

Page 116: ...sius The percent LED lights when values are displayed as a percentage or when the open loop set point is displayed This LED indicates the status of a profile When lit a profile is running When flashin...

Page 117: ...prior to operation Operations page Used to monitor or change runtime settings Factory Page Used to enable password protection create a custom Home Page and perform other tasks that do not have an effe...

Page 118: ...ne Aggressiveness Critical Critical damped aggressiveness of autotuning calculations User Failure Action User When user switches to manual mode controller sets output power to last open loop set point...

Page 119: ...wer output will never be greater than the value specified and will represent the value at which output scaling stops Table A 5 Pyrolyzer settings Setup Page Output 2 Parameter Default Comment Display...

Page 120: ...ftware Active Level High Action Function User Set Restore Function Instance 1 Table A 8 Pyrolyzer settings Setup Page Global1 Parameter Default Comment Display Software Display Software Display Units...

Page 121: ...y Software Analog Input Value The process value C Input Error The cause of the most recent error Possible displays listed below None Open Fail Shorted Measurement Error Bad Calibration Data Ambient Er...

Page 122: ...ontrol Loop 1 Parameter Default Comment Display Software Display Software Control Mode Auto The loop will use automatic control Autotune Set Point 90 The percentage of the current set point that will...

Page 123: ...1 Parameter Default Comment Display Software Display Software Alarm Low Set Point 5 C The set point that will trigger a low alarm Alarm High Set Point 5 C The set point that will trigger a high alarm...

Page 124: ...rameter that will appear in the custom Home Page Instance ID 1 Table A 16 Pyrolyzer settings Lock Page Lock 1 Parameter Default Comment Display Software Display Software Operations Page 2 The security...

Page 125: ...D 100 Ohm TC Linearization S For Type S thermocouple RTD Leads 2 The number of leads on the RTD wired to this input Units Process The type of units measured by the sensor Scale Low 0 00 The low scale...

Page 126: ...elay 0 0 User Failure Action User When user switches to manual mode controller sets output power to last open loop set point entered by user Input Error Failure Off When an input error switches contro...

Page 127: ...than the value specified and will represent the value at which output scaling begins Output High Power Scale 70 The power output will never be greater than the value specified and will represent the v...

Page 128: ...play Software Display Software Active Level High Action Function User Set Restore Function Instance 1 Table A 23 Oven settings Setup Page Global 1 Parameter Default Comment Display Software Display So...

Page 129: ...il Shorted Measurement Error Bad Calibration Data Ambient Error RTD Error Not Sourced Calibration Offset The offset applied to the input reading to compensate factors that cause the input reading to v...

Page 130: ...the controller will automatically control to Idle Set Point 25 0 C The closed loop set point that can be triggered by an event state Heat Proportional Band 14 0 C The PID proportional band for the he...

Page 131: ...The parameter that will appear in the custom Home Page Instance ID 1 Table A 29 Oven settings Factory Page Custom Setup 2 Parameter Default Comment Display Software Display Software Parameter Active S...

Page 132: ...ance Locked Access Level 1 Display Software Display Software Rolling Password Off User Password 63 Administrator Password 156 Each menu in the Factory page and each page except the Factory page has a...

Page 133: ...UW Type valves After unpacking the valve do not remove the protective tape from the valve ports until you are ready to install the valve As supplied all surfaces are clean and free of contaminants and...

Page 134: ...ot disassemble the valve unless the system malfunction is definitely isolated to the valve perform all other system checks first If disassembly is required make certain that the following instructions...

Page 135: ...the rotor from the valve body with the magnet Once the rotor is removed note the orientation of the rotor tab which is marked with an ID letter denoting the type of seal material Follow these instruct...

Page 136: ...s shown in Figure B 4 2 Insert the rotor into the valve body being careful that the tab does not touch the polished interior of the valve body Make sure the rotor tab Figure B 4 is fully inserted into...

Page 137: ...rotor is replaced If a high temperature valve WT or UWT series is used at less than 300 C it may become sticky or difficult to turn This tendency can usually be eliminated by repeating the conditioni...

Page 138: ...ure O ring kit VICI P N ORT 1 Apply air pressure to the actuator inlet nearest the valve Then use the open end wrench to remove the air supply lines from the actuator Figure B 5 2 Remove the valve and...

Page 139: ...nd the rest of the assembly together pull the female end cap all the way off If the bearing and washers fall out set them aside 6 Repeat the procedure with the actuator inverted so that the cylinder s...

Page 140: ...O rings to be replaced are in the two end caps and the O ring plate The internal end cap O rings are easier to access if the washers and bearing are removed Follow the steps below 1 Use a small screw...

Page 141: ...ft into the O ring plate as far as it will go as shown in Figure B 10 3 Place the washers and bearing in the male end cap thin washers in first as shown Figure B 9 One of the flats on the drive shaft...

Page 142: ...ived Follow the instructions below 1 Switch the actuator from one position to the other several times to make sure that the play in the coupling mechanism has been absorbed 2 Visually inspect the valv...

Page 143: ...to go through the three small O rings Pressing the plate in dislodges the O rings do not press the plate in 6 The two bearing plates are identical except that one has three countersunk holes to accept...

Page 144: ...Rotary Valve Service Rebuild the Assembly B 12 SOLA II User Guide Thermo Fisher Scientific Figure B 12 Exploded view of two position actuator...

Page 145: ...Thermo Fisher Scientific SOLA II User Guide C 1 Appendix C Dinfa Valve Service Figure C 1 Dinfa valve mounting parts locator Figure C 2 Position of heat transfer tube in oven Overview...

Page 146: ...o Fisher Scientific Figure C 3 Dinfa 8 port liquid injection valve sample load position Note To set up two injections minute set the injection cycle to 30 sections and the injection time to 15 seconds...

Page 147: ...alling the insulation in a continuous run starting with the clean air tubing Secure the insulation with a hose clamp 2 Adjust the clean air 2 regulator to 190 cc min approximately 90 psig with the ove...

Page 148: ...Dinfa Valve Service Overview C 4 SOLA II User Guide Thermo Fisher Scientific Figure C 6 Dinfa 8 port liquid injection valve Figure C 7 Close up of slider...

Page 149: ...nal ensure the injection cycle is set for 30 seconds and injection is set for 15 seconds If the analyzer response time is slower with the Dinfa valve The heat transfer tube is not insulated properly o...

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Page 151: ...n the SOLA II standard serial Modbus and a TCP IP Modbus network using 10 Base T TCP IP Bridge board installed inside the SOLA II enclosure SOLA II Modbus configuration must be set to 38400 baud with...

Page 152: ...twork and assign an IP address 1 Locate the IPSetup exe utility that is included with the disk that ships with the TCP IP Bridge option 2 Run the IPSetup exe utility from any IBM compatible PC connect...

Page 153: ...p utility successfully you can access instrument control via the browser interface Open your browser and enter http followed by the IP address into the address line of the browser For example if the I...

Page 154: ...le Format to exit this screen Figure D 5 Accessing this display allows you to view activity for the last 24 hours in a table format You can also save the data and import it into a Microsoft Excel spre...

Page 155: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 5 Figure D 6 Analyzer setup Figure D 7 Stream setup Figure D 8 Modbus setup...

Page 156: ...TCP IP Bridge The Browser Interface D 6 SOLA II User Guide Thermo Fisher Scientific Figure D 9 Dual range setup Figure D 10 Inject setup Figure D 11 Autocal setup...

Page 157: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 7 Figure D 12 Alarm setup Figure D 13 Calibration setup Figure D 14 Density compensation setup...

Page 158: ...orm with additional fields in order to identify the sample With this version you can also print results on any local printer attached to the PC that is running the web browser Figure D 15 At line grab...

Page 159: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 9 Figure D 17 Sample results...

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Page 161: ...ead Input Registers 05 Set Single Coil 06 Set Single Holding Register 15 Set Multiple Coils 16 Set Multiple Holding Registers Table E 2 Coil Number Description 1 Enable Modbus Remotes1 2 Stream Select...

Page 162: ...Reserved 28 Reserved 29 Reserved 30 Reserved 31 Reserved 32 Reserved 33 Reserved 34 Reserved 35 Reserved 36 Reserved 37 Reserved 38 Reserved 39 Reserved 40 Reserved 1 If this coil is set to 1 by the...

Page 163: ...Autocal Error 10008 Purge Fault 10009 Stream Selected 0 Stream 1 1 Stream 2 10010 Valve Fault 10011 Purging 10012 Calibrating 10013 Suspended 10014 Autocal Performed Clear after read 10015 New Cal Fac...

Page 164: ...30007 Reserved 30008 Reserved 30009 Normalized Detector reading kHz 30010 Detector Lamp Voltage 30011 Detector PMT Voltage 30012 Detector Chamber Temperature deg C 10 30013 Detector Lamp Intensity Hz...

Page 165: ...0 Reserved Table E 5 Holding Register Number Description 40001 High Cal Frequency kHz 40002 Low Cal Frequency kHz 40003 Stream 1 Recorder Full Scale 40004 Stream 2 Recorder Full Scale 40005 Injection...

Page 166: ...Set Point 40024 Density 4 mA g cc 1000 40025 Density 20 mA g cc 1000 40026 Stream 1 Recorder Low Scale 40027 Stream 2 recorder Low Scale 40028 Stream 1 Density Correction Factor 1000 40029 Stream 2 De...

Page 167: ...Description 40045 Passcode 40046 Fast Average seconds 40047 Average Override 40048 Grab Sample Average Time 40049 Grab Sample ID 40050 Grab Sample Accepted RSD 40051 Transmix Factor Not Used 40052 St...

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Page 169: ...oppy disk to the c Program Files NationalInstruments Lookout subdirectory on the computer hard drive Remove the disk from the drive and store in a safe place 2 Click on sIIcfg l4p or sIIdl l4p to open...

Page 170: ...ftware F 2 SOLA II User Guide Thermo Fisher Scientific b Select Object Modify Modbus1 Figure F 1 c Edit the Modbus object to select a different COM port or Modbus Ethernet Figure F 2 Figure F 1 Figure...

Page 171: ...obtain the correct IP address b Set the identifier to 1 If a serial port is used for the connection configure the serial port parameters as follows a Select Lookout Options Serial Ports b Verify that...

Page 172: ...by other programs using ODBC or SQL see the Lookout software manual provided with the system or instructions in the software you are using for more information Data from the analyzer is also saved on...

Page 173: ...he screen A trend plot of the densitometer inputs can be displayed by clicking the Trend g cc button Zero and full scale values for the plot are determined by the 4 mA and 20 mA density settings in th...

Page 174: ...reen and returns the plot to real time data display The total time period displayed on the plot can be varied from 5 minutes to 24 hours by moving the slider below the plot area The hypercursor in the...

Page 175: ...controls screen 1 Remote Cal When turned ON this control causes the analyzer to perform a calibration and update the calibration factor The Allowed Deviation and Recal Deviation values are ignored 2 C...

Page 176: ...the main screen display the status of the analyzer by placing a green indicator to the right of Calibrating Purging or Suspended If the indicators are not green the system is running a sample analysi...

Page 177: ...10 psig a time delay relay begins its timed cycle Typically the time delay is used to ensure that at least four volumes of air are exchanged in the enclosures before power is applied to the system The...

Page 178: ...the oven door Instruments with a T4 rating must be allowed to cool for at least 140 minutes before opening the oven door Caution Failure to allow adequate cooling before opening the oven can lead to i...

Page 179: ...lay time delay typically set from 480 to 600 seconds see application notes for individual system X Purge pressure Minimum 10 psig Y Purge pressure analyzer purge Set to approximately 10 psig or as spe...

Page 180: ...r to drawings provided with the system for connection information and power requirements Customers must provide a suitable power switch near the system for use by maintenance personnel Warning Electri...

Page 181: ...g up any analyzer system that uses the X Purge system Caution Do not open the explosion proof X Purge enclosure in a hazardous area even when de energized unless area has been properly tested and is k...

Page 182: ...r pressure regulators set too low c Oven door open or leaking air d Electronic enclosure door open or leaking air 7 Complete the remaining steps listed in the startup procedure included in the startup...

Page 183: ...upon interruption of main analyzer power you may elect to implement one of the following Install the appropriate Intrinsically Safe IS barriers on Modbus and or discrete signals Utilize the X Purge s...

Page 184: ...wer than the initial setting when received from Thermo Fisher Caution If the timer setting is too short the analyzer system is not purged adequately before power is applied This can result in equipmen...

Page 185: ...Thermo Fisher Scientific SOLA II User Guide H 1 Appendix H Software Menu Tree Figure H 1 Top level menus configuration subgroups...

Page 186: ...Software Menu Tree H 2 SOLA II User Guide Thermo Fisher Scientific Figure H 2 Diagnostics subgroups...

Page 187: ...Thermo Fisher Scientific SOLA II User Guide I 1 Appendix I PUVF Optical Bench Figure I 1 Optical bench assembly exploded diagram...

Page 188: ......

Page 189: ...ctronics can process The voltage applied to the PMT is a negative DC voltage and the lower the PMT voltage the greater the sensitivity of the detector Looking at previous applications as examples a SO...

Page 190: ...med purge time Note that the analyzer will not update readings during this period The Dual PMT Supply option requires a different version of the SOLA II software installed in the unit to operate prope...

Page 191: ...on will provide two 4 20 mA signals one for each range If it is desired to monitor only one 4 20 mA signal then Auto Range can be selected A contact output indicates which calibration is used by the a...

Page 192: ...ine Grab Sample function either calibration can be selected to measure the sample If the sample concentration range is unknown the sample can be measured first on the highest calibration range and dep...

Page 193: ...o o o o o Furnace o o o o o o AC DC Distribution x o o o o o Main Power Supply x o o o o o Cabling x o o o o o Indicates that this toxic or hazardous substance contained in all of the homogeneous mat...

Page 194: ......

Page 195: ...eter are connected to the return of the SOLA II supply loop It is acceptable to run three wires between the devices and jumper terminals 2 and 4 together at the density meter and connect either termin...

Page 196: ...three wire terminal block four in total If the jumper is installed the 24VDC current loop power is supplied by the SOLA II If the jumper is left open power is not supplied by the SOLA II For the Sara...

Page 197: ...3 Figure L 5 shows the configuration for using one Sarasota FD910 density meter on a dual stream system Note The jumper for loop power is NOT installed for stream 2 J9 Figure L 5 Sarasota FD910 densit...

Page 198: ......

Page 199: ...ct name SOLA II as the search term and click the Resources tab Table M 1 Technical bulletins TB Title TB 0417 001 Replacing a Watlow Series 93 Temperature Controller with a Watlow EZ ZONE PM6 Series C...

Page 200: ...Thermo Fisher Scientific SOLA II User Guide M 2 THIS PAGE INTENTIONALLY BLANK...

Page 201: ...ith the SOLA II Trace refer to the next paragraph Combustion gas for the SOLA II Trace Results reported from the field as well as measurements conducted in the factory indicate that when the sample ma...

Page 202: ...he performance specifications are not altered that is the repeatability will not be guaranteed to be lower than 1 of 2ppm similarly the limit of detection also remains 1 25 of 2ppm 25ppb The highest r...

Page 203: ...ale 62 5 2 of range example range 200ppm repeatability 4ppm 1 of range example range 200ppm repeatability 2ppm Thermo Fisher Scientific SOLA II User Guide O 1 SOLA 11 for Condensable Vapours CV The SO...

Page 204: ...a certifications Since the SOLA II CV is modified from the standard SOLA II analyser the hazardous area approvals may vary please consult the factory for the latest approvals for installation in hazar...

Page 205: ...Thermo Fisher Scientific 81 Wyman Street P O Box 9046 Waltham Massachusetts 02454 9046 United States www thermofisher com...

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