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074-594-P1H Micro GC Fusion Operating Manual

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9.10.10.6 Second Level Calibration

If a second level calibration is required, a calibration gas standard of different
concentration levels must be run using the same analytical method as the first level
calibration. A multi-point calibration utilizes multiple data points from runs of the
different calibration gas cylinders. The plot of area count (μV) versus concentration
(mol% or ppm) will be used to calculate the concentration of an unknown amount of
the calibrated compound.

1 Calibrate a single level by following Single Level Calibration [

2 Introduce a second level calibration gas.
3 Conduct an analysis of the second level calibration gas. INFICON recommends

conducting multiple runs of each calibration gas and using the last run to perform
the calibration. Doing so thoroughly purges the sample path with the calibration
gas, which ensures the best calibration accuracy.

4 In the data browser, select the data file for the calibration gas corresponding to

the second level.

5 Click the icon to enter the calibration window.
6 By default, Module A will display.
7 Click and a window is displayed. Select Add new level to calibration. Click the

icon.

8 The Concentration and Area (μV) columns will be blank. The name of the

calibration will be replaced with the currently selected run.

9 Type the Concentration of the compound as listed on the calibration gas

standard certificate of analysis. An area count (in μV) will populate in the Area
column.

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Summary of Contents for Micro GC Fusion 2-Module

Page 1: ...Operating Manual Micro GC Fusion Gas Analyzer 074 594 P1H ...

Page 2: ...INFICON Two Technology Place East Syracuse NY 13057 9714 ...

Page 3: ...tem 24 5 Product Overview 26 5 1 2 Module Chassis 26 5 2 4 Module Chassis 28 5 3 Sample Inlets 30 5 3 1 Front Sample Inlet 30 5 4 Carrier Gas Connections 31 5 5 Venting Connections 33 5 5 1 ANALYTICAL Vent 34 5 5 2 REFERENCE Vent 34 5 5 3 PUMP Vent 34 5 5 4 HIGH PRESSURE PURGE Vent 34 5 6 Front Panel Display 35 5 7 GC Module 36 5 7 1 Injection 36 5 7 1 1 Variable Volume Injector 37 5 7 1 2 Variabl...

Page 4: ...1 Tablet 48 5 11 1 2 Computer 48 5 11 2 Tablet Web Browser Requirement 48 5 11 3 Computer Web Browser Requirement 48 5 12 Wireless Regulatory Compliance Information 49 5 12 1 Regulatory Compliance Information for UNITED STATES Users 49 5 12 1 1 FCC Statement 49 5 12 1 2 FCC RF Exposure Statement 50 5 12 2 Regulatory Compliance for CANADIAN Users 50 5 12 2 1 Industry IC Notices 50 5 12 3 Regulatory...

Page 5: ...lter 67 6 3 3 Setting Carrier Gas Pressure 67 6 3 4 Purging and Connecting Carrier Gas Line 68 6 4 Installing the Sample Inlet Filter 69 6 4 1 Sample Inlet Filter Parts List 69 6 4 2 Tools Required 69 6 4 3 Sample Inlet Filter Assembly Installation 69 6 5 Installing the Rack Mount Kit 71 6 5 1 Rack Mount Kit PN 952 4100 G1 Parts 71 6 5 2 Required Tools 71 6 5 3 Rack Mount Kit Installation 71 6 6 I...

Page 6: ...cro GC Fusion Chassis Installation Side Install 114 6 15 2 4 Module Micro GC Fusion Chassis Installation Side Install 121 6 15 3 4 Module Micro GC Fusion Chassis Installation Front Install 128 6 15 4 Change Mounting Bracket Orientation 137 7 Connecting to a Sample 139 7 1 Introduction 139 7 2 Purging the Sample Path 139 7 3 Front Sample Inlet 139 7 3 1 Front Sample Inlet 140 7 3 2 Front Sample Inl...

Page 7: ...od or Sequence 166 9 4 4 Calibrate Method 166 9 4 5 Delete Method Sequence 166 9 4 6 Import Method 167 9 4 7 Export Method 167 9 4 8 Load Method or Sequence 168 9 4 9 Preset Methods and Sequences 169 9 4 10 Add Sequence 170 9 4 11 Edit Sequence 171 9 5 View System Status 174 9 6 Run Method or Sequence 176 9 6 1 Run Method 176 9 6 2 Run Sequence 177 9 6 3 Stop a Sequence 177 9 7 View Chromatogram 1...

Page 8: ...te the Area of a Single Peak 220 9 10 10 6 Second Level Calibration 223 9 10 10 7 Manual Response Factors 226 9 10 10 8 Auto Calibration 228 9 10 11Reprocess Runs 231 9 11 Micro GC Fusion Offline Analysis 233 9 11 1 Initializing Micro GC Fusion Offline Analysis 233 9 11 2 Tray Icon 234 9 11 2 1 Launch the Browser 234 9 11 2 2 Restart Service 235 9 11 2 3 Exit Service 235 9 11 3 Saving a Method 236...

Page 9: ...eplacement 257 10 4 1 List of Required Tools 257 10 4 2 Removal of the JP 100 257 10 4 2 1 2 Module JP 100 Removal 257 10 4 2 2 4 Module JP 100 Removal 260 10 4 3 Replacing the JP 100 263 10 4 4 GC Module Removal Procedure for 2 Module System 265 10 4 5 GC Module Replacement Procedure for 2 Module System 269 10 4 6 GC Module Removal Procedure for 4 Module System 273 10 4 7 GC Module Replacement Pr...

Page 10: ...303 13 1 3 Refinery Gas Checkout Gas 304 13 2 Replacement Parts 305 13 2 1 GC Module Replacement 305 13 2 2 Micro GC Fusion Accessories 308 13 2 3 Spare and Consumable Parts 309 13 3 Software and Computers 310 13 4 Installation and Familiarization Training 310 14 Checkout Gas Chromatograms 311 14 1 Introduction 311 14 2 10 m Rt Msieve 5A 312 14 2 1 Universal Checkout Gas Using Helium Carrier Gas 3...

Page 11: ...eliable However INFICON assumes no responsibility for its use and shall not be liable for any special incidental or consequential damages related to the use of this product Due to our continuing program of product improvements specifications are subject to change without notice Copyright 2019 All rights reserved Reproduction or adaptation of any part of this document without permission is unlawful...

Page 12: ...2 Declaration of Conformity INFICON 12 319 074 594 P1H Micro GC Fusion Operating Man ual 2 Declaration of Conformity ...

Page 13: ...INFICON Declaration of Conformity 2 074 594 P1H Micro GC Fusion Operating Manual 13 319 ...

Page 14: ...iately notify Seller in writing of such non conformity specifying in reasonable detail the nature of such non conformity If Seller is not provided with such written notification Seller shall not be liable for any further damages which could have been avoided if Seller had been provided with immediate written notification THIS WARRANTY IS MADE AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES EXPRESS OR...

Page 15: ...o GC Fusion Operating Manual 15 319 These instructions do not provide for every contingency that may arise in connection with the installation operation or maintenance of this equipment Should you require further assistance please contact INFICON ...

Page 16: ...carbon dioxide hydrogen helium neon krypton Light Hydrocarbons methane ethane ethylene acetylene propane propylene butane pentane hexane C3 C5 olefins C7 C12 saturated hydrocarbons volatile organic compounds VOC Common Micro GC Fusion applications include compositional analysis for natural gas natural gas odorants refinery gas fixed gas syngas fuel cell biogas biomethane landfill gas flue gas mine...

Page 17: ...n electronic pressure control system a MEMS based micro thermal conductivity detector µTCD Chromatography software included with Micro GC Fusion may be operated from the instrument front panel display or by a networked computer Both the analytical method and the resulting data files are stored on the Micro GC Fusion hard drive 4 3 Definition of Notes Cautions and Warnings When using this manual pl...

Page 18: ...following warnings and cautions The user must read and understand all warnings and cautions and develop specific procedures to mitigate the unique combination of hazards presented by their application CAUTION Use Micro GC Fusion in an upright position CAUTION Only technically qualified personnel should perform the procedures and maintenance described in this manual WARNING Micro GC Fusion has a he...

Page 19: ...ceeding 172 kPa 25 psi will damage Micro GC Fusion and require factory repair CAUTION When the Integrated Sample Conditioner is installed a pressurized sample of up to 6 895 kPa 1 000 psi can be connected to the Micro GC Fusion inlet Exercise caution when handling the high pressure samples CAUTION Micro GC Fusion is ventilated using an internal fan The air inlet on the front of Micro GC Fusion mus...

Page 20: ...the INFICON supplied mounting kit Using unspecified mounting hardware may result in personal injury caused by unstable instrument mounting CAUTION The 2 module Micro GC Fusion remains powered on even if it is placed into standby mode Disconnect the power supply to completely power off the instrument WARNING Dangerous voltages may be present in a 4 module Micro GC Fusion whenever the power cord or ...

Page 21: ...o GC Fusion Any interruption of the protective earth circuit inside or outside of the 4 module Micro GC Fusion or disconnection of the protective earth terminal is likely to make the instrument dangerous This symbol indicates where the protective earth ground is connected inside the 4 module Micro GC Fusion Never unscrew or loosen this connection ...

Page 22: ...ysis CAUTION Micro GC Fusion is intended for gas sampling only Liquid injections will damage the instrument The optional Integrated Sample Conditioner is recommended when the sample gas is at high pressure up to 6 895 kPa 1 000 psi The Integrated Sample Conditioner reduces the sample gas pressure to approximately 83 kPa 12 psi and heats the sample to a constant temperature to optimize analysis rep...

Page 23: ...performance fused silica capillary columns to perform GC separation Two types of capillary columns are used Porous Layer Open Tubular PLOT PLOT columns have small particles coated on the inner surface of the column and separation is based on gas solid partitioning Common PLOT columns are Molsieve Q Bond U Bond and Alumina PLOT columns separate based on com pound polarity Wall Coated Open Tubular W...

Page 24: ...generated based on compound type and concentration Micro GC Fusion MEMS based µTCD provides excellent sensitivity A detection limit of 1 ppm can be achieved for some compounds when the analysis method is optimized The µTCD detects the difference in thermal conductivity of the gas traveling through the reference side pure carrier gas versus the gas traveling through the analytical side carrier gas ...

Page 25: ...me analytical conditions an unknown sample is then injected into the GC to determine its composition based on the pre determined peak retention time Quantitation of the target compounds in a GC analysis can be obtained by measuring the corresponding peak area presented in a chromatogram The peak area is proportional to the analyte concentration detected and can be obtained by integrating the peak ...

Page 26: ...e 2 module Micro GC Fusion chassis houses up to two analytical GC modules electrical components and internal plumbing The front panel display provides access to basic operating interfaces and controls Heated sample inlet 1 16 in Swagelok male connector A 1 8 in Quick Connect is provided if the optional Integrated Sample Conditioner is installed Front panel display See Front Panel Operation 149 for...

Page 27: ...Fi Antenna Boosts wireless signal strength and improves connectivity 4 HIGH PRESSURE PURGE VENT Vent for the Integrated Sample Conditioner if configured 5 CARRIER C1 and C2 Carrier gas connections with 1 8 in Swagelok connectors 6 PUMP Vent for the pump 7 AUX I O The AUX I O can be configured to remotely start or cancel sample runs 8 24V 24 V dc input from the external V ac V dc power adaptor 9 RJ...

Page 28: ...and controls Heated sample inlet The inlet is a 1 16 in Swagelok male connector A 1 8 in quick connect is provided if the optional integrated sample conditioner is installed Front panel display See Front Panel Operation 149 for details about using the front panel dis play to access routine operating controls On Standby button Use the illuminated On Standby button to power on or place the instrumen...

Page 29: ...GH PRESSURE VENT Vent for the integrated sample conditioner if configured 7 Wi Fi Antenna Boost wireless signal strength and improves connectivity 8 RJ 45 LAN connector Wired LAN connection 9 AUX I O The auxillary I O interface can be configured to remotely start or cancel sample runs 10 USB connectors Two USB interfaces are provided 11 Grounding Connect to the grounding when installed in a rack 1...

Page 30: ...ro GC Fusion allowing for parallel analysis on multiple GC modules The front sample inlet is heated and deactivated to avoid sample condensation and adsorption Inlet temperature can be set in the method which may range 30 140 C 86 284 F WARNING Micro GC Fusion has a heated inlet which is hot to the touch CAUTION Sample inlet gas pressure must be less than 172 kPa 25 psi Exceeding 172 kPa 25 psi wi...

Page 31: ...l of the 4 module chassis When one carrier gas connector is configured it supports the operation of all GC modules When two carrier gas connectors are configured on the 2 module chassis one will support GC module A and the other will support GC module B For the 4 module chassis the carrier gas connector can be configured with One carrier gas connector for Modules A and B one carrier gas connector ...

Page 32: ...an ual CAUTION Carrier gas inlet rear of instrument pressure must be between 400 427 kPa 58 62 psi Use a dual stage regulator on the carrier gas cylinder to ensure the pressure range is maintained Exceeding 565 kPa 82 psi may damage Micro GC Fusion and require factory repair ...

Page 33: ...AL REFERENCE PUMP HIGH PRESSURE PURGE VENT ANALYTICAL REFERENCE and PUMP vents require 1 8 in Swagelok connectors The HIGH PRESSURE PURGE VENT available only when the Integrated Sample Conditioner is installed requires a 1 8 in Swagelok connector Micro GC Fusion instruments shipped before October 2019 may have Luer Lock connectors for the ANALYTICAL REFERENCE and PUMP vents ...

Page 34: ...mbly In Backflush mode the PUMP vent is also used to vent the backflushed sample exhaust from the pre column 5 5 4 HIGH PRESSURE PURGE Vent When the Integrated Sample Conditioner is installed the HIGH PRESSURE PURGE VENT will require a 1 8 in Swagelok connector The high pressure sample will be regulated down to about 345 kPa 50 psi by the Integrated Sample Conditioner and then vented through the H...

Page 35: ...play The front panel display is used to load a stored method sequence run the loaded method sequence view run data and view system status For more details see Front Panel Operation 149 Complex operations such as method or sequence development require a separate computer with a larger display screen ...

Page 36: ...me sample source 5 7 1 Injection A gas sample is injected into Micro GC Fusion through the front and is directed to one or more GC modules simultaneously The MEMS injector on the GC module contains a sample loop and micro diaphragm valves which are used to direct the sample and carrier gas flows The sample volume is determined by the Inject ms time setting in the method The injector temperature is...

Page 37: ...e required Valid Inject ms time set points for the Variable Large Volume Injector range from 10 to 450 ms A typical set point is 100 ms An Inject ms time of 0 ms results in no injection Values less than 10 ms may result in poor repeatability Longer injection times allow larger volumes of sample to be injected which results in higher sensitivity on the µTCD The Variable Large Volume Injector may be...

Page 38: ...esult in a fixed injection volume This is best used for component concentrations above 0 1 and will result in higher precision For component concentrations below 0 1 the backflush injector can be operated as a variable volume injector An Inject ms time greater than 10 ms will allow larger sample volumes to be injected which in turn results in higher sensitivity on a µTCD Backflush times vary with ...

Page 39: ...column temperature can then be ramped to increase the elution speed of heavier components 5 7 3 Detection Micro GC Fusion uses a MEMS based µTCD and has a detection range from low ppm to high percent The Fusion Auto Sensing Technology FAST Enabled detector system automatically adjusts detector gain during a single sample run effectively eliminating the need of two sensitivity settings when analyzi...

Page 40: ... some compounds when the analyses method is optimized The µTCD detects the difference in thermal conductivity of the gas traveling through the reference column pure carrier gas versus the gas traveling through the analytical column carrier gas plus the sample gas The difference generates an electrical signal which when plotted over time creates a chromatogram for the sample gas ...

Page 41: ...ule and sends the data signal back to the software The GC module controller board is installed on the Micro GC Fusion chassis frame and is connected to the GC module interface board 5 7 4 2 GC Module Interface Board The GC module interface board is the interface between the GC module controller board and the analytical hardware components including electronics on the injector the resistively heate...

Page 42: ...nsistent µTCD external temperature allows for accurate and repeatable area counts even when the Micro GC Fusion is subjected to wide ambient temperature ranges This is important in applications such as natural gas or chemical process control monitoring where measurements are made at instrument locations that are subjected to wide temperature ranges The JP 100 has two method parameters located in t...

Page 43: ...talled It maintains the incoming sample at 100 C 212 F and reduces sample pressure from up to 6 895 kPa 1 000 psi down to approximately 83 kPa 12 psi prior to the sample being injected into the GC module WARNING Gas pressure on the HIGH PRESSURE PURGE VENT may be up to 448 kPa 65 psi Extreme caution must be taken to vent the high pressure sample to avoid personal injury ...

Page 44: ...midity 5 to 95 non condensing Altitude 2 000 m 6 562 ft Pollution degree 2 per EN 61010 Vibration MIL STD 810F 514 5C Highway Truck Vibration 4 module chassis Specification Maximum weight 15 4 kg 33 8 lb Dimensions L x W x H 47 5 x 43 2 x 27 1cm 18 7 x 17 x 10 7 in Installation Overvoltage Category II per IEC 60664 Power supply input 100 to 240 V ac 50 to 60 Hz 7A Power supply output 24 V dc 42 A ...

Page 45: ...essure 6 895 kPa 1 000 psi Minimum sample pressure 34 5 kPa 5 psi suggested for optimal purging 5 10 4 Gas Liquid Separator Gas Liquid Separator Specification Sample inlet 1 16 in Swagelok Maximum sample pressure 172 kPa 25 psi 5 10 5 Pressure Reducer and Gas Liquid Separator Pressure Reducer and Gas Liquid Separator Specification Sample inlet 1 8 in Swagelok Maximum sample pressure 3 450 kPa 500 ...

Page 46: ...ation Fused silica Wall coated open tubular WCOT Porous layer open tubular PLOT 5 10 9 Thermal Conductivity Detector Thermal Conductivity Detector Specification Internal volume 240 nL MEMS Detection limit 1 ppm n Hexane WCOT columns Linear dynamic range 10 6 10 5 10 10 Carrier Gas specifications Carrier Gas Specification Connector type 1 8 in Swagelok Source External pressurized cylinder Types Hel...

Page 47: ...eb browser This web based user interface can automatically adjust to the display screen size providing the user with the option of using computing devices with different screen sizes and resolutions The software user interface described in this operating manual references features delivered in Fusion software v1 8 release Updates to the software user interface will be described in the future revis...

Page 48: ...omputer RAM 2 GB minimum Hard Drive 100 GB minimum CPU 1 5 GHz minimum Screen Size 12 in minimum Resolution 1024 x 768 pixels minimum Network Connectivity Wi Fi or RJ 45 wired 5 11 2 Tablet Web Browser Requirement Micro GC Fusion supports the following tablet web browsers Android 4 stock browser Chrome or Firefox for Android Safari on iOS 6 for iPad Symbian is not supported 5 11 3 Computer Web Bro...

Page 49: ...t If the original antenna is damaged please contact the INFICON service department for a replacement antenna 5 12 1 Regulatory Compliance Information for UNITED STATES Users 5 12 1 1 FCC Statement This equipment has been tested and found to comply with the limits for a Class B digital device pursuant to Part 15 of the FCC rules These limits are designed to provide reasonable protection against har...

Page 50: ...liance information for Micro GC Fusion This equipment contains an OEM Embedded Wireless Bridge Ethernet to Wireless LAN Module This device complies with RSS 210 of Industry Canada IC and is subject to the following two conditions 1 This device may not cause harmful interference 2 This device must accept any interference received including interference that may cause undesired operation 5 12 2 1 In...

Page 51: ...pectrum Matters ERM Electromagnetic Compatibility EMC standard for radio equipment and services Part 17 Specific conditions for 2 4 GHz wideband transmission systems and 5 GHz high performance RLAN equipment EN 61010 1 Safety requirements for electrical equipment for measurement control and laboratory use 5 12 3 1 European User Restrictions CAUTION European usage restrictions apply to this instrum...

Page 52: ...o GC Fusion tyyppinen laite on direktiivin 1999 5 EY oleellisten vaatimusten ja sitä koskevien direktiivin muiden ehtojen mukainen Dutch Hierbij verklaart INFICON Inc dat het toestel Micro GC Fusion in overeenstemming is met de essentiële eisen en de andere relevante bepalingen van richtlijn 1999 5 EG Bij deze verklaart INFICON Inc dat deze Micro GC Fusion voldoet aan de essentiële eisen en aan de...

Page 53: ...C Fusion è conforme ai requisiti essenziali ed alle altre disposizioni pertinenti stabilite dalla direttiva 1999 5 CE Spanish Por medio de la presente INFICON Inc declara que el Micro GC Fusion cumple con los requisitos esenciales y cualesquiera otras disposiciones aplicables o exigibles de la Directiva 1999 5 CE Portugese INFICON Inc declara que este Micro GC Fusion está conforme com os requisito...

Page 54: ...itioner AUX I O power cord and factory checkout gas type Number for Module A a three digit number that specifies injector type column type and length detector type and venting connector type Number for Module B a three digit number that specifies injector type column type and length detector type and venting connector type At least one module must be specified for a system The module part number f...

Page 55: ...connector type Number for Module C a three digit number that specifies injector type column type and length detector type and venting connector type Number for Module D a three digit number that specifies injector type column type and length detector type and venting connector type At least three modules must be specified for a system The module part number for Module D is only specified when Modu...

Page 56: ... inlet Philips 2 screwdriver for rack mounting The following tools and parts are included in the optional Install Kit PN 952 021 G1 to facilitate installation If the optional install kit was not purchased the tools and parts below must be provided by the user upon installation PN Description Quantity 059 0442 Ball valve 2 way 0 125 tube brass RoHS 2 pc 059 0449 Union tee 0 125 Tube 0 437 nut brass...

Page 57: ...n CAUTION Carrier gas inlet rear of instrument pressure must be between 400 427 kPa 58 62 psi Use a dual stage regulator on the carrier gas cylinder to ensure the pressure range is maintained Exceeding 565 kPa 82 psi may damage Micro GC Fusion and require factory repair Moisture hydrocarbon trap PN G2870A 01 is required for the carrier gas when using Molsieve or Alumina columns CAUTION To protect ...

Page 58: ...ecific to the analysis Calibration gas must be available at the time of installation Calibration gas must closely resemble the composition of the actual process gas A regulator if necessary to reduce calibration gas pressure below 69 kPa 10 psi at the Micro GC Fusion inlets The regulator must be clean grease free and non venting Copper or stainless steel tubing pre cleaned 1 16 in OD for calibrati...

Page 59: ...ures higher than 172 kPa 25 psi must be reduced When a Pressure Reducer and Gas Liquid Separator PN 952 033 G1 is installed a sample pressure of up to 3 450 kPa 500 psi can be introduced 6 1 5 Installation Space and Venting Installation space required for Micro GC Fusion is an additional 6 5 cm 2 5 in to the front back and sides of the instrument Dimensions of a 2 module Micro GC Fusion 46 2 x 19 ...

Page 60: ...l trap or reaction medium Avoid venting Micro GC Fusion into drafty areas such as in front of a heating cooling vent 6 1 6 Power Requirement Standard 100 240 V ac 50 to 60 Hz 5A minimum electric outlet for 2 module systems Standard 100 240 V ac 50 to 60 Hz 7A minimum electric outlet for 4 module systems Maximum power for a 2 module Micro GC Fusion system 300W Uninterruptible AC power source with s...

Page 61: ...y 100 GB CPU 1 5 GHz Screen size 12 in Resolution 1024 x 768 pixels Network Connectivity Wi Fi or RJ 45 wired 6 1 8 EZ IQ Computer Requirement A driver software can be installed on the EZ IQ chromatography software to control Micro GC Fusion Minimum hardware configuration required to run the optional EZ IQ software RAM 2 GB Memory 10 GB CPU 2 GHz Resolution 1024 x 768 pixels Network connectivity R...

Page 62: ...GC Fusion hostname and static IP address when Dynamic Host Configuration Protocol DHCP is used to assign the Micro GC Fusion IP address 6 1 10 Web Browser Requirement Micro GC Fusion supports the following tablet web browsers Android 4 stock browser Google Chrome or Firefox for Android Safari on iOS 6 for iPad Symbian is not supported Micro GC Fusion supports the following computer web browsers Go...

Page 63: ...952 417 G1 Nut and ferrule set 0 062 and 0 125 1 pc 600 1190 P4 Ethernet communication cable 4 3 m 1 pc 074 666 P1 Micro GC Fusion quick start guide 1 pc 6 2 2 2 Configuration Dependent Parts Sample inlet parts PN Description Inlet Quantity 952 423 P1 Filter and holder assembly 0 062 Front 1 pc FRL 1269 Dual end ferrule for 1 16 in inlet Front 2 pc 952 418 G1 Gas sample tube 0 062 with nuts Front ...

Page 64: ...f Micro GC Fusion The vent ports on the back of Micro GC also use 1 8 in Swagelok connectors This section reviews how to construct Swagelok connections and connect tubing to a fitting such as the sample inlet s carrier gas inlet s vents or the gas supply tank Materials Needed 1 8 in OD pre cleaned copper or stainless steel tubing 1 8 in Swagelok nuts and front and back ferrules Two 7 16 in wrenche...

Page 65: ...emale fitting steady and another 7 16 in wrench to turn the Swagelok fitting 8 Unscrew the Swagelok fitting Connect the tubing with the Swagelok fitting and ferrules to the pencil marked location Tighten the nut 1 4 turn past finger tight CAUTION Do not overtighten Overtightening can damage the fitting and restrict gas flow Micro GC Fusion is equipped with a 1 16 in sample inlet Swagelok connector...

Page 66: ...Gas cylinders may present a hazard under extreme temperature conditions Do not store gas cylinders in the path of heated oven exhausts or other sources of heat Do not expose cylinders to extreme cold or heat It is recommended to store or place cylinders in a temperature controlled environment WARNING Wear eye protection when using compressed gas WARNING Many gases are explosive when their concentr...

Page 67: ...ints to Micro GC Fusion 15 cm 6 in Cut off valve not provided Install the carrier gas particulate filter using the supplied fittings within 15 cm 6 in of the Micro GC Fusion fitting to maximize its effectiveness Use a cut off valve not provided for ease of maintenance The valve should be packless sealed to atmosphere and grease free Do not use common industrial or home supply ball valves Chemical ...

Page 68: ...nk and flush the carrier gas supply line with carrier gas for five to ten seconds DANGER Many gases are explosive when their concentration builds up over time through leaks poor connections or a loss of ventilation Verify system integrity prior to using hydrogen or other gases in enclosed environments WARNING Safely vent carrier and sample streams potentially toxic noxious asphyxiant oxygen displa...

Page 69: ...g capability as the 10 micron filter 6 4 1 Sample Inlet Filter Parts List Description PN Sample inlet filter assembly 952 423 P1 Dual ended ferrule FRL 1269 Replacement filter disks 5 pk 059 0718 6 4 2 Tools Required Two 7 16 in wrenches One 5 16 in wrench 6 4 3 Sample Inlet Filter Assembly Installation 1 Shut off sample flow to Micro GC Fusion 2 Reduce the temperature of the sample inlet by loadi...

Page 70: ...Filter disk Dual ended ferrule 6 Place the dual ended ferrule inside Part A 7 Connect the sample inlet filter to the sample inlet 8 Turn Part A clockwise until finger tight then use a 7 16 in wrench to tighten an additional 1 4 turn CAUTION Do not overtighten the sample inlet filter assembly to Micro GC Fusion This will damage the dual ended ferrule 9 Finger tighten the sample line to the male por...

Page 71: ...750 lg phil oval head SS 8 074 683 P1 Micro GC Fusion rack mount IS 1 PN 070 2026 is preassembled on PN 952 4005 P2 and 952 4006 P2 at the factory 6 5 2 Required Tools Phillips head screw driver 3 mm hex driver 6 5 3 Rack Mount Kit Installation The following procedure indicates the necessary materials and proper procedure when installed the 4 module Micro GC Fusion into a rack 1 Ensure the instrum...

Page 72: ...ck mount brackets onto the unit prior to rack installation if access to the underside is not available ð Attach the four retainer nuts to the left bracket PN 952 4006 P2 in the four hole locations ð Place the left bracket PN 952 4006 P2 on the rack as shown below and line up the holes with the retainer nuts ð Thread the oval head screw PN 090 077 through the washer PN 070 2028 as shown then screw ...

Page 73: ... ð To attach the right bracket PN 952 4005 P2 repeat step 3 4 Once both brackets are secure gently place Micro GC Fusion onto rack mount brackets 5 Line up the holes on the bottom of the unit to the holes in the brackets 6 Secure the instrument on the brackets with the provided flat Phillips head screw PN 090 062 7 Micro GC Fusion is now attached to the rack ...

Page 74: ...UTION The gas liquid separator filters out liquid droplets in a gas sample It is not intended for liquid injections CAUTION Sample inlet gas pressure must be less than 172 kPa 25 psi Exceeding 172 kPa 25 psi will damage Micro GC Fusion and require factory repair WARNING Gas pressure on the gas liquid separator sample vent may be up to 172 kPa 25 psi Extreme caution must be taken when venting the h...

Page 75: ...t tubing for the 2 module Micro GC Fusion 1 952 4029 P1 1 16 in SS sample output tubing for the 4 module Micro GC Fusion 1 059 0696 Nut 0 062 tube 0 312 hex 0 031 LG SS RoHS 1 059 0697 Ferrule set 0 062 tube SS RoHS 1 084 031 Washer 4 flat SS 2 B3079191X Screw M3 x 8 2 HDW 2170 Filter membrane replacement 1 B307919X screw x 2 084 031 washer x 2 952 4029 P4 1 16 in sample output tubing for 2 module...

Page 76: ...ts in a gas sample It is not intended for liquid injections WARNING Gas pressure on the gas liquid separator sample vent may be up to 172 kPa 25 psi Extreme caution must be taken when venting the high pressure sample to avoid personal injury 6 6 4 1 2 Module Chassis To install the gas liquid separator onto a 2 module Micro GC Fusion 1 Press the On Standby button once to shutdown Micro GC Fusion Th...

Page 77: ... the gas liquid separator for the 2 module chassis as shown Hold the gas liquid separator so that the slots on the gas liquid separator align with the holes on Micro GC Fusion 7 Use a 2 mm hex driver to secure the gas liquid separator to the Micro GC Fusion chassis bottom with the two washers 084 031 and the two 8 mm M3 screws B3079191X 8 Turn Micro GC Fusion back to the upright position ...

Page 78: ...separator lays flat on the surface 10 Insert the sample output tubing for the 2 module chassis 952 4029 P4 into the Valco fitting on the gas liquid separator Do not tighten The tubing should be loose 11 Place the 1 16 in nut 059 0696 and the ferrule set 059 0697 onto the end of the sample output tubing going to Micro GC Fusion ...

Page 79: ...eparator sample vent to a fume hood or other safe location 15 Reconnect all electrical cables including the power cable and Ethernet cable 16 Reconnect the carrier gas and venting connections 17 Turn on Micro GC Fusion Connect a sample to the sample inlet on gas liquid separator to perform an analysis WARNING Safely vent carrier and sample streams potentially toxic noxious asphyxiant oxygen displa...

Page 80: ...strument may be damaged if the incoming sample pressure is greater than 172 kPa 25 psi 6 6 4 2 4 Module Chassis To install the gas liquid separator onto a 4 module Micro GC Fusion 1 Press the On Standby button once to shutdown Micro GC Fusion This shutdown procedure cools down the analytical columns before powering down and may take 1 to 2 minutes 2 Remove all electrical cables including the power...

Page 81: ...d separator for the 4 module chassis as shown Hold the gas liquid separator so that the slots on the gas liquid separator align with the holes on Micro GC Fusion 6 Use a 2 mm hex driver to secure the gas liquid separator to the Micro GC Fusion chassis bottom with the two washers 084 031 and the two M3 x 8 screws B3079191X 7 Turn Micro GC Fusion back to the upright position ...

Page 82: ... for the 4 module chassis 952 4029 P1 into the Valco fitting on the gas liquid separator Do not tighten The tubing should be loose 10 Place the 1 16 in nut 059 0696 and the ferrule set 059 0697 onto the end of the sample output tubing going to Micro GC Fusion 11 Connect the sample output tubing from the gas liquid separator to the Micro GC Fusion sample inlet and tighten using a 5 16 in wrench ...

Page 83: ... to the sample inlet on the gas liquid separator to perform an analysis WARNING Safely vent carrier and sample streams potentially toxic noxious asphyxiant oxygen displacing or flammable gases outside Micro GC Fusion and away from the operating area Vent toxic gases to a fume hood chemical trap or reaction medium CAUTION Ensure the vent tubing is not inclined upward to prevent potential liquid acc...

Page 84: ...s Dynamic Host Configuration Protocol DHCP by default This means no static IP address is preassigned from the factory When Micro GC Fusion is connected to a computer through a direct Ethernet cable and the computer is configured to accept an IP address automatically Micro GC Fusion will dynamically assign an IP address to the computer such that both devices are connected automatically Under dynami...

Page 85: ...nstallation 6 074 594 P1H Micro GC Fusion Operating Manual 85 319 3 Click System Configuration 4 Uncheck the Static IP Address checkbox to achieve dynamic IP addressing 5 Micro GC Fusion is now setup to use DHCP ...

Page 86: ...his static IP address Three blocks of IP address spaces are reserved by the Internet Assigned Numbers Authority IANA for private internets INFICON recommends using these IP addresses for setting up a static IP address on Micro GC Fusion Start IP Address End IP Address Remarks 10 0 0 0 10 255 255 255 24 bit block 10 8 prefix one class A 172 16 0 0 172 31 255 255 20 bit block 172 16 12 prefix 16 con...

Page 87: ...P1H Micro GC Fusion Operating Manual 87 319 3 Click System Configuration 4 In the System Configuration window ð Check the Static IP Address ð Enter the static IP address Subnet Mask and Default Gateway if applicable ð Click the icon ...

Page 88: ... To connect a computer or a device to Micro GC Fusion through the wireless connection 1 Locate the wireless connection serialnumber local on the web enabled wireless device tablet computer smartphone under available networks 2 Connect using the wireless password ex inficongc 3 Open a supported web browser 4 Type 10 10 0 1 in the address bar to access the Micro GC Fusion main screen Micro GC Fusion...

Page 89: ...ick System Administration 3 Click System Configuration 4 In the System Configuration window clear the Wireless check box 6 8 2 Changing the Wireless Password 1 Click the icon 2 Click System Administration 3 Click System Configuration 4 In the System Configuration window select the Wireless check box and type a new Password ...

Page 90: ...the power connector is properly connected 2 Micro GC Fusion ships with a country specific power cord Connect the end of this power cord to the 24 V dc power supply PN 952 435 P1 3 Connect the other end of the power cord to the 100 240 V ac power source With the power supply properly connected Micro GC Fusion can be powered on by pressing the On Standby button on the front panel CAUTION Using an al...

Page 91: ...usion Operating Manual 91 319 6 10 Carrier Gas Configuration By default Micro GC Fusion is set to use helium carrier gas for all GC modules 1 Click the icon to change the carrier gas type 2 Click System Administration 3 Click System Configuration ...

Page 92: ...NFICON 92 319 074 594 P1H Micro GC Fusion Operating Man ual 4 In the System Configuration window select the desired carrier gas from the shortcut menu for each GC module 5 Click Pressure Units to switch from psi to kPa ...

Page 93: ... Micro GC Fusion Operating Manual 93 319 6 11 Set Instrument Time To set Micro GC Fusion to the same time as the connected device 1 Click the icon to change the instrument time 2 Click System Administration 3 Click System Configuration ...

Page 94: ...6 Installation INFICON 94 319 074 594 P1H Micro GC Fusion Operating Man ual 4 In the System Configuration window click the icon to set the instrument time ...

Page 95: ... other end can be fitted with a desired connector type 2 Module chassis 4 Module chassis The AUX I O connector pin outputs are listed in the table below Pin Function Color 1 Provides 5 mA remote input Black 2 REMOTE_START input White 3 REMOTE_START input Red 4 Variable GND Green 5 Provides 5V pull up for logic command Orange 6 Provides 5V pull up for logic command Blue 7 Contact closure output FAU...

Page 96: ...art cancel circuitry Purpose Pin Connection Action Remote Start Pin 1 and pin 2 Connect together to activate circuit Pin 3 and pin 4 No action when open Trigger REMOTE_START when closed Remote Cancel Pin 9 and pin 10 Connect together to activate circuit Pin 11 and pin 12 No action when open Trigger REMOTE_CANCEL when closed If the REMOTE_CANCEL contacts are closed Micro GC Fusion opens the READY_O...

Page 97: ...he instrument The proper USB cable is provided with the Valco stream selector Sample streams can be connected to the Valco stream selector with any one of the following valve types SD Dead ended sample streams are dead ended at the stream selection valve SC Common outlet all sample streams vent to a common outlet port SF Flow through each sample stream continuously flows through the stream selecti...

Page 98: ...the Valco stream selector accessories two 1 4 in wrench one 5 16 in wrench one 7 16 in wrench 1 16 in OD stainless steel sample line s 6 13 1 2 Valco Stream Selector Accessories INFICON offers a 10 port SD and a 10 port SF Valco stream selector as an accessory When sample or calibration gas is in short supply and sample composition does not change drastically over time the dead ended SD Valco stre...

Page 99: ...ccessories have 1 16 in sample line filters installed at each inlet port These sample lines are leak checked at the factory and are labeled to provide clear identification For instance the sample port 1 is labeled as 1 IN and sample port 2 is labeled as 2 IN The outlet sample line going into the GC is labeled as OUT TO GC 6 13 1 3 10 Port SD Valco Stream Selector Accessory Description Quantity Pho...

Page 100: ...6 Installation INFICON 100 319 074 594 P1H Micro GC Fusion Operating Man ual Description Quantity Photo Power cord 1 Manual remote 1 USB cable 1 Nut and ferrules 11 each ...

Page 101: ...tion 6 074 594 P1H Micro GC Fusion Operating Manual 101 319 6 13 1 4 10 Port SF Valco Stream Selector Accessory Description Quantity Photo 10 Port SF Valco stream selector 1 Power supply 1 Power cord 1 Manual remote 1 ...

Page 102: ...ity Photo USB cable 1 Nuts and ferrules 21 of each 6 13 1 5 Installing the 10 Port SD Valco Stream Selector Accessory 1 Identify sample line 1 IN and remove the black filter caps from the desired sample line ports 2 Place a union fitting and ferrule onto a 1 16 in OD stainless steel sample line ...

Page 103: ...on fitting and then tighten it again 6 Repeat steps 1 5 for sample lines to 2 IN filter 3 IN filter etc until the desired number of sample lines are connected 7 Place a union fitting and ferrule onto a 1 16 in OD stainless steel sample line 8 Connect the 1 16 in OD stainless steel tubing to the OUT TO GC union 9 While holding the OUT TO GC fitting with a 1 4 in wrench use a 1 4 in wrench to turn t...

Page 104: ...ing a 5 16 in wrench 12 Plug the DC power connector on the power supply into the back of the Valco stream selector Connect the AC power connector on the power supply into a 100 240V ac power source 13 Connect the USB Type B connector of the USB cable to the back of the Valco stream selector Connect the USB Type A connector of the USB slot in the back of Micro GC Fusion ...

Page 105: ... the internal actuator 15 To validate that the Valco stream selector was installed successfully open the Micro GC Fusion Main Page on any supported web browser or wireless device The Valve Position quick select menu will appear enabling the user to select a valve position 16 For instructions on Valco stream selector configuration see Valco Stream Selector Operation 237 ...

Page 106: ... sample line ports 2 Place a union fitting and ferrule onto a 1 16 in OD stainless steel sample line 3 Connect the 1 16 in sample line to the 1 IN filter on the Valco stream selector 4 While holding the filter with a 7 16 in wrench use a 1 4 in wrench to turn the union fitting Over tighten by 1 2 turn to swage the union fitting and ferrule onto the 1 16 in sample line 5 Loosen the union fitting an...

Page 107: ...ENT union on the Valco stream selector 9 While holding the union with a 1 4 in wrench use a 1 4 in wrench to turn the union fitting Over tighten by 1 2 turn to swage the union fitting and ferrule onto the 1 16 in sample line 10 Loosen the union fitting and then tighten it again 11 Repeat steps 7 9 to connect vent lines to POS 2 VENT POS 3 VENT etc to the corresponding venting lines If connecting a...

Page 108: ...wage the union fitting and ferrule onto the 1 16 in sample line 14 Loosen the fitting and then tighten it again 15 Swage the 1 16 in OD stainless steel tubing to the Micro GC Fusion 1 16 in front inlet using a 5 16 in wrench 16 Plug the DC power connector on the power supply into the back of the Valco stream selector Connect the AC power connector on the power supply into a 100 240V ac power sourc...

Page 109: ...nect the USB Type B connector of the USB cable to the back of the Valco stream selector Connect the USB Type A connector of the USB slot in the back of Micro GC Fusion 18 Connect the Manual Controller to the back of the Valco stream selector to manually control the internal actuator ...

Page 110: ...The Valve Position quick select menu will appear enabling the user to select a valve position 20 For instructions on Valco stream selector configuration see Valco Stream Selector Operation 237 WARNING Safely vent carrier and sample streams potentially toxic noxious asphyxiant oxygen displacing or flammable gases outside Micro GC Fusion and away from the operating area Vent toxic gases to a fume ho...

Page 111: ...ont Panel Language Selection Micro GC Fusion provides the option of using the English or Chinese language on the front panel display To change the front panel display language 1 Click the icon to change the instrument language 2 Click System Administration 3 Click System Configuration ...

Page 112: ... 594 P1H Micro GC Fusion Operating Man ual 4 In the System Configuration window click the drop down box under Front Panel Language and select the desired language 5 Refresh the front panel display to allow the new setting to take effect ...

Page 113: ...s 100 mL min the output pressure from the device to Micro GC Fusion may exceed the acceptable pressure range causing instrument damage CAUTION Blocking off the venting port during operation significantly increases the output pressure from the device to Micro GC Fusion When this happens the Micro GC Fusion connected to the device may be damaged if the incoming sample pressure is greater than 172 kP...

Page 114: ...ing items These items are needed to install the device on the side of a 2 module Micro GC Fusion chassis PN Description Quantity 059 0696 5 16 in female nut 1 059 0697 1 16 in ferrule set 1 059 0336 1 16 in Valco male nut 1 059 0335 1 16 in ferrule 1 952 229 G1 sample tube 1 pressure reducer and gas liquid separator assembly 1 There are three tubes in kit PN 952 229 G1 and the medium length tube i...

Page 115: ...lation 1 Turn off the instrument by following the system shutdown procedure in Shutdown Procedure 251 2 Disconnect all the electrical cables including the power cable and Ethernet cable from the instrument 3 Disconnect the sample gas connection s the carrier gas connection s and the venting connections from the instrument 4 Ensure that Bracket C is positioned with one large and two small holes at ...

Page 116: ...g bracket to the positions shown If the nut positions need adjustment relax the nuts adjusting the mounting bracket and re tighten the nuts using a 3 8 in wrench 6 Clamp the mounting bracket onto the left side of the instrument 7 Ensure the bottom mounting bracket hole is fitted into the lower left chassis foot ...

Page 117: ...al 117 319 8 Adjust the nut position to remove the gap between the mounting bracket and the chassis top 9 Tighten all nuts with a 3 8 in wrench to fix the bracket on the instrument chassis 10 Put the Valco ferrule PN 059 0335 and the nut PN 059 0336 on the inlet tube ...

Page 118: ... turn the nut into the detail until it is finger tight Using the 1 4 in open ended wrench turn the nut 1 4 turn 90 past the point where the ferrule first starts to grab the tubing The amount of force required can vary considerably due to the friction between the nut and the treads and the composition and wall thickness of the tubing used 12 Put the 5 16 in Swagelok nut PN 059 0696 and the 1 16 in ...

Page 119: ...he 1 16 in sample tubing with the Swagelok fittings onto the instrument sample inlet Tighten 1 2 turn past finger tight using the 5 16 in wrench 14 The pressure reducer and gas liquid separator installation is complete Reconnect the power cable the Ethernet cable and the carrier gas lines ...

Page 120: ...en the pressurized sample is connected 16 Install a user provided 1 8 in sample line with the female Swagelok fittings preinstalled 17 Connect a vent line to the vent fitting using 1 8 in Swagelok fittings Run the exhaust to a fume hood or other designated area for hazardous waste disposal 18 Slowly open the dial to allow the sample to flow through the device Check the flow indicated on the flow g...

Page 121: ...nt toxic gases to a fume hood chemical trap or reaction medium 6 15 2 4 Module Micro GC Fusion Chassis Installation Side Install The pressure reducer and gas liquid separator includes the following items These items are needed to install the device on the side of a 4 module Micro GC Fusion chassis PN Description Quantity 059 0696 5 16 in female nut 1 059 0697 1 16 in ferrule set 1 059 0336 1 16 in...

Page 122: ...installation 1 Turn off the instrument by following the system shutdown procedure in Shutdown Procedure 251 2 Disconnect all the electrical cables including the power cable and Ethernet cable from the instrument 3 Disconnect the sample gas connection s the carrier gas connection s and the venting connections from the instrument 4 Ensure that Bracket C is positioned with two small holes at the bott...

Page 123: ... the positions shown If the nut positions need adjustment relax the nuts adjusting the mounting bracket and re tighten the nuts using a 3 8 in wrench 6 Clamp the mounting bracket onto the left side of the instrument with the large hole on the bottom of the mounting bracket fitting into the left front foot of the instrument ...

Page 124: ...ual 7 Push the top of the mounting bracket towards the instrument until it fits tightly 8 Adjust and tighten all the nuts using a 3 8 in wrench to fix the mounting bracket on the instrument chassis 9 Put the Valco ferrule PN 059 0335 and the nut PN 059 0336 on the inlet tube ...

Page 125: ... the nut into the detail until it is finger tight Using the 1 4 in open ended wrench turn the nut 1 4 turn 90 past the point where the ferrule first starts to grab the tubing The amount of force required can vary considerably due to the friction between the nut and the treads and the composition and wall thickness of the tubing used 11 Put the 5 16 in Swagelok nut PN 059 0696 and the 1 16 in ferru...

Page 126: ...e 1 16 in sample tubing with the Swagelok fittings onto the instrument sample inlet Tighten 1 2 turn past finger tight using the 5 16 in wrench 13 The pressure reducer and gas liquid separator installation is complete 14 Reconnect the power cable the Ethernet cable and the carrier gas lines ...

Page 127: ... the pressurized sample is connected 16 Install a user provided 1 8 in sample line with the female Swagelok fittings preinstalled 17 Connect a vent line to the vent fittings using 1 8 in Swagelok fittings Run the exhaust to a fume hood or other designated area for hazardous waste disposal 18 Slowly open the dial to allow the sample to flow through the device Check the flow indicated on the flow ga...

Page 128: ...me hood chemical trap or reaction medium 6 15 3 4 Module Micro GC Fusion Chassis Installation Front Install The pressure reducer and gas liquid separator includes the following items These items are needed to install the device on the front of a 4 module Micro GC Fusion chassis PN Description Quantity 059 0696 5 16 in female nut 1 059 0697 1 16 in ferrule set 1 059 0336 1 16 in Valco male nut 1 05...

Page 129: ...g this installation 1 Turn off the instrument by following the system shutdown procedure in Shutdown Procedure 251 2 Disconnect all the electrical cables including the power cable and Ethernet cable from the instrument 3 Disconnect the sample gas connection s the carrier gas connection s and the venting connections from the instrument 4 Ensure that Bracket C is positioned with two small holes at t...

Page 130: ... mounting bracket to the positions shown If the nut positions need adjustment relax the nuts adjust the mounting bracket and re tighten the nuts using a 3 8 in wrench 6 Clamp the mounting bracket on the instrument front with the mounting bracket bottom to the right side of the instrument left front foot ...

Page 131: ... GC Fusion Operating Manual 131 319 7 Put the two M3 screws PN B3079191X through the two small holes in the mounting bracket bottom and into the instrument chassis bottom with a 2 0 hex driver 8 Loosen the top two nuts on the mounting bracket ...

Page 132: ...ting Man ual 9 Slide in bracket E Bracket E 10 Fit the two inserts of bracket E into the air vent Push or pull the front cover as required to align it into the air vent opening 11 Tighten the two nuts using a 3 8 in wrench to ensure that bracket E does not fall off ...

Page 133: ...ounting bracket on the instrument chassis 13 Put the Valco ferrule PN 059 0335 and the nut PN 059 0336 on the inlet tube 14 Insert the sample tubing with the Valco fittings into the fitting detail on the Genie filter Push the tubing all the way into the detail so that it seats firmly Manually turn the nut into the detail until it is finger tight ...

Page 134: ...grab the tubing The amount of force required can vary considerably due to the friction between the nut and the treads and the composition and wall thickness of the tubing used 16 Put the 5 16 in Swagelok nut PN 059 0696 and the 1 16 in ferrule set PN 059 0697 on the other end of the sample tube 17 Insert the 1 16 in sample tubing with the Swagelok fittings onto the instrument sample inlet ...

Page 135: ...he pressure reducer and gas liquid separator installation is complete Reconnect the power cable the Ethernet cable and the carrier gas lines 20 Before connecting the pressurized sample to the device close the metering valve by turning the dial fully clockwise to ensure no sample flow through the device when the pressurized sample is connected ...

Page 136: ... device Check the flow indicated on the flow gauge and set the limit to less than 100 mL min 24 Turn on Micro GC Fusion The instrument is ready to perform an analysis CAUTION If the flow rate through the device exceeds 100 mL min the output pressure from the device to Micro GC Fusion may exceed the acceptable pressure range causing instrument damage WARNING Safely vent carrier and sample streams p...

Page 137: ... Operating Manual 137 319 6 15 4 Change Mounting Bracket Orientation 1 Loosen the lower three nuts inside the mounting bracket using a 3 8 in wrench 2 Turn the mounting bracket upside down 3 Install the top two nuts in the back of the mounting bracket ...

Page 138: ... 138 319 074 594 P1H Micro GC Fusion Operating Man ual 4 Remove the two bottom nuts 5 Align the three holes and screws and then press the mounting bracket and the device together Reattach the three nuts using a 3 8 in wrench ...

Page 139: ...nlet to remove residual gas in the sample line When the Integrated Sample Conditioner is configured on an instrument the Micro GC Fusion main page provides a command button to purge the sample line and the internal volume of the sample conditioner Refer to Purge Integrated Sample Conditioner 250 7 3 Front Sample Inlet Micro GC Fusion provides flexible inlet options Depending on the configuration a...

Page 140: ...25 psi will damage Micro GC Fusion and require factory repair WARNING Micro GC Fusion has a heated inlet which is hot to the touch 7 3 2 Front Sample Inlet Integrated Sample Conditioner When an Integrated Sample Conditioner is installed the front sample inlet is replaced by a 1 8 in Quick Connect CAUTION The 1 8 in HIGH PRESSURE PURGE connector on the back panel should not be restricted when a pre...

Page 141: ...ures must not exceed 172 kPa 25 psi or 6 895 kPa 1 000 psi when the optional Integrated Sample Conditioner is installed CAUTION Sample inlet gas pressure must be less than 172 kPa 25 psi Exceeding 172 kPa 25 psi will damage Micro GC Fusion and require factory repair CAUTION When using the Integrated Sample Conditioner sample inlet pressure must not exceed 6 895 kPa 1 000 psi Exceeding 6 895 kPa 1 ...

Page 142: ...me 3 Disconnect the syringe from the sample gas and connect it to the GC inlet 4 Depress the plunger using a slight pressure to inject when the GC is ready to sample 7 5 1 Syringe Sampling Kits The Ship Kit Syringe Luer Adapator PN 952 024 G1 includes a luer fitting which will adapt the PTFE luer lock termination on the gas tight syringe to the 1 16 in sample inlet on Micro GC Fusion The short nee...

Page 143: ...he Syringe Luer Adapter clockwise until finger tight 7 6 Sampling Using Bags 1 Open a new sample bag 2 Connect the sample bag to the sample source 3 Open the sample source 4 Fill the sample bag close it and disconnect from the sample source 5 Close the sample source 6 Connect the sample bag to the Micro GC Fusion inlet using stainless steel or Teflon tubing An adapter may be required to connect th...

Page 144: ... PN 059 0264 to adapt the polypropylene tube fitting on a sample bag to a 1 16 in stainless steel sample line The Ship Kit SS Adapter and 10 Pack 3L Sample Bag PN 952 027 G1 includes one Ship Kit SS Adapter for Sample Bag PN 952 026 G1 and ten 3 L sample bags with polypropylene screw cap valve PN 070 1726 7 6 2 Installing a SS Adapter onto a Sample Bag 1 Remove the 3 16 in nut from the reducing un...

Page 145: ... nut with the narrow end facing outwards ð Place the Teflon front ferrule into the nut with the narrow end facing outwards The two ferrules are designed to fit together 4 Screw the 3 16 in stainless steel nut with the Teflon ferrules back into the reducing union PN 059 0298 5 Insert the 1 4 in tube fitting on the 3 L sample bag into the 3 16 in end of the SS Adapter for the Sample Bag and screw cl...

Page 146: ... Separator The gas liquid separator provides gas liquid separation through a Genie filter Refer to Installing the Gas Liquid Separator 74 for the device installation procedure CAUTION Sample inlet gas pressure must be less than 172 kPa 25 psi Exceeding 172 kPa 25 psi will damage Micro GC Fusion and require factory repair ...

Page 147: ...quid particulates in the sample The maximum sample input pressure is 3450 kPa 500 psi Refer to Pressure Reducer Genie Filter and Gas Liquid Separator 113 for the device installation procedure The pressure reducer and gas liquid separator is not compatible with the integrated sample conditioner of the gas liquid separator PN 952 022 G1 CAUTION The gas liquid separator filters out liquid droplets in...

Page 148: ...ner is factory installed It maintains the incoming sample at 100 C 212 F and reduces the sample pressure from up to 6 895 kPa 1 000 psi down to 83 kPa 12 psi prior to the sample being injected into the GC module WARNING Gas pressure on the HIGH PRESSURE PURGE VENT may be up to 448 kPa 65 psi Extreme caution must be taken to vent the high pressure sample to avoid personal injury ...

Page 149: ...iled operation such as editing a method viewing previous runs editing integration events and entering calibration data can only be performed by connecting an external computer or tablet The front panel user interface described in this section references features delivered in Fusion software v1 8 release 8 2 Launch Software The Micro GC Fusion front panel display turns on when the On Standby button...

Page 150: ...usion Operating Manual Wrench Y Access to system status The figure and table below illustrate the labels and buttons on the front panel display 1 2 3 4 5 Item Name Function 1 Method or Sequence Preset Buttons Provides access to stored methods or sequences 2 RUN Button Initiates a sample run based on the loaded method or sequence 3 Method or Sequence Loaded Displays the loaded method or sequence 4 ...

Page 151: ...e Operation 158 Methods cannot be created or edited on the Micro GC Fusion front panel display See Method Development 161 to develop a method on a tablet or computer Perform the following steps to load a method or sequence onto the front panel display 1 Select the desired method or sequence preset button on the front panel display 2 The center button will display Loading until the instrument has r...

Page 152: ...he desired method or sequence is loaded If not load the desired method or sequence by following the steps in Select and Load a Method or Sequence 151 2 Tap the green RUN button to begin a sample run 3 The RUN button displays Running and the process of the run is indicated by the movement of the blue band on the circumference of the button 4 Once the run is completed and the starting method conditi...

Page 153: ...play changes to a red STOP button which can be used to stop a running sequence 1 While a sequence is running tap the STOP button to abort the sequence 2 Micro GC Fusion finishes the current run and returns to the initial state of the currently loaded method This may take a few minutes depending on the progress and duration of the interrupted method A notification is displayed advising the sequence...

Page 154: ...ation message to enter the report window 2 Alternately tap the icon followed by View Result to view the report 3 The chromatogram displays on the top half of the screen A table of the compound names RT s retention time in seconds Area µV peak area in µV and Conc mole or Conc ppm concentration in mole or ppm is displayed Tap the and icons on the right to scroll up or down ...

Page 155: ...perating Manual 155 319 4 To optimize screen resolution the table only displays analysis results for one module at a time The user can select which module to display using a drop down control Tap the module name to select the analysis result on a different module ...

Page 156: ...rating Man ual 8 7 View System Status Tap the icon to display the System Status screen Tap the desired module The following information is displayed module serial number and part number installed module information temperature and pressure set points and real time readings ...

Page 157: ...ed in the method The System Status window displays both the set points and the actual readings of the temperatures and pressures for the Micro GC Fusion analytical components 8 8 Front Panel Language Micro GC Fusion provides the option of using the English or Chinese language on the front panel display Refer to Front Panel Language Selection 111 for the procedure to change the language setting ...

Page 158: ...tware v1 8 release 9 2 Launch Software User Interface To access the Micro GC Fusion software user interface 1 Open a supported web browser on a computer or tablet Refer to Computer Web Browser Requirement 48 2 Type http followed by either the Micro GC Fusion hostname or IP address in the web browser address bar Bonjour Print Service for Windows is required for a Windows computer to recognize the h...

Page 159: ...ler Information Y Access to operating manual Wrench Y Access to system status The figure and table below illustrate the tabs labels and buttons on the main page 1 2 3 4 5 6 7 8 9 10 Item Name Function 1 Run tab Displays the method or sequence preset buttons and the RUN button 2 Chromatogram Tab Displays the chromatogram of the current run in real time 3 Report Tab Displays the analysis result of t...

Page 160: ...quence 9 Notifications Label Displays system status or error messages 10 Hostname and IP Address Label Displays the instrument network hostname and IP address 9 3 Micro GC Fusion Workflow The following outlines key steps in the Micro GC Fusion workflow 1 Method Development 2 View Instrument Status 3 Run Method 4 View Chromatogram 5 View Report 6 View Data Browser 7 Calibration ð Integration Parame...

Page 161: ...ed on the main page 3 Front Panel Preset Allows selection of pre defined method and sequences names to be displayed on the front panel display The table below illustrates the icons for method and sequence options Item Name Function Add Method or Sequence Allows for the creation of a method or sequence Edit Edits selected method Copy Copies selected method Delete Deletes selected method Calibrate D...

Page 162: ...ON 162 319 074 594 P1H Micro GC Fusion Operating Man ual 9 4 1 Add Method 1 Click the icon 2 In the window enter a method name in the Name field 3 Select the Method option 4 Click the icon 5 The Method Editor window is displayed ...

Page 163: ...ighted method The Method Editor window is displayed 3 In the Method Editor window edit method parameters of each GC module Continuous mode is not available with backflush module Enhanced injection is not available with backflush and fixed volume injectors 4 When finished editing the method parameters click the icon to save the method or click the icon to leave the method editor without saving ...

Page 164: ... height for low level components NOTE Not available with backflush or fixed volume injectors Injection pressure psi The additional pressure for enhanced injections This parameter can be set between10 to 50 or disabled NOTE Not available with backflush or fixed volume injectors Backflush time if configured s Time between sample injection and injector backflush action to vent undesired compounds fro...

Page 165: ...he column fan to allow Micro GC Fusion to start the run at a lower temperature Sample conditioner enable heater N A Enables the sample conditioner if installed Sample conditioner purge time s Duration that the sample conditioner is purged if installed Sample conditioner flow rate N A Sets the sample conditioner purge flow rate to low or high if installed Column Length Maximum Ramp Rate 8 m 5 C s 1...

Page 166: ...unction to display the copied method in the methods list Alternately press F5 on the keyboard 9 4 4 Calibrate Method In the Methods Sequences window click the icon to display the calibration interface See Calibration 200 9 4 5 Delete Method Sequence 1 In the Method Sequences window select the desired method 2 Click the icon 3 Click OK to confirm the deletion CAUTION Deleting a method from the Meth...

Page 167: ...icon 2 In the Method window click Choose File 3 Navigate to locate the desired method file 4 Type the method name in the Name field 5 Click the icon to complete the method upload action 9 4 7 Export Method 1 In the Methods Sequences window select the desired method 2 Click the icon 3 The method is exported to the browser s default download folder ...

Page 168: ...ICON 168 319 074 594 P1H Micro GC Fusion Operating Man ual 9 4 8 Load Method or Sequence 1 In the Methods Sequences window select the desired method 2 Click Load 3 Micro GC Fusion is ready to run the loaded method or sequence ...

Page 169: ...t methods and sequences can be loaded by selecting the desired method from the Micro GC Fusion main page A maximum of ten methods or sequences can be added to the front panel display 1 In the Methods Sequences window select the desired methods or sequences to Preset by selecting the check box next to the method or sequence 2 Click the icon to display the main page and verify that the selected meth...

Page 170: ...n multiple runs of the same sample or different methods are desired a sequence can be defined to automate the runs Intervals between each run can be defined 1 Click the icon 2 In the window type a sequence name in the Name field 3 Select the Sequence option 4 Click the icon The Sequence Editor window opens ...

Page 171: ... method ð Run Method Runs the method selected in Load Method once the method set points have been reached ð NOTE Separate Load Method and Run Method commands allow the user to input a delay between the two ð Load and Run Method Loads the selected method Once the method set points are reached a run is initiated ð Calibration Runs Loads and runs the selected method Once all runs are complete the are...

Page 172: ...e the number of step repetitions If desired add a delay to the repetitions When the step repetition is changed a delay between each repetition in minutes is displayed 5 There is an option to add a delay to the step by clicking the icon followed by the icon ð Type the delay time in minutes ...

Page 173: ...on ð To select a method click the method shortcut menu Type the number of step repetitions 7 Click the icon to select the number of Repetitions for the defined sequence or select Continuous to run the sequence indefinitely 8 To remove a method or delay in the sequence click the icon to the right of the method or delay 9 Click the icon to save the sequence and return to the Methods Sequences window...

Page 174: ... real time readings Once a method starts loading the actual temperature and pressure readings equilibrate to the set points defined in the method The System Status window displays both the set points and the actual readings in parentheses of the temperatures and pressures for the Micro GC Fusion analytical components In the System Status window Module A is displayed above Module B Physically in th...

Page 175: ...ings In the System Status window Module A is displayed above Module B Module B above Module C and Module C above Module D Physically in the 4 module Micro GC Fusion instrument Module A is the bottom module and Module B is the top module of the left side of the instrument On the right side of the instrument Module C is the bottom module and Module D is the top module ...

Page 176: ...usion is ready to run when the green RUN button displays 2 Type a sample name in the Name Run field on the main page if desired If no name is specified the run is identified by the method name 3 Type a descriptive or identifying word or phrase in the Tag Run field if desired ð Click the icon after typing the tag or phrase Tag s entered are associated with the run and are used to facilitate sample ...

Page 177: ... the bottom of the screen ð Mouse over the icon to identify the sequence that is currently running and the current status of the sequence ð Mouse over the icon to identify the method in the sequence that is currently running 9 6 3 Stop a Sequence To stop a sequence 1 In the Run tab click the red STOP button 2 Micro GC Fusion finished the current run and returns to the initial state of the currentl...

Page 178: ...arted the Chromatogram tab displays automatically A real time chromatogram is displayed for each configured GC module Once the run is completed the Report tab is displayed Chromatograms of previous runs can be viewed in the Data Browser See Data Browser 185 A real time chro matogram is not avail able on the front panel display ...

Page 179: ...atogram hold down the left mouse button and drag the cursor to create a rectangular area over the region Release the left mouse button to zoom in 9 7 2 Reset Zoom To return to the default chromatogram view double click on the chromatogram Click the right mouse button to return to the previous zoom after multiple zoom actions are performed ...

Page 180: ...4 594 P1H Micro GC Fusion Operating Man ual 9 7 3 Expand Chromatogram To expand individual chromatograms click the icon Use the shortcut menu on the right hand side to select the desired chromatogram To return to the original view select All ...

Page 181: ... the chromatogram to display a rolling black ball and a legend displaying x and y coordinates points on the chromatogram The x axis is the retention time in seconds The y axis is the peak height in µV If hovering over a named peak the RT s and the Height in µV are displayed If the peak has been calibrated Conc mol or Conc ppm are displayed ...

Page 182: ...When a run is completed calibrated compound names retention times area counts height counts compound concentrations if calibrated and normalized amounts are displayed in the Report tab Click mol to change the view to ppm and vice versa The total un normalized concentration is displayed at the bottom ...

Page 183: ...equences can be scheduled to run on a specific day and time repeatedly or several times per week To schedule a method or sequence 1 Click the icon 2 Click Schedule 3 Click the icon to add a scheduled event 4 Click the event shortcut menu and select an event 5 Click the method or sequence from the shortcut menu ...

Page 184: ...shortcut menus 7 Alternately click Repeat and select a day and time to repeat the event 8 Click the icon to save the event 9 A confirmation method is displayed If an event is scheduled to start while another method or sequence is running the event will fail to start and be removed from the list A message is displayed ...

Page 185: ...data stored on Micro GC Fusion The following actions can be accomplished through the interactive user interface View Chromatogram and Report View Run Information an Acquisition Parameters Overlay Multiple Runs Filter and Search Runs Export Runs Import Runs Delete Runs Print Chromatogram or Reports Edit Integration Parameters Calibration Reprocess Runs ...

Page 186: ...the computer Delete Deletes the selected run s to the computer Select All Highlights and selects all runs Clear All Selected Clears selected runs Print Prints the selected chromatogram s or report s Zoom Out Returns the user to the previous zoom Toggle Integration Events Displays the peak integration lines This view is displayed by default Toggle Peaks Displays the peak names entered during calibr...

Page 187: ... run is selected Double click a run to view the chromatogram or report A icon appears to the left of the selected run s and the corresponding chromatogram is displayed to the right Alternately click a run to highlight it and click the icon in the bottom left hand corner to view it 2 To view the corresponding report click the icon 3 To deselect the viewed runs in the Data Browser window click the i...

Page 188: ...n Highlighted runs that are not viewed and do not show a icon are considered selected runs The following functions can only be accomplished by selecting the desired runs export run s reprocess run s delete run s In the above figure one run is being viewed and three runs are selected To highlight and select all runs on the run list click the icon To clear the selected runs click the icon ...

Page 189: ... P1H Micro GC Fusion Operating Manual 189 319 9 10 1 2 Hide or Show Run List The run list can be hidden to maximize the chromatogram or report display area To hide the data run list click the icon To show the data run list click the icon ...

Page 190: ...atogram Information Information such as integration lines peak names area shading and the temperature profile can be displayed on the chromatogram Select the desired icon to display the chromatogram information Icon Description Toggle integration events Toggle peaks Toggle areas Toggle temperature profile ...

Page 191: ...ck the icon to the right of the selected run to view information such as Acquisition Source Updated On Tags System and the module serial number s 2 Click the icon to view the run acquisition parameters such as column temperatures and pressures Changes can be made to the acquisition parameters but the method must be saved with a different name ...

Page 192: ...s double click the runs The icon appears to the left Alternately highlight the run s and click the icon To remove a single chromatogram from view double click the run to remove the icon next to it To remove all chromatograms from view click the icon When multiple runs are overlaid a legend appears in the upper right hand cover to indicate which runs are being displayed ...

Page 193: ...1H Micro GC Fusion Operating Manual 193 319 9 10 3 1 Toggle Chromatogram Information To display integration lines peak names areas or the temperature profile for a specific run within the overlaid chromatogram click on the run in the legend ...

Page 194: ...y runs within a user specified time period 1 Click the icon 2 Select the Start Date option and click on the date and time shortcut menus Click on a date and time to add it to the field 3 Select the End Date option and click on the date and time shortcut menus Click on a date and time to add it the field Click on the icon to apply the filter ...

Page 195: ...2 Select Search Type the parameter to search 3 Click the icon to apply the search 9 10 6 Export Runs Raw data and peak information can be exported as a report Reports can be exported into the following formats JSON Micro GC Fusion native file format NOTE Micro GC Fusion software is the most effective tool to view and reprocess exported run s CSV Comma separated text file format that can be easily ...

Page 196: ... Select remaining link in the top right corner 3 Type the file name in the Name field This name is saved onto the computer 4 From the Format shortcut menu select JSON 5 From the Data shortcut menu select All or Compound Trend 6 Click the icon The file s are downloaded to the browser s default downloads folder A single file has a fusion data extension Multiple files download as a zip file containin...

Page 197: ... menu select All or Compound Trend 6 Click the icon The file s will download to the browser s default downloads folder 7 Open the file using Microsoft Excel or Notepad When exporting All data the raw data is present in the file This enables the user to construct a chromatogram in Microsoft Excel When multiple runs are selected Compound Trend is the only available option Compound Trend contains onl...

Page 198: ...on 2 Navigate to the run s A singe file with a fusion data extension can be imported Multiple files can be imported by selecting a compressed file with a zip extension 3 Click Open 9 10 8 Delete Runs 1 Select the run s to delete 2 Click the icon 3 A window will display Are you sure you want to delete the X selected run s 4 Click the icon to delete the run s CAUTION Deleting a run from the Data Bro...

Page 199: ...esired run s to view the chromatogram s or report s 2 Click the icon to select the chromatogram s or the icon to select the report s The chromatogram and the report cannot be printed on the same page 3 Click the icon 4 In the window that appears select the printer settings To save the file as an Adobe PDF click Save Otherwise click Print ...

Page 200: ...hrough specialty gas companies 9 10 10 1 Access the Calibration Window through the Data Browser The calibration window is in the data browser 1 Click the icon 2 Click Data Browser to open the data browser window 3 Select a run to calibrate Only one run can be calibrated at a time 4 Click the icon to open the calibration window ð Clicking this icon opens the integration parameters and calibration i...

Page 201: ...ents applied Runs conducted before the change can be reprocessed to reflect the new changes 1 In the data browser ensure that the desired run is selected 2 Click the icon to enter the calibration window 3 Click the Integration tab 4 Click the icon Select the module from the shortcut menu 5 Click the icon to add an integration parameter to the list A blank row is displayed 6 For more control over p...

Page 202: ...n 205 ð Min Height Threshold See Min Height Threshold 206 ð No Peaks See No Peaks 207 ð Start Sensitivity See Start Sensitivity 208 ð Stop Sensitivity See Stop Sensitivity 209 ð Peak Sensitivity See Peak Sensitivity 210 ð Forced Baseline See Forced Baseline 211 ð Negative Peaks See Negative Peaks 212 ð Integration changes are applied to the chromatogram automatically but are not automatically save...

Page 203: ...g Manual 203 319 9 10 10 2 1 Baseline Window The Baseline Window parameter changes the size of the search window used at each point along the peak Valid Value set points are between 0 and 20 Changing this parameter changes the way the peak integrates to the baseline ...

Page 204: ...ng Man ual 9 10 10 2 2 Group Peaks The Group Peaks parameter sums the area underneath all peaks within a specified retention time range A black bar is displayed above the grouped peaks Once a retention time range is specified the group can be calibrated in the Compound tab ...

Page 205: ...ing Manual 205 319 9 10 10 2 3 Manual Integration The Manual Integration parameter allows the user to enter a start and stop time to manually integrate a peak Manual integration provides finer control of the baseline integration for a specified retention time range ...

Page 206: ...Operation INFICON 206 319 074 594 P1H Micro GC Fusion Operating Man ual 9 10 10 2 4 Min Height Threshold The Min Height Threshold parameter allows the user to specify the minimum peak height the integrator detects ...

Page 207: ...INFICON Software Operation 9 074 594 P1H Micro GC Fusion Operating Manual 207 319 9 10 10 2 5 No Peaks The No Peaks parameter stops integration within a specified retention time range ...

Page 208: ...influences the start point of peaks within a specified retention time range Valid Value set points are 0 to 100 with 50 being the default Values closer to 0 will start the peak sooner values closer to 100 will start the peak later It is recommended to increment the Value by steps of 1 from the default setting to move the start point of the peaks ...

Page 209: ...nfluences the stopping point of peaks within a specified retention time range Valid Value set points are 0 to 100 with 50 being the default Values closer to 0 will stop the peak sooner values closer to 100 will stop the peak later It is recommended to increment the Value by steps of 1 from the default setting to move the end point of the peaks ...

Page 210: ...erating Man ual 9 10 10 2 8 Peak Sensitivity The Peak Sensitivity parameter allows the increase or decrease of the sensitivity of the auto integration software Decreasing the value provides more sensitive results Increasing the value can reduce noise or undesired peaks ...

Page 211: ...ting Manual 211 319 9 10 10 2 9 Forced Baseline The Forced Baseline parameter allows the user to specify a retention time where the baseline starts for succeeding peaks For peaks eluting before the specified retention time the baseline end changes when appropriate ...

Page 212: ...Operation INFICON 212 319 074 594 P1H Micro GC Fusion Operating Man ual 9 10 10 2 10 Negative Peaks The Negative Peaks parameter allows the user to enter a start and stop time to manually integrate a negative peak ...

Page 213: ...ulate the concentration of an unknown concentration of the calibrated compound INFICON recommends conducting multiple runs of the calibration gas and using the last run to perform the calibration This thoroughly purges the sample path with the calibration gas and ensures the best calibration accuracy 1 In the Data Browser window select the data file for the calibration gas 2 Click the icon to ente...

Page 214: ...ding the peak 8 Type the concentration of the compound as listed on the calibration gas standard certificate of analysis Click mole under Concentration to change units to ppm and vice versa An area count in μVs is generated in the Area column The Fit Type Linear Forced Zero populates by default 9 Click on the icon to display the calibration curve A goodness of fit R 2 value displays The slope of t...

Page 215: ... to 11 for each additional module 13 Click the icon to save the calibration to the method A window will prompt the user to save the calibration To override the current method use the original method name An icon will indicate that there are unsaved changes 14 Click the icon 15 A message will prompt the user to reload the method and apply the calibration The method is now calibrated for a single le...

Page 216: ...To reprocess the calibrated run with the new information click the icon A confirmation message will display Are you sure you want to reprocess the X selected run s Click the icon to reprocess the run 17 A confirmation message will display 18 Click the icon to exit the calibration window ...

Page 217: ... replace all area counts for all compounds To recalibrate a method using a new run 1 Conduct an analysis of the calibration gas standard INFICON recommends conducting multiple runs of each calibration gas and using the last run to perform the calibration Doing so thoroughly purges the sample path with the calibration gas which ensures the best calibration accuracy 2 In the Data Browser window sele...

Page 218: ... all compounds in the run The name of the calibration will be replaced with the currently selected run When using average replicates one of the data files used in the calculation will be used as the reference chromatogram for the calibration 5 If using a new calibration gas standard type the Concentration of the compound as listed on the calibration gas standard certificate of analysis 6 Click the...

Page 219: ...ew information click the icon A confirmation message will display Are you sure you want to reprocess the X selected run s Click the icon to reprocess the run To apply the new calibration to prior runs select the desired runs from the list before clicking the icon 10 A confirmation message will display 11 Click the icon to exit the calibration window 12 Click the updated method preset to reload the...

Page 220: ...are generated automatically once the peak is entered into the table When recalibrating a user may want to only change integration on a single peak 1 Conduct an analysis of the calibration gas standard INFICON recommends conducting multiple runs of each calibration gas and using the last run to perform the calibration Doing so thoroughly purges the sample path with the calibration gas which ensures...

Page 221: ...he icon next to the edited compound to populate a new area count If the selected run is not the calibration reference data file the calibration reference data file will open to acquire the new data to update the area This insures consistency in respect to which data file was used to perform the calibration 354097 6 uV ...

Page 222: ...con 10 A message will prompt the user to reload the method and apply the calibration 11 To reprocess the calibrated run with the new information click the icon A confirmation message will display Are you sure you want to reprocess the X selected run s Click the icon to reprocess the run To apply the new calibration to prior runs select the desired runs from the list before clicking the icon 12 A c...

Page 223: ...ation gas 3 Conduct an analysis of the second level calibration gas INFICON recommends conducting multiple runs of each calibration gas and using the last run to perform the calibration Doing so thoroughly purges the sample path with the calibration gas which ensures the best calibration accuracy 4 In the data browser select the data file for the calibration gas corresponding to the second level 5...

Page 224: ...ion level select the level from the shortcut menu 11 Click on the icon to display the calibration curve A second level calibration point will display on the curve 12 Click the Fit Type shortcut menu to change the fit type if desired 13 Click the icon to select another module if configured Otherwise skip to step 15 ...

Page 225: ...eprocess the calibrated run with the new information click the icon A confirmation message will display Are you sure you want to reprocess the X selected run s Click the icon to reprocess the run To apply the new calibration to prior runs select the desired runs from the list before clicking the icon 18 A confirmation message will display 19 Click the icon to exit the calibration window 20 The met...

Page 226: ...ieu of calibration gas To access the Manual Response Factor 1 Click the icon 2 Click Data Browser to open the data browser window 3 Select a run to calibrate Only one run can be calibrated at a time 4 Click the icon to open the calibration window 9 10 10 7 1 Typing a Manual Response Factor To enter a known response factor 1 In the calibration window select Manual Response from the Fit Type shortcu...

Page 227: ...brated compound a multiplication factor can be used to calibrate the desired compound To use the response factor of a calibrated compound 1 In the calibration window select Manual Response from the Fit Type shortcut menu for the desired compound 2 From the shortcut menu select the compound to use as a reference Ex CO2 3 In the area count field type the known multiplication factor Ex 1 1 4 Click th...

Page 228: ... 170 2 From the shortcut menu select Calibration Runs 3 Type the number of step repetitions and the method If desired add a delay between each repetition 4 Type the number of runs to average and the level in which the averaging should take place ð Average Last The number of previous runs used when averaging component areas This is known as Average Replicates ð Level The level in which the auto cal...

Page 229: ...d 9 10 10 8 3 Multi Level Calibration using a Valco Stream Selector 1 Create a sequence called Auto Calibration See Add Sequence 170 2 Add a Valco Stream Selector switching event and switch to the first calibration gas 3 Click the icon and select Calibration Runs 4 Type the number of step repetitions and the method If desired add a delay between each repetition 5 Type the number of runs to use whi...

Page 230: ...GC Fusion Operating Man ual 10 Type 2 for a level 2 calibration 11 Repeat steps 7 through 10 until you have reached the desired number of levels 12 Click to save the sequence 13 Run the Auto Calibration sequence after all the calibration gases are connected ...

Page 231: ... after a run is completed without adjusting the calibration information After a run is performed 1 In the data browser click on the run 2 Click the icon to open the calibration window By default Module A will display 3 Click the icon to select another module if desired 4 Integration parameters can be edited in the Integration tab The retention time windows can be edited in the Compounds tab ...

Page 232: ...desired runs 7 Click the icon to reprocess the runs A window appears Are you sure you want to reprocess the X selected run s Click the icon to reprocess or to exit the window 8 A confirmation message will display 9 Click the icon to exit the calibration window 10 View the desired run s by double clicking on the run or by selecting the run and clicking the icon 11 The chromatogram s and report s wi...

Page 233: ... same as the Data Browser operation document in Data Browser 185 Micro GC Fusion Offline Analysis is a licensed product The license certificate PN 952 035 G1 provides the license certificate ID and software download instructions The software installation procedure is available on the Micro GC Fusion product website 9 11 1 Initializing Micro GC Fusion Offline Analysis The Micro GC Fusion Offline An...

Page 234: ...Offline Analysis service is running in the background The tray icon is identical to the desktop icon The tray icon can be used to launch the browser restart service and exit service 9 11 2 1 Launch the Browser The Micro GC Fusion Offline Analysis interface can be launched from the tray icon in two ways 1 Left click on the tray icon 2 Right click on the try icon and select Launch Browser ...

Page 235: ...nection issues with the user interface The background service restart can also be accomplished by double clicking on the Micro GC Fusion Offline Analysis icon 9 11 2 3 Exit Service To stop running the Micro GC Fusion Offline Analysis service right click on the system tray icon and click Exit This will shut down the service running in the background However all of the data will be saved when restar...

Page 236: ...is 1 Acquisition parameters ð Click the icon to view the acquisition parameters such as column temperatures and pressures ð After reviewing the method save by clicking the icon and the method will download to the computer 2 Calibration While in the calibration screen click the icon to download the new method Any method that has been downloaded can be uploaded to an instrument ...

Page 237: ...truments Co Inc to perform analyses on multiple gas streams Refer to Valco Stream Selector 97 for an introduction to the connection between a Valco stream selector and a Micro GC Fusion and supported valve types 9 12 1 Valco Stream Selector Configuration To access the Valco stream selector valve configuration 1 Click the icon 2 Click the System Administration button 3 Click on Valco Configuration ...

Page 238: ...n 9 12 1 1 Position Assignments Individual valve positions can be assigned with unique names 1 Click on the desired position 2 Type a name in the field Unnamed positions will retain their original position number 9 12 1 2 Purge Position To assign a purge position 1 Select the Returns to Purge Position option 2 Click the icon next to the desired purge position The icon will turn white to indicate t...

Page 239: ... in Tag Run desired 3 Click the RUN button to initiate a run and the selected valve position 9 12 3 Running a Sequence Using a Valco Stream Selector To create a sequence using a valve 1 Click the icon 2 Click the Method Sequences button 3 Click the icon 4 In the pop up window type a sequence name in the Name field 5 Select the Sequence option 6 Click the icon The Sequence Editor window opens 7 Cli...

Page 240: ...n INFICON 240 319 074 594 P1H Micro GC Fusion Operating Man ual 10 Click the icon to add a valve position 11 Select the desired valve position from the shortcut menu 12 Click the icon followed by the icon to add an event ...

Page 241: ...ent from the shortcut menu 14 Click the icon to add addition events delays or port positions 15 Click the icon to select the number of Repetitions for the defined sequence or select Continuous to run the sequence indefinitely 16 Click the icon to save the sequence and return to the Methods Sequences window ...

Page 242: ...d must be calibrated for a meaningful logfile When the Valco Stream Selector is connected the name of the run field is replaced by the port name defined in the Valve Configuration screen 9 13 1 Install Python Software Python is a free and open source scripting language that is widely used for scientific data analysis To install Python download the latest installer from https www python org Either ...

Page 243: ...ick the Windows Start button and type cmd into the search bar Click the cmd program to open the Windows command prompt 2 In the command prompt window type pip install U requests python dateutil 3 Press the Enter key Once finished exit the command prompt If the error Pip is not recognized as an internal or external command appears check that python exe was added to the path in Step 2 Including U in...

Page 244: ...CSV Script The CSV script must be updated to connect to Micro GC Fusion and to specify the location for the CSV logfile on the computer 1 Once downloaded to the computer right click the csv log py file 2 Select Edit with IDLE or Open with Notepad 3 Under IP Address of MicroGC Fusion instrument is a host variable which must be changed to the IP address of the instrument Replace the quoted name with...

Page 245: ... 1 Double click on the csv log py file A window and confirmation message will display This method will not show any errors if present 2 Once the script is running information will be automatically added to the CSV file at the completion of the run A confirmation message will display in the Python window Do not close this Python window when appending to the logfile Closing the Python window will te...

Page 246: ... press the F5 key A Python window will display A confirmation message will display Logging analysis from instrument X X X X 3 Once the script is running information will be automatically added to the CSV file at the completion of the run A confirmation message will display in the Python window Do not close this Python window when appending to the logfile Closing the Python window will terminate th...

Page 247: ...9 13 5 Viewing the CSV File A CSV file will generate with the name of the method Any run using that method will append to the method specific file Each method will have its own CSV file To view the file right click on the file and select Open with Microsoft Excel or Open with Notepad ...

Page 248: ...B Access PN 952 389 G1 must be purchased from INFICON and installed on the Micro GC Fusion Each License Certificate ID enables one Micro GC Fusion to be controlled by EZ IQ or OpenLAB EZChrom If EZ IQ or OpenLAB EZChrom are to control two Micro GC Fusions then two License Certificates are needed one for each Micro GC instrument The License Certificate for EZ IQ or OpenLAB Access PN 952 389 G1 prov...

Page 249: ...6 for the detailed procedure 2 Close the corresponding pins on the AUX I O connector to trigger the REMOTE_START action Refer to The AUX I O Connector 95 for the AUX I O pinouts and contact closure actions If a run is in progress when the external triggering action is issued the external triggering action is discarded The name of the run will be defaulted to the loaded method name or the loaded se...

Page 250: ... Micro GC Fusion will purge the Integrated Sample Conditioner with a fresh sample from the sample line for the defined amount of time 9 16 2 Manual Purging The user can perform a manual purge of the integrated sample conditioner by clicking on the purge sample conditioner icon located at the bottom of the web user interface A manual purge uses high flow rate mode to purge the sample path CAUTION T...

Page 251: ...ode CAUTION Bypassing the shutdown procedure and abruptly disconnecting the power supply to Micro GC Fusion may result in instrument damage In the event the instrument is unresponsive the recommended shutdown procedure can be bypassed by pressing the On Standby button for 3 or more seconds until the front panel display turns off CAUTION The instrument remains powered while in standby mode Disconne...

Page 252: ... for an extended period of time after Micro GC Fusion has been stored in a shipping case for an extended period of time periodically as needed to refresh column performance 10 2 1 Bakeout from System Status Perform the following steps to implement a bakeout on Micro GC Fusion Depending on the column type bakeout temperatures will be set according to the isothermal temperatures indicated in Create ...

Page 253: ...ys observe the column phase and module temperature limitations in the table Column Type Temperature Programmed Max C Duration Max Minutes Isothermal Temperature Max C Duration Max Minutes Rt Molsieve 250 5 225 120 Rt U Bond 120 5 120 120 Rt Q Bond 250 5 225 120 Rt Alumina 200 5 180 120 Rtx 1 or Rxi 1ms 250 5 225 120 To create a bakeout method 1 Click the icon 2 Click the Methods Sequences button 3...

Page 254: ...to the recommended bakeout temperature described in the table for each configured module ð Set the Inject ms time and Sample Pump Time s to 0 8 Click the icon to save the method The Methods Sequences window will display 9 In the Methods Sequences screen click the Bakeout method and click the LOAD button to load the Bakeout method onto Micro GC Fusion ...

Page 255: ...of the software To update the Micro GC Fusion software to the latest version 1 Download the latest software from the software download area on the INFICON website ð Go to www INFICON com ð Click Downloads ð Click the Software tab ð Locate and click the Micro GC Fusion software ð Read any release notes or Read Me files ð Fill in user information requested and click Start Download ð The software dow...

Page 256: ...he instrument will reboot after the software update and may be temporarily unavailable Refresh the web browser 1 2 minutes after the system reboot to reconnect with the instrument 8 The On Standby button on the instrument front panel will be temporarily disabled during the system reboot This prevents unintended instrument shutdown in the software update process CAUTION Do not shutdown or disconnec...

Page 257: ...tem 265 or GC Module Removal Procedure for 4 Module System 273 CAUTION Only technically qualified personnel should perform the procedures and maintenance described in this manual 10 4 1 List of Required Tools open ended wrenches 1 4 in and 5 16 in 2 5 mm ball point L handle hex driver PN 070 1999 2 0 mm hex wrench 4 module only 2 5 mm hex wrench 4 module JP 100 removal only Phillips screwdriver 10...

Page 258: ...gas connections and venting connections CAUTION Sample gas and carrier gas must be properly disconnected before the JP 100 to prevent instrument damage from pressurized gases 4 Set Micro GC Fusion on its left side as shown 5 Remove the bottom eight screws with the 2 5 mm ball point hex driver 6 Turn Micro GC Fusion back to its upright position With finger tips grasp the bottom lips of the housing ...

Page 259: ...sconnect the fan cable from the cable extension 8 Remove the retaining screw holding the JP 100 in place with the 2 5 mm ball point hex driver 9 Slide the JP 100 up and out of the instrument 10 See GC Module Removal Procedure for 2 Module System 265 to continue the module removal process ...

Page 260: ...o GC Fusion power cable must be disconnected before JP 100 removal operation to prevent potential electrical damage to the instrument 3 Disconnect sample gas connection s carrier gas connections and venting connections CAUTION Sample gas and carrier gas must be properly disconnected before the JP 100 to prevent instrument damage from pressurized gases 4 Set Micro GC Fusion upright and remove the s...

Page 261: ...t the front of the unit 7 Remove the top foam by grasping one front corner and the opposite back corner and pulling straight up 8 Remove the foam by the right side of each module by pulling it straight up out of the unit 9 The 4 module Micro GC Fusion contains two JP 100 units 10 Disconnect the fan cable from the cable extension ...

Page 262: ...he retaining screw holding the JP 100 in place with the 2 5 mm ball point hex driver ð For modules A B remove the retaining screw holding the JP 100 in place with the 2 5 mm ball point hex wrench 12 Slide the JP 100 up and out of the instrument 13 See GC Module Removal Procedure for 4 Module System 273 to continue the module removal process ...

Page 263: ...replaced replace the JP 100 1 Ensure that the fan is properly seated inside the JP 100 2 Slide the JP 100 into position ð The fan cable should sit between the two fan ports on the JP 100 3 Connect the fan cable to the cable extension ð The fan cable should be routed between the reference and analytical exhaust vents on the top module ...

Page 264: ...10 Routine Operation INFICON 264 319 074 594 P1H Micro GC Fusion Operating Man ual 4 Tighten the retaining screw into the bracket of the bottom module 5 Repeat for additional JP 100 if configured ...

Page 265: ...n Procedure 251 2 Remove all external electrical cables including power cable and Ethernet cable WARNING The Micro GC Fusion power cable must be disconnected before module removal operation to prevent potential electrical damage to the instrument 3 Disconnect sample gas connection s carrier gas connections and venting connections CAUTION Sample gas and carrier gas must be properly disconnected bef...

Page 266: ...m apart and lift the housing off Micro GC Fusion 7 Remove the side foam by pulling it sideways to free it from the dovetail joint at the bottom 8 Remove the rear foam by pulling it sideways out of the instrument back 9 From the left side of the Micro GC Fusion chassis frame use a Phillips head screwdriver to loosen the two captive screws that hold the GC module To remove the lower GC module loosen...

Page 267: ...two screws The figure indicates screw positions for both the upper and lower GC modules Upper module Lower module 10 Use a 5 16 in open end wrench to disconnect the sample line nut CAUTION Sample gas and carrier gas must be properly disconnected before the module removal to prevent instrument damage from pressurized gases 11 Gently pull the GC module off the electrical connector no more than 2 cm ...

Page 268: ...om the standoffs and the electrical connector Lifting from the bottom may cause damage to both connectors and cause failures when the module is reinstalled or replaced 12 Using a 2 5 mm ball point hex driver unscrew the two carrier gas manifold screws on the upper GC module 13 Loosen and remove the venting connectors at the rear of the GC module by turning counterclockwise 14 Remove the GC module ...

Page 269: ...uctions in GC Module Removal Procedure for 2 Module System 265 2 Position the replacement module into the chassis 3 Connect the venting connectors at the rear of the replacement module Rotate them clockwise until finger tight 4 Use a 2 5 mm ball point hex driver to replace the two carrier gas manifold screws onto the GC module Tighten them until they are snug CAUTION Do not over tighten the screws...

Page 270: ...GC module controller board and the GC module interface board are securely connected 7 From the left side of the chassis frame use a Phillips head screwdriver to tighten the two captive screws to secure the GC module in place CAUTION Do not over tighten the screws to avoid module damage 8 Connect the sample line to the GC module injector manifold Finger tighten the connection and then use a 5 16 in...

Page 271: ...l 271 319 CAUTION Over tightening the sample line nut may damage the thread on the GC module 9 Repeat steps 2 to 8 if replacing both modules 10 When all the GC modules are replaced replace the rear foam 11 Replace the side foam Ensure the dovetail joint is oriented as shown ...

Page 272: ...point hex driver to replace the eight bottom screws 15 Return Micro GC Fusion to the upright position 16 Connect the sample gas connection s carrier gas connections and venting connections 17 Connect the external electrical cables including the power cable and the Ethernet cable 18 Power up the instrument by pressing the On Standby button on the front panel Micro GC Fusion automatically recognizes...

Page 273: ...rocedure 251 2 Remove all external electrical cables including power cable and Ethernet cable WARNING The Micro GC Fusion power cable must be disconnected before module removal operation to prevent potential electrical damage to the instrument 3 Disconnect sample gas connection s carrier gas connections and venting connections CAUTION Sample gas and carrier gas must be properly disconnected before...

Page 274: ...posite back corner and pulling straight up 8 Remove the foam by the right side of each module by pulling it straight up out of the unit 9 Remove the rear foam by pulling it sideways out of the instrument back 10 From the left side of the Micro GC Fusion chassis frame use a Phillips head screwdriver to loosen the two captive screws that hold the GC module To remove the lower GC module loosen the tw...

Page 275: ...ons for both the upper and lower GC modules Upper Module Lower Module 11 Use a 5 16 in open end wrench to disconnect the sample line nut CAUTION Sample gas and carrier gas must be properly disconnected before the module removal to prevent instrument damage from pressurized gases WARNING The sample inlet may be hot to the touch use care when removing the sample line nut 12 Gently pull the GC module...

Page 276: ...ailures when the module is reinstalled or replaced 13 Using a 2 5 mm ball point hex driver unscrew the two carrier gas manifold screws on the upper GC module 14 Loosen and remove the venting connectors at the rear of the GC module by turning counterclockwise 15 Remove the GC module by pulling it sideways and then lifting straight up out of the chassis 16 Repeat the same procedure steps 9 14 to rem...

Page 277: ...wing the instructions in GC Module Removal Procedure for 4 Module System 273 2 Position the replacement module into the chassis 3 Connect the venting connectors at the rear of the replacement module Rotate them clockwise until finger tight 4 Use a 2 5 mm ballpoint hex driver to replace the two carrier gas manifold screws onto the GC module until snug CAUTION Do not over tighten the screws to avoid...

Page 278: ...GC module controller board and the GC module interface board are securely connected 7 From the left side of the chassis frame use a Phillips head screwdriver to tighten the two captive screws to secure the GC module in place CAUTION Do not over tighten the screws to avoid module damage 8 Connect the sample line to the GC module injector manifold Finger tighten the connection and then use a 5 16 in...

Page 279: ... 9 Repeat steps 2 to 8 if replacing both modules 10 When all the GC modules are replaced replace the rear foam 11 Replace the side foam Ensure the dovetail joint is oriented as shown 12 Replace the top foam by grasping one front corner and the opposite back corner and pressing straight down 13 Replace the two small air filters on the top at the front of the unit ...

Page 280: ... Return Micro GC Fusion to the upright position 17 Connect the sample gas connection s carrier gas connections and venting connections 18 Connect the external electrical cables including the power cable and Ethernet cable 19 Power up the instrument by pressing the On Standby button on the front panel Ensure the modules heat to ready status Micro GC Fusion automatically recognizes the new or replac...

Page 281: ...ckwise Part B Part A To GC Filter disk Dual ended ferrule 6 Remove and discard the used filter disk from Part A 7 Insert a new filter disk PN 5183 4652 into Part A Avoid handling the replacement filters Wear laboratory gloves when performing this procedure 8 Reassemble the sample inlet filter by using two 7 16 in wrenches with one holding the Part A steady and another to tighten Part B clockwise 9...

Page 282: ...ure 251 2 Remove all the external electrical cables including the power cable and Ethernet cable 3 Disconnect the sample gas connection s carrier gas connections and venting connections 4 Set Micro GC Fusion on its left side The integrated sample conditioner filter PN 059 0682 is accessed from the bottom of the Micro GC Fusion as shown 5 Using a 3 16 in Allen wrench remove the hex plug that covers...

Page 283: ... unit 7 Use forceps to place a new filter into the unit Ensure the flat side of the filter faces the forceps 8 Replace the hex plug 9 Reconnect the external electrical cables including the power cable and Ethernet cable sample gas connection s carrier gas connection s and venting connections 10 Micro GC Fusion is now ready to use ...

Page 284: ... parameter is insufficient Increase the Inject ms time There is contamination in the system Conduct a bakeout to clean the columns Refer to Bakeout from System Status 252 The instrument not sufficiently warmed up Allow at least 3 minutes for Micro GC Fusion to warm up There is an external leak Check carrier gas lines using a leak detector and tighten all fittings There is a loose fitting Tighten a...

Page 285: ...st 15 seconds There is a malfunction in the column or injector Check the flow rate of the columns by attaching a flow meter to the analytical and reference vents on the back of Micro GC Fusion If there is no flow from either or both vents contact INFICON See Service and Technical Support 299 There is a malfunction in the sample pump or the sample pump does not turn on Listen for the noise from the...

Page 286: ... gas lines using a leak detector and ighten all fittings Integration events are not optimized Ensure all of the peaks of interest are identified and fully integrated Refer to Integration Parameters 201 The Backflush Time method parameter is set too early if applicable Increase the Backflush Time until all peaks of interest appear on the chromatogram Inverted peaks are present or large broad humps ...

Page 287: ...eak Contact INFICON See Service and Technical Support 299 There is a significant negative baseline but peaks still appear The reference column is damaged Check the flow coming out of the reference vents If there is no flow contact INFICON See Service and Technical Support 299 There is poor separation resulting in partial or full co elution of desired compounds There is contamination in the system ...

Page 288: ...wireless verify that the device is connected to the Micro GC Fusion wireless connection Refer to Wireless Connection 88 Verify Micro GC Fusion is powered on Connect directly to a PC using an Ethernet cable to bypass the wireless connection The IP address is incorrect Verify the Micro GC Fusion IP address by looking at the front panel display Refer to Connecting to a Computing Device 158 The web br...

Page 289: ... cable is fully seated The GC will not power on The power supply has been damaged Replace the power supply Refer to Connecting the Power Supply 90 There is a malfunctioning circuit board Contact INFICON See Service and Technical Support 299 The 4 module chassis fuse is damaged Replace the fuse on the back of the 4 module Micro GC Fusion The carrier gas depletes prematurely There is an external lea...

Page 290: ...after taking the suggested measure s contact INFICON 11 2 1 Chromatographic Problems Unexpected chromatographic behavior may be the result of Electronic or mechanical failure Contaminants in gas lines injectors columns and detectors Incorrect or inappropriate set points Leaks bleed or other chromatographic difficulties These conditions often interact For example baseline problems may arise from an...

Page 291: ...e column Baseline is erratic moves up and down wander Potential column leak Change the sample conditioner filter If there is a leak at the detector end of the column the retention times will be stable from run to run but sensitivity will be reduced If there is a leak at the inlet end of the column there will be reduced flow through the column an increase in retention time and reduced sensitivity I...

Page 292: ...s Noise gradually increases to an unacceptable level This symptom indicates gradual buildup of the noise source rather than an abrupt change as described above If the cause of the noise is not found contact INFICON 11 2 1 1 4 Baseline Spiking Spikes are isolated baseline disturbances and usually appear as sudden large upscale movements If these spikes are accompanied by noise address the noise pro...

Page 293: ...d column temperature In the System Status window ensure the actual pressures and temperatures match their set points If the actual pressures and temperatures do not match the set points power Micro GC Fusion off restart and download the method again If this does not solve the problem contact INFICON 11 2 1 2 2 Retention Time Wander Reproducibility Reproducibility is erratic for successive runs of ...

Page 294: ... to change the carrier gas 11 2 1 3 3 Extra Peaks Extra or ghost peaks are peaks that appear during a blank or sample run Ghost peaks appear even when no sample is injected and are also found among the actual component peaks during a sample run Ghost peaks appear during a blank run when The column has been heated and idle for an extended period of time Carrier gas and plumbing contain impurities s...

Page 295: ... pure Gaussian shape although some asymmetry is always present particularly near the baseline Some common types of deformed peaks are described below 11 2 1 3 4 1 Peak Fronting The peak rises normally then drops sharply to the baseline Fronting is usually caused by column overload Reduce the sample Inject ms time If using a variable volume or fixed volume injector do not reduce the Inject ms time ...

Page 296: ... separate at the lower temperature the tailing was caused by unresolved peaks Tailing can also be caused by a low Sample Inlet Heater Temperature Increase the Sample Inlet Heater Temperature and repeat the analysis 11 2 1 3 4 3 Deformed Peak Apex Top apex of the peak is deformed or flat A deformed peak apex is usually caused by detector saturation Reduce the sample Inject ms time If using a variab...

Page 297: ...ise from incorrect Micro GC Fusion parameter settings wrong peak identification windows and inappropriate peak detection parameters These conditions cause an erroneous calculation of the mole percent composition of samples Troubleshoot the method if the following symptoms are observed in the reports and chromatograms when running a calibration standard Zero mole percent composition for components ...

Page 298: ...2 2 Correcting Instrument Parameter Settings Recalibrating Changes to Column Pressure Column Temperature Inject ms time and Backflush Time if applicable may cause peak retention times to shift and peak areas to change The retention times and associated peak windows will require adjustment Therefore the method should be recalibrated Recalibrate Micro GC Fusion as instructed in Calibration 200 ...

Page 299: ...uct specific technical support through Fusion Syr inficon com To submit a repair request in North America fill out a Service Request Form at http service inficon com 12 2 Returning Micro GC Fusion to INFICON Do not return a Micro GC Fusion or a GC module to INFICON without first speaking with a Customer Support Representative A Return Material Authorization RMA number must be obtained from the Cus...

Page 300: ...perating Man ual 12 4 Service Contract INFICON offers service contracts for an out of warranty Micro GC Fusion INFICON will conduct an evaluation to verify the condition of an out of warranty Micro GC Fusion before agreeing to offer a service contract Contact INFICON for details ...

Page 301: ...llation Their compositions are defined to demonstrate instrument performance for common Micro GC applications At the factory the Universal checkout gas is used by default unless otherwise specified The checkout gas selection is made when configuring a Micro GC Fusion instrument part number INFICON PN Description 952 607 P1 Universal Checkout Gas Cylinder 952 607 P3 Natural Gas Checkout Gas Cylinde...

Page 302: ...sal checkout gas is not intended to be a substitute for a calibration standard for any specific applications INFICON recommends acquiring a calibration standard gas that meets composition requirements appropriate for the specific application Components Concentration Mole hydrogen 10 00 oxygen 1 00 nitrogen balance methane 5 00 ethane 0 10 ethylene 0 20 carbon dioxide 1 00 carbon monoxide 1 00 acet...

Page 303: ...table below for the component concentrations Natural gas checkout gas is not intended to be a substitute for a calibration standard for any specific applications INFICON recommends acquiring a calibration standard gas that meets composition requirements appropriate for the specific application Components Concentration Mole nitrogen 1 50 methane balance ethane 9 00 carbon dioxide 1 50 propane 6 00 ...

Page 304: ...r any specific applications INFICON recommends acquiring a calibration standard gas that meets composition requirements appropriate for the specific application Components Concentration Mole hydrogen 10 00 oxygen 0 19 nitrogen balance carbon monoxide 1 00 carbon dioxide 3 00 methane 5 00 ethane 4 00 ethylene 2 00 acetylene 1 00 propane 2 00 propylene 1 00 isobutane 0 30 n butane 0 15 1 butene 0 30...

Page 305: ...Replacement Accessory parts Spare and consumable parts 13 2 1 GC Module Replacement A GC module is a self contained gas chromatograph that can perform sample injection separation and detection GC modules can be changed in the instrument for either maintenance or application adaption purposes Refer to GC Module Replacement 257 for instructions on how to remove and replace a GC module The following ...

Page 306: ...CMR RR2 FV Rt Q Bond 12 m 0 25 mm N A N A TCD2 Active GCMR TR2 VV Rt Q Bond 12 m 0 25 mm N A N A TCD2 Active GCMR UR2 VLV Rt Q Bond 12 m 0 25 mm N A N A TCD2 Active GCMR RR4 FV Rt U Bond 12 m 0 25 mm N A N A TCD2 Active GCMR TR4 VV Rt U Bond 12 m 0 25 mm N A N A TCD2 Active GCMR UR4 VLV Rt U Bond 12 m 0 25 mm N A N A TCD2 Active GCMR W81 BF Rt U Bond 8 m 0 25 mm Rt Q Bond 1 m 0 25 mm TCD2 Active G...

Page 307: ...B 10 m 0 25 mm N A N A TCD2 Active GCMR TW0 VV Rt Stabilwax DB 10 m 0 25 mm N A N A TCD2 Active GCMR UW0 VLV Rt Stabilwax DB 10 m 0 25 mm N A N A TCD2 Active GCMR R45 FV CP Sil13CB 16 m 0 15 mm N A N A TCD2 Active GCMR T45 VV CP Sil13CB 16 m 0 15 mm N A N A TCD2 Active GCMR U45 VLV CP Sil13CB 16 m 0 15 mm N A N A TCD2 Active GCMR RM4 FV CP Sil19CB 4 m 0 15 mm N A N A TCD2 Active GCMR TM4 VV CP Sil...

Page 308: ...1 Ship kit install maintenance 952 029 G1 Gas liquid separator 952 024 G1 Ship kit syringe luer adapter 952 025 G1 Ship kit 50 ml syringe and luer adapter 952 026 G1 Ship kit SS adapter for sample bag 952 027 G1 Ship kit SS adapter and 10 pack 3 L ALTEF 952 033 G1 Pressure reducer and gas liquid separator 952 415 P1 Dual stage regulator with a CGA 350 connection 952 416 P1 Dual stage regulator wit...

Page 309: ...37 Antenna swivel 2 4 GHz SMA M WI FI 059 0682 Filter element 7 µm pore SS RoHS for sample conditioner 059 0701 Filter inline 0 125 tube 2 µm pore brass RoHS for carrier gas 059 0718 Frit disk 10 µm 0 062 OD 5 pack RoHS for sample inlet 068 0419 Power cord SL 16 SL 3 Australia 1 8 m 068 0433 Power cord USA 10A 125V 6 ft 068 0434 Power cord Euro 10A 250V 2 5 m 068 0590 Power cord UK 10A BLK PVC 220...

Page 310: ...r Modbus Computers INFICON PN Description 930 760 G1 Laptop computer Windows 10 USA 930 760 G2 Laptop computer Windows 10 Europe 930 760 G3 Laptop computer Windows 10 UK 930 760 G4 Laptop computer Windows 10 China Australia 13 4 Installation and Familiarization Training Micro GC Fusion installation and familiarization trainings are available to install the instrument and familiarize the user with ...

Page 311: ...Micro GC Fusion columns are provided in this chapter to demonstrate typical peak elution order when these checkout gases are used at the customer site during product acceptance Actual retention times and area counts will vary from column to column The following column types are included in this chapter Rt Msieve 5A see 10 m Rt Msieve 5A 312 Rt Q Bond see 12 m Rt Q Bond 314 Rxi 1ms see 10 m Rxi 1ms...

Page 312: ...t Gas Using Helium Carrier Gas Peak Number Compound Concentration mole 1 oxygen 1 00 2 nitrogen 81 24 3 methane 5 00 4 carbon monoxide 1 00 Helium is not an acceptable carrier gas for hydrogen analysis 1 2 3 4 Column Temperature Profile 110 C 10 s hold 200 C 30 s hold 2 5 C s Column Pressure 25 psi Inject ms Time 30 ms Backflush Time 25 s ...

Page 313: ...drogen in a sample Analysis of other fixed gases is possible using argon carrier gas but with reduced sensitivity when compared with helium carrier gas Peak Number Compound Concentration mole 1 hydrogen 10 00 2 oxygen 1 00 3 nitrogen 81 24 4 methane 5 00 5 carbon monoxide 1 00 1 2 3 4 5 Column Temperature Profile 100 C 90 s hold Column Pressure 35 psi Inject ms Time 30 ms Backflush Time 25 s ...

Page 314: ...Concentration mole 1 composite air 93 24 2 methane 5 00 3 carbon dioxide 1 01 4 combined ethylene acetylene 0 25 5 ethane 0 10 6 propylene 0 05 7 propane 0 10 8 n butane 0 05 9 n pentane 0 05 10 n hexane 0 05 Ethylene and acetylene co elute on Rt Q Bond column 1 2 3 4 5 6 7 8 9 10 Column Temperature Profile 65 C 20 s hold 220 C 50 s hold 1 C s Column Pressure 30 psi Inject ms Time 30 ms ...

Page 315: ...Number Compound Concentration mole 1 nitrogen 1 50 2 methane 75 32 3 carbon dioxide 1 50 4 ethane 8 99 5 propane 6 00 6 isobutane 3 01 7 n butane 2 00 8 isopentane 1 02 9 n pentane 0 50 10 n hexane 0 10 11 n heptane 0 05 1 2 3 4 5 6 7 8 4 9 10 11 Column Temperature Profile 55 C 20 s hold 230 C 50 s hold 1 C s Column Pressure 30 psi Inject ms Time 30 ms ...

Page 316: ...14 4 10 m Rxi 1ms 14 4 1 Universal Checkout Gas Using Helium Carrier Gas Peak Number Compound Concentration mole 1 propane 0 10 2 n butane 0 05 3 n pentane 0 05 4 n hexane 0 05 1 2 3 4 Column Temperature Profile 60 C 20 s hold 110 C 20 s hold 0 8 C s Column Pressure 17 psi Inject ms Time 30 ms ...

Page 317: ...ral Gas Checkout Gas Using Helium Carrier Gas Peak Number Compound Concentration mole 1 propane 6 00 2 isobutane 3 01 3 n butane 2 00 4 isopentane 1 02 5 n pentane 0 50 6 n hexane 0 10 1 2 3 4 5 6 Column Temperature Profile 50 C 10 s hold 150 C 20 s hold 2 C s Column Pressure 20 psi Inject ms Time 30 ms ...

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