Index
291
Symptoms of malfunctions
baseline is falling, 72
baseline is high, 72
baseline is rising, 72
baseline wanders, 73
chromatographic symptoms, 70 – 74
difficulty in mass filter electronics, 84
difficulty with the EM supply, 84
difficulty with the fan, 85
difficulty with the HED supply, 85
difficulty with the high vacuum pump, 85
error messages, 84 – 88
fan is not operating, 69
foreline pressure has exceeded 300 mTorr, 86
foreline pressure is too high, 79
foreline pressure is too low, 80
foreline pump is not operating, 68
gauge controller displays 9.9+9 and then goes
GC does not turn on, 68
GC/MSD interface will not heat up, 83
general symptoms, 68 – 69
high abundances at
m/z
18, 28, 32, 44 or at
m/
high background, 75
high mass sensitivity is poor, 78
internal MS communication fault, 86
ion source will not heat up, 82
isotopes missing or ratios are incorrect, 75
LEDs are all blinking, 69
lens supply fault, 86
log amplifier ADC error, 86
mass assignments are incorrect, 76
mass filter (quad) heater will not heat up, 83
mass spectral symptoms, 75 – 78
MSD does not turn on, 68
MSD is on but status LEDs are all blinking, 69
no peaks, 70, 86
peak widths are inconsistent, 76
peaks are fronting, 71
peaks are tailing, 71
peaks have flat tops, 72
peaks have precursors, 76
peaks have split tops, 72
poor repeatability, 74
poor sensitivity, 74
power indicator on the gauge controller does
pressure symptoms, 79 – 81
relative abundance of
m/z
retention time drifts (all peaks), 73
status LEDs are all blinking, 69
temperature control disabled, 87
temperature control fault, 87
temperature symptoms, 82 – 83
the high vacuum pump is not ready, 87
the system is in standby, 87
the system is in vent state, 88
there is no emission current, 88
there is not enough signal to begin tune, 88
vacuum manifold pressure is too high, 79
vacuum manifold pressure is too low, 80
Summary of Contents for 5973
Page 1: ...H Hardware Manual HP 5973 Mass Selective Detector ...
Page 3: ...HP 5973 Mass Selective Detector Hardware Manual ...
Page 25: ...1 Installing GC Columns To condition a capillary column 25 ...
Page 30: ...30 ...
Page 37: ...2 Operating the MSD To view MSD analyzer temperature and vacuum status 37 ...
Page 39: ...2 Operating the MSD To set monitors for MSD temperature and vacuum status 39 ...
Page 41: ...2 Operating the MSD To set the MSD analyzer temperatures 41 ...
Page 43: ...2 Operating the MSD To set the interface temperature from the ChemStation 43 ...
Page 51: ...2 Operating the MSD To remove the MSD covers 51 Upper cover Lower cover ...
Page 92: ...92 ...
Page 105: ...4 Maintaining the MSD To drain the foreline pump 105 Fill cap Drain plug Pump motor ...
Page 113: ...4 Maintaining the MSD To separate the MSD from the GC 113 ...
Page 121: ...4 Maintaining the MSD To reconnect the MSD to the GC 121 ...
Page 141: ...4 Maintaining the MSD To lubricate the side plate O ring 141 Side plate O ring ...
Page 159: ...4 Maintaining the MSD To remove a filament 159 Filament 2 Filament 1 ...
Page 161: ...4 Maintaining the MSD To reinstall a filament 161 Filament 2 Filament 1 ...
Page 210: ...210 ...
Page 214: ...214 ...
Page 232: ...232 7 Analyzer Analyzer heaters and radiators ...
Page 280: ...280 ...
Page 294: ...294 Index ...
Page 296: ...294 Chapter ...
Page 297: ...H Manual Part Number G1099 90027 Copyright 1998 Hewlett Packard Printed in USA 11 98 ...