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Description of instrument

— 4

SPECTRO ARCOS FHX3X — 08.02.2022

6.2

Preparation of the instrument ............................................................................................ 32

6.3

Switch on the instrument, ready for operation, plasma start ............................................. 32

6.4

Switch off the instrument/plasma ...................................................................................... 34

6.5

Carrying out the measurement ......................................................................................... 35

6.5.1

Preparing the measuring procedure .................................................................... 35



Spectrum calibration of the optical system .......................................................... 35



Calibrating a method ............................................................................................ 37

6.5.2

Start the measurement ........................................................................................ 38

Maintenance ..................................................................................................... 39

7.1

Maintenance schedule ...................................................................................................... 39

7.2

Cleaning the plasma torch ................................................................................................ 41

7.3

Cleaning the load coil ........................................................................................................ 45

7.4

Cleaning the nebulizer (standard Crossflow Nebulizer) .................................................... 46

7.5

Cleaning the spray chamber (standard Scott Chamber) .................................................. 48

7.6

Checking the aerosol formation of the nebulizer .............................................................. 50

7.7

Optimizing the nebulizer gas flow ..................................................................................... 50

7.8

Cleaning the Side-On Plasma Interface (SPI) .................................................................. 51

7.8.1

Removing the SPI ................................................................................................ 51

7.8.2

Cleaning the lens and the SPI ............................................................................. 53

7.8.3

Installing the lens and the SPI ............................................................................. 54

7.9

Cleaning the optical plasma interface (OPI) (Multiview EOP only) ................................... 55

7.9.1

Removing the OPI ............................................................................................... 55

7.9.2

Cleaning the sampler ........................................................................................... 57

7.9.3

Cleaning the lens ................................................................................................. 58

7.9.4

Installing the lens and the OPI ............................................................................. 59

7.10

Installing/removing of the Dual Side-On Interface (DSOI) ................................................ 60

7.11

Mirror – cleaning the blind plug, torch adapter, and DSOI ................................................ 62

7.12

Pump tubing maintenance ................................................................................................ 63

7.13

Cleaning agents ................................................................................................................ 64

Troubleshooting ................................................................................................ 65

Spare parts and consumables .......................................................................... 71

De-commissioning ............................................................................................ 71

Manufacturer address ...................................................................................... 71

EC Declaration of Conformity ........................................................................... 71

Содержание 76004567

Страница 1: ...die Datei verschoben umbenannt oder gel scht Stellen Sie sicher dass die Verkn pfung auf die korrekte Datei und den korrekten Speicherort zeigt SPECTRO ARCOS FHX3X Optical emission spectrometer with i...

Страница 2: ......

Страница 3: ...3 Connections right hand side 16 3 4 Connections analysis room 17 3 5 Peristaltic pump 18 3 6 Sample introduction system 19 3 7 Plasma torch box 20 Plasma torch box SOP 20 Plasma torch box EOP 21 Pla...

Страница 4: ...ard Scott Chamber 48 7 6 Checking the aerosol formation of the nebulizer 50 7 7 Optimizing the nebulizer gas flow 50 7 8 Cleaning the Side On Plasma Interface SPI 51 7 8 1 Removing the SPI 51 7 8 2 Cl...

Страница 5: ...e analysis of liquids The peristaltic pump is used to feed in the sample Subsequently the liquid sample is nebulized and fed into the plasma as an aerosol The high temperature of the plasma 6 000 8 00...

Страница 6: ...Symbols used The following symbols are used in these abbreviated operating instructions and or on the instrument If required additional important information is available in connection with these sym...

Страница 7: ...eavy and its center of gravity is located in the optical system front left side of the instrument Only service personnel authorized by the manufacturer are permitted to unpack install set up and conne...

Страница 8: ...output This applies especially to all components of the sample introduction system and in particular to the plasma torch Operate the instrument only using system networks with protective ground PE co...

Страница 9: ...zer and it must not be moved during operation During the operation of the instrument compliance with the ambient conditions according to the technical specification is mandatory During operation adequ...

Страница 10: ...sion of the instrument and its safety devices without complying with the applicable rules and regulations Bypassing or deactivating safety and protective devices Improper use of accessories or periphe...

Страница 11: ...The sample material may be toxic and or corrosive Ensure that the sliding door is closed during the operation Ensure that the external exhaust system functions properly Warning Hot surface The plasma...

Страница 12: ...d in the work zone Warning High voltage Higher electrical voltages occur inside the spectrometer Shut down the instrument immediately if it is damaged Never tamper with the safety devices If you suspe...

Страница 13: ...mple introduction Compliance with the safety instructions in the SPECTRO ARCOS FHX3X operating manual and the external automatic sample introduction is mandatory In order to provide protection against...

Страница 14: ...to the right of the instrument 3 1 Front side Fig 1 No Component No Component 1 Plasma torch box inspection window 6 Connection to sample introduction system 2 Plasma torch box housing 7 Peristaltic...

Страница 15: ...rument SPECTRO ARCOS FHX3X 08 02 2022 15 3 2 Rear panel Fig 2 No Component No Component 1 Generator exhaust 4 Air filter behind service flap 2 Extraction box housing plasma torch 5 UV Plus purifier 3...

Страница 16: ...ment 16 SPECTRO ARCOS FHX3X 08 02 2022 3 3 Connections right hand side Fig 3 No Component No Component 1 Main switch 4 Oxygen connection option 2 PC connection 5 Argon connection 3 Plasma status port...

Страница 17: ...ctions analysis room Fig 4 No Component No Component 1 Nebulizer gas 4 Gas connection Spectro Intelligent Valve System SIVS optional 2 Additional gas connection 5 Control system Spectro Intelligent Va...

Страница 18: ...COS FHX3X 08 02 2022 3 5 Peristaltic pump Information Check the peristaltic pump s hoses for damage and replace the hoses regularly Fig 5 no Component no Component 1 Leadthrough to sample introduction...

Страница 19: ...6 Sample introduction system Fig 6 No Component No Component 1 Plasma torch 6 Argon connection 2 Clamp 7 Nebulizer 3 Spray chamber 8 Spherical joint seal 4 Spray chamber outlet 9 90 Spray chamber ada...

Страница 20: ...ltiView DSOI the plasma torch is in the vertical position When using instruments with Multiview optional the plasma torch can be installed horizontally EOP or vertically SOP DSOI depending on the Mult...

Страница 21: ...rface OPI necessary for the axial version is equipped with an air cooling system Fig 8 No Component No Component 1 Extraction box housing and torch 6 Elbow adapter 2 Load coil 7 Nebulizer gas connecti...

Страница 22: ...l Side Optical Interface optional Fig 9 No Component No Component 1 Extraction box housing and torch 5 Plasma torch bracket 2 DSOI Dual Side On Interface optional 6 Plasma torch 3 DSOI argon connectio...

Страница 23: ...o 32 A slow blow Sound pressure level max 55 dBA Protection class IP 20 IEC 60529 Contamination class Contamination class II laboratory environment Stability according to DIN EN 61010 1 compliant if c...

Страница 24: ...n Oxygen supply for auxiliary gas optional for organic applications only Inlet pressure during operation 4 0 bar 58 psi Quality 4 5 99 995 Flow rate The flow rate depends on the application Extraction...

Страница 25: ...rument The instrument is front heavy and its center of gravity is located in the optical system front left side of the instrument The instrument weighs approx 249 kg approx 548 lbs and its weight is n...

Страница 26: ...he instrument must be accessible from the front and from both sides for maintenance purposes Set up the instrument accordingly A table of corresponding dimensions and load carrying capacity is require...

Страница 27: ...ual clean office environment contains 18 to 36 million particles per cubic meter of indoor air To avoid instrument damage the instrument must also be set up in an environment which is free from corros...

Страница 28: ...f 8 bar 116 psi The tubing for the argon supply system is included in SPECTRO s scope of supply 5 m long OD ID 8 6 mm This tubing is screwed to the connection point on the right hand side of the instr...

Страница 29: ...ystem functions properly Depending on the sample material used it may be necessary to subject the exhaust air to treatment in order to remove contaminants If necessary the exhaust gases must be cleane...

Страница 30: ...acity at the nozzle 1 rear Generator extraction or without extraction 2 front Plasma torch box housing 250 300 m h 150 177 CFM or blowing into the room without obstruction Dependent on ambient tempera...

Страница 31: ...torch plasma interface and induction coil wearing protective gloves and safety goggles is mandatory Warning Risk of injury Glass parts may break when handled incorrectly and cause cutting injuries Wh...

Страница 32: ...e plasma torch box is open If the window protective pane is damaged do not use the instrument The instrument must only be started with the blind plug and plasma torch inserted or only with the plasma...

Страница 33: ...nt control parameters 5 Purge the sample introduction system for 2 minutes with argon by clicking the Purge button Ensure that the pressure clamps of the peristaltic pump are clamped tightly around th...

Страница 34: ...instrument The plasma extinguishes 3 Press the X button in the upper right hand corner of the application window in order to end the instrument s software program ICP ANALYZER PRO The program is termi...

Страница 35: ...suring samples Spectrum calibration of the optical system The spectrum calibration of the optics is mandatory after a software message spectrum drift after the system has been switched on and after th...

Страница 36: ...mmercial solutions for the spectrum calibration optimization or equipment check are available from your local SPECTRO organization In order to proceed with the spectrum calibration proceed as follows...

Страница 37: ...e standards with the lowest concentrations and then the ones with higher concentrations 3 Use the peristaltic pump in order to feed the corresponding sample to the sample introduction system 4 Click o...

Страница 38: ...ok and a method must be created first To do this use the online help 2 Feed the sample to be measured to the sample introduction system by means of the peristaltic pump 3 Press the Measure button in o...

Страница 39: ...g maintenance tasks Start of work Tasks to be performed Check the gas supply Minimum residual pressure in bottle 40 bar Peristaltic pump tubing and sample introduction system tubing Check for damage a...

Страница 40: ...Clean if required see page 45 Pump tubes Check for damage Replace if required see page 63 DSOI Dual Side On Interface optional Check mirror replace if necessary see 62 UV PLUS purifier Use the instrum...

Страница 41: ...bucket must be used to collect the larger pieces first In order to remove small parts and glass fragments a suitable vacuum must be used Warning Toxic substances The cleaning solution is corrosive Wh...

Страница 42: ...the clamping screw 1 If necessary use a screwdriver or another suitable tool to loosen the clamping ring 2 Pull the torch 3 slightly out of the adapter Remove the hoses A C Pull the torch out of the a...

Страница 43: ...15 minutes Subsequently rinse the torch with distilled water and let it dry completely Fig 15 8 Use a lint free cloth in order to clean the adapter subsequently proceed with a visual inspection 9 Re m...

Страница 44: ...022 Inserting the plasma torch I Insert the torch in the appropriate position and turn the lever 2 clockwise until it snaps into place Fig 17 Radial plasma observation SOP DSOI The plasma torch has be...

Страница 45: ...on the sample introduction system wearing protective gloves and safety goggles is mandatory If glass is broken a suitable container bucket must be used to collect the larger pieces first In order to...

Страница 46: ...contain hazardous sample residues When working on the sample introduction system wearing protective gloves and safety goggles is mandatory Compliance with the safety data sheets as well as the H and P...

Страница 47: ...ion When heavy contamination must be removed another suitable acid or aqua regia may be required If there are deposits on the capillary tube remove them very carefully with a fine copper wire Extreme...

Страница 48: ...s When working on the sample introduction system wearing protective gloves and safety goggles is mandatory Compliance with the safety data sheets as well as the H and P phrases that apply to the sampl...

Страница 49: ...ous substance Observe the corresponding information on hazardous materials Subsequently use a laboratory cleaning agent for removing traces of fatty substances streaks if required Now use distilled wa...

Страница 50: ...If this is not the case the nebulizer may be clogged and must be cleaned see page 46 Fig 19 5 Reinstall the components Checking of aerosol generation is now complete 7 7 Optimizing the nebulizer gas...

Страница 51: ...l for 10 to 15 minutes before commencing work on them When working on the plasma torch plasma interface and induction coil wearing protective gloves and safety goggles is mandatory Warning Risk of inj...

Страница 52: ...he spray chamber 4 Remove the spray chamber 5 and the spherical joint seal 5 Loosen the plasma torch 3 by turning the lever 2 counterclockwise 6 Remove the plasma torch Fig 20 7 The SPI has a latch 4...

Страница 53: ...ve Check the lens for contamination When cleaning the lens proceed as follows if necessary 1 Loosen the light channel sleeve 1 Fig 22 2 Insert a clean peek sample needle or similar type of object 1 th...

Страница 54: ...ens for the SPI SOP MULTIVIEW application can be distinguished by the straight edge on two sides 3 Lay the second PTFE ring 4 on top of it 4 Moderately tighten the light channel sleeve 5 including the...

Страница 55: ...ce The plasma torch plasma interface and load coil may be very hot Let the components cool for 10 to 15 minutes before commencing work on them When working on the plasma torch plasma interface and ind...

Страница 56: ...the spray chamber 4 Remove the spray chamber 4 and the spherical joint seal 5 Loosen the plasma torch 1 by turning the lever 3 counterclockwise 6 Remove the plasma torch Fig 25 7 The OPI has a latch 1...

Страница 57: ...down This prevents dirt particles from falling into the OPI Fig 27 2 Clean the sampler under running water using a nailbrush When heavy contamination must be removed a suitable acid may be used Then...

Страница 58: ...ove Check the lens for contamination When cleaning the lens proceed as follows if necessary 1 Use the OPI tool 2 to loosen the retaining collar 1 at the rear Fig 28 2 Insert a clean peek sample needle...

Страница 59: ...shed by its straight edge on one side 3 Lay the second Teflon ring 3 on top of it 4 Screw the adjusting collar 2 moderately tight using the tool 1 Fig 30 5 Insert the OPI into the instrument following...

Страница 60: ...ss parts may break when handled incorrectly and cause cutting injuries When working on the sample introduction system wearing protective gloves and safety goggles is mandatory If glass is broken a sui...

Страница 61: ...he DSOI Careful not to touch the sensor mirror in the DSOI s bayonet 2 Fig 32 6 Insert the supplied blind plug into the opening on the torch box Careful not to touch the sensor mirror in the blind plu...

Страница 62: ...crew it onto the interface and tighten it moderately Notice Instrument damage measurement error The surface of the mirror is sensitive and must not be touched If the lens surface is touched with the f...

Страница 63: ...retaining clamp from the peristaltic pump 4 Fold the retaining clip vertically upwards and remove the clip from the shaft Subsequently remove the connected capillary hoses and the hose from the retain...

Страница 64: ...ocedure if a hazardous substance has been spilled on or into the instrument Unless otherwise stated in the respective instructions the cleaning agents listed here are preferred for cleaning purposes C...

Страница 65: ...ectly Plasma stopped Dmb timeout The generator could not establish communication with the gas control unit Turn off the instrument and restart it again If the problem persists please contact the SPECT...

Страница 66: ...stment as required Turn off the instrument and restart it again If the problem persists please contact the SPECTRO Service Department Internal LPF fan error The fan of the low pass filter does not wor...

Страница 67: ...t exceeding the maximum value was detected during the plasma start Restart the instrument If the problem persists please contact the SPECTRO Service Department Internal temperature error Ensure that t...

Страница 68: ...Check the working coil ensuring it is not deformed and it is clean The windings must be evenly distributed the coil must not be inclined to one side If OK repeat the test If impurities have accumulat...

Страница 69: ...ch Data cable not plugged in or defective Check cable Address incorrect or used for a different purpose Enter the correct IP address online help Only qualified IT staff are permitted to enter the addr...

Страница 70: ...r leaks and eliminate these Plasma extinguishes when nebulizer gas flow is switched on Sample introduction tube not connected to the nebulizer Connect the tube and check fitting Oxygen in sample intro...

Страница 71: ...les ensures the safe operation and achievement of the specified output This applies especially to all components of the sample introduction system and in particular to the Plasma torch 10 De commissio...

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