Markes International UNITY-Air Server-xr, Руководство по установке

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QUI-1122
Page 3
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3.3.1 Installing the Transfer Line onto the GC ....................................................................... 14
3.3.2 Installing the fused silica transfer line insert ................................................................ 16
3.3.3 Connecting the transfer line to UNITY–Air Server-xr .................................................... 17
3.4 Installing the cold trap ................................................................................................................. 20
3.5 Connecting the Air Server-xr to the UNITY-xr .............................................................................. 23
3.6 Sample line connection ............................................................................................................... 24
3.7 Configuring the dryer (optional) ................................................................................................... 24
3.8 Check for gas leaks ...................................................................................................................... 27
4. Installing Markes Instrument Control (MIC) software .................................................................... 28
4.1 System Configuration ................................................................................................................... 28
4.2 Running the software ................................................................................................................... 28
4.2.1 Configuring the software ................................................................................................ 28
4.2.2 Detecting the UNITY–Air Server-xr ................................................................................. 31
5. Installation qualification .................................................................................................................. 32
5.1 Leak Testing ................................................................................................................................. 32
5.2 Conditioning the cold trap ........................................................................................................... 32
5.3 System checkout .......................................................................................................................... 34
6. Configuration of UNITY–Air Server-xr Electronic Gas Control –
instrument specific guides............................................................................................................... 35
6.1 UNITY–Air Server-xr Electronic Gas Control with the Agilent 6890GC ...................................... 35
6.1.1 Procedure ........................................................................................................................ 35
6.1.2 6890 inlet settings ......................................................................................................... 36
6.2 UNITY–Air Server-xr Electronic Gas Control with the Agilent 7890GC ...................................... 37
6.2.1 Procedure ........................................................................................................................ 37
6.2.2 7890 Inlet Setup ............................................................................................................. 38
6.2.3 7890 Inlet Settings ......................................................................................................... 38
6.3 UNITY–Air Server-xr Electronic Gas Control with the Shimadzu QP 2010 (Plus)
GCMS fitted with AFC ................................................................................................................... 39
6.3.1 Gas connections between UNITY–Air Server-xr and the Shimadzu AFC ..................... 39
6.3.2 Configuring the Shimadzu GC software ........................................................................ 40
6.3.3 Flow stability .................................................................................................................... 41
6.3.4 Ready / Start connections between UNITY–Air Server-xr and Shimadzu GC ............. 42
6.4 UNITY–Air Server-xr Electronic Gas Control with the Thermo DPFC .......................................... 43
6.4.1 Procedure ........................................................................................................................ 43
6.4.2 Configuring the Thermo GC software ............................................................................ 43
6.5 UNITY–Air Server-xr Electronic Gas Control with the Thermo 1300 Series GC ........................ 44
6.5.1 Installing the Markes TD to the Thermo Scientific TRACE Series 1300 GC ............... 44
6.6 Testing the ECC setup .................................................................................................................. 47