Environmental Conditions for An Installation Location........................59
Checking the Contents....................................................................59
Assembling ..........................................................................................60
Removal of Transport Screws ..........................................................60
Tubing Arrangements .....................................................................61
UI Pad...........................................................................................62
Spare Parts Available ............................................................................65
Operation ........................................................................................67
General Information about Entering Parameters ......................................71
Setup ..................................................................................................72
Selecting the Communication Channel..............................................72
Setting the Liquid Crystal Display Contrast........................................73
Setting of Standard Xenon Lamp Lifetime .........................................74
Operating Instructions...........................................................................76
To Adjust the Auto Zero..................................................................76
Setting the Wavelength ..................................................................76
Setting the Utility ...........................................................................77
Setting the GLP Function.................................................................84
Spectrum Measurement ..................................................................91
Setting of Recorder and Spectrum Output Factors.............................95
Operation of Marker .......................................................................98
Setting of Time Program .................................................................98
Edit the Wavelength Program .............................................................. 105
Shutdown Procedure........................................................................... 108
Flushing the Flow Cell After Use........................................................... 109
Before Performing Analysis .................................................................. 110
Characteristics of Organic Solvents ................................................ 112
Cautions on Static Electricity ......................................................... 116
Maintenance..................................................................................117
Operational Check .............................................................................. 119
Performance Check............................................................................. 120
Energy Check of Xe Lamp ............................................................. 120
Check of Wavelength Accuracy by Using Hg Lamp .......................... 120
Check of Sensitivity ...................................................................... 120
Check and Calibration of Wavelength Accuracy ............................... 130
Check of Leak Sensor ................................................................... 132
Periodic Checks .................................................................................. 134
Maintenance & Inspection Methods ...................................................... 135
Energy Check of Xe Lamp ............................................................. 135
Wavelength Accuracy Check Using Hg Lamp................................... 135
Check of Lamp Logbook................................................................ 135
Check and Washing of Flow Cell Unit.................................................... 136
Check and Washing of Flow Cell .................................................... 136
Disassembly and Cleaning of Flow Cell ........................................... 138
Leakage from the Flow Cell ........................................................... 140
Cautions on Storage of the Flow Cell.............................................. 141
Lamp Replacement ............................................................................. 142
How to Replace the Xenon Lamp ................................................... 142
Fuse Replacement .............................................................................. 153
Troubleshooting ............................................................................155
Warnings ........................................................................................... 157
Troubleshooting ................................................................................. 158
Error Messages................................................................................... 160
Appendix .......................................................................................163
DESCRIPTION OF CONTACT SIGNALS .................................................. 165
Outline ........................................................................................ 165
TERMINOLOGY................................................................................... 166
Index.............................................................................................171
Summary of Contents for 200A Series
Page 1: ...SERIES 200A FLUORESCENCE DETECTOR User s Guide LIQUID CHROMATOGRAPHY ...
Page 5: ...Introduction ...
Page 6: ......
Page 15: ...Safety Practices ...
Page 16: ......
Page 17: ......
Page 33: ...Safety Practices 33 Figure 2 2 Overview of the warning labels on the front of the instrument ...
Page 35: ...System Description 35 System Description ...
Page 36: ...36 Series 200a Fi User s Guide ...
Page 55: ...Installation 55 Installation ...
Page 56: ...56 Series 200a Fi User s Guide ...
Page 66: ...66 Series 200a Fi User s Guide ...
Page 67: ...Operation 67 Operation ...
Page 68: ...68 Series 200a Fi User s Guide ...
Page 117: ...Maintenance 117 Maintenance ...
Page 118: ...118 Series 200a Fl User s Guide ...
Page 154: ...154 Series 200a Fl User s Guide ...
Page 155: ...Troubleshooting ...
Page 156: ...156 ...
Page 162: ...162 Series 200a Fl User s Guide ...
Page 163: ...Appendix 163 Appendix ...
Page 164: ...164 Series 200a Fl User s Guide ...
Page 170: ...170 Series 200a Fl User s Guide ...