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HPLC · SMB · Osmometry

KNAUER

Wissenschaftliche Geräte GmbH

Hegauer Weg 38

14163 Berlin, Germany

Phone: +49 30 809727-0

Telefax: +49 30 8015010

E-Mail: [email protected]

Internet: www.knauer.net

www.knauer.net

KNAUER Wissenschaftliche Geräte GmbH

The information in this document is subject to

change without prior notice. Translation of the

original German edition of this manual, version 1.2

2015-05-13

Printed in Germany on environmentally friendly

paper from sustainable forests.

See up-to-date manuals online:

www.knauer.net/downloads

AZURA are registered trademarks of

KNAUER Wissenschaftliche Geräte GmbH

Содержание Azura P 6.1L

Страница 1: ...HPLC Pump P 6 1L User Manual V6890...

Страница 2: ...nstallation 15 Transport 15 Operating Environment 16 Setup 16 Unpacking 17 Capillary and Fittings 17 Connecting the Solvent Bottles 17 Pre Installed Capillary 18 Integrating the Pump into an HPLC Flow...

Страница 3: ...ply 34 Operation 35 Initial Start Up 35 Pump Head 35 De Aerating the Pump 35 Switch On 36 Control 37 Control with Chromatography Software 37 Control with Control Unit 37 Control with Mobile Control 37...

Страница 4: ...aximum Pressure 58 P 6 1L General 58 Repeat Orders 60 Modules 60 Accessories and Spare Parts 60 Disposal 72 Legal Information 73 Warranty Conditions 73 Transport Damage 73 HPLC Glossary 74 Index 76 To...

Страница 5: ...y analysis Chemical analysis Food analysis Pharmaceutical analysis Environmental analysis Device Variants The P 6 1L is available in three different options Isocratic pump Binary pump HPG pump Quatern...

Страница 6: ...ted inline fil ter a venting screw and a mixer are also part of the pump Rear View On the back of pump the connectors for LAN and power chord are located as well as the serial number of the device an...

Страница 7: ...onstant pressure The flow and pressure which liquids can be conveyed with depend on the pump head Pump Heads Pump heads for several areas of application are available for the pump P 6 1L Legend 1 Seri...

Страница 8: ...Mode This mode protects the column from excessive fluctuations in pressure If the maximum pressure is reached the user can decide if the pump should be switched off or continue running with constant...

Страница 9: ...r the specified temperature range 2 not recommended in combination with PEEK small parts and PEEK capillary Less suitable solvents Diethylamine 0 1 DEA Dilute phosphoric acid Dimethyl sulfoxide DMSO M...

Страница 10: ...wledge regarding substances that are suitable only to a limited extent for use in liquid chromatography Knowledge regarding the health risks of chemicals Participation during an installation of a devi...

Страница 11: ...companies for laboratory work Filtration of substances under analysis Use of inline filters Once they have been used never re use capillaries in other areas of the HPLC system Only use a given PEEK f...

Страница 12: ...fectious or radioactive substances poses a hazard for all persons during operation repair sale and disposal of a device power cable Defective power cables are not to be used to connect the device and...

Страница 13: ...posed of properly Symbols and Signs The following symbols and signs can be found on the device in the chromatography software or in the user manual Symbol Meaning Warning signs High voltage hazard Ele...

Страница 14: ...m our website Device data For a secure transport note the weight and dimensions of the pump see Technical Data CAUTION Damage to the device by lifting on protruding housing parts Lift the device on th...

Страница 15: ...The requirements and a description can be found in the following section Sunlight Protect the device against direct exposure to sun light AC system Set up the device at a location not exposed to air d...

Страница 16: ...ttles tubing with pre installed solvent filters is used The tubing is connected to the device with flange less fittings Note Do not use tools so as to not damage the fittings Procedure Process 1 Set u...

Страница 17: ...the HPLC system with capil lary Procedure Process Figure 1 Slide the flangeless fit ting 1 over the tub ing 2 Slide the lock ring 2 over the tubing cap with the sealing ring 3 Note the direction of th...

Страница 18: ...tallation plan for capillary and tubing on the isocratic version of the pump If you own a different version of the pump see the corresponding chapter for installation instructions The gray lines repre...

Страница 19: ...sponding chapter for installation instruc tions The gray lines represent the connection of the solvents to the pump and the black lines represent the connection of the piston backflushing Piston backf...

Страница 20: ...d prior to use Next steps Integrate the pump into the HPLC flow system Connecting the Solvent Selection Valve to the Solvent Note The Solvent Selection valve is readily connected to the 2 chan nel deg...

Страница 21: ...tion is re used Since the flow path is circular only one bottle is used for the flushing solution Connecting the Degasser The degasser outlet is readily connected to the valve block Flow path solvent...

Страница 22: ...e Sol vent The 4 channel degasser contains four degassing chambers Each degassing chamber has an inlet and an outlet on the front of the pump Prerequisite The device has been switched off The power pl...

Страница 23: ...lushing removes salts and other substances from the area behind the pump head seals To do this connect a bottle with flushing solution to the flush pump and the piston backflushing The silicone tubing...

Страница 24: ...he front cover has been removed Procedure Process Figure 1 Plug one silicone tube onto the inlet 3 of the flush pump and con nect to the flushing solution bottle 2 Plug a second silicone tube onto a v...

Страница 25: ...d via the Control Unit The Con trol Unit connector is located on the side of the device 3 Connect the nozzle and the funnel 4 Push the other end of the hose onto the noz zle 5 of the leak tray Abb 22...

Страница 26: ...Switch on the device and run the chromatography software Configuring the LAN Settings The LAN uses only one server which is normally the router from that the devices automatically receive their IP ad...

Страница 27: ...rnet In contrast the LAN ports serve to set up a network from devices and a computer To avoid interference we recommend operating the HPLC system separately from the company network You will find patc...

Страница 28: ...ck that the IP address range of the router and of the com pany network do not overlap 2 In case of an overlap change the IP address range of the router 3 Use the patch cable to connect the router WAN...

Страница 29: ...Signal Explanation Analog GND Reference point of the voltage at the signal inputs Analog out Voltage range 0 5 V scalable Analog in Voltage range 0 10 V 10 V according to maximum flow rate Start GND...

Страница 30: ...st 10 mA After receiving a signal short circuit to ground from an external device an error message appears and the device stops Error GND Reference point of the voltage at the signal inputs 24V Event...

Страница 31: ...Pulse 5 V for at least 1000 ms 3OC TTL output Levels passive 0 V active 5 V Pulse 5 V for at least 1000 ms GND Reference point of the voltage at the signal inputs 4TTL TTL compatible output Levels pas...

Страница 32: ...CAUTION Electrostatic discharge can destroy the electronics Wear a protective bracelet against electrostatic discharge and ground Relay contact The contact is on a floating basis Its setting depends o...

Страница 33: ...ripple residual current voltage peaks and electromagnetic interference The connectors for the mains voltage are grounded accord ingly The device receives sufficient power with reserve capacity The de...

Страница 34: ...tion to the router is established The chromatography software has been installed by KNAUER or a company authorized by KNAUER The capillary has been connected Pump Head To bring a newly installed pump...

Страница 35: ...p suction and close the venting screw Result After de areating excess air is removed from the pump head and the capillary Switch On Note Prior to switching on the pump you should de aerate it to remov...

Страница 36: ...edition version A 04 05 or higher or with ClarityChrom version 5 0 2 or higher You find a detailed description on chromatography soft ware in a corresponding user manual Control with Control Unit To...

Страница 37: ...confirmation of flawless condition at delivery check if the delivery is complete certification on the functionality of the device Operation Qualification OQ The Operation Qualification includes an ex...

Страница 38: ...eck after each step if the problem is solved If the problem cannot be located call the Technical Support Average Useful Life OQ Test 1 to 5 days week Every 6 months More than 5 days week or 24 hours d...

Страница 39: ...e devices and the com puter Has this been successful 7 Replace the patch cable to the device with that no connec tion could be established Has this been successful 8 Make sure that the IP port of the...

Страница 40: ...t Pump head leaks Inspect the inlet and outlet screw fit tings of the pump head If the pump head seals are defective solvent enters the piston backflush ing inform the Technical Support Exchange the p...

Страница 41: ...act the Technical Support Component settings not compatible with gradient setup Change the Setup settings or change the gradient in the pro gram or in Setup E Error input activated Eliminate the short...

Страница 42: ...stem Minimum pressure Sys tem stopped Increase the pressure or adjust the lower pressure limit Restart the system Motor failure max current Restart the device If this system message occurs repeatedly...

Страница 43: ...number Create and edit a program Program is running Quit program or wait until pro gram has been completed Pump head type head data uninitialized Restart the device Check whether a pump head with RFI...

Страница 44: ...omatography software This program is used in WAKEUP First quit or delete wakeup pro gram wu Wake Up then edit or delete data by means of the chromatography software Too many lines in program Check the...

Страница 45: ...CAUTION Device damage because of leaks If leaks occur after maintenance and assembly replace the capillary connections with new ones Users may perform the following maintenance tasks themselves Repla...

Страница 46: ...of the device can be cleaned with a mild commercially available cleaning solution or with isopropanol Checking the Fittings Check if all fittings are tight If fittings are not tight re tighten fitting...

Страница 47: ...terial Flushing solution silicone tube Next steps Bring the pump into operation again Putting the Pump Out of Operation The pump is designed for use with different solvents If the pump is out of opera...

Страница 48: ...ions remove the pump head and pack the device for transport or storage Preparing the Pump Head for Storage Prerequisites The power plug has been pulled Auxiliary material Syringe Flushing solution CAU...

Страница 49: ...head is stored and re used later flush it and fill it with isopropanol Afterwards seal the inlets and outlets with cap fittings CAUTION Damage to the pistons if they tilt Undo or tighten diagonally op...

Страница 50: ...Check Valve The pump head is equipped with two check valves Prerequisite The pump head has been purged The capillary and tubing have been removed The pump head has been removed Tools Open end wrench...

Страница 51: ...The check valves have dried CAUTION Damage to components caused by overtightened fittings Note the torque of the fittings For stainless steel fittings 5 Nm For PEEK fittings maximum 1 Nm or finger ti...

Страница 52: ...ing the Inline Filter Below the pressure sensor you find the fitting of the inline filter Prerequisite The pump has been rinsed Tools Open end wrench size 1 4 Open end wrench size 13 Procedure Process...

Страница 53: ...nless steel fittings 5 Nm For PEEK fittings 1 Nm Next steps Reinstall the capillary at the pressure sensor below the fitting of the inline filter 3 Loosen the fitting of the inline filter 1 with the o...

Страница 54: ...rench size 1 4 Allen wrench 2 mm and 2 5 mm Torque wrench CAUTION Damage to components caused by overtightened fittings Note the torque of the fittings For stainless steel fittings 5 Nm For PEEK fitti...

Страница 55: ...ol Unit Mobile Control or the standby button only in standalone mode Setup Pump type Isocratic analytical HPLC pump Variants of the pump head 5 ml min stainless steel 10 ml min stainless steel 50 ml m...

Страница 56: ...alytical HPLC pump with degasser Variants of the pump head 5 ml min stainless steel 10 ml min stainless steel 10 ml min ceramic Degasser 4 channels Teflon AF Special feature Automatic adaption of LPG...

Страница 57: ...200 bar 2900 psi Solvent conveyance Variants Isocratic HPLC pump Quaternary low pressure gradient pump Binary high pressure gradient pump Conveyance Double piston pump Pulsation com pensation Active p...

Страница 58: ...ption of hydro chloric acid and halogenated hydrocar bons in particular hexafluoroisopropanol HFIP Wetted materials PEEK Tefzel Teflon AF Vacuum chamber Polypropylene and stainless steel Vacuum pump L...

Страница 59: ...number Pump P 6 1L isocratic with 10 ml stain less steel pump head APH30EA Pump P 6 1L isocratic with 10 ml ceramic pump head APH60EB Pump P 6 1L isocratic with 50 ml stain less steel pump head APH30...

Страница 60: ...ead ruby sapphire G0924C Inline filter Inline filter cartridge 10 50 ml vol 60 l G1451 Inline filter cartridge 10 50 ml vol 20 l G1451A Inline filter cartridge 10 ml vol 60 l bio G1452 Inline filter c...

Страница 61: ...ld devices manufactured by KNAUER back to the dis tributor the importer or the company free of charge but would be charged for the disposal Accessories kit P 6 1L binary FPH35 Tool AZURA tool kit A103...

Страница 62: ...by the manu facturer free of charge This warranty excludes the following accidental or willful damage damage or errors caused by third parties that are not contrac tually related to the manufacturer a...

Страница 63: ...t Hand held device with a touchscreen to drive single AZURA devices locally Dead vol ume Volume of capillary and system components between mixer injector and column as well as between column and detec...

Страница 64: ...ycles by a valve block which is connected upstream The gradient is generated before the pump Mixer Component for the homogeneous mixing of solvents for the generation of a gradient Mobile Control Mobi...

Страница 65: ...s Machinery Machinery Directive 2006 42 EC EMC EMC Directive 2004 108 EC IEC 61000 3 2 2012 IEC 61326 1 2011 Disposal RoHS Directive 2011 65 EU WEEE Directive 2012 19 EU Safety Low Voltage Directive 2...

Страница 66: ...74 Contact data 46 Control 26 37 chromatography software 37 Control Unit 26 37 Mobile Control 37 Control Unit 8 9 26 37 47 74 D Dead volume 74 decontamination 13 Degasser 11 22 74 Degasser module tech...

Страница 67: ...fiers 9 O OpenLAB 9 37 47 Operating hours 47 OQ 38 P Packing list 17 PEEK 10 Acetonitrile 18 pH 75 Pin header 30 wire 33 Piston backflushing 9 11 51 flushing solution 11 Piston backflusing connect 24...

Страница 68: ...less steel 9 Storage pump head 49 Switch on 36 System Messages 41 T Technical data binary pump 56 degasser module 59 delay volume 56 57 flow rate 58 general 58 gradient formation 56 57 isocratic pump...

Страница 69: ...r te GmbH All rights reserved The information in this document is subject to change without prior notice Translation of the original German edition of this manual version 1 2 2015 05 13 Printed in Ger...

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