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Section 7
Maintenance
7-3
1.
The spare soda lime/desiccant
bottle (in the spare parts kit) is
shipped without chemicals. You
will need to procure chemicals
locally. When handling chem-
icals, observe all manufacturer’s
safety warnings.
WARNING
Viton gasket in lid
Polyester fiber in
bottle
2.
Fill the bottle slightly more than
half full with soda lime. Fill to the
neck with magnesium perchlorate.
Tap the sides of the bottle to settle
the chemicals. Insert a polyester
fiber wad (provided), packing
firmly. This helps keep dust from
escaping. Make sure the filter disc
in the lid is intact; replace if
necessary.
Filter
Mg(ClO
4
)
2
Soda
Lime
3.
Remove the old bottle; insert the
new bottle into the bottle cover
bottom first, and reattach the cover
to the analyzer. Note that there is
a small wad of polyester fiber in
the bottom of the nickel-plated
bottle cover, to prevent the soda
lime/desiccant bottle from rattling.
New bottle
Hole in cap
Nickel-plated
bottle cover
Polyester fiber
WARNING
Magnesium perchlorate is the recommended desiccant since it does not
interact with CO
2
.
Do not use any other desiccant
. Several grades of
magnesium perchlorate are available from commercial suppliers. In general,
the more granular (as opposed to powdery) the grade the better. One type
that works well is marketed under the name
Dehydrite
, and is available
(catalog number C260-M61) from Thomas Scientific, P.O. Box 99,
Swedesboro, NJ 08085-6099. (609) 467-2000. See List of Suppliers,
Appendix B.