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multi EA 4000

Contents

7.3

Operation with Cl module ....................................................................................... 114

7.3.1

Replacing the sulfuric acid/cleaning the sulfuric acid container ............................. 114

7.3.2

Servicing/replacing the quartz glass combustion tube ............................................ 115

7.3.3

Servicing the combined electrode ........................................................................... 117

7.3.4

Servicing the measuring cells .................................................................................. 118

7.3.5

Replacing the adsorption agent .............................................................................. 119

7.4

Operation with the automatic TIC solids module .................................................... 119

7.4.1

Cleaning the TIC reactor of the automatic TIC solids module .................................. 120

7.4.2

Cleaning the condensation coil ............................................................................... 121

7.4.3

Removing and replacing the pump hose ................................................................. 122

7.4.4

Cleaning the condensate container ......................................................................... 125

7.5

Manual TIC solids module ....................................................................................... 125

7.5.1

Cleaning the TIC reactor at the manual TIC solids module ...................................... 126

7.6

Replacing the water traps ....................................................................................... 126

Fault removal ............................................................................................................... 127

8.1

General information ................................................................................................ 127

8.2

Error messages in multiWin .................................................................................... 127

window ...................................................................... 133

8.4

Equipment fault ...................................................................................................... 135

8.4.1

Basic device ............................................................................................................. 135

8.4.2

C/S module ............................................................................................................. 135

8.4.3

Cl module ................................................................................................................ 136

8.5

Device communication fault .................................................................................... 137

8.6

Analytical problems ................................................................................................. 138

8.6.1

C/S determination ................................................................................................... 138

8.6.2

Cl determination ..................................................................................................... 139

8.6.3

TIC determination (automatic TIC solids module)................................................... 140

8.6.4

TIC determination (manual TIC solids module)....................................................... 140

8.6.5

Measurements in pyrolysis mode (EC) .................................................................... 141

Transport and storage ................................................................................................. 142

9.1

Transport ................................................................................................................ 142

9.1.1

Preparing the analyzer for transport ....................................................................... 142

9.1.2

Removing the heating elements and furnace cartridge .......................................... 144

9.1.3

Transport notes ....................................................................................................... 146

9.1.4

Moving the analyzer in the laboratory .................................................................... 146

9.2

Storage .................................................................................................................... 147

Disposal ......................................................................................................................... 148

Specification ................................................................................................................. 149

11.1

Technical data ......................................................................................................... 149

11.2

Standards and directives ......................................................................................... 151

Содержание Analytik Jena multi EA 4000

Страница 1: ...Operating Manual multi EA 4000 Elementary analyzer C S and Cl solids analysis...

Страница 2: ...ttp www analytik jena com multi EA and multiWin are registered trademarks of Analytik Jena AG in Germany Microsoft and Windows are registered trademarks of Microsoft Corp The identification with or TM...

Страница 3: ...8 3 2 3 Components for measuring gas drying and cleaning 19 3 2 4 Indicator and control elements connections 21 3 3 C S module 24 3 4 Cl module 25 3 4 1 Coulometer assembly and measuring cell 26 3 4 2...

Страница 4: ...urement 74 6 3 Determination of carbon after pyrolysis 77 6 3 1 Preparing the multi EA 4000 and C S module 77 6 3 2 Performing the determination of carbon after pyrolysis 77 6 4 Cl determination 80 6...

Страница 5: ...ule 126 7 6 Replacing the water traps 126 8 Fault removal 127 8 1 General information 127 8 2 Error messages in multiWin 127 8 3 Displays in the DEVICE STATUS window 133 8 4 Equipment fault 135 8 4 1...

Страница 6: ...ring gas drying and cleaning at the aut TIC solids module 34 Figure 24 Dust filter before the changeover valve 34 Figure 25 Connections at the automatic TIC solids module 35 Figure 26 Manual TIC solid...

Страница 7: ...are indicated by warning triangles and a signal word The type source and consequences of the danger are stated together with notes on preventing the danger The elements of the control and analysis pro...

Страница 8: ...EA 4000 enables the rapid sulfur and or carbon determination in construc tion materials such as cement or plaster in ceramic materials or glass samples Due to the many configuration options the multi...

Страница 9: ...bility claims are excluded for personal injury and property damage due to one or several of the following causes use of the multi EA 4000 analyzer other than intended improper commissioning operation...

Страница 10: ...ions leading to personal in jury or material damage The safety symbols must not be removed Damaged safety symbols must be replaced immediately The following safety symbols have been attached to the an...

Страница 11: ...in the use of the analyzer The instruction must also include conveying the content of this user manual and the user manuals of other system components or add on equipment The analyzer may pose dangers...

Страница 12: ...tections have been fitted and the analyzer is completely empty To prevent health damage the following must be observed when moving the ana lyzer in the laboratory lifting and carrying For reasons of...

Страница 13: ...bustion tube The furnace operates with temperatures of up to 1500 C The hot components furnace gas sluice dust trap boat must not be touched during or directly after the operation of the analyzer In m...

Страница 14: ...upplies disconnected from the mains if there is any interference with the electric components 2 5 4 Safety instructions for compressed gas cylinders and systems The carrier gases argon and or oxygen a...

Страница 15: ...auxiliary and operating materials The following has to be observed The relevant regulations and the notes in the safety data sheets of the manufactur ers have to be observed and complied with regards...

Страница 16: ...t must be reinstalled correctly immediately after comple tion of the service and repair work and be checked for operation The exterior of the analyzer may only be cleaned with a damp not dripping clot...

Страница 17: ...ng the autosampler FPG 48 manual using manual feed The device system can be combined with scales with an interface to the control com puter which automatically transfer the sample volume for the calcu...

Страница 18: ...bust corrosion resistant and low in wear Thanks to the HTC technology samples can be digested without catalysts at temperatures of up to 1500 C For especially difficult matrices the combustion tempera...

Страница 19: ...combustion furnace differs by less than 50 K from the target temperature If the temperature differs by more than 50 K from the target temperature the pump and gas flows are automatically deactivated...

Страница 20: ...The drying tube filled with magnesium perchlorate as a desiccant has been installed in the gas path for drying the measuring gas during C S determination A halide trap U tube is has been installed in...

Страница 21: ...d halide trap 3 2 4 Indicator and control elements connections The green LED at the left door of the analyzer illuminates after the analyzer has been switched on Figure 6 Status light at the basic dev...

Страница 22: ...e combus tion furnace with gas sluice and gas hoses for oxygen and argon Through the channel 4 in Figure 8 the measuring gas and bypass hoses can be routed to the Cl module Figure 8 Connections on the...

Страница 23: ...ily operation the multi EA 4000 is switched on and off from the On Off switch at the front 1 in Fig ure 7 The analyzer is then still e g ventilated when switched off During extended in terruptions of...

Страница 24: ...ng the CO2 SO2 measurement the CO2 SO2 molecules are sometimes detected by spec trometry for a longer low gas flow or shorter higher gas flow time Using the VITA method dwell time coupled integration...

Страница 25: ...7 Gas outlet pump connection to the multi EA 4000 8 Gas connection Cl connection to the Cl module 9 Gas inlet analyte measuring gas inlet 10 mains plug connection 11 Fuse holder 12 Mains switch 3 4 C...

Страница 26: ...ring Magnetic stirring Indication principle Alternating current bi am perometry Alternating current bi am perometry Generation principle anodic silver dissolution anodic silver dissolution Generator c...

Страница 27: ...g cell design 1 Knurled head screws 2 Cover 3 Opening for electrode labeled 4 Opening for olive to connect extraction hose or direct injection 5 Electrode space with silver anode 6 Magnetic stirring r...

Страница 28: ...apter 4 Measuring gas outlet with boat connection 5 Argon supply at the gas sluice Hydrogen chloride HCl has a high affinity with water and therefore dissolves in con densed water During analysis this...

Страница 29: ...ll is routed via the adsorption tube Here the acidic acid vapor escaping from the electrolyte is removed Active carbon is used as ad sorption agent 1 Adsorption tube 2 Halide trap Figure 17 Halide tra...

Страница 30: ...dule has additional interfaces on the rear for the communication with the multi EA 4000 and the autosampler The inter face assignment has been described in section Positioning the multi EA 4000 Cl p 5...

Страница 31: ...on based on direct method The automatic TIC solids module is only suitable for automatic operation in combina tion with the multi EA 4000 C or multi EA 4000 C S and the autosampler FPG 48 The automati...

Страница 32: ...Layout The quartz tube is attached to the ceramic combustion tube with a coupling A knurled ring with screw thread claps the TIC reactor and seals the connection through pressure on the inner sealing...

Страница 33: ...vapor condenses The measuring gas water mixture is passed via a hose to the gas fluid separator consisting of a con densate container and a Peltier cooling block The measuring gas is passed via the s...

Страница 34: ...ids module 1 Halide trap 2 Condensate container 3 Peltier cooling block 4 Drying tube 5 Condensation coil A dust filter has been placed between the halide trap 1 in Figure 23 and the change over valve...

Страница 35: ...for connection to the C S module 6 valve HT connection remains empty 7 COM HT connection for connection to the com bustion module HTS1500 of the multi EA 4000 8 waste connection for the waste hose to...

Страница 36: ...of samples only Automated sample supply with an autosampler is not possible 1 Manual TIC solids module 2 C S module 3 Basic device multi EA 4000 Figure 26 Manual TIC solids module 3 6 1 Technical dat...

Страница 37: ...id and heats the mixture slightly to speed up the reaction 1 Supply of phosphoric acid hose no 6 2 Measuring gas outlet 3 Supply of carrier gas oxygen 4 Erlenmeyer flask 5 Magnetic stirring rod 6 Magn...

Страница 38: ...module A drying tube filled with magnesium perchlorate as a desiccant is installed in the gas path immediately downstream of the reactor The desiccant cartridge is followed by two water traps The larg...

Страница 39: ...Halide trap Figure 30 Measuring gas drying and cleaning at the man TIC solids module 1 Power input module with mains switch and fuse holder 2 Measuring gas outlet analyte 3 Carrier gas connection O2...

Страница 40: ...movement of the ceramic hook with the straight aligned sample boats into the combustion furnace In the manual sample feed it is important that with highly reactive samples the transfer into the combu...

Страница 41: ...the total carbon and total sulfur in solid and paste like sam ples using high temperature oxidation in an oxygen flow A sample aliquot is weight precisely in a combustion boat and transferred complete...

Страница 42: ...e used when the sample contains easily purgeable or ganic substances as benzene cyclohexane chloroform etc The differential method should not be used when the TIC content of the sample is significantl...

Страница 43: ...nd carbon as for the TC TS analysis Because the acid only releases CO2 from carbonates and hydrocarbonates elementary carbon or the carbon from carbides cyanides isocyanates and thiocyanates is also d...

Страница 44: ...d to the analytical task dependent on the measuring range and sample matrix With the multi EA 4000 multipoint calibrations are performed with variable sample volumes and constant concentrations 4 5 2...

Страница 45: ...the concentrations determined for the individual detections The boat blank is determined by introducing an empty boat or a boat with additives for the sample into the combustion furnace and analyzing...

Страница 46: ...for high concentrations to be determined For Cl content in the lower concentration range no gas splitting is used All of the measuring gas passes the drying unit and the measuring cell For working wi...

Страница 47: ...resistant surface Do not locate the analyzer near sources of electromagnetic interference Avoid direct sunlight and radiation from heaters onto the analyzer If necessary provide air conditioning Never...

Страница 48: ...lose the flow regulators for argon oxygen Ar O2 and oxy gen O2 by turning them clockwise 1 2 in Figure 2 p 19 Adjust the gas flows later according to the method used 5 2 Unpacking and placing the anal...

Страница 49: ...yte O2 Oxygen gas connection Mains cable Mains connection com1 C S module COM pump in C S module pump Ar Gas connection for argon only required for Cl measurement and determination of carbon after pyr...

Страница 50: ...Commissioning multi EA 4000 50 Figure 32 multi EA 4000 C S Hose diagram...

Страница 51: ...on gas connection Mains cable Mains connection com1 Cl module COM pump in Cl module pump waste out Open outlet for the exhaust air of the analyzer Additional Cl module connec tions Target Socket for m...

Страница 52: ...Commissioning multi EA 4000 52 Figure 33 multi EA 4000 Cl Hose diagram...

Страница 53: ...rolysis waste out Open outlet for the exhaust air of the analyzer Additional C S module con nections Target PC USB port for connection to the computer Cl Coul Cl module Cl Coul scale External scales o...

Страница 54: ...Commissioning multi EA 4000 54 Figure 34 multi EA C S Cl for C S measurements Hose diagrams...

Страница 55: ...multi EA 4000 Commissioning 55 Figure 35 multi EA 4000 C S Cl for Cl measurements...

Страница 56: ...ion for argon only required for Cl measurement and pyrolysis waste out Open outlet for the exhaust air of the analyzer Additional C S module con nections Target PC USB port for connection to the compu...

Страница 57: ...multi EA 4000 Commissioning 57 Figure 36 Automatic TIC solids module Hose diagrams...

Страница 58: ...Commissioning multi EA 4000 58 Figure 37 multi EA 4000 C S with automatic TIC solids module...

Страница 59: ...C S module COM pump in Open Ar Argon gas connection waste out Open outlet for the exhaust air of the analyzer C S module connections Target PC USB port for connection to the computer scale External sc...

Страница 60: ...Commissioning multi EA 4000 60 Figure 38 multi EA 4000 with man TIC solids module Hose diagrams...

Страница 61: ...multi EA 4000 Commissioning 61 Figure 39 multi EA 4000 C S Cl with man TIC solids module...

Страница 62: ...he autosampler is parallel to the basic device and level with the work ing tube If the sample boat is inserted into the furnace at an angle or not at the right height relative to the working tube the...

Страница 63: ...the eye of the boat into the hook and carefully move the boat manually into the furnace Make sure that the hook is not wedged or angled If not change the position of the autosampler 11 Check the star...

Страница 64: ...left hand boat position 5 Check that the gripper is centered above the opening of the adjustment aid and can enter the opening without ob struction Correct the alignment in the x and y directions usin...

Страница 65: ...WARDS BACKWARDS adjust the position in the cut out The gripper must be adjusted flush right and centered in the cut out The gripper must hover approx 1 mm above the cut out The sampler arm must not e...

Страница 66: ...oat from the furnace and the hook 3 Slide the ceramic hook manually to the stop plate 4 Reinitialize the device 5 4 3 Retrofitting the sampler FPG 48 with a boat storage For measurements using the aut...

Страница 67: ...the slot 7 Adjust the ceramic hook in the start position The hook tip must be flush with the right hand edge of the left hand boat position here position 37 Place a straight paper or plastic strip e...

Страница 68: ...ioning the manual sample feed During sample feed operation there is a risk of burns at the hot boat and ceramic hook After pulling out of the furnace the boat and hook remain hot for a long time 1 Gas...

Страница 69: ...ales to the power supply and switch on 3 Set the baud rate to 9600 4 For further configurations see the documentation of the scales To transfer the sample weight proceed as follows 5 Start the measure...

Страница 70: ...the TIC reactor The analysis modules have been connected The manual sample feed or the autosampler have been positioned and adjusted The PC is connected and the multiWin software installed 1 Open the...

Страница 71: ...A 4000 and C S module WARNING Risk of electric short circuit In the combustion furnace HTS1500 very high electrical currents occur in spite of a low voltage max 14 V The combustion tube is part of the...

Страница 72: ...tion Position ing the multi EA 4000 C S p 49ff 1 Assemble the gas sluice Ensure correct fit of the sealing ring see arrow Screw the base element and pressure ring together using 3 hexagon socket screw...

Страница 73: ...do so push the hose onto the gas connection and se cure it with the union nut 7 Pull off the dust trap contact guard from the opening on the left side of the basic device see Figure below 8 Place the...

Страница 74: ...mination remove the halide trap and connect an empty U tube instead The halide trap binds some of the sulfur For C S determination the use of the halide trap must therefore be considered With low sulf...

Страница 75: ...so first activate the sensors Select the menu command DEVICE DEVICE EDIT Enable the ELEMENTS to be analyzed If both carbon sulfur and chlorine are enabled click on CERAMIC TUBE CS in the list COMBUSTI...

Страница 76: ...BLANK NOMINAL VALUE Target concentration for calibration standards or AQS standard OPERANDS Input of the sample weight Populate the autosampler Use the and buttons to move the sample rack to the desir...

Страница 77: ...lored 4 Position the sampler FPG 48 see section Connecting and using the au tosampler p 62 6 3 2 Performing the determination of carbon after pyrolysis CAUTION During the operation of the sampler and...

Страница 78: ...PERATURE 850 C EC PURGE TIME 300 s 7 After the run in time set the following gas flows pump O2 Set the intake flow until in the STATUS ANALYZER window the value NOMINAL 100 10 is displayed correspondi...

Страница 79: ...and the change over from oxygen to argon takes place Now set the argon flow at the Ar O2 rotameter to 2 3 2 5 l min This flow configuration is retained for the subsequent pyrolysis measurement The sam...

Страница 80: ...ufficiently before conversion NOTICE Alkaline salts hand perspiration cause crystallizations in the quartz glass when heat ing the combustion furnace which reduce the service life of the tube Where po...

Страница 81: ...prox 2 5 cm quartz wool and push the cotton plug into the end of the tube 2 Place the sealing ring into the pressure ring of the gas sluice 3 Push the quartz tube into the pressure ring until the gas...

Страница 82: ...nt 6 Remove the heat guard To do so release 2 slotted screws with a screwdriver 7 Slide the quartz tube with gas sluice up to the stop into the combustion furnace In the process insert the guide pins...

Страница 83: ...se no 17 to the gas connection 3 4 Push the flame sensor onto the gas connection and attach with the brass screw 2 Tighten screw finger tight 5 Connect the cable of the flame sensor to the valve conne...

Страница 84: ...container above the PTFE tray 4 Attach the gas outlet of the combustion tube to the inlet of the sulfuric acid container using the spherical joint connection 1 5 Secure the spherical joint connection...

Страница 85: ...c acid containers without split outlet the bypass hose remains unattached 11 Slide the measuring gas hose transparent and the bypass hose black through the channel in the multi EA 4000 If necessary pu...

Страница 86: ...atin in a beaker with 400 ml ultrapure water allow to swell for 3 hours and then dissolve whilst heating to 35 45 C 3 Solution B2 Dissolve 1 0 g thymol and 0 3 g thymol blue in a beaker in 500 ml meth...

Страница 87: ...le Make sure that the pin of the measuring cell points to the front and is engaged in the guide slot of the holder 1 Connection for the combined electrode 2 Measuring gas connection at the combined el...

Страница 88: ...e menu item SYSTEM COMPONENT TEST in the CL AMP tab NOTICE To protect the combined electrode against wear note the following Always add fresh electrolyte to the measuring cell before the end point rou...

Страница 89: ...The following gas flows must be configured for this purpose Gas flows for measurements without gas splitting pump O2 Ar approx 600 ml min 300 400 ml min 300 400 ml min The following should be noted wh...

Страница 90: ...ding position numbers However it does not need to be without gaps NAME Sample ID With an automatic sample ID can be created ANALYSIS TYPE Selection of the analysis type SAMPLE DAILY FACTOR DETERMINATI...

Страница 91: ...he boat into the hot zone confirm the on screen prompt with OK NOTICE The boat must be moved extremely slowly to allow the pyrolysis gases to develop slowly and incinerate completely If the sample is...

Страница 92: ...TS1500 very high electrical currents occur in spite of a low voltage max 14 V The combustion tube is part of the cover of live components Only switch on the analyzer with the combustion tube inserted...

Страница 93: ...together gas tight to prevent ambient air entering the system or measuring gas escaping at this point 1 Assemble the components of the coupling for connect ing the ceramic tube and TIC reactor Only t...

Страница 94: ...Ceramic cannula with sealing ring 2 Quartz glass TIC reactor 3 Pump hose with connection to TIC reactor 4 hose pump 5 Knurled ring 1 Slide the TIC reactor 2 into the coupling until it touches the cer...

Страница 95: ...ect the measuring gas outlet 1 with hose no 72 to the top end of the cooling coil on the rear of the TIC solids module 9 Slide the hose for the oxygen supply no 17 onto the re actor connection for the...

Страница 96: ...ion for the direct method 6 5 3 TIC determination with the automatic TIC solids module CAUTION During autosampler operation there is a risk of burns at the hot boat and ceramic hook After pulling out...

Страница 97: ...intake flow at the pump valve of the multi EA 4000 8 Weigh the sample on a ceramic boat The sample weight for TIC determination must be max 50 mg Cover the sample with some annealed quartz sand The q...

Страница 98: ...ents measuring gas from escaping through the open inlet 6 5 4 TOC determination based on differentiation method CAUTION During autosampler operation there is a risk of burns at the hot boat and cerami...

Страница 99: ...boat 1 for TIC determination must be max 50 mg Cover the sample with some annealed quartz sand The quartz sand improves the wetting of the sample with acid 9 Start the measurement by clicking on START...

Страница 100: ...the entire sample The measuring gas from the purged TIC is passed via the measuring gas drying and cleaning of the automatic TIC solids module to the detector in the C S module Boat 1 is then pulled o...

Страница 101: ...rom the sample Phosphoric acid is unsuitable for the direct determination of the TOC Perform a measurement as follows 1 Fill the acid bottle with 10 hydrochloric acid 2 Switch on the basic device mult...

Страница 102: ...With an automatic sample ID can be created ANALYSIS TYPE Selection of the analysis type SAMPLE DAILY FACTOR DETERMI NATION CALIBRATION MEASUREMENT AQA MEASUREMENT or DET BOAT BLANK NOMINAL VALUE Targ...

Страница 103: ...C S module All other connections can remain as they are 2 Check the hoses see hose diagram Figure 38 p 60 and Figure 39 p 61 3 Connect the manual TIC solids module to the C S module C S module connect...

Страница 104: ...into the plastic insert in the upper housing 2 Screw the dispenser onto the bottle Connect the hose for supplying acid to the valve and to the TIC head 3 Switch on the basic device multi EA 4000 the...

Страница 105: ...alysis group for storing the measuring data 15 Create an analysis sequence Add the desired number of samples to the sample table with Enter the following data Column Description NAME Sample ID With an...

Страница 106: ...and the same speeds are used in each measurement The analyzer starts processing the analysis sequence The MEASUREMENT ANALYSIS window opens 19 After completing the measurement stop the magnetic stirr...

Страница 107: ...llulose immediately Clean the device with a damp cloth Do not wet the safety notices at the device with solvent Replace damaged safety notices 7 1 2 Check tube connection Screw connections of various...

Страница 108: ...currents occur in spite of a low voltage max 14 V The combustion tube is part of the cover of live components Only switch on the analyzer with the combustion tube inserted Always switch off the analyz...

Страница 109: ...from the basic device through the opening on the right hand side 9 Pull the gas sluice off the ceramic tube with a twisting motion 10 Inspect the wide green sealing ring in the gas sluice see arrow f...

Страница 110: ...7 to the gas sluice 3 Place the dust trap onto the ceramic tube Align the dust trap with the gas connec tion pointing up Press the dust trap slightly against the tube towards the tube axis until the d...

Страница 111: ...off the opening The dust trap is now visible 3 Detach the measuring gas hose hose no 1 from the dust trap 4 Slightly pull the dust trap to detach it NOTICE The dust trap might come loose abruptly Sup...

Страница 112: ...p magnesium perchlorate away from flames The oxidant can make a fire worse Drying tubes are used in the following measurement arrangements C S measurement at the multi EA 4000 basic device TIC measure...

Страница 113: ...pper wool 1 Unscrew the red union nuts from the U tube and pull the U tube out of the clamps 3 2 Pull out the depleted copper wool or brass wool from the U tube with a tweezers or a small hook 3 Inspe...

Страница 114: ...wool in the halide trap is replaced analogous to the replacement of the halide trap in the basic device multi EA 4000 see section Replace the halide trap p 113 7 3 1 Replacing the sulfuric acid clean...

Страница 115: ...nserted Always switch off the analyzer from the mains switch at the rear of the device for conversions and mainte nance to the combustion tube or combustion furnace WARNING The concentrated sulfuric a...

Страница 116: ...ove and empty the acid container 5 Pull the gas hose off the gas inlet connection of the quartz tube 2 When using the flame sensor Unscrew the flame sensor see section Connecting the flame sensor opti...

Страница 117: ...ty or damage the electrode Therefore make sure that the electrolyte never dries on the combined electrode For brief interruptions of operation one day to the next Store the electrode in the electrolyt...

Страница 118: ...electrode it will get stuck on the electrode When pulling off the hose the electrode might break 7 3 4 Servicing the measuring cells Since the introduction of hot reaction gases during the measuremen...

Страница 119: ...l the adsorption agent 5 Seal one side of the glass tube with cotton wool and fill with adsorption agent 6 Seal the glass tube with cotton wool 7 Screw the filled adsorption tube back on finger tight...

Страница 120: ...cur in spite of a low voltage max 14 V The combustion tube is part of the cover of live components Only switch on the analyzer with the combustion tube inserted Always switch off the analyzer from the...

Страница 121: ...reactor for cracks and blow outs NOTICE Only re use intact reactors 11 If applicable clean the reactor with a suitable solvent and brush or cellulose 12 Rinse the reactor with ultrapure water and all...

Страница 122: ...s module back into its origi nal position 12 Re assemble the TIC reactor and FPG 48 see section Connect the TIC reactor and sampler p 94 and Connecting and using the autosampler p 62 7 4 3 Removing an...

Страница 123: ...p hose between the two plastic stoppers 2 in Figure 49 in the hose cartridge 7 Insert the hose cartridge into the pump and allow it to engage 8 Screw the pump hose to the TIC reactor NOTICE The TIC re...

Страница 124: ...pure water 6 Check the pump body and roller carrier for wear NOTICE Notify customer service if pump body and roller carrier are strongly af fected 1 Conveyor belt 2 Groove 3 Metal adapter 4 Hose guide...

Страница 125: ...pprox 1 cm onto the glass connections of the con densate container 7 5 Manual TIC solids module Maintenance task Maintenance interval Remove splashes of chemicals from the hous ing Immediately Clean t...

Страница 126: ...order and installa tion direction specified Replace the water traps dependent on the sample matrix but no later than after 6 months as follows 1 Pull the water traps out of the 2 retaining clips 2 De...

Страница 127: ...edied the Analytik Jena AG service department must always be informed This also applies for the repeated occurrence of individual faults For the fault diagnosis the zip file created must be sent by em...

Страница 128: ...rror when opening the port Cause Remedy Communication problems Disconnect USB connection between the control module and PC and re connect after approx 10 s Initialize Another program is using the inte...

Страница 129: ...meout during measurement cancellation Acknowledge message Initialize 24 Timeout Measurement Cause Remedy Timeout during measurement Maximum integration time has been exceeded Check analyzer Check meth...

Страница 130: ...or Analog values out of range C sensor Analog values out of range coarse Cause Remedy The analog values of the detector are outside the operating range Check the quality of the carrier gas Initialize...

Страница 131: ...rrect status Cause Remedy communication faulty Acknowledge message Initialize Check titration cell status via menu item SYSTEM COMPONENT TEST tab CL AMP 135 Cl sensor incorrect version Cause Remedy tr...

Страница 132: ...tion Cause Remedy No communication with scales Check connection Check configuration of scales 291 Scales incorrect weight unit Cause Remedy Currently only one unit g is permitted Set the unit gram g i...

Страница 133: ...or specific Red Component is not ready for measurement Run in time not yet complete wait for run in time to complete Faults fault finding read information on the corresponding component in multiWin vi...

Страница 134: ...135 warm up time detector is not yet ready for operation wait until the warm up time is complete after activation approx 30 min Device not ready for measurement CI AMP Display rot Description inactive...

Страница 135: ...ulty Switch off the analyzer from the mains switch Inform Service No intake flow at the pump flow regulator Cause Solution Pump not switched on Check temperature difference Wait for the temperature di...

Страница 136: ...of the NDIR detector differ from the target value and are outside tolerances Note Measurements can still continue Check the oxygen supply of the gas supply Check the oxygen supply at the flow regulato...

Страница 137: ...ication fault Software does not respond Cause Solution Computer crash Switch off analyzer completely incl basic device printer sampler and external PC restart the system af ter a few seconds multiWin...

Страница 138: ...ation Recovery generally too low Cause Solution Desiccant too moist Sooted filter and measuring gas hoses Leaks Inspect and replace desiccant Inspect and replace filter Inspect the dust trap if heavil...

Страница 139: ...ule Only start the multiWin program approx 3 min after switching on the analyzer Recovery too low split factor 1 4 Cause Solution Sulfuric acid too diluted Check and replace the sulfuric acid Sooted c...

Страница 140: ...ad e g 25 HCl NOTICE Do not use HCl permanently Scattering measurements Cause Solution Sample not distributed evenly across the entire boat length The sample must be evenly distributed to allow the sa...

Страница 141: ...tion Pyrolysis period selected too short The pyrolysis period should be min 3 min to ensure that all organic compounds are fully digested and purged Pyrolysis temperature chosen too high At temperatur...

Страница 142: ...EA 4000 and packaged separately before a transport Reinstallation and recommissioning of the basic device may only be performed by the Analytik Jena AG customer service or trained specialist personnel...

Страница 143: ...multi EA 4000 Drain and clean the sulfuric acid container see section Replac ing the sulfuric acid cleaning the sulfuric acid container p 114 9 Pull the measuring gas hose transparent and the bypass h...

Страница 144: ...n the device is cold or allow the device to cool down sufficiently best overnight Caution when opening the right side panel There is a risk of injury from sharp edged components The high temperature c...

Страница 145: ...aided wires Pull out the cable with braided wires from the top by twisting them to and fro slightly 8 Detach the two screws 2 3 attaching the furnace car tridge and mounting plate in the analyzer 9 Un...

Страница 146: ...nd the formation of condensate is thus prevented in the transport con tainer 9 1 4 Moving the analyzer in the laboratory CAUTION Unintentional dropping of the analyzer poses a risk of injury and the a...

Страница 147: ...ion observe the notes in section Site requirements p 47 9 2 Storage NOTICE Environmental influences and condensate formation can destroy individual compo nents of the analyzer The analyzer must only b...

Страница 148: ...al center for correct disposal according to the appropriate legal guidelines The electrolyte solution is carefully neutralized and collected as silver salt residue in containers This should be correct...

Страница 149: ...ghing in porcelain or quartz glass boats Automatic sampler or manual feed Gas supply Oxygen min 2 5 and argon 4 6 with inlet pressure 200 400 kPa 29 58 psi Control analysis control and anal ysis softw...

Страница 150: ...se desiccant Air pressure 70 106 kPa Operating system Windows 7 Professional or later Processor Intel Core I3 or better Working memory 4 GB Free hard disk space 40 GB Drive CD ROM drive for installati...

Страница 151: ...rds meeting the requirements of EU directives 2014 35 EU and 2014 30 EU The device leaves the factory in a sound condition as far as technical safety is concerned To maintain this condition and to ens...

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