3-38 | Model 933S UV Analyzer
Sample System Leak Check
The analyzer has been checked at the factory for pressure leaks. However,
fittings can loosen during transport, and the Sample, Vent, and other lines are
installed on-site. Therefore, the entire sample system should be checked for
leaks before any sample gas is introduced into the system for the first time or
following the replacement of any lines/fittings or Measuring Cell parts.
Hazardous Locations
Before proceeding, test the area around the analyzer for explosive
gases and proceed only when the area is found to be safe.
Do not remove the cover of the Explosion-Proof Digital Communica-
tions Port on the front of the Lower Enclosure, do not connect a serial
cable to the Communications Port, do not open the Upper/Lower En-
closures, and do not power up/down the analyzer or computer if there
is an explosive gas atmosphere present.
Preventing leaks in the sample system is critical to ensure proper ana-
lyzer operation. If sample gas migrates into the Optical Bench Assembly
or Reflector Block due to a leak in the Measuring Cell, the optics will
become damaged and most likely require replacement. Most leaks are
preventable with the regular replacement of the Measuring Cell o-rings.
To leak check the sample system:
1. Using the Configurator Software, change the
Flow Control
setting to ‘
0’
(
auto
). Click
OK
then
Apply
. Do not save the changes to EEPROM.
2. If the analyzer uses
Measured
Pressure Compensation (optional),
change it to
Fixed
mode so that a “
f: Sample gas pressure too low
”
alarm does not occur. To do this, view the
Cell/Misc Parameters
dialog
box and enter a value in the
Default Cell Pres
(pressure compensation)
field that is the same as, or approximately, the Measuring Cell pressure.
Refer to “Cell/Miscellaneous (Compensation) Parameters” in Chapter 4.
Close the sample inlet valve. Backpurge the analyzer sample system
with Zero gas for 2–3 minutes.
3. Change the
Flow Control
setting to ‘
4’
(
shut-in/shut-off
). Click
OK
then
Apply
. Do not save the changes to EEPROM.
Bleed down the sample system to atmospheric pressure (check gauge).
To avoid tearing the Membrane Filters in the Filterblock, always bleed
down the sample system pressure on the downstream (outlet) side of
the Filterblock. Pressure differentials of more than 210 KPA (30 PSI)
from the inlet side to the outlet side can tear the Filters and they will
have to be replaced.
!
WARNING
!
CAUTION
!
CAUTION
This procedure
assumes communication with
the analyzer has already been
established.
Setup (tab)
Gas Calibration<<Flow
Control>>
Setup (tab)
Cell/Misc
Summary of Contents for 933S
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Page 52: ...3 6 Model 933S UV Analyzer Figure 3 1 Analyzer backpan dimensions European...
Page 91: ...Installation and Start Up 3 45 Figure 3 24 Column Profile...
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Page 190: ...6 14 Model 933S UV Analyzer Figure 6 3 1 Standard Range Cell 40 cm or smaller...
Page 191: ...Maintenance and Troubleshooting 6 15 Figure 6 3 2 Low Range White Cell 81 2 cm P N 100 1780 1A...
Page 197: ...Maintenance and Troubleshooting 6 21 Figure 6 4 Column Block assembly...
Page 246: ...6 70 Model 933S UV Analyzer Figure 6 18 Microcontroller board P N 100 1781 SW400...
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Page 272: ...A 8 Model 933S UV Analyzer Lower Enclosure Layout WX 14838...
Page 274: ...A 10 Model 933S UV Analyzer RS 232 Communications Cable Connections 300 9480...
Page 279: ...Appendix A Drawings A 15 Optical Bench Board P N 100 1662...
Page 280: ...A 16 Model 933S UV Analyzer PMT Buffer Board 100 0140...
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