4
Maintaining the MSD
101
Maintaining the vacuum system
The vacuum system requires some periodic maintenance
As listed earlier in Table 4, some maintenance tasks for the vacuum system
must be performed periodically. These include:
• Checking the foreline pump fluid (every week)
• Checking the calibration vial (every 6 months)
• Replacing the foreline pump oil (every 6 months; every 3 months for CI
MSDs using ammonia reagent gas)
• Checking the diffusion pump fluid (once a year)
Failure to perform these tasks as scheduled can result in decreased instru-
ment performance. It can also result in damage to your instrument.
Other procedures should be performed as needed
Tasks such as replacing a foreline vacuum gauge or triode gauge tube should
be performed only when needed. See Chapter 3,
Troubleshooting the MSD
,
on page 65 and see the online help in the MSD ChemStation software for
symptoms that indicate this type of maintenance is required.
More information is available
If you need more information about the locations or functions of vacuum
system components, refer to Chapter 5,
Vacuum System
, on page 183.
Most of the procedures in this chapter are illustrated with video clips in the
HP 5973 MSD Reference Collection CD-ROM.
Summary of Contents for 5973
Page 1: ...H Hardware Manual HP 5973 Mass Selective Detector ...
Page 3: ...HP 5973 Mass Selective Detector Hardware Manual ...
Page 25: ...1 Installing GC Columns To condition a capillary column 25 ...
Page 30: ...30 ...
Page 37: ...2 Operating the MSD To view MSD analyzer temperature and vacuum status 37 ...
Page 39: ...2 Operating the MSD To set monitors for MSD temperature and vacuum status 39 ...
Page 41: ...2 Operating the MSD To set the MSD analyzer temperatures 41 ...
Page 43: ...2 Operating the MSD To set the interface temperature from the ChemStation 43 ...
Page 51: ...2 Operating the MSD To remove the MSD covers 51 Upper cover Lower cover ...
Page 92: ...92 ...
Page 105: ...4 Maintaining the MSD To drain the foreline pump 105 Fill cap Drain plug Pump motor ...
Page 113: ...4 Maintaining the MSD To separate the MSD from the GC 113 ...
Page 121: ...4 Maintaining the MSD To reconnect the MSD to the GC 121 ...
Page 141: ...4 Maintaining the MSD To lubricate the side plate O ring 141 Side plate O ring ...
Page 159: ...4 Maintaining the MSD To remove a filament 159 Filament 2 Filament 1 ...
Page 161: ...4 Maintaining the MSD To reinstall a filament 161 Filament 2 Filament 1 ...
Page 210: ...210 ...
Page 214: ...214 ...
Page 232: ...232 7 Analyzer Analyzer heaters and radiators ...
Page 280: ...280 ...
Page 294: ...294 Index ...
Page 296: ...294 Chapter ...
Page 297: ...H Manual Part Number G1099 90027 Copyright 1998 Hewlett Packard Printed in USA 11 98 ...