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Calibration

IV-4

Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide

The Thermo Scientific Orion 2117HL chloride analyzer utilizes pressure,

gravity and fluid dynamics as the principal force of operation for the

fluidic system.

Air Regulation

Figure IV-3

Air Pump

Содержание Orion 2117HL

Страница 1: ...Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide ...

Страница 2: ...nk ROSS Resolution SAOB SMART AVERAGING Smart CheK SMART STABILITY Stacked Star Navigator 21 Stat Face The Enhanced Lab ThermaSense Triode TRIUMpH Unbreakable pH Universal Access are trademarks of Thermo Fisher Guaranteed Success and The Technical Edge are service marks of Thermo Fisher PerpHecT meters are protected by U S patent 6 168 707 PerpHecT ROSS electrodes are protected by U S patent 6 168...

Страница 3: ...r II 1 Mounting and Plumbing Instructions II 2 Sample Requirements II 3 Electrical Wiring II 4 Safety Requirements II 4 Warning Labels and Locations II 5 Wiring the Analyzer II 6 Terminal Assignments II 8 Electrode Wiring Assignments II 9 Installation of New Electrode Cables II 10 Installation of a New Chloride Electrode II 11 Installation of the ATC Probe II 11 Installation of a New Reference Ele...

Страница 4: ...e V 1 Maintenance Schedule V 1 Weekly Maintenance V 1 Monthly Maintenance V 2 Yearly Preventative Maintenance V 4 Chapter VI Troubleshooting VI 1 Diagnostics Mode VI 1 Slope Problems VI 9 Troubleshooting Matrix VI 11 Error Event Codes VI 14 Resetting the Analyzer VI 17 Serial Number and Software Revision VI 18 Service and Repair VI 19 Chapter VII Customer Service VII 1 Notice of Compliance VII 1 W...

Страница 5: ...em The system must optimize the fluidic design with the sensing technology to provide accurate and precise results with an almost instantaneous indication of chloride concentration changes The 2117HL chloride analyzer meets all of the criteria for accurate and dependable chloride monitoring and more The 2117HL analyzer incorporates innovative technologies that include Premium electrodes Accurate a...

Страница 6: ...ble measurements and a wide measurement range with selectable resolution Measures chloride ion activity in aqueous solutions quickly accurately and economically Premium reference and sensing electrodes Superior accuracy and stability over a wide temperature range Advanced flow cell design with air stirring Automatic sample handling and contamination control with no moving parts Patented scrolling ...

Страница 7: ...d then flows into an atmospheric drain via the diverter valve Principles of Operation Safety Drain for Overflow RestrictorTubing Pressurizes Reference Filling Solution Bottle Flow Meter Valve Positions Calibration Mode PUSH Sample Measure Mode PULL Analyzer 1 2 3 4 5 Power 4 20mA Output Air Pump Flow Meter Inlet Valve Bypass Needle Valve and Filter Regulator Valve Reference Solution Calibration Po...

Страница 8: ...nt isopotential point The above equation indicates that the measured potential varies with both temperature and the concentration of the ion of the interest In order to eliminate error caused by fluctuations in sample temperature the 2117HL microprocessor constantly updates temperature corrections from data supplied by the ATC probe From the Nernst equation the theoretical response of a chloride i...

Страница 9: ...bility is reached Adding standard 2 preferably 10 times more concentrated than standard 1 increases the concentration dC2 in the sample reservoir Again the new potential E2 is measured and stored when the reading is stable Now we have the following three unknowns Es Eo S Ts 298 15 log Cs Ciso E1 Eo S T1 298 15 log Cs dC1 Ciso E2 Eo S T2 298 15 log Cs dC1 dC2 Ciso S is the Slope at 25 C 298 15 K T ...

Страница 10: ...ation To perform an offline calibration a sample is taken from the bypass of the analyzer the sample concentration value is stored in memory the sample is analyzed by an alternate method of choice the previously stored reading is adjusted to the lab method result and the analyzer is then returned to the analysis mode The term offline calibration refers only to the fact that a sample from 2117HL an...

Страница 11: ...Display Warning Icon Mode Indicator Keypad Status Indicators Mounting Hole Inlet Valve Pressure Regulator Reference Filling Solution Restructor Tube Assembly Air Pump Bypass Needle Valve Inlet Filter Reagent Manifold Flow Cell Reservoir Siphon Tube Flow Cell Block Flow Meter Calibration Port Diverter Valve Figure I 3 Fluidics Diagram ...

Страница 12: ... Contains the chloride sensing electrode reference electrode and ATC probe Diverter Valve Allows the flow cell reservoir to fill during calibration by forming a closed loop system Chloride Electrode Senses chloride ions in the sample stream and produce an electrical potential dependent on sample concentration Reference Electrode Provides a constant reference potential and completes the measurement...

Страница 13: ...the Setup Mode for instructions A pH ORP module or conductivity module can be added by the operator to the second channel of the Thermo Scientific Orion 2117HL chloride analyzer for the ultimate flexibility in measurement capabilities The 2100 series pH ORP and conductivity analyzers provide accurate and reliable measurements in ultra pure water as well as the harshest industrial environments Comb...

Страница 14: ...emperature probe chloride electrode box reference electrode box chloride standard solutions kit five 2 oz bottles of 29 600 ppm chloride standard the options kit and user guide CD 3 Remove the cardboard retaining shell by sliding it over the entire mounting board and the analyzer 4 Carefully remove the entire mounting board with analyzer from the inner box Note Do not lift or pull the analyzer by ...

Страница 15: ... sampling point as possible This ensures the fastest possible response to a changing sample condition Refer to the Appendix Sample Conditions section For proper flow cell operation the analyzer must be installed straight and level upon its mounting location Failure to level the analyzer may cause poor siphoning in the flow cell 1 Prepare the mounting holes Carefully lift the analyzer and bolt it i...

Страница 16: ...ove moderate amounts of particulates Flow rate 40 mL minute nominal Pressure 8 to 100 psig Consult Technical Support for details on sample handling if the pressure is outside of this range Temperature Temperature must be between 5 and 35 C Chloride level Chloride levels are read directly in ppb or ppm when calibrated with Thermo Scientific Orion 29 600 ppm high level chloride standard Sample alkal...

Страница 17: ... hazard disconnect the power prior to opening the analyzer Before connecting the analyzer to the main make sure that the voltage lies within either range 85 to 132 V 200 mA or 170 to 264 V 100 mA 50 to 60 Hz AC Cutting off the power by disconnecting power source will not reset the analyzer This analyzer incorporates a non volatile memory and will maintain calibration and settings after power failu...

Страница 18: ...follow these instructions may result in injuries The safety warning icons are used in two locations on the analyzer Faceplate Refer to Figure II 2 Power supply Refer to Figure II 3 Note Replace the fuse only with a fuse of same rating Ch 1 status Ch 2 status t Ch 1 t Ch 2 Figure II 2 Faceplate Fuse Holder Fuse Fuse Power Supply Fuse Type 115V 250V 200mA Fast Acting 230V 250V 100mA Fast Acting 170 ...

Страница 19: ...ver 2 mm blade flat head screwdriver 1 Open the faceplate loosen the four screws using a Phillips head screwdriver The electronics faceplate will open via the hinge pin connection 2 Remove one or two of the two unused cable glands as required for wiring power cable or auxiliary connections Power cable optional hole locations are shown in Figure II 4 3 Select and install the appropriate size cable ...

Страница 20: ...ation 6 Plug the terminal connector into the power supply Refer to Figure II 3 7 Select the correct fuse from the fuse kit Install by inserting the fuse in the fuse holder and secure it using the twist and lock method The fuses are clearly labeled with the appropriate voltages for your system Refer to Figure II 3 Refer to the table below for fuse selection AC Voltage Fuse Rating 115V 200mA 250V Fa...

Страница 21: ...2 31 Preamp ground 5 Air pump ISE only 13 Relay 3 32 Shield 6 Shield ground for conductivity 14 Relay 3 33 Shield 7 Do not connect 15 Do not connect 34 Jumper to pin 26 when using preamp 8 Do not connect 16 Temperature ground 17 Temperature drive 18 Temperature sense 19 Solution ground 20 Conductivity drive 21 Conductivity sense 22 Conductivity sense 23 Conductivity drive 24 Reference electrode 25...

Страница 22: ...erature sense Jumper to 17 19 Solution ground Connect red wire 2001SC pH Electrode 24 Reference electrode Connect black wire 26 Sensing electrode Connect clear wire 110250 ORP Electrode 19 Solution ground Connect black wire 24 Reference electrode Connect purple wire 26 Sensing electrode Connect coax center wire 2002CC and 2002SS Conductivity Probes 6 Shield ground for conductivity Connect clear wi...

Страница 23: ...iring location 1 Open the ferrite using a flat tip screwdriver to lift the latch of the ferrite 2 Feed the cable wires through the center of the ferrite and then loop the cable wires around the ferrite core and through the center of the ferrite again 3 Place the ferrite at the bottom of the analyzer chassis near its edge Adjust the ferrite location on the cable so the ferrite is near the top of th...

Страница 24: ... cell cap Refer to Figure II 8 for the location 3 Plug the electrode cable marked Sensing into the top of the electrode Be sure to push back the black cap to verify a secure connection between the male and female pin connection prior to tightening 4 Tighten the screw cap connection to the cable Note Do not twist the cable while tightening the connection Twisting may cause damage requiring prematur...

Страница 25: ...e the 1 4 inch tubing over the sidearm The outside tubing should extend 3 8 to 1 2 inches over sidearm Refer to Figure II 9 5 Remove the cap and fluid seal from reference electrode fill solution bottle Cat No 100057F4 Hold the bottle in an upright position Check that the rubber gasket is properly aligned and then connect the cap end of the tubing assembly to the bottle The 1 8 inch tubing should e...

Страница 26: ... its PVC base abuts the bottle Mark and date the level of filling solution in the reservoir The electrolyte solution will begin to flow into the reference electrode Caution Failure to pressurize the filling solution bottle will lead to noisy and drifting output signals 9 Plug the electrode cable marked Reference into the top of the electrode and tighten the screw cap Be sure to push back the black...

Страница 27: ...n type of board installed and selected measurement parameter D Measurement Units Left and right side of middle and bottom display lines ISE board ppm or ppb auto ranging pH mV board pH or mV Conductivity board µS cm or mS cm conductivity MΩ cm resistivity SAL1 or SAL2 in the marquee salinity PCT1 or PCT2 in the marquee concentration and TDS1 or TDS2 in the marquee TDS Depends on type of board inst...

Страница 28: ... of screen Scroll down digit numbers Scroll down through a list of options in setup and cal modes Use to edit numeric values Use to select available options 0 through 9 selectable by digit first digit sometimes selectable 0 through 19 Enters log view mode Use to view data in calibration measure and status logs function Enters negative positive sign when editing numbers Enter function Use to accept...

Страница 29: ...mum Press to save the entered parameter for the selected menu option Press to exit the current screen and return to the previous screen Press to exit the setup mode and return to the measure mode If is pressed will not return the operator to the setup mode The operator must reenter the setup mode by pressing If a single channel analyzer is in use all of the menu options are accessible by pressing ...

Страница 30: ...tor to enter system password Marquee ENTER PASSWORD Main display top PASS Main display bottom 0000 flashing Correct password Allows operator to enter setup mode for custom programming options Incorrect password Password incorrect or not entered correctly System password Marquee SYSTEM PASS INCORRECT Main display E035 Calibration password Marquee CAL PASS INCORRECT Main display E034 Verify password...

Страница 31: ...ontact Technical Support at 1 800 225 1480 Set the date in US or Europe format Enter month day and year Default date System will continue to keep date and time due to battery back up operator must set in accordance to local time zone If the battery is removed the system will show 01 01 2000 Set the time Enter hour and minutes in 24 hour format Default time System will continue to keep date and tim...

Страница 32: ...if the keypad and software are not responding refer to Chapter VI Resetting the Analyzer Warning Resetting the analyzer will lose all stored information including relay logs and calibration settings Set the automatic lighting options for the backlit display AUtO Brightness will change in response to ambient light source On Backlit display is always on OFF Backlit display is always off Default disp...

Страница 33: ...n Set the number of significant digits mV display option and concentration units displayed when in the measure mode Set the number of significant digits displayed measure mode Scroll through 2 3 or 4 significant digits Default significant digits 3 Enable mV values to be displayed on the second line Scroll between On or OFF Default mV setting OFF Set the displayed concentration units Scroll through...

Страница 34: ...ng for all alarms OFF Set the two analog current outputs SOUt and tOUt Scroll between 4 20 mA or 0 20 mA current signals The outputs share a common return but are isolated from the main circuitry of the analyzer Default output current 4 20 mA Scroll between logarithmic LOg and linear LIn scale for SOUt Set the low and high limits for the sensor output SOUt Default 1 0 ppb low and 100 ppb high Set ...

Страница 35: ...ault setting 720 hours Set values for customized Double Known Addition DKA Programmable for volume mL of flow cell concentration ppm and volume mL of standard 1 concentration ppm and volume mL of standard 2 and volume mL of additions Default flow cell volume 95 0 mL Default concentration Std1 2 96 Default volume addition Std1 0 5 mL Default concentration Std2 2 96 Default volume addition Std2 1 5 ...

Страница 36: ...mode indicator in the mode window HOLD is displayed while in the setup mode The system will enter the setup mode at the last saved menu option PASS DATE TIME LOG RSET DISP MEAS HOLD TADJ ALRM mAMP mADJ TEST CAL DKA SEL SCrn The displayed menu options depend on the measurement capability of the analyzer Press to loop through the menu options Press to select the desired menu option and enter the sub...

Страница 37: ... mADJ TEST CAL PH SEL SCrn SEL SCrn SEL SCrn SEL SCrn SEL SCrn SEL SCrn SEL SCrn SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL CH1 SEL SCrn SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 SEL CH2 The list of menu options shown for CH2 are examples only The displayed menu options for CH2 depend on the measurement capability of the channel If only one bo...

Страница 38: ...SET UP NEW SYSTEM PASSWORD PASS change flashing digit Do not scroll first digit above 9 Press to accept the system password and advance to the next screen to set the calibration password 0 0 0 0 SET UP NEW CALIBRATION PASSWORD PASS first digit flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remainin...

Страница 39: ... advance to the next screen 01 01 2000 ENTER DATE MM DD YYYY US or ENTER DATE DD MM YYYY EUrO Month Day 2 0 Year or Day Month 2 0 Year first digit flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits ENTER DATE MM DD YYYY US or ENTER DATE DD MM YYYY EUrO Month Day 2 0 Year or Day Month 2...

Страница 40: ...24HR TIME HOUR MINUTE hour minute first digit flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits ENTER 24HR TIME HOUR MINUTE hour minute change flashing digit Set in 24 hour time format Press to accept the time setting and return to the main setup mode TIME flashing SEL SCrn Press to s...

Страница 41: ...Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits SET LOG TIME IN HOUR MINUTE hour minute LOg change flashing digit To disable the log enter 0000 for the log interval The minimum log interval is 1 minute and the maximum log interval is 99 hours and 59 minutes Press to accept the log setting an...

Страница 42: ...ss Press When the reset is complete the system will return to the measure mode The operator will need to re enter the setup mode to continue programming the setup parameters Press to return to the setup mode PUSH TEST VIEW ENTER TO RESET rSEt This command resets all previously set parameters to factory default values Use this command only to set the analyzer to original factory setup values To Abo...

Страница 43: ...Display Notes DISP DISP flashing SEL SCrn Press to set the lighting option for the backlit display AUtO BACK LITE LItE AUtO flashing Press to scroll through AUtO OFF and On settings BACK LITE LItE AUtO OFF or On flashing Press to accept the display setting and return to the main setup mode DISP flashing SEL SCrn Press to scroll to the next menu ...

Страница 44: ... a menu option and customize the parameter refer to the menu option displays that are shown on the following pages for detailed instructions CH1 flashing SEL SCrn Press to scroll to the next menu Default Operator Action Scrolling Marquee Main Display Notes CH2 CH2 flashing SEL SCrn CH2 will not be shown in scrolling marquee if only one board is installed Press to set the channel 2 specific menus i...

Страница 45: ...GLE CHANNEL DISPLAY OFF flashing Press to scroll between OFF and On SHOW MV ON SINGLE CHANNEL DISPLAY OFF or On flashing Press to accept the setting and advance to the next screen AUtO SELECT ISE UNIT UnIt AUtO flashing Press to scroll through AUtO PPb and PP SELECT ISE UNIT UnIt AUtO PPb or PP flashing PP is used as an abbreviation for ppm Press to accept the setting and return to the main setup ...

Страница 46: ...R HOLD STATE LAST OR USER VALUE LASt flashing Press to scroll between LASt and USEr ENTER HOLD STATE LAST OR USER VALUE LASt or USEr flashing Press to accept the setting and advance to the next screen 21 0 ENTER FIXED USER VALUE IN mA first digit flashing Displayed if USEr was selected in previous screen Press to set the first digit Press to move to the next digit Press to set the values of the re...

Страница 47: ...LD cont d Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SEL SCrn Displayed for two channel analyzer Press to return to the channel specific menu options in the setup mode Action required for two channel analyzer HOLD flashing SEL SCrn SEL CH1 or SEL CH2 on main display of two channel analyzer Press to scroll to the next menu ...

Страница 48: ... to the next digit Press to set the value of the next digit TEMPERATURE ADJUSTMENT AdJ c change flashing digit The maximum temperature adjustment is 5 0 C Press to set a positive or negative temperature value TEMPERATURE ADJUSTMENT AdJ c Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SEL SCrn Displayed for two channel analyzer Press to return to the channel speci...

Страница 49: ...screen 100 ppb Set the HI or LO value for rLY1 Press to move the decimal point Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits ENTER VALUE rLY1 change flashing digit Displayed if HI or LO was selected for rLY1 in previous screen Press to accept the setting and advance to the next screen Acti...

Страница 50: ...Y2 in previous screen Press to accept the setting and advance to the next screen Action required if HI or LO was selected for rLY2 in previous screen OFF SELECT CALIBRATION HOLD ERROR OR OFF rLY3 OFF flashing Press to scroll through OFF CAL HOLd and Err SELECT CALIBRATION HOLD ERROR OR OFF rLY3 OFF CAL HOLd or Err flashing Press to accept the setting and return to the main setup mode CH1 or CH2 fl...

Страница 51: ...d advance to the next screen 1 ppb mA SENSOR OUTPUT LOW VALUE LO first digit flashing Press to move the decimal point Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits mA SENSOR OUTPUT LOW VALUE LO change flashing digit Press to accept the setting and advance to the next screen 100 ppb mA SENS...

Страница 52: ...PUT LOW VALUE LO C change flashing digit Press to accept the setting and advance to the next screen 45 0 C mA TEMP OUTPUT HIGH VALUE HI c first digit flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits mA TEMP OUTPUT HIGH VALUE HI c change flashing digit Press to accept the setting and ...

Страница 53: ...A OUTPUT ADJUSTMENT AdJ 0 0 last flashing digit Press to set the sensor mA offset value Press to set a positive or negative sensor mA offset SENSOR 4 20mA OUTPUT ADJUSTMENT AdJ 0 0 change flashing digit Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SEL SCrn Displayed for two channel analyzer Press to return to the channel specific menu options in the setup mode ...

Страница 54: ...t the temperature mA offset value Press to set a positive or negative temperature mA offset TEMP 4 20mA OUTPUT ADJUSTMENT AdJ 0 0 change flashing digit Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SEL SCrn Displayed for two channel analyzer Press to return to the channel specific menu options in the setup mode Action required for two channel analyzer mADJ flash...

Страница 55: ...ress to scroll between SOUt and tOUt settings and select tOUt SELECT TEMP OR SENSOR OUTPUT 4 20 tOUt flashing Press to display the tOUt low value Actual low value displayed mA TEMP OUTPUT LOW VALUE LO c 4 0 mA are sourced at output terminal 11 Press to display the tOUt high value Actual high value displayed mA TEMP OUTPUT HIGH VALUE HI c 20 mA are sourced at output terminal 11 Press to accept the ...

Страница 56: ...UTPUT 4 20 SOUt flashing Press to display the SOUt low value Actual low value displayed mA SENSOR OUTPUT LOW VALUE LO 4 0 mA are sourced at output terminal 9 Press to display the SOUt high value Actual high value displayed mA SENSOR OUTPUT HIGH VALUE HI 20 0 mA are sourced at output terminal 9 Press to accept the test and return to the main setup mode CH1 or CH2 flashing SEL SCrn Display for two c...

Страница 57: ...2 test Actual rLY2 status Press to set the rLY2 setting OFF or On USE ARROWS TO TOGGLE RELAY 2 rLY2 OFF or On Relay contact according to screen indication Press to accept the rLY2 test and move to the rLY3 test Actual rLY3 status Press to set the rLY3 setting OFF or On USE ARROWS TO TOGGLE RELAY 3 rLY3 OFF or On Relay contact according to screen indication Press to accept the rLY3 test and return ...

Страница 58: ...set the value to 0000 Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits ENTER CALIBRATION FREQUENCY IN HOURS CAL change flashing digit Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SEL SCrn Displayed for two channel analyzer Press to return to the channel sp...

Страница 59: ...hange flashing digit Press to accept the setting and advance to the next screen 2 96 SET STD1 CONCENTRATION IN PERCENT PARTS PER HUNDRED PCt flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits SET STD1 CONCENTRATION IN PERCENT PARTS PER HUNDRED PCt change flashing digit Press to accept ...

Страница 60: ...g digit Press to accept the setting and advance to the next screen 1 50 mL SET STD2 VOLUME IN mL Std2 flashing Press to set the first digit Press to move to the next digit Press to set the values of the remaining digits and press to move through the remaining digits SET STD2 VOLUME IN mL Std2 change flashing digit Press to accept the setting and return to the main setup mode CH1 or CH2 flashing SE...

Страница 61: ...pears in the main display 5 Press 6 Press to toggle between On and OFF settings for the air pump power Select the OFF setting Changing the air pump setting to On or OFF will be indicated by a click sound 7 Press to accept the setting and return to the TEST menu 8 Press to return to the measure mode 1 Shut off sample flow prior to the analyzer inlet Refer to Chapter IV Flow Regulation 2 Disconnect ...

Страница 62: ...ow rate through the analyzer to 40 mL min 2 Remove the protective cap from the reference electrode Re install the electrodes on the analyzer Be careful not to disconnect the reservoir tubing from the reference electrode sidearm 3 Allow the analyzer to stabilize for approximately 1 hour and then recalibrate the system Refer to Chapter IV Performing a DKA Calibration Start Up ...

Страница 63: ...how to properly configure the 2117HL analyzer The value of the calibration standards volume of the calibration standards and the volume of the flow cell must be entered in the setup mode Adjust the flow cell volume according to the precise factory calibration volume that is printed on the side of each flow cell Use the 29 600 ppm high level chloride standard Cat No 211740HL as both standard 1 Std1...

Страница 64: ...r to Chapter IV Rinsing the Flow Cell For accurate volume displacement install the chloride sensing electrode reference electrode and ATC probe in their respective flow cell cap ports Refer to Chapter II Installation of a New Chloride Electrode Chapter II Installation of the ATC probe and Chapter II Installation of a New Reference Electrode Close the calibration port When rinsing the flow cell bef...

Страница 65: ... the ball in the flow meter indicates the correct flow rate reading see D The flow rate should be adjusted to 40 mL minute Pull out the knob to unlock the setting and adjust the flow rate Turn the knob clockwise to increase the flow rate Turn the knob counterclockwise to decrease the flow rate Push in the knob to lock the setting 4 Push in the diverter valve on the flow cell The flow cell will beg...

Страница 66: ... High Level Chloride Analyzer User Guide The Thermo Scientific Orion 2117HL chloride analyzer utilizes pressure gravity and fluid dynamics as the principal force of operation for the fluidic system Air Regulation Figure IV 3 50 40 30 20 10 Air Pump ...

Страница 67: ...or technique refer to the Appendix Pipet Operation section Do not touch the pipet tip with bare fingers Risk of contamination is possible Use powder free gloves to prevent contamination When using a pipet to inject standards during calibration use a fresh pipet tip for each standard and each injection When a fresh tip is installed rinse the tip with the same concentration standard as the intended ...

Страница 68: ...Actual concentration reading 2 Press to initiate the calibration CAL appears as mode 3 If the calibration password is active enter the calibration password by pressing to set the first digit to move to the next digit to set the values of the remaining digits and to move through the remaining digits Press to accept the password ENTER PASSWORD PASS 4 CH1 or CH2 flashing CAL CHnL Displayed for two ch...

Страница 69: ...URING BACKGROUND WAIT 2 MINUTES Actual readings flashing System circulates sample Minutes will be counted down on the marquee 13 Wait 0 to 8 minutes AWAITING DATA STABILITY Actual readings flashing System continuously evaluates the data until a stable condition is met If there is a calibration error the appropriate error message will be displayed 14 Add standard 1 through the calibration port Pipe...

Страница 70: ... the 0 5 mL pipet ADD STD2 PRESS ENTER Add Std2 For calibration standard 2 use the 29 600 ppm high level chloride standard Cat No 211740HL 19 Press ADD STD2 PRESS ENTER Add Std2 20 Wait 2 minutes MEASURING STD2 CIRCULATING WAIT 2 MINUTES Actual readings flashing System circulates sample Minutes will be counted down on the marquee 21 Wait 0 to 8 minutes AWAITING DATA STABILITY Actual readings flash...

Страница 71: ...R TO ACCEPT OR PRESS EXIT TO ABORT WITHOUT SAVING Calculated Slope and E0 If is pressed refer to the Calibration Abort Steps section 24 Pull the diverter valve out Turn the inlet valve on Close the calibration port on the flow cell cap PULL DIVERTER VALVE OUT TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER FLO On 25 Press PULL DIVERTER VALVE OUT TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER FLO On...

Страница 72: ...TED PRESS ENTER CAL Abrt Exit 4 Press to abort the calibration CALIBRATION ABORTED PRESS ENTER CAL Abrt Exit 5 Pull the diverter valve out Turn the inlet valve on Close the calibration port on the flow cell cap PULL DIVERTER VALVE OUT TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER FLO On Exit 6 Press PULL DIVERTER VALVE OUT TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER FLO On Exit 7 No operator a...

Страница 73: ... and the electrodes are working properly and then repeat the calibration INVALID SLOPE PRESS ENTER E042 The calculated slope was invalid Standard values were likely entered in the wrong sequence or wrong standard values were entered Error 107 Press to abort the calibration and refer to Exit 3 CALIBRATION DATA TOO CLOSE TOGETHER PRESS ENTER E107 Use new standards Perform electrode cleaning conditio...

Страница 74: ...ation and refer to Exit 3 Verify that the correct standards were used during the calibration the standard values were entered correctly and in the right order and the electrodes are working properly and then repeat the calibration CH1 BAD OFFSET PRESS ENTER E125 Use new standards Perform electrode cleaning conditioning and troubleshooting Error 126 Press to abort the calibration and refer to Exit ...

Страница 75: ...centration values and the standard 1 and standard 2 volume values to be used Let VC Flow cell volume Default 95 0 mL C1 Standard 1 concentration Default 2 96 C2 Standard 2 concentration Default 2 96 V1 Volume of standard 1 added Default 0 50 mL V2 Volume of standard 2 added Default 1 50 mL dC1 Concentration change due to the first addition dC2 Concentration change due to the second addition dC1 C1...

Страница 76: ...flow cell to calibration level V0 approximately 95 mL 2 Record the concentration displayed when the reading is reasonably stable C0 3 Add standard 1 volume V1 with concentration C1 4 When the reading is reasonably stable record the concentration CS 5 The recorded value should be within 10 of the calculated value according to CS C0 x V0 C1 x V1 V0 V1 C1 should be the chloride concentration actually...

Страница 77: ...hannel that will be calibrated and press to begin the calibration CH1 or CH2 flashing CAL CHnL Action required for two channel analyzer 6 DKA or OFFL flashing CAL tYPE 7 Press to select OFFL and press to accept the setting OFFL flashing CAL tYPE 8 Wait 1 to 10 minutes MEASURING SAMPLE WAIT 1 MINUTE AWAITING DATA STABILITY Actual readings flashing System continuously evaluates the data until a stab...

Страница 78: ...t will be calibrated and press to begin the calibration CH1 or CH2 flashing CAL CHnL Action required for two channel analyzer 15 Press to select OFFL and press to accept the setting OFFL flashing CAL tYPE 16 Enter the concentration value of the QC sample obtained from laboratory analysis Press to move the decimal point and set the value as ppm or ppb Press to set the first digit Press to move to t...

Страница 79: ... the installation date of the electrode 1 Check that the sample flow rate is 35 to 45 mL minute To alter the flow rate pull out the locking knob of the pressure regulator then rotate the black knob to increase clockwise or decrease counterclockwise sample flow Push in the locking knob of the pressure regulator to lock the flow rate 2 Inspect the analyzer for leakage 3 Check that there are no error...

Страница 80: ... air pump is left on it will spatter filling solution as the bottle is removed 1 Turn off the air pump Refer to Chapter III Shutdown and Start Up Procedure 2 Remove the hollow push pin on the discharge tube of the air pump from the base of the filling solution bottle 3 Remove the filling solution bottle from the clip Unscrew the cap and discard the bottle 4 Remove the cap and seal from a new refer...

Страница 81: ...ch 4 Separate the filter cap with bypass needle valve assembly from the filter body retaining the ring 5 Remove the filter element and soft gasket if necessary 6 Replace the gasket and press a new sintered element into the filter body 7 Replace the hex cap and bypass needle valve assembly and reposition the bypass drain line into the drain assembly 8 Retighten the hex cap to approximately 75 pound...

Страница 82: ... the MSDS instruction MSDS files can be downloaded at www thermo com processwater Valve Stem O rings 1 Remove the two screws that hold the valve stem assembly in place 2 Gently pull on the valve stem to remove 3 Slide off the two old O rings and replace them It is not necessary to remove the retaining ring 4 Place the assembly back into the manifold block and tighten screws Note Do not use O ring ...

Страница 83: ...sen the restrictor tube fitting from the left side of the flow cell block 4 Pull out the restrictor tube assembly at each end 5 Unscrew the clip behind flow cell that holds the restrictor tube to the panel 6 Replace with a new restrictor tubing assembly 7 Be sure all of the fittings are secure to prevent leaks 8 Open the inlet valve to start sample flow through the analyzer Replacement of Restrict...

Страница 84: ...ress to step through the menu items CH1 CALIBRATION SLOPE AND E0 CH2 CALIBRATION CELL CONSTANT CH1 ERROR LIST PRESS VIEW CH2 ERROR LIST PRESS VIEW CH1 SELECT TIME DATE TO VIEW MEASUREMENT LOG CH2 SELECT TIME DATE TO VIEW MEASUREMENT LOG SELECT TIME DATE TO VIEW STATUS LOG SOFTWARE REV NUMBER CH1 SERIAL NUMBER CH2 SERIAL NUMBER CH1 MODEL NUMBER CH2 MODEL NUMBER CH1 MEASURE mV AND NOISE CH2 MEASURE ...

Страница 85: ...tion Press to view the last twelve calibrations Calibration Log Default Operator Action Scrolling Marquee Main Display Notes Calibration Log Press while in the measure mode to enter the diagnostics mode or or CALIBRATION SLOPE AND E0 Slope E0 CALIBRATION OFFSET mV offset CALIBRATION CELL CONSTANT Cell Constant Press to display the calibration time and date CALIBRATION TIME DATE HH MM MM DD or DD M...

Страница 86: ...or codes 1 5 indicates that one of five error codes is being displayed Press to scroll through the error list Press to display a description of each error code on the marquee Error List Default Operator Action Scrolling Marquee Main Display Notes Error List ERROR LIST PRESS VIEW E Press to display the description of the error code on the marquee Actual description of error code E Press to scroll t...

Страница 87: ...entries Measurement Log Default Operator Action Scrolling Marquee Main Display Notes Measurement Log SELECT TIME DATE TO VIEW MEASUREMENT LOG HH MM MM DD or DD MM Press to scroll through the log entries SELECT TIME DATE TO VIEW MEASUREMENT LOG HH MM MM DD or DD MM Press to scroll between the measurement log and the data and time display Actual temperature value for logged measurement Concentration...

Страница 88: ...cessors Status Log Software Revision Default Operator Action Scrolling Marquee Main Display Notes Status Log SELECT TIME DATE TO VIEW STATUS LOG HH MM MM DD or DD MM Press to scroll through the log entries SELECT TIME DATE TO VIEW STATUS LOG HH MM MM DD or DD MM Press to toggle between the log code and the data and time PRESS UP DOWN KEY TO VIEW STATUS LOG Event code Press to proceed to the next m...

Страница 89: ...outputs Electronics Serial Number Model Number mV and Noise Measurements mA Output Values Default Operator Action Scrolling Marquee Main Display Notes Electronics Serial Number SERIAL NUMBER Press to proceed to the next menu Model Number MODEL NUMBER Press to proceed to the next menu mV and Noise Measurements MEASURE mV AND NOISE Current mV measurement and noise Press to proceed to the next menu m...

Страница 90: ... main display 6 Verify that the display segments are functional and press to proceed to the keypad test Display Test Default Operator Action Scrolling Marquee Main Display Notes Display Test PRESS ENTER FOR THE DISPLAY TEST dISP tESt Press to start the test Verify that all of the display segments are on and that the LED colors are functional All segments on All segments on System will cycle throug...

Страница 91: ...w key is not pressed within 10 seconds Keypad Test Default Operator Action Scrolling Marquee Main Display Notes Keypad Test KEYPAD TEST PRESS ALL KEYS ONE AT A TIME 0 Press all keys one at a time in any order KEYPAD TEST PRESS ALL KEYS ONE AT A TIME Display will show numbers 1 through 8 as keys are pressed After the first key is pressed error E033 will be displayed if a new key is not pressed with...

Страница 92: ... anions such as chloride Knowing electrode and analyzers parameters like offset potential slope etc allows testing of various instruments by applying a known mV voltage Input Signal Expected Reading 0 5 mV 0 1 0 mV 0 5 mV to 0 5 mV 1000 mV 1001 5 mV to 998 5 mV 1000 mV 998 5 mV to 1001 5 mV Background concentration too high for the standards used Standards contaminated or incorrectly made verify c...

Страница 93: ...ng the Analyzer Improper pipet technique refer to the Appendix Pipet Operation and Technique section Background concentration too high for the standards used Cables interchanged verify wiring of cable connections to terminal strip Refer to Chapter II Wiring the Analyzer Check the connection of the cable markers for the corresponding electrode Cable markers are the white tape at the cap connector o...

Страница 94: ...e Drift Sample concentration varying Check sample status Perform a span check and if span check passes the analyzer is okay Blocked junction on reference electrode Make sure electrolyte is flowing properly and the bottle is pressurized by the air pump Chloride or reference electrode failure Check the cable connections and location of wiring to terminal strip Refer to Chapter II Reference electrode...

Страница 95: ... concentration too high for standards Repeat calibration using custom higher concentration standards Refer to Chapter IV Pipet technique error Use the correct pipet techniques Refer to the Appendix section Flow cell contaminated Rinse the flow cell with deionized water Flush the flow cell overnight at calibration liquid level Refer to Chapter IV Electronics failure or bad setup Reset the analyzer ...

Страница 96: ...de or reference electrode failure Electrode is shorted cracked or damaged Install a new electrode Refer to Chapter II Electronics failure or bad setup Reset the analyzer Refer to Chapter VI Analyzer out of calibration Recalibrate the analyzer Refer to Chapter IV Low Readings Analyzer out of calibration Recalibrate the analyzer Refer to Chapter IV Sample is very pure Check sample status Perform a s...

Страница 97: ... channel 2 disengaged closed C500 CAL MODE Calibration mode entered R400 MEAS MODE Measure mode entered S600 SETUP MODE Setup mode entered E028 POWER FAIL Brown out or power failure and system has stopped processing Verify custom settings E033 KEYPAD FAILURE User did not press the keys during a diagnostic mode keypad test or keypad broken Repeat diagnostic mode keypad test E034 CAL PASS INCORRECT ...

Страница 98: ...nsor value above Sout high limit value on channel 1 Verify user selectable Sout high limit value in setup mode E128 CH1 SOUT mA UNDER RANGE Measured sensor value below Sout low limit value on channel 1 Verify user selectable Sout low limit value in setup mode E129 CH1 TOUT mA OVER RANGE Measured temperature value above Tout high limit value on channel 1 Verify user selectable Tout high limit value...

Страница 99: ...lectrode cables are faulty or electrode junction is fouled E109 CH1 BAD SLOPE Last calibration produced a bad slope on channel 1 Slope is less than 45 mV decade or more than 62 mV decade or the calibration standards may have been interchanged Recalibrate the analyzer using fresh standards Recalibrate using the correct sequence of standards E110 CH2 BAD SLOPE Last calibration produced a bad slope o...

Страница 100: ...ings Operator Action Scrolling Marquee Main Display Notes Press in the measure mode to enter the setup mode Last menu used in setup mode SEL SCrn SETUP appears as mode Press until RSET appears in the marquee RSET flashing SEL SCrn Press to reset the analyzer PRESS TEST VIEW ENTER TO RESET rSEt Press Press Press When the reset is complete the system will return to the measure mode The operator will...

Страница 101: ...ttings and calibrations are preserved and analyzer returns to the measure mode The actual value for concentration and temperature will be displayed if the electrodes are properly installed If the system does not reset contact Technical Support at 1 800 225 1480 for assistance In the event you require technical assistance please have the serial number available when calling for assistance along wit...

Страница 102: ...a second or third year Provides access to the manufacturer s technical experts at Thermo Scientific Orion Support Call Center 1 800 225 1480 Monday through Friday 8 00 AM to 5 00 PM EST After telephone consultation we will send you required parts for installation by your on site technician With in house resources at a premium many organizations require immediate access to manufacturer expertise Pu...

Страница 103: ...rely on us to provide you with an efficient and quality installation and the start up support you need to be up and running quickly Our service representatives are highly trained experienced and certified for your product and will be there to make sure that your instrumentation delivers to specifications This is a one day service engineer on site visit to your facility for remedial service events ...

Страница 104: ...o noise emissions from digital apparatus set out in the Radio Interference Regulations of the Canadian Department of Communications Le présent appareil numérique n émet pas de bruits radioélectriques dépassant les limites applicables aux appareils numériques de la class A prescrites dans le Régiement sur le brouillage radioélectrique édicté par le ministère des Communications du Canada This produc...

Страница 105: ...ts for electrical equipment for measurement control and laboratory use general requirements EMC Electromagnetic Compatibility EMC 89 336 EEC EN 61326 1 2006 Electrical equipment for measurement control and laboratory use This product has been manufactured in compliance with the provisions of the relevant manufacturing and test documents and processes These documents and processes are recognized as...

Страница 106: ...ernational coordinator for details For customers in the U S rush orders received before 12 pm Eastern Time will be shipped the same day Rush orders received after 12 noon Eastern Time will be shipped the next business day For customers and dealers in Canada rush orders will be shipped within 2 business days For customers and dealers outside the U S and Canada contact your international coordinator...

Страница 107: ...ent from manufacturer Older items 9 digit parts and discontinued items cannot be returned for credit Manufacturer must be notified within 30 days of receipt of invoice of any item or billing discrepancies All substantiated claims will be remedied by a credit memo and a new order placed for short shipment Any shipment discrepancy claimed after 30 days of invoice date will not be honored and credit ...

Страница 108: ...The warranty described is exclusive and in lieu of all other warranties whether statutory express or implied including but not limited to any implied warranty of merchantability or fitness for a particular purpose and all warranties arising from the course of dealing or usage of trade The buyer s sole and exclusive remedy is for repair or replacement of the non conforming part thereof or refund of...

Страница 109: ...Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide A 1 Appendix 17 26 8 5 Mounting Dimensions ...

Страница 110: ... default 59 2 mV decade Slope range 62 0 mV decade to 45 0 mV decade CISO 35 5 ppm Volume of flow cell 95 mL Concentration of standard 1 added during calibration 2 96 Volume of standard 1 added during calibration 0 50 mL Concentration of standard 2 added during calibration 2 96 Volume of standard 2 added during calibration 1 50 mL ISE Default Values ...

Страница 111: ...l reading within 2 minutes of injecting a standard solution Units Displayed ppb ppm auto ranging Temperature Compensation Automatic mV Measurement Range 1999 9 mV Resolution 0 1 mV Relative Accuracy 0 5 mV 0 1 Temperature Measurement Range 10 to 120 C Resolution 0 1 C Relative Accuracy 0 5 C Failure Detection Manual compensation ATC Probe 30 K thermistor LED Status Indicator Green OK Yellow Warnin...

Страница 112: ...res Type Custom backlit LCD Size 54 x 76 mm 2 1 8 in x 3 in Marquee Temperature operator prompts Middle Line Concentration error codes Lower Line mV selectable Text Display Scrolling marquee for English language instructions on setup calibration and diagnostics Calibration DKA Calibration Yes DKA Calibration Points 3 points Offline Calibration Yes Offline Calibration Points 1 point Pre programmed ...

Страница 113: ...lectable Alarm Outputs Number of Relay Outputs 3 Maximum Relay Load 250 VAC 5 A 30 VDC 5 A resistive load only Minimum Value Alarm Yes Maximum Value Alarm Yes Error Alarm Yes Calibration offline Alarm Yes Programmable Min And Max Values Yes Analyzer Features Non volatile Memory Yes Battery Backup Replaceable Yes Data Logging Yes Keypad 8 electromechanical keys with graphic overlay Software Feature...

Страница 114: ...x 27 cm 26 x 17 x 11 inch Fits on 1817HL panel mounting footprint Weight 22 7 kg 50 lbs Physical Size of Electronics Module 144 x 144 x 187 mm 5 67 x 5 67 x 7 36 inch Weight 1 7 kg 3 75 lbs Power Input 85 to 132 VAC 200 mA or 170 to 264 VAC 100 mA 50 to 60 Hz Environmental Operating Conditions Waterproof Enclosure IP66 NEMA 4X Overvoltage Category II Ambient Temperature 5 to 45 C Relative Humidity...

Страница 115: ...er guide and options kit 211750HL 2117HL High Level Chloride Annual Consumables Kit for one year operation includes chloride standard solutions kit 211740HL chloride sensing electrode 210017 reference electrode 100057 1 x 4 oz bottle of reference electrode filling solution 100057F4 O ring kit 2100OK check valve 2100VC pipet tips 204846 001 restriction tube assembly 2100RT and inlet filter with gas...

Страница 116: ...lyzers 2100PH2 Second channel module for pH ORP 2100CD2 Second channel module for conductivity 21GRABXP Grab sampler FAST QC upgrade module to fit existing 2111XP 2111XPEN 2110XP 2110XPEN 2117HL 2117HLEN 2117XP 2117XPEN 2120XP and 2120XPEN analyzers 21GRBT Replacement bottle for 2100 series grab sampler 21GRPA Air pump replacement kit for 2100 series grab sampler 21GRFK Fittings kit for 2100 serie...

Страница 117: ...e assembly 2100VC Check valve 181170 2 Inlet filters 2100EC 2 x 1 meter electrode cables for 210017 and 100057 electrodes 2117HLM Flow cell manifold for 2117HL analyzer only 2117PN Pressurized needle assembly for reference filling solution bottle 2100OK O ring kit 2100FK115 Fuse kit assembly 115 V 2100FK230 Fuse kit assembly 230 V 2100PS Power supply assembly 2117HLEP 2117HL electronics faceplate ...

Страница 118: ...ectrode 210017 reference electrode 100057 1 x 4 oz bottle of reference electrode filling solution 100057F4 O ring kit 2100OK check valve 2100VC pipet tips 204846 001 restriction tube assembly 2100RT and inlet filter with gaskets 181170 1 2117HLCAL Calibration Kit includes carrying case 0 5 mL pipet 204847 001 box of pipet tips 204846 001 wash bottle 5 x 2 oz bottle of 29 600 ppm high level chlorid...

Страница 119: ...ease the tip point the pipet at suitable waste receptacle and press the tip ejector with your thumb You can attach the pipet shelf hanger on a counter pipet stand or anywhere where you want to hang your pipet Clean the area where you plan to attach the shelf hanger Apply two stickers to the underside of the shelf hanger Press the shelf hanger firmly into place on a shelf counter top or pipet stand...

Страница 120: ...pipeting Hold the pipet in an upright position while aspirating liquid The grippy should rest on your index finger Make sure that the tips pipet and solution are at the same temperature Fill a clean reservoir with the liquid to be dispensed 1 Depress the push button to the first stop 2 Dip the tip under the surface of the liquid in the reservoir to a depth of about 1 cm and slowly release the push...

Страница 121: ......

Страница 122: ... 232 6000 Dom Fax 1 978 232 6015 Int l Fax 978 232 6031 Europe P O Box 254 3860 AG Nijkerk Wallerstraat 125K 3862 CN Nijkerk Netherlands Tel 31 033 2463887 Fax 31 033 2460832 Asia Pacific Blk 55 Ayer Rajah Crescent 04 16 24 Singapore 139949 Tel 65 6778 6876 Fax 65 6773 0836 www thermo com processwater 2009 Thermo Fisher Scientific Inc All rights reserved ...

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