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Configuration 

Calibration 

Thermo Fisher Scientific 

SOLA II User Guide    6-23 

3.

 

Enter the concentration of the low calibration standard. Note that if using 
only one calibration standard and no injections to calibrate the 
background, enter zero. See 

“Performing a Low Calibration at Zero”

 for 

more. 

 

Figure 6–51.  

4.

 

Set the number of readings the analyzer should average during calibration 
(1–60 readings). 

 

Figure 6–52.  

5.

 

Begin a calibration for the high concentration standard. See 

“Performing a 

High Calibration”

 for more. 

 

Figure 6–53.  

 

 

 

 

 

 

Содержание SOLA II

Страница 1: ...SOLA II Sulfur Online Analyzer User Guide P N 90 1307 0 Revision AB Part of Thermo Fisher Scientific...

Страница 2: ...SOLA II Sulfur Online Analyzer User Guide P N 90 1307 0 Revision AB...

Страница 3: ...rning is a registered trademark of Dow Corning Corporation All other trademarks are the property of Thermo Fisher Scientific Inc and its subsidiaries Thermo Fisher Scientific Thermo Fisher makes every...

Страница 4: ......

Страница 5: ...O 5625 F 08 2007 Revised per ECO 5921 G 10 2007 Revised per ECO 6018 H 03 2008 Revised per ECO 6230 J 04 2008 Revised per ECO 6320 K 06 2008 Revised per ECO 6419 M 04 2009 Revised per ECO 6903 N 05 20...

Страница 6: ......

Страница 7: ...6 Injection Valve 2 7 Specifications 2 8 Parts List 2 10 Spare Parts 2 15 Storage 2 21 Installation 3 1 Requirements 3 1 Sample Line Installation 3 2 Sample Tubing Preparation 3 2 Electrical Connecti...

Страница 8: ...ng a High Calibration 6 20 The Calibrate High Function 6 20 The Recalibrate High Function 6 20 Adjusting the Reading 6 21 Calibration Setup Menu Items 6 22 Density Compensation Setup 6 25 Viewing Alar...

Страница 9: ...n A 3 Pyrolyzer Settings A 3 Oven Settings A 11 The Lockout Menu A 18 Rotary Valve Service B 1 Initial Precautions B 1 Valve Disassembly B 2 Cleaning the Valve Body B 3 Cleaning the Rotor B 4 Rotor As...

Страница 10: ...idation History F 5 Stream Plot F 5 Detector Status F 6 Alarms Status F 6 Remote Controls F 7 Analyzer Status F 8 Configuration F 8 The X Purge System G 1 Description G 1 X Purge Specifications G 3 In...

Страница 11: ...allation J 4 Toxic Hazardous Substances Tables K 1 Connecting to a Sarasota FD910 Density Meter L 1 Purpose L 1 Connections L 1 Connecting One Density Meter to a Dual Stream System L 3 Related Technic...

Страница 12: ......

Страница 13: ...safely install operate and maintain the system described however personnel are still responsible for considering all actions and procedures for potential hazards or conditions that may not have been...

Страница 14: ...ytical systems which must be understood by all persons installing using or maintaining the analyzer system This information is designed to aid personnel in the safe installation operation and service...

Страница 15: ...els Appropriate precautions must be taken to prevent sparks present in the analyzer environment that may ignite combustible materials Precautions must also be taken to prevent electrical shock if the...

Страница 16: ......

Страница 17: ...transfers a small amount of sample approximately 1 0 L into an air carrier gas The air sample mixture passes through the mixing chamber to ensure complete mixing and then flows to the pyrolyzer The py...

Страница 18: ...such as H2S COS methyl mercaptan benzothiophenes dibenzothiophenes sulfides disulfides and thiols Consider the measurement of a sample of diesel gasoline or another common petroleum fraction such as n...

Страница 19: ...ure that only light from SO2 is measured Once the proper wavelength of light is selected its intensity is measure by a photomultiplier tube PMT The PMT converts light energy to electrical energy throu...

Страница 20: ...UV light onto a mirror assembly The mirror assembly contains four selective mirrors that reflect only the wavelengths that excite SO2 molecules As the excited SO2 molecules decay to lower energy state...

Страница 21: ...thing of measurement signal using moving average Measuring total sulfur with the PUVF detection method requires the conversion of all sulfur compounds in the sample to SO2 This is typically accomplish...

Страница 22: ...g consists of multiple small tubes encased in a large outer tube Air circulates through the outer tube with sample passing through the inner tube Moisture passes from the sample through the tubing whe...

Страница 23: ...asured quantities of the sample stream into a controlled carrier airflow An auxiliary airflow is added to this sample and air mixture The sample then passes to the mixing chamber where it vaporizes if...

Страница 24: ...T4 optional with back up purge system standard SOLA II IECEx G Ex pz IIC T Gc T3 and T4 with back up purge system Zone 1 G Ex px IIC T Gb X Purge system T3 and T4 with back up purge system Table 2 2 A...

Страница 25: ...ser interface 4 buttons with context sensitive functions Streams Dual streams optional with autostream select or DCS control of stream selection Alarms Standard I O board time out oven pyrolyzer tempe...

Страница 26: ...others application dependent Kalrez Viton The following table lists the SOLA II SOLA II Trace parts Note Unless otherwise specified the parts listed below are for the SOLA II and the SOLA II Trace un...

Страница 27: ...to mixer TE 8852 Filter detector HA 100153 Filter disposable PUVF inlet not used with Perm A Pure 47 1362 0 Filter inlet 2 micron used for sample and air inlet HA 101291 Filter Perm A Pure Dryer 25 1...

Страница 28: ...One year spare parts kit Valco valve gas phase applications 97 1590 0 One year spare parts kit Valco valve liquid phase applications TE 4811 O ring TE 4808 O ring between reaction chamber 63 1150 0 O...

Страница 29: ...Socket assembly PMT 97 1646 0 Quick repair kit 97 1644 0 N2 addition field installation 97 1651 0 Solenoid manifold adapter kit 31 0030 Solenoid 24 Vdc 5 port 4 way 2 position manifold mount 31 1367 0...

Страница 30: ...nylon 1 4 OD x 0 035 wall 40 0609 Tubing FEP 0 125 OD x 0 062 ID high temperature 40 0600 Tubing 1 8 OD x 0 085 ID 0 020 304SS 97 1591 1 Two year spare parts kit Dinfa valve liquid phase applications...

Страница 31: ...8 ID x 5 7 8 OD 1 8 width 1 Thermocouple pyrolyzer S type 4 Rotor liquid sample valve 1 0 l 4 port or 6 port 1 O ring kit for liquid injection valve actuator 1 Filter inline 2 micron 1 8 tube 1 Filter...

Страница 32: ...4 Ferrules for pyrolyzer tube fittings graphite 2 Pyrolyzer tube looped 2 Pyrolyzer O ring 5 5 8 ID x 5 7 8 OD 1 8 width 2 Rotor 10 port gas 97 1591 2 Two year spare parts kit Valco valve gas phase a...

Страница 33: ...1589 1 Startup spare parts kit Dinfa valve liquid phase applications Qty Includes 4 Ferrules for pyrolyzer tube fittings graphite 2 Pyrolyzer tube looped 2 Pyrolyzer O ring 5 5 8 ID x 5 7 8 OD 1 8 wid...

Страница 34: ...8 width 1 Filter inline 2 micron 1 8 tube connections 1 Thermocouple pyrolyzer S type 97 1591 1 Two year spare parts kit Dinfa valve liquid phase applications 1 Slider block 1 2 l 1 UV flash lamp 2 F...

Страница 35: ...ort 1 16 150 psi 175 C 1 Optical bench assembly 1 Trigger pak for SO2 bench 1 Pyrolyzer assembly 1 Board power supply for SO2 bench 1 Board flasher supply for SO2 bench 1 PCA SOLA II I O circuit PCBA...

Страница 36: ...ve replacement parts P N Description 89 2803 0 Solenoid relay PCB 29 1230 0 Heater for pyrolyzer assembly HA 101812 Ferrules for pyrolyzer tube fittings graphite 30 1025 0 Pyrolyzer tube looped 63 113...

Страница 37: ...Guide 2 21 P N Description TE 8666 PUVF flash lamp 89 2897 0 CPU 89 2898 0 I O PCB 85 1164 0 Power supply 24 Vdc DIN rail mount If storing the instrument the storage environment should be protected an...

Страница 38: ......

Страница 39: ...ications Mounting requirements The mounting site must be as close as possible to the sampling point The analyzer must be sheltered from extreme weather conditions Avoid mounting the analyzer in high v...

Страница 40: ...n on contact When using isopropyl alcohol avoid breathing the vapors and contact with the skin Appropriate measures must be taken to prevent ignition of the isopropyl alcohol vapors Use isopropyl alco...

Страница 41: ...wire copper or tin plated copper power wire rated for at least 600 Vac and 20 A at the required length Warning This apparatus must be earth grounded Warning Installation of this instrument requires an...

Страница 42: ...ers Chapter 6 Open Open Analyzer operation for streams is performed as specified in the Stream Setup parameters Chapter 6 Close Shorted to associated ground terminal Remote Measurement Range Control T...

Страница 43: ...concentration in the sample Full scale 20 mA DC represents the measured concentration specified in High Range or Low Range depending on range selected Analog Output 2 This 4 20 mA DC signal represent...

Страница 44: ...ponse time System gases meet quality and quantity pressure and flow specifications according to Chapter 2 PUVF vent is vented to atmospheric pressure PUVF vent is NOT connected to headers with varying...

Страница 45: ...b Ensure the power voltage and frequency matches the instrument requirements c Ensure a suitable circuit breaker and power switch is installed d Ensure the instrument is properly grounded e Inspect al...

Страница 46: ...ecified in the application notes shipped with the instrument or as recorded in the system logbook Note that the pyrolyzer and oven do not begin heating immediately due to the safety interlocks Note Th...

Страница 47: ...le when the instrument temperatures reach operating levels 8 Allow the analyzer system to stabilize Monitor the measured values on the front panel for consistent analysis readings to determine when th...

Страница 48: ...id manifold regulator to 0 psig Doing so blocks sample flow to the injection valve and purges sample from the injection valve 2 Observe reported sulfur value 3 Do not interrupt power instrument air ca...

Страница 49: ...ed in an ATEX hazardous area with a T4 rating do not open the oven door for 140 minutes Caution Failure to allow adequate cooling time before opening the oven can lead to equipment damage or injury to...

Страница 50: ......

Страница 51: ...er the passcode as seen in Figure 5 1 2 Press the button below Ent Enter and Figure 5 2 appears 3 To increase the first digit s value press the button below the up arrow Decrease the value by pressing...

Страница 52: ...sample flow to the analyzer 4 Apply power to the instrument 5 Analysis begins automatically when the pyrolyzer reaches operating temperature If you need to change the configuration press any button an...

Страница 53: ...ght The PUVF includes a system to monitor and compensate for decreases in the UV light output as the bulb ages However in the case of injection valve failure the PUVF system begins rapidly increasing...

Страница 54: ...Operation Injection Valve Failure Alarm 5 4 SOLA II User Guide Thermo Fisher Scientific Figure 5 4 Sample diverter valves Figure 5 5 Sample diverter valves functional diagram...

Страница 55: ...tream Setup Clock Setup Modbus Setup Dual Range Setup Inject Setup Autocal Setup Alarms Setup Calibration Setup and Density Compensation Setup Figure 6 1 Top level configuration menu 1 Access the subm...

Страница 56: ...re 6 4 4 The Average Time submenu allows you to set the averaging time The average time is a period 1 240 seconds during which the analyzer takes SO2 measurements used to determine a moving average of...

Страница 57: ...l it reaches the programmed average time Figure 6 6 6 The fast average time provides the ability to respond to changes faster without sacrificing stability achieved using a longer average time Note Bo...

Страница 58: ...2 The Stream Mode submenu allows you to configure the analyzer to continuously monitor stream 1 Stream 1 continuously monitor stream 2 Stream 2 or to alternate between the streams Timed Stream Figure...

Страница 59: ...o reduce the flow in order to conserve calibration validation standards You can program each stream for high or low flows If equipped with the second stream option the analyzer has NO and NC pneumatic...

Страница 60: ...e Thermo Fisher Scientific Figure 6 13 1 Access the Clock Setup menu to change the time and date Figure 6 14 2 Enter the time in hh mm ss 24 hour format and the date in the following screen in mm dd y...

Страница 61: ...COM 3 and COM 4 Figure 6 17 2 Select one of the baud rates available for RS485 Com 3 38400 19200 9600 4800 2400 and 1200 bps or select Disable Figure 6 18 3 Set the ID network address for Com 3 The a...

Страница 62: ...full scale value When the signal drops below 90 of the low range full scale value the system switches back to low range When Remote Range Select is enabled output scaling is controlled by a remote co...

Страница 63: ...on the 4 20 mA signal Figure 6 23 Set the 20 mA scaling for the high and low ranges for stream 2 using the submenus for stream 2 1 Enter the Inject Setup menu to set injection parameters Figure 6 24...

Страница 64: ...een 2 and 9999 seconds A 6 port valve injects at each actuator move in both positions Thus if a 6 port valve is used set the rate to twice the desired injection interval Figure 6 26 1 Enter this menu...

Страница 65: ...hen an automatic calibration is performed the analyzer calculates the percentage the new calibration factor deviates from the previous calibration factor If the percentage deviation is less than the a...

Страница 66: ...e manually initiated adjust reading function Setting both deviations to the same value disables the autocal making it a validation only function The autocal validation functions can be used with a pro...

Страница 67: ...Sample Flow alarm is available if the flow meter option is present The set point for the low sample flow alarm is a percentage of the 4 20 mA signal from the flow meter Figure 6 35 3 To set up a Cham...

Страница 68: ...ld activate The value can be from 0 to 1200 V Figure 6 37 5 Set up a Lamp Voltage Rate of Change alarm by entering the rate of change in lamp voltage at which the alarm should activate The value can b...

Страница 69: ...ect latching the alarm must be acknowledged before it will clear Figure 6 40 8 Set the High Alarm for stream 1 by entering the first level of high concentration for stream 1 at which the alarm should...

Страница 70: ...SOLA II calibration Figure 6 43 Prior to calibrating the instrument the sulfur concentration expected at the two points must be entered in the calibration setup menus Configuration Calibration Setup...

Страница 71: ...w cal value 0 00 ppm Low cal 555 600 kHz High cal value 100 00 ppm High cal 15000 000 kHz Figure 6 44 Typical SOLA II calibration The high and low calibration can be performed independently Changing e...

Страница 72: ...he Calibration Setup menu can be used to correct the calibration by moving the line without changing the slope see Figure 6 47 Enabling the Autocal function will cause the software to perform this cor...

Страница 73: ...low calibration value to zero 2 Exit the Calibration Setup menu 3 Reduce the pressure at the solenoid manifold air regulator to zero this is the bottom regulator located in the pneumatic cabinet Lower...

Страница 74: ...e concentration of the standard used 2 Step down to the Average Cal Readings screen It is recommended that you set this value to the maximum 240 3 Exit the Calibration Setup menu and go to Configurati...

Страница 75: ...through the injection valve 3 Let the reported concentration reach a new value and stabilize 4 Go to Configuration Calibration Setup Recalibrate High Press YES to accept the new high calibration At t...

Страница 76: ...structions on the various calibration functions are discussed in the previous sections Figure 6 48 Main menu heading 1 Select the engineering unit related to the concentration entered for the calibrat...

Страница 77: ...ne calibration standard and no injections to calibrate the background enter zero See Performing a Low Calibration at Zero for more Figure 6 51 4 Set the number of readings the analyzer should average...

Страница 78: ...standard See Performing a High Calibration for more You can do the same for the low concentration standard by accessing the Recalibrate Low menu item not shown See Performing a Low Calibration at Zer...

Страница 79: ...ter inputs the densities that correspond to 4 mA and 20 mA must be entered The analyzer maintains a moving average of the 4 20 mA readings and converts the readings to g cc using a linear interpolatio...

Страница 80: ...er Guide Thermo Fisher Scientific 1 Enter the Density Compensation Setup menu Figure 6 59 2 Select Live If you are using stream 2 be sure the menu item is for stream 2 Figure 6 60 3 Enter the density...

Страница 81: ...he densitometer used Figure 6 62 In the following screen Figure 6 63 enter the density that corresponds to the 20 mA output of the densitometer Figure 6 62 Figure 6 63 The following provides instructi...

Страница 82: ...ensation Setup 6 28 SOLA II User Guide Thermo Fisher Scientific 2 Enter the correction factor The value may be from 0 to 9 999 Figure 6 65 Note that when using a correction factor you do not need to e...

Страница 83: ...Chapter 7 Viewing Alarms The second top level menu is the View Ack Alarm menu Figure 7 1 Access this menu to review all active alarms Use the up and down arrows to scroll through the alarms individual...

Страница 84: ......

Страница 85: ...TX Pulse UV Control Figure 8 1 The Input Output Test menu consists of four groups of submenus Set Outputs Menu View Mux Analogs 4 20 mA Inputs and View Digital Inputs Figure 8 2 In the Set Outputs gr...

Страница 86: ...ream 1 to 4 8 12 16 or 20 mA Stream 2 4 20 mA Press Enter to change the 4 20 mA output for stream 2 to 4 8 12 16 or 20 mA Sample Solenoid Controls the sample diverter Stream 1 Solenoid Controls the va...

Страница 87: ...s menu Note that all signals are displayed as raw frequencies Figure 8 4 Following are the analogs in the order they appear within menu 1 ADC 0 Lamp V 2 ADC 1 Chamber Flow 3 ADC 7 Pressure 4 ADC 9 PMT...

Страница 88: ...he Watlow alarm input1 I O Board Displays the status of all eight inputs simultaneously Zero 0 denotes open One 1 denotes closed CPU Digital In Dip Switches Displays the positions of dip switches loca...

Страница 89: ...g are the menu items within the View Parameters menu Table 8 3 Menu Item Description At line sample Access this item to view the latest at line sample results Sample AVG The Average Concentration of t...

Страница 90: ...so displays the gain currently selected PMT Signal kHz The actual frequency proportional to the PMT output also displays the gain currently selected PMT Voltage The input voltage to the PMT Internal T...

Страница 91: ...Signal Gain Select the amplifier gain 1 2 5 10 20 50 100 Note The selection is only valid when auto gain is turned OFF Test Gains Place the gain selection under manual control to verify the functional...

Страница 92: ......

Страница 93: ...rom a source other than the regular process input The sample to be analyzed is introduced into the instrument in the same manner that a calibration standard is There are three parameters to configure...

Страница 94: ...omputed as a percentage of the computed average If it is less than or equal to the programmed value the analyzer reports a successful sample If it is greater than the programmed value an error is repo...

Страница 95: ...st strap is not available be sure to touch a grounded metal object before touching any internal components Handle all printed circuit boards by the edges Carefully observe the instructions in each pro...

Страница 96: ...pressure compressed air Use a soft paintbrush or cloth to remove stubborn dirt Use the following leak test procedure to verify that there are no system leaks 1 Set the sample and air regulators for ze...

Страница 97: ...ument logbook 10 Allow the analyzer to warm up until it stabilizes Figure 10 1 Three way valve for measuring flow rates 1 Obtain a precision flow measurement instrument such as a bubble meter 2 Ensure...

Страница 98: ...2 port and adjust the CLEAN AIR 2 regulator to obtain the required flow 10 Turn the MEAS CLEAN AIR 2 3 way valves to point up for normal operation 11 Restart the analyzer according to Chapter 5 For d...

Страница 99: ...event burns The pyrolyzer heater is enclosed in the pyrolyzer housing which is shown in the figure below Figure 10 2 Pyrolyzer housing The following table lists the part numbers for the parts referenc...

Страница 100: ...t down the analyzer system Allow the system to cool completely 2 Carefully remove the two sample tubes from the top of the pyrolyzer housing using a backup wrench to keep the stainless steel fittings...

Страница 101: ...ion will be attached to the lid Figure 10 4 Carefully lift all of it out to avoid damaging the pyrolyzer tube Figure 10 4 Housing lid with insulation and pyrolyzer tube attached 9 As shown in Figure 1...

Страница 102: ...nd the heater wires and remove the wire sleeves Set the sleeves and fittings aside 11 Loosen the thermocouple fitting and remove the thermocouple from the housing Set it aside for re installation late...

Страница 103: ...er Scientific SOLA II User Guide 10 9 Figure 10 7 Insert replacement heater into housing Figure 10 8 Heater wires fed through fittings 14 Slide the wire sleeves onto the heater wires Tighten the stain...

Страница 104: ...the hole Remove the bit and then carefully feed the thermocouple tube through the stainless steel fitting on the housing Figure 10 10 Tighten the thermocouple fitting to secure it to the housing Figur...

Страница 105: ...11 around it Figure 10 13 Figure 10 13 Pyrolyzer housing O ring 19 Gently slide the lid into the housing Note The pyrolyzer tube insulation and Kaowool insulation should still be attached to the lid S...

Страница 106: ...ng to the oven enclosure using the screws removed earlier two mounting screws on top of housing two on bottom 23 If necessary reconnect the wires from the oven temperature switches 24 Reconnect the he...

Страница 107: ...n will be attached to the lid Figure 10 15 Carefully lift all of it out of the housing Figure 10 15 Housing lid with insulation and pyrolyzer tube attached 3 To remove the existing pyrolyzer tube unsc...

Страница 108: ...0 17 Apply the Kaowool insulation 6 Holding the insulation and pyrolyzer tube gently attach the housing lid against the insulation allowing both ends of the tube to come out of the lid approximately 1...

Страница 109: ...zer Heater to re install the housing and complete this procedure Coking carbon buildup can occur in the pyrolyzer reaction tube when sample or calibration flow is too high or when there is no airflow...

Страница 110: ...the troubleshooting guidelines presented in Table 10 4 may be helpful in isolating the fault Additional information can be obtained from the following sources System drawings Application notes for the...

Страница 111: ...2 Sample diverter valve may be inhibiting sample flow Remove the analyzer from suspend mode correct any alarm conditions and or ensure solenoid air manifold is set at 60 psig ALARM displayed Sample Fl...

Страница 112: ...e flasher lamp trigger pak or lamp intensity control electronics Replace valve rotor In extreme cases replace entire valve head Check filtration system to ensure particulate is not getting to the inje...

Страница 113: ...locations 12320 Cardinal Meadow Drive Sugar Land TX 77478 USA 1 800 437 7979 Unit 702 715 7 F Tower West Yonghe Plaza No 28 Andingmen East Street Beijing 100007 CHINA 86 10 8419 3588 86 10 8419 3580 f...

Страница 114: ...ment shall be Buyer s exclusive remedy against Thermo Fisher Thermo Fisher shall not be liable for labor charges or other losses or damages of any kind or description including but not limited to inci...

Страница 115: ...ange This appendix provides basic operating instructions and default configuration settings For complete operating information and troubleshooting refer to the EZ ZONE PM PID Controller user s manual...

Страница 116: ...sius The percent LED lights when values are displayed as a percentage or when the open loop set point is displayed This LED indicates the status of a profile When lit a profile is running When flashin...

Страница 117: ...prior to operation Operations page Used to monitor or change runtime settings Factory Page Used to enable password protection create a custom Home Page and perform other tasks that do not have an effe...

Страница 118: ...ne Aggressiveness Critical Critical damped aggressiveness of autotuning calculations User Failure Action User When user switches to manual mode controller sets output power to last open loop set point...

Страница 119: ...wer output will never be greater than the value specified and will represent the value at which output scaling stops Table A 5 Pyrolyzer settings Setup Page Output 2 Parameter Default Comment Display...

Страница 120: ...ftware Active Level High Action Function User Set Restore Function Instance 1 Table A 8 Pyrolyzer settings Setup Page Global1 Parameter Default Comment Display Software Display Software Display Units...

Страница 121: ...y Software Analog Input Value The process value C Input Error The cause of the most recent error Possible displays listed below None Open Fail Shorted Measurement Error Bad Calibration Data Ambient Er...

Страница 122: ...ontrol Loop 1 Parameter Default Comment Display Software Display Software Control Mode Auto The loop will use automatic control Autotune Set Point 90 The percentage of the current set point that will...

Страница 123: ...1 Parameter Default Comment Display Software Display Software Alarm Low Set Point 5 C The set point that will trigger a low alarm Alarm High Set Point 5 C The set point that will trigger a high alarm...

Страница 124: ...rameter that will appear in the custom Home Page Instance ID 1 Table A 16 Pyrolyzer settings Lock Page Lock 1 Parameter Default Comment Display Software Display Software Operations Page 2 The security...

Страница 125: ...D 100 Ohm TC Linearization S For Type S thermocouple RTD Leads 2 The number of leads on the RTD wired to this input Units Process The type of units measured by the sensor Scale Low 0 00 The low scale...

Страница 126: ...elay 0 0 User Failure Action User When user switches to manual mode controller sets output power to last open loop set point entered by user Input Error Failure Off When an input error switches contro...

Страница 127: ...than the value specified and will represent the value at which output scaling begins Output High Power Scale 70 The power output will never be greater than the value specified and will represent the v...

Страница 128: ...play Software Display Software Active Level High Action Function User Set Restore Function Instance 1 Table A 23 Oven settings Setup Page Global 1 Parameter Default Comment Display Software Display So...

Страница 129: ...il Shorted Measurement Error Bad Calibration Data Ambient Error RTD Error Not Sourced Calibration Offset The offset applied to the input reading to compensate factors that cause the input reading to v...

Страница 130: ...the controller will automatically control to Idle Set Point 25 0 C The closed loop set point that can be triggered by an event state Heat Proportional Band 14 0 C The PID proportional band for the he...

Страница 131: ...The parameter that will appear in the custom Home Page Instance ID 1 Table A 29 Oven settings Factory Page Custom Setup 2 Parameter Default Comment Display Software Display Software Parameter Active S...

Страница 132: ...ance Locked Access Level 1 Display Software Display Software Rolling Password Off User Password 63 Administrator Password 156 Each menu in the Factory page and each page except the Factory page has a...

Страница 133: ...UW Type valves After unpacking the valve do not remove the protective tape from the valve ports until you are ready to install the valve As supplied all surfaces are clean and free of contaminants and...

Страница 134: ...ot disassemble the valve unless the system malfunction is definitely isolated to the valve perform all other system checks first If disassembly is required make certain that the following instructions...

Страница 135: ...the rotor from the valve body with the magnet Once the rotor is removed note the orientation of the rotor tab which is marked with an ID letter denoting the type of seal material Follow these instruct...

Страница 136: ...s shown in Figure B 4 2 Insert the rotor into the valve body being careful that the tab does not touch the polished interior of the valve body Make sure the rotor tab Figure B 4 is fully inserted into...

Страница 137: ...rotor is replaced If a high temperature valve WT or UWT series is used at less than 300 C it may become sticky or difficult to turn This tendency can usually be eliminated by repeating the conditioni...

Страница 138: ...ure O ring kit VICI P N ORT 1 Apply air pressure to the actuator inlet nearest the valve Then use the open end wrench to remove the air supply lines from the actuator Figure B 5 2 Remove the valve and...

Страница 139: ...nd the rest of the assembly together pull the female end cap all the way off If the bearing and washers fall out set them aside 6 Repeat the procedure with the actuator inverted so that the cylinder s...

Страница 140: ...O rings to be replaced are in the two end caps and the O ring plate The internal end cap O rings are easier to access if the washers and bearing are removed Follow the steps below 1 Use a small screw...

Страница 141: ...ft into the O ring plate as far as it will go as shown in Figure B 10 3 Place the washers and bearing in the male end cap thin washers in first as shown Figure B 9 One of the flats on the drive shaft...

Страница 142: ...ived Follow the instructions below 1 Switch the actuator from one position to the other several times to make sure that the play in the coupling mechanism has been absorbed 2 Visually inspect the valv...

Страница 143: ...to go through the three small O rings Pressing the plate in dislodges the O rings do not press the plate in 6 The two bearing plates are identical except that one has three countersunk holes to accept...

Страница 144: ...Rotary Valve Service Rebuild the Assembly B 12 SOLA II User Guide Thermo Fisher Scientific Figure B 12 Exploded view of two position actuator...

Страница 145: ...Thermo Fisher Scientific SOLA II User Guide C 1 Appendix C Dinfa Valve Service Figure C 1 Dinfa valve mounting parts locator Figure C 2 Position of heat transfer tube in oven Overview...

Страница 146: ...o Fisher Scientific Figure C 3 Dinfa 8 port liquid injection valve sample load position Note To set up two injections minute set the injection cycle to 30 sections and the injection time to 15 seconds...

Страница 147: ...alling the insulation in a continuous run starting with the clean air tubing Secure the insulation with a hose clamp 2 Adjust the clean air 2 regulator to 190 cc min approximately 90 psig with the ove...

Страница 148: ...Dinfa Valve Service Overview C 4 SOLA II User Guide Thermo Fisher Scientific Figure C 6 Dinfa 8 port liquid injection valve Figure C 7 Close up of slider...

Страница 149: ...nal ensure the injection cycle is set for 30 seconds and injection is set for 15 seconds If the analyzer response time is slower with the Dinfa valve The heat transfer tube is not insulated properly o...

Страница 150: ......

Страница 151: ...n the SOLA II standard serial Modbus and a TCP IP Modbus network using 10 Base T TCP IP Bridge board installed inside the SOLA II enclosure SOLA II Modbus configuration must be set to 38400 baud with...

Страница 152: ...twork and assign an IP address 1 Locate the IPSetup exe utility that is included with the disk that ships with the TCP IP Bridge option 2 Run the IPSetup exe utility from any IBM compatible PC connect...

Страница 153: ...p utility successfully you can access instrument control via the browser interface Open your browser and enter http followed by the IP address into the address line of the browser For example if the I...

Страница 154: ...le Format to exit this screen Figure D 5 Accessing this display allows you to view activity for the last 24 hours in a table format You can also save the data and import it into a Microsoft Excel spre...

Страница 155: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 5 Figure D 6 Analyzer setup Figure D 7 Stream setup Figure D 8 Modbus setup...

Страница 156: ...TCP IP Bridge The Browser Interface D 6 SOLA II User Guide Thermo Fisher Scientific Figure D 9 Dual range setup Figure D 10 Inject setup Figure D 11 Autocal setup...

Страница 157: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 7 Figure D 12 Alarm setup Figure D 13 Calibration setup Figure D 14 Density compensation setup...

Страница 158: ...orm with additional fields in order to identify the sample With this version you can also print results on any local printer attached to the PC that is running the web browser Figure D 15 At line grab...

Страница 159: ...TCP IP Bridge The Browser Interface Thermo Fisher Scientific SOLA II User Guide D 9 Figure D 17 Sample results...

Страница 160: ......

Страница 161: ...ead Input Registers 05 Set Single Coil 06 Set Single Holding Register 15 Set Multiple Coils 16 Set Multiple Holding Registers Table E 2 Coil Number Description 1 Enable Modbus Remotes1 2 Stream Select...

Страница 162: ...Reserved 28 Reserved 29 Reserved 30 Reserved 31 Reserved 32 Reserved 33 Reserved 34 Reserved 35 Reserved 36 Reserved 37 Reserved 38 Reserved 39 Reserved 40 Reserved 1 If this coil is set to 1 by the...

Страница 163: ...Autocal Error 10008 Purge Fault 10009 Stream Selected 0 Stream 1 1 Stream 2 10010 Valve Fault 10011 Purging 10012 Calibrating 10013 Suspended 10014 Autocal Performed Clear after read 10015 New Cal Fac...

Страница 164: ...30007 Reserved 30008 Reserved 30009 Normalized Detector reading kHz 30010 Detector Lamp Voltage 30011 Detector PMT Voltage 30012 Detector Chamber Temperature deg C 10 30013 Detector Lamp Intensity Hz...

Страница 165: ...0 Reserved Table E 5 Holding Register Number Description 40001 High Cal Frequency kHz 40002 Low Cal Frequency kHz 40003 Stream 1 Recorder Full Scale 40004 Stream 2 Recorder Full Scale 40005 Injection...

Страница 166: ...Set Point 40024 Density 4 mA g cc 1000 40025 Density 20 mA g cc 1000 40026 Stream 1 Recorder Low Scale 40027 Stream 2 recorder Low Scale 40028 Stream 1 Density Correction Factor 1000 40029 Stream 2 De...

Страница 167: ...Description 40045 Passcode 40046 Fast Average seconds 40047 Average Override 40048 Grab Sample Average Time 40049 Grab Sample ID 40050 Grab Sample Accepted RSD 40051 Transmix Factor Not Used 40052 St...

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Страница 169: ...oppy disk to the c Program Files NationalInstruments Lookout subdirectory on the computer hard drive Remove the disk from the drive and store in a safe place 2 Click on sIIcfg l4p or sIIdl l4p to open...

Страница 170: ...ftware F 2 SOLA II User Guide Thermo Fisher Scientific b Select Object Modify Modbus1 Figure F 1 c Edit the Modbus object to select a different COM port or Modbus Ethernet Figure F 2 Figure F 1 Figure...

Страница 171: ...obtain the correct IP address b Set the identifier to 1 If a serial port is used for the connection configure the serial port parameters as follows a Select Lookout Options Serial Ports b Verify that...

Страница 172: ...by other programs using ODBC or SQL see the Lookout software manual provided with the system or instructions in the software you are using for more information Data from the analyzer is also saved on...

Страница 173: ...he screen A trend plot of the densitometer inputs can be displayed by clicking the Trend g cc button Zero and full scale values for the plot are determined by the 4 mA and 20 mA density settings in th...

Страница 174: ...reen and returns the plot to real time data display The total time period displayed on the plot can be varied from 5 minutes to 24 hours by moving the slider below the plot area The hypercursor in the...

Страница 175: ...controls screen 1 Remote Cal When turned ON this control causes the analyzer to perform a calibration and update the calibration factor The Allowed Deviation and Recal Deviation values are ignored 2 C...

Страница 176: ...the main screen display the status of the analyzer by placing a green indicator to the right of Calibrating Purging or Suspended If the indicators are not green the system is running a sample analysi...

Страница 177: ...10 psig a time delay relay begins its timed cycle Typically the time delay is used to ensure that at least four volumes of air are exchanged in the enclosures before power is applied to the system The...

Страница 178: ...the oven door Instruments with a T4 rating must be allowed to cool for at least 140 minutes before opening the oven door Caution Failure to allow adequate cooling before opening the oven can lead to i...

Страница 179: ...lay time delay typically set from 480 to 600 seconds see application notes for individual system X Purge pressure Minimum 10 psig Y Purge pressure analyzer purge Set to approximately 10 psig or as spe...

Страница 180: ...r to drawings provided with the system for connection information and power requirements Customers must provide a suitable power switch near the system for use by maintenance personnel Warning Electri...

Страница 181: ...g up any analyzer system that uses the X Purge system Caution Do not open the explosion proof X Purge enclosure in a hazardous area even when de energized unless area has been properly tested and is k...

Страница 182: ...r pressure regulators set too low c Oven door open or leaking air d Electronic enclosure door open or leaking air 7 Complete the remaining steps listed in the startup procedure included in the startup...

Страница 183: ...upon interruption of main analyzer power you may elect to implement one of the following Install the appropriate Intrinsically Safe IS barriers on Modbus and or discrete signals Utilize the X Purge s...

Страница 184: ...wer than the initial setting when received from Thermo Fisher Caution If the timer setting is too short the analyzer system is not purged adequately before power is applied This can result in equipmen...

Страница 185: ...Thermo Fisher Scientific SOLA II User Guide H 1 Appendix H Software Menu Tree Figure H 1 Top level menus configuration subgroups...

Страница 186: ...Software Menu Tree H 2 SOLA II User Guide Thermo Fisher Scientific Figure H 2 Diagnostics subgroups...

Страница 187: ...Thermo Fisher Scientific SOLA II User Guide I 1 Appendix I PUVF Optical Bench Figure I 1 Optical bench assembly exploded diagram...

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Страница 189: ...ctronics can process The voltage applied to the PMT is a negative DC voltage and the lower the PMT voltage the greater the sensitivity of the detector Looking at previous applications as examples a SO...

Страница 190: ...med purge time Note that the analyzer will not update readings during this period The Dual PMT Supply option requires a different version of the SOLA II software installed in the unit to operate prope...

Страница 191: ...on will provide two 4 20 mA signals one for each range If it is desired to monitor only one 4 20 mA signal then Auto Range can be selected A contact output indicates which calibration is used by the a...

Страница 192: ...ine Grab Sample function either calibration can be selected to measure the sample If the sample concentration range is unknown the sample can be measured first on the highest calibration range and dep...

Страница 193: ...o o o o o Furnace o o o o o o AC DC Distribution x o o o o o Main Power Supply x o o o o o Cabling x o o o o o Indicates that this toxic or hazardous substance contained in all of the homogeneous mat...

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Страница 195: ...eter are connected to the return of the SOLA II supply loop It is acceptable to run three wires between the devices and jumper terminals 2 and 4 together at the density meter and connect either termin...

Страница 196: ...three wire terminal block four in total If the jumper is installed the 24VDC current loop power is supplied by the SOLA II If the jumper is left open power is not supplied by the SOLA II For the Sara...

Страница 197: ...3 Figure L 5 shows the configuration for using one Sarasota FD910 density meter on a dual stream system Note The jumper for loop power is NOT installed for stream 2 J9 Figure L 5 Sarasota FD910 densit...

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Страница 199: ...ct name SOLA II as the search term and click the Resources tab Table M 1 Technical bulletins TB Title TB 0417 001 Replacing a Watlow Series 93 Temperature Controller with a Watlow EZ ZONE PM6 Series C...

Страница 200: ...Thermo Fisher Scientific SOLA II User Guide M 2 THIS PAGE INTENTIONALLY BLANK...

Страница 201: ...ith the SOLA II Trace refer to the next paragraph Combustion gas for the SOLA II Trace Results reported from the field as well as measurements conducted in the factory indicate that when the sample ma...

Страница 202: ...he performance specifications are not altered that is the repeatability will not be guaranteed to be lower than 1 of 2ppm similarly the limit of detection also remains 1 25 of 2ppm 25ppb The highest r...

Страница 203: ...ale 62 5 2 of range example range 200ppm repeatability 4ppm 1 of range example range 200ppm repeatability 2ppm Thermo Fisher Scientific SOLA II User Guide O 1 SOLA 11 for Condensable Vapours CV The SO...

Страница 204: ...a certifications Since the SOLA II CV is modified from the standard SOLA II analyser the hazardous area approvals may vary please consult the factory for the latest approvals for installation in hazar...

Страница 205: ...Thermo Fisher Scientific 81 Wyman Street P O Box 9046 Waltham Massachusetts 02454 9046 United States www thermofisher com...

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