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Revision 14 

 

144 

August 02, 2019 

6.6  Calibrating/Validating the Analyzer 

 

The analyzer must be calibrated using known certified standards.  The concentration of the 

calibration gas should be 50 - 75 % of the full scale required for the analyses. There are three 

ways to calibrate the system: 

•

 Manual Calibration (Section 6.6.1) 

•

 Manually Initiated Auto Calibration (Section 6.6.2) 

•

 Auto Calibration (Section 6.6.3) 

 

6.6.1  Manual Calibration  

 

If this option is employed, the analyzer is equipped with a manually operated 3-way valve that 

can be used to introduce calibration gas to the analyzer.   

 

To perform a manual calibration: 

 

a)  Place the analyzer in Bypass mode by pressing  the Bypass button on the handheld 

keypad.  This will disable any alarm outputs. 

 

b)  Connect calibration gas to the Calibration port of the analyzer.  Set the output pressure of 

the calibration standard to the same pressure that the sample gas is normally provided at  

(this is typically 15 psig). 

 

 If, as is usually the case, the analyzer is running in auto sequence mode, 

when calibration gas is introduced all outputs and data logs will be 

updated with information that is generated while the calibration gas is 

running.  If this is not desired, then the analyzer can be placed in 

Reference

 

Mode.  While the analyzer is in Reference Mode, any data will be logged as 

Reference data, not as stream data.  To place the analyzer in reference 

mode, use the GUI to initiate the 

Reference 1 Manual

  sequence (Section 

5.10). 

 

 If the analyzer is to be calibrated while the analyzer is still running the auto 

sequence, it is important to disable the High High alarm if the calibration 

gas is higher than the alarm setpoint. 

 

c)  Turn the 3-way valve to introduce calibration gas to the analyzer. 

 

d)  Allow the analyzer to analyze the calibration gas until the readings become stable.  This 

typically takes 15 to 30 minutes.  

 

e)  Once the readings become stable, note of the current analyzer reading. 

 

f)  To calibrate the analyzer, an adjustment must be made to the analyzer’s 

Gain Factor

 on 

the 

Streams

 tab (Section 5.10) or on the hand held keypad.  The new Gain Factor can be 

calculated by the below formula: 

 

Содержание ProTech903

Страница 1: ...Analyzer OPERATION MANUAL P N MA2554 Revision 14 August 2019 Galvanic Applied Sciences Inc 7000 Fisher Road S E Calgary Alberta T2H 0W3 Canada Phone 403 252 8470 Toll Free 1 866 252 8470 E mail servic...

Страница 2: ......

Страница 3: ...n this manual is subject to change without notice and does not represent a commitment on the part of Galvanic Applied Sciences Inc No part of this manual may be reproduced or transmitted in any form o...

Страница 4: ...eraction Features 19 2 4 2 Display Board Communication Ports 20 2 5 CHASSIS 20 2 6 TAPE TRANSPORT SYSTEM 21 2 6 1 Supply and Take up Reels 21 2 6 2 Optical Encoder 22 2 7 SAMPLE CHAMBER ASSEMBLY 23 2...

Страница 5: ...G THE PROTECH903 ANALYZER VIA THE HANDHELD KEYPAD 54 4 1 INTRODUCTION 54 4 2 THE FRONT PANEL LEDS 54 4 3 THE MAIN PAGE OF THE LCD DISPLAY 56 4 3 1 Status Indicator Lines 57 4 3 2 Central Region 58 4 3...

Страница 6: ...5 10 3 3 Frequency 105 5 10 3 4 Analog Output Override 105 5 10 3 5 Stream Calibration Used 106 5 10 3 6 Alarms 106 5 10 4 Calibration Reference and Zero Gas Tabs 107 5 10 4 1 Calibration Tab 107 5 1...

Страница 7: ...ration 134 6 2 3 General Guidelines for Editing Parameters 134 6 3 COMMONLY EDITED PARAMETERS 135 6 3 1 The Streams Tab 135 6 3 2 Sequencer Tab 136 6 4 LESS COMMONLY EDITED ANALYZER PARAMETERS 137 6 4...

Страница 8: ...S TAB 161 8 4 COMMONLY OBSERVED PROBLEMS 164 SECTION 9 PROTECH903 H2S ANALYZER WIRING BOOK 166 SECTION 10 TECHNICAL SPECIFICATIONS 176 11 1 PERFORMANCE SPECIFICATIONS 176 11 2 FUNCTIONS 176 11 3 COMMU...

Страница 9: ...ury The Warning symbol indicates a hazardous situation that if not avoided could result in death or serious injury The Caution symbol with the safety alert symbol indicates a hazardous situation that...

Страница 10: ...ting the main power source may not remove power from the analog output signals Any safety recommendations or comments contained herein are suggested guidelines only Galvanic Applied Sciences Inc bears...

Страница 11: ...cility transportation charges prepaid or accept the return of the defective Product and refund the purchase price paid by Buyer for that Product If requested by Buyer Seller will use its best efforts...

Страница 12: ...the processor or software or firmware will be uninterrupted or error free The warranty herein applies only to Products within the agreed country of original end destination Products transferred outsi...

Страница 13: ...cetate Reaction Rate Method The total sulfur option includes a high temperature oven that is used to convert sulfur containing compounds to H2S using H2 The analyzer can use two different analysis alg...

Страница 14: ...uces dead volume providing faster response time Rapid measurement of the extent to which H2S exceeds pre set alarm levels If the total sulfur option is included H2S and total sulfur can be measured in...

Страница 15: ...us aspects of the application program on the personal computer Section 6 Operating the System describes how to set up the system to perform analyses Section 7 Maintenance includes a discussion of acti...

Страница 16: ...of the analyzer is presented in Figure 2 1 The total sulfur version of the ProTech903 includes the total sulfur furnace Section 2 9 An external sample conditioning system is available as an option Sec...

Страница 17: ...2 7 Sample Flow Related Components Section 2 8 The total sulfur version of the ProTech903 includes the total sulfur furnace Section 2 9 Total Sulfur Option An external sample conditioning system is a...

Страница 18: ...s Associated with the Motherboard The main processor daughter board and an optional Ethernet card are associated with the motherboard 2 2 3 AC and DC Power Supply The motherboard houses the AC and DC...

Страница 19: ...re are on the safe side These connections are used for the keypad wiring power to both the sensor block and the Optical Encoder and signal wiring to carry communications between the sensor block and t...

Страница 20: ...re are jumpers located on the bottom left hand corner of the CPU board that need to be set if this jack is to be used or if the Ethernet card is used The Ethernet Card option and the RJ 9 22 jack cann...

Страница 21: ...feet in length The tape is threaded over the lower tape guide past the sample chamber assembly and compression head over the two upper tape guides and finally over the Optical Encoder pulley before r...

Страница 22: ...ween subsequent stains tape wastage is minimized and tape life is maximized When the motor advances the take up reel causing the tape to move the movement of the tape causes the capstan on the pulse c...

Страница 23: ...Strip and the Rear Window Assembly The Rate Read Aperture strip and the Rear Window are made of a clear plastic to allow the light from the sensor block to pass through to the tape to correctly measur...

Страница 24: ...gas is high it may be necessary to reduce the quantity of gas that passes onto the tape to react with the lead acetate otherwise the rate of color change will be too fast for the system to correctly a...

Страница 25: ...he sensor block is shown in Figure 2 8 Figure 2 8 Sensor Block From Left Top View Side View and Installed View The sensor block measures the intensity of light reflected off of the lead acetate tape T...

Страница 26: ...in the tape transport system that seals the lead acetate tape up against the sample chamber so that the lead acetate can react with the hydrogen sulfide in the gas stream The compression head is shown...

Страница 27: ...e system is shown in Figure 2 10 and the humidifier used with the total sulfur option is shown in Figure 2 11 Figure 2 10 Nafion Humidifier Figure 2 11 Total Sulfur Option Humidifier The humidifier is...

Страница 28: ...tem It is mounted on the upper access door on the chassis The standard rotameter on the chassis is shown in Figure 2 12 The knob on the bottom of the rotameter is used to control the flow of the sampl...

Страница 29: ...ressure across the sample chamber Pressure can also be affected by a strong wind blowing across the vent When this happens a slight change in the pressure of the sample between the tape and the sample...

Страница 30: ...r to hydrogen sulfide is covered in ASTM Method D4468 85 Total Sulfur in Gaseous Fuels by Hydrogenolysis and Rateometric Colorimetry A few typical reactions are shown in Table 2 2 Table 2 2 Total Sulf...

Страница 31: ...mperature is monitored using a temperature switch wired into a discrete input on the I O board and by a thermocouple interface in which case temperature is available for readout on the LCD If the temp...

Страница 32: ...tch between calibration and sample gas to allow the system to be calibrated The standard filter housing is a Headline housing consisting of a disposable filter element and a sweep associated with it S...

Страница 33: ...red AC or DC The total sulfur option requires 250 W at 120 VAC or 230 VAC 3 2 2 Location of the System The system is designed to be operated at ambient temperatures from 10 50oC Galvanic offers comple...

Страница 34: ...ion 14 34 August 02 2019 Figure 3 1 Dimensions ProTech903 Class I Division 1 Dimensions Front and Side View Figure 3 2 Dimensions ProTech903 Class I Division 1 with Total Sulfur Option Front and Side...

Страница 35: ...Revision 14 35 August 02 2019 Figure 3 3 Dimensions ProTech903 Class I Division 2 Dimensions Front and Side View...

Страница 36: ...losure must be closed and sealed before powering up the analyzer in a classified area None of the explosion proof enclosures including the display cover should be opened until the area is known to be...

Страница 37: ...zer configurations and archive data USB Port The analyzer to PC via a standard USB A to USB A cable included with the analyzer The COM port used to connect to the system cannot be used for any other p...

Страница 38: ...e GASProTech903_vxxx_date exe to install the program xxx is the version number and the date of generation the file will be indicated e g GASProTech903_v100_Aug 15 2011a indicates version 100a generate...

Страница 39: ...e not using the USB mode of communication between the analyzer and the computer skip step b and continue to Section 3 5 4 b Connect the USB to USB cable that is provided with the system to the analyze...

Страница 40: ...l end of this cable to the male 9 pin serial port on the PC If you choose to use RS 232 communication it will be necessary to change the position of a pair of dipswitches located on bottom left hand c...

Страница 41: ...Settings button Figure 3 9 on the button bar of the application program to access the Communications Setup dialog box window Figure 3 10 Figure 3 9 Communication Settings Button Figure 3 10 Communicat...

Страница 42: ...ccess an outside line or a 1 is required to communicate with a computer that is outside the immediate telephone calling area make certain that the appropriate numbers are included e g 914035551212 The...

Страница 43: ...1 to 255 As an alternative put a checkmark in the All Stations checkbox which will cause the analyzer to poll all possible Modbus addresses The Timeouts field provides two options Backoff Timer and R...

Страница 44: ...rom writing any changes to these settings Update mode allows the operator to make changes to settings in the application program and write these changes to the analyzer This mode is password protected...

Страница 45: ...eypad Connect the keypad to the military connector on the left side of the chassis 3 5 2 Installing the Sensing Tape The sensing tape is installed in the tape enclosure Figure 3 15 presents a photo of...

Страница 46: ...oove in the sample chamber 8 and has no creases e Pull the tape up over the upper sample chamber guide pin 5 f Thread the tape over the black aluminium grey plastic capstan of the Optical Encoder 6 No...

Страница 47: ...line on the front of the humidifier with the 5 Acetic Acid solution included in the system crate Once filled replace the plug and place the humidifier into the system chassis behind the lower door Con...

Страница 48: ...width is set to Zero 0 before installing the quartz tube inside the furnace enclosure The furnace enclosure must be allowed to cool for at least 1 hour prior to initiating these procedures Do NOT rem...

Страница 49: ...ction tube sides of the two ultra torr elbows inside the furnace assembly b Carefully slide the new tube into the furnace Slide the old nuts and ferrules onto the two ends of the tube as well as two n...

Страница 50: ...nnecting it to the system c If the analyzer is equipped with the total sulfur option set the sample flow meter to a flow of 0 5 and the hydrogen flow meter to a flow of 1 5 If the total sulfur measure...

Страница 51: ...with the seal somewhere in the chassis 3 7 3 Leak Testing the Total Sulfur Accessory Connect the USB to USB cable from the laptop to the analyzer and log onto the analyzer using the Galvanic GUI soft...

Страница 52: ...nside the enclosure especially the two on the reaction tube itself are as tight as possible Again be careful not to break the tube while tightening the fittings e Once all leaks have been fixed replac...

Страница 53: ...calibration gas of known concentration to the calibration port and perform a manual reference run Repeat this step for the second stream if applicable If the reading on the analyzer LCD screen is with...

Страница 54: ...personal computer is provided as discussed in Section 5 The overall operation of the analyzer is controlled by the parameters that are resident in the analyzer When parameters are established via the...

Страница 55: ...lid This LED indicates that at least one alarm has been triggered BYPASS Yellow blinks This LED blinks yellow if the unit is in bypass mode WARNING Red solid Red blinks This LED is used for the follow...

Страница 56: ...r Section 4 3 3 Figure 4 2 The LCD Display Main Page The information presented by the display is dependent on the system configuration and the parameters that have been selected by the operator The va...

Страница 57: ...ero and span calibration This code is seen on power up and during a user forced sensor calibration through the keypad IDLE The system is waiting for a measurement from the sensor This code is seen on...

Страница 58: ...eys change as the operator selects a specific function as described in Section 4 4 to 4 9 Table 4 3 LCD Main Screen Function Key Definitions F Key Code Meaning F1 STRM Stream menu Allows the operator...

Страница 59: ...isplay to access the menus that present a variety of system parameters The keypad is shown in Figure 4 3 Figure 4 3 The Keypad The keypad includes 20 keys Eleven keys are used to enter numerical data...

Страница 60: ...or is used to select a sub menu BYPASS Pressing this key will put the analyzer into Bypass mode Pressing this key again will exit Bypass mode TAPE ADVANCE Pressing this key will cause the analyzer to...

Страница 61: ...each page H2S H 16 00 OFF This line indicates the set point for the H2S High Alarm and the current status of the alarm The alarm set point can be edited by pressing the EDIT key on the keypad while t...

Страница 62: ...recall what the previous value was CALGAS 18 0 18 0 This line is used to indicate the concentration of the calibration gas To change the setting press the EDIT button The operator will be prompted to...

Страница 63: ...e main screen a list of all alarms is presented e g Off line The Alarm LED will be lit when an alarm condition has been detected The possible alarms are listed in Table 4 5 A detailed discussion of th...

Страница 64: ...tions 4 7 1 through 4 7 4 mV Run State Time 6 1H1 S1 115 10 0 ppm F1 F2 F3 F4 SQNC IO READ SCHED Figure 4 7 Display Menu 4 7 1 The SQNC Menu A typical SQNC Sequence menu is presented in Figure 4 8 The...

Страница 65: ...Analyzer Reading menu is presented in Figure 4 10 The values that are presented are the most recent value for the various reading for each analysis e g S1 H2S 10 0 means that the last reading for H2S...

Страница 66: ...be entered followed by the ENTER key ACK_AL This field is used to acknowledge all latched alarms To acknowledge the latched alarms press the EDIT key and use the ENTER key to toggle the value to ON N...

Страница 67: ...ollowed by the ENTER key SEN CAL This field is used to initiate a sensor calibration see Section 7 3 4 8 2 The DIO Menu Digital Inputs Outputs When DIO F2 is pressed on the Configuration page Figure 4...

Страница 68: ...column is the present reading mV Run State Time 6 1H1 S1 115 A1_1 50 00F 12 38 Al 2 50 00 12 39 Al_3 50 00 12 44 Al_4 50 00 60 74 F1 F2 F3 F4 PGUP Up Down PGDN Figure 4 15 The AIO Display 4 8 4 The MS...

Страница 69: ...ailed discussion of the protocol to connect the two units is presented in Section 3 4 The graphical user interface is a Windows based application program which provides the analytical results and allo...

Страница 70: ...g box Figure 5 3 will be presented Figure 5 3 Select Mode Dialog Box c The Read Only option will allow the operator to view data parameters and analyzer settings but will not allow the operator to cha...

Страница 71: ...is presented in Section 5 2 2 The Upgrade Window option is used to install new software c Others Menu The Others menu contains Update Mode used to change from Read Only mode to the Update mode of ope...

Страница 72: ...u Section 5 2 1 In addition a field indicates the status of the analyzer and can contain three possible values OFF LINE which means that the GUI is not connected to an analyzer READ ONLY which means t...

Страница 73: ...Revision 14 73 August 02 2019 Communications Settings Allows the user to set up the communications options for the link between the GUI and the analyzer...

Страница 74: ...ge Once Reads back all the data points on the current screen Pushing this button allows the user to check and ensure that any changes written to the analyzer have been accepted Synchronize Time Update...

Страница 75: ...ion has been saved to a file previously pressing this button will overwrite the existing configuration file If offline a saved configuration file needs to be opened before one can be saved Save Config...

Страница 76: ...uts WET Allows the operator to configure the four discrete Wet inputs of the analyzer Outputs Allows the operator to configure the behaviour of the relays solenoids and analog outputs Sequences Allows...

Страница 77: ...you go through the tabs and make the desired changes the Write Current Page to Analyzer button allows you to store and view your analyzer configuration and its behavior before you make a final decisio...

Страница 78: ...ow Once Accept is pressed a command to the analyzer will be sent that will start the process of copying data from analyzer volatile memory to the analyzer hard flash memory This process takes about 30...

Страница 79: ...automatically polls the analyzer every three seconds allowing the user to be able to monitor the status of the analyzer on a continuous basis Figure 5 8 Analysis Tab 5 4 1 Field Names and Explanation...

Страница 80: ...tector output in millivolts This reading starts at around 1000mV at the start of an analysis and drops as the analysis proceeds This value can be displayed as live mV LmV on the display see Section 4...

Страница 81: ...tream was run Reference 1 The Reference 1 field either shows the current analysis reading if highlighted blue or the last reading when that stream was run A reference gas is used as a periodic calibra...

Страница 82: ...on the analyzer electronics board Analog outputs can be configured from the GUI Section 5 13 or by using the keypad Section 4 8 3 Relays shows the current status of the six relays The circle beside e...

Страница 83: ...ete input label indicates that the particular discrete input has been triggered while a green circle indicates that the particular discrete input has not been triggered Setting up discrete inputs is d...

Страница 84: ...ape more than a certain number of rotations without getting a corresponding signal from the Optical Encoder that controls the tape advance If this alarm triggers it will generally indicate a problem w...

Страница 85: ...ss High High Alarm is the second warning set point in a concentration range where the operator may need to take actions to alleviate this alarm Many users will use this set point to Shut in the proces...

Страница 86: ...ive concentration data hourly averages and other important data When this screen is first accessed an empty screen is presented Figure 5 11 Figure 5 11 Archive Tab To download archival data press the...

Страница 87: ...Enter key on the keyboard This will pull up the number of records entered in the field as shown in Figure 5 12 Figure 5 12 Archive Window Data Displayed The Seq field identifies each data point in a s...

Страница 88: ...one standard deviation away from the mean in both directions The yellow boxes at either end of the plot adjacent to solid blue line contain the numerical value of the average The yellow boxes at eith...

Страница 89: ...Brings up a dialogue box that allows the user to set the minimum and maximum value for the y axis scale Print N A Prints the chart to the printer of the user s choice Copy to Clipboard N A Copies the...

Страница 90: ...the data that they wish to display starting at a certain date and ending at a certain date Figure 5 14 Date Sorting Selection Dialog Box Today shows only data obtained on the current date Yesterday s...

Страница 91: ...s EXACTLY equal to the number entered will be displayed For example if 1000 was entered into the dialogue box only data exactly equal to 1000 will be displayed Ending Digits When this operator is used...

Страница 92: ...e as Legal CSV Saves all the archive data not just the number of records currently being displayed for all tabs as a CSV file The dialogue box as shown in Figure 5 16 is shown when saving to a CSV fil...

Страница 93: ...alyzer is set up at the factory Any data point of the user s choosing can be logged in each of these three logs at a frequency of the user s choosing The frequency of logging in seconds is entered int...

Страница 94: ...e log configuration will be automatically written to the analyzer If the data point is in Log Periodic 1 3 ensure that a frequency is entered for the data point Changing the frequency time within a gi...

Страница 95: ...bed in Section 5 7 for the Archive tab should be used Since the Event Log does not contain numerical data numerical sorting is not possible but it is possible to sort it according to the type of event...

Страница 96: ...Revision 14 96 August 02 2019 Figure 5 19 Event Log...

Страница 97: ...neral Section 5 9 1 Global Alarms Section 5 9 2 Whenever any change is made to a changeable field the change must be written to the analyzer before leaving that page by pressing the Temporary Write To...

Страница 98: ...the analyzer s serial number The Tag field tells the operator which site the analyzer is installed at and the Location field tells the operator where in the site the analyzer is installed Do not chang...

Страница 99: ...s of measurement will change the displayed unit for ALL tape length related fields and automatically convert the numerical value in each field to the selected system of measurement By default the anal...

Страница 100: ...pe Advance Limit is set to 60 seconds The actual Tape advance time will vary depending on the darkness of the tape staining The Tape Length Remaining field is set by default to 20 ft 6 1m If the analy...

Страница 101: ...of streams that are present in the system and the configuration shown in Figure 5 19 corresponds to a system with 4 streams that is capable of measuring H2S and total sulfur and presents the tab to e...

Страница 102: ...which can be edited i e 4 streams each with 6 gas run type tabs H2S Total Sulfur Calibration Reference 1 and 2 and Zero For a given stream the three parameters and three check boxes on the left of the...

Страница 103: ...calibration gas with a known concentration in the unit they wish to display The Cal Correction Enable check box is used to indicate that the calibration run is used to change the gain factor If this b...

Страница 104: ...able during this time period Typically the sample delay is around 120 to 180 seconds for the fixed time analysis and the sample interval is around 30 60 seconds This gives a total cycle time of 3 to 4...

Страница 105: ...se that relay or solenoid to energize when one of the analysis modes is running Figure 5 24 The Switching Field 5 10 3 3 Frequency If the Time check box is checked see Section 5 10 3 1 the operator ca...

Страница 106: ...Alarms The Alarms field Figure 5 25 is used to assign the alarms to the appropriate relay or solenoid and enter the level at which the alarm should be triggered All alarm types can be configured to tr...

Страница 107: ...s alarm will be listed in the Analyzer Alarm list as well as in the Event Log and the red ALARM LED on the front panel of the analyzer will also be lit Any outputs associated with this alarm mode will...

Страница 108: ...nalyzer will read on a gas that contains no H2S Running a zero run will result in a zero offset being calculated for the analyzer The Zero run can be set up similarly to the Calibration and Reference...

Страница 109: ...ndicates the number of consecutive runs to be averaged to obtain the concentration reading The Calibration Reference and Zero gas runs have the ability to average the concentration reading over a numb...

Страница 110: ...n type of run or to monitor external pressure or temperature switches for example Each discrete input is configured in the same manner It is important to know that these dry contacts are for devices t...

Страница 111: ...abled and will not respond to any inputs If the Alarm checkbox is checked the condition of each discrete input will be logged in the Event Log 5 11 3 Polarity If the Active On radio button is selected...

Страница 112: ...ired for these inputs is 4 24 VDC The Input WET tab allows the user to configure these discrete inputs in any manner These inputs can be configured to trigger a certain type of run or to monitor exter...

Страница 113: ...Any changes should be performed by an authorized operator The Outputs tab Figure 5 28 allows the user to configure the behavior of the six onboard relays 8 solenoids and 6 analog outputs The Outputs...

Страница 114: ...indicates that the output is not latched while a red circle indicates that the output is latched Acknowledge All latched outputs can be cleared by pressing the Acknowledge All Latches button in the to...

Страница 115: ...ms and the Manual Sequencer area 5 14 1 Enables Entire Sequencer Operation Checkbox The Enables Entire Sequencer Operation checkbox must be checked for sequencer operations to execute If this box is n...

Страница 116: ...cannot be interrupted midway through if they are entered via the Streams tab while they can be interrupted if they are programmed on the Sequencer tab To delete a run highlight it use press the Delet...

Страница 117: ...o initiate a Manual sequence Figure 5 33 Manual Sequencer Fields 5 14 6 Manual Sequencer 1 8 Each of the eight manual sequencer boxes include the following options Run and Loop Enable Checkboxes When...

Страница 118: ...eckbox should be checked to enable the dedicated digital contact chosen from the radio buttons below for that manual sequencer to initiate 5 15 Ports Tab The Ports tab Figure 5 32 shows the configurat...

Страница 119: ...Modbus and every user may desire a slightly different configuration this manual will only cover the basics of Modbus configuration If the user requires assistance in setting up a Modbus configuration...

Страница 120: ...field for Modicon with Floating Point will read MODICON32 The other field is called Address and the user must input the desired Modbus address for the analyzer into this field 5 16 1 Enron An Enron M...

Страница 121: ...to remotely These would include such things as tape length calibration gas concentration and gain factor 5 16 3 Modicon with Floating Point Just like the Modicon 16 Modbus list the Modicon with Floati...

Страница 122: ...Revision 14 122 August 02 2019 Figure 5 38 Typical Modicon with Floating Point List...

Страница 123: ...olean unsigned long and float Most data points are either Boolean or Float Floats can be output in the short and long nodes but the decimal points will be lost Certain data points have specific units...

Страница 124: ...Revision 14 124 August 02 2019 Figure 5 40 Expanded Modbus Nodes...

Страница 125: ...buttons which are described below Analog Input 1 and 2 normally setup as default 4 20 mA inputs but all the inputs can be scaled to what the operator requires Analog Input 3 default setup is for a th...

Страница 126: ...Span fields will be activated and the appropriate values can be entered Capture Zero used to capture the A D bits that are associated with a 4mA input during the calibration of the analog input Scaled...

Страница 127: ...start and stop timer set points Figure 5 42 Timers Tab It is important to note that any conditional events will only commence after the previous run is completed For example if a Zero gas run is sched...

Страница 128: ...o whatever is scheduled in that column to run every hour 5 18 2 Analysis The Enable checkbox must be checked before any of the gas runs listed below can be executed on a timer For any of the analysis...

Страница 129: ...outputs and test the operation of any of the relays or solenoids under direct board control This feature is useful during analyzer commissioning Figure 5 43 Maintenance Tab Changing Parameters on the...

Страница 130: ...of this condition Direct board control will automatically be disabled if the user changes to any other screen in the application program However it will not automatically be disabled should the appli...

Страница 131: ...Output Zero button Then press the Auto Cal button located below the Meter Reading field This will cause the analog output to be calibrated to exactly 4 mA d Once the multimeter reads the exact value p...

Страница 132: ...02 2019 5 20 Factory Tab The Factory tab is password protected All the parameters on this tab are set in the factory and should only be changed by authorized personnel or under the direction of Galvan...

Страница 133: ...nected to the personal computer and the Update mode all input and output devices have been interfaced In this chapter we will simply point out how each tab in the application program fits into the ent...

Страница 134: ...Analyzer button Figure 6 1 or the Permanent Configuration Write to the Analyzer button Figure 6 2 Figure 6 1 Write Current Page to Analyzer Button Figure 6 2 Permanent Configuration Write to the Anal...

Страница 135: ...d zero samples A maximum of four streams can be analyzed and the level of H2S and the total sulfur concentration can be measured if the total sulfur option is included in the system The Streams tab Fi...

Страница 136: ...encer tab Figure 6 4 is used to create analyzer gas run sequences The user can set up the analyzer gas run sequences to initiate either automatically or manually A detailed discussion of the Sequencer...

Страница 137: ...ers are set when the analyzer is initially installed and once they are set they are infrequently edited 6 4 1 The Global Tab The Global tab Figure 6 5 used to establish a broad range of system related...

Страница 138: ...WET tab Figure 6 6 and Inputs DRY tab are identical and allow the operator allows the user to configure these discrete inputs in any manner These inputs can be configured to trigger a certain type of...

Страница 139: ...the behaviour of the 6 onboard relays and 8 solenoids It is also where the analyzers Analog Outputs are named and configured The Output tab is divided into 2 main sections Digital Output and Analog O...

Страница 140: ...offers another powerful way to trigger conditional gas run requests other than the ones on the Streams Tab Manual Sequences can also be triggered using start and stop timer set points A detailed discu...

Страница 141: ...Figure 6 9 shows the configuration of the 3 main communications ports on the analyzer the Front Panel Serial Port RS 232 the ISO 485 Port RS 485 and the MODEM Port RS 232 A detailed discussion of the...

Страница 142: ...ge number of possible configurations for Modbus and every user may desire a slightly different configuration this manual will only cover the basics of Modbus configuration If the user requires assista...

Страница 143: ...lyzer s outputs The Analog output loop test can be performed by using the Analog Output Test feature to deliver 0 25 50 75 and 100 of full scale or any other test values The outputs can also be adjust...

Страница 144: ...lly the case the analyzer is running in auto sequence mode when calibration gas is introduced all outputs and data logs will be updated with information that is generated while the calibration gas is...

Страница 145: ...sed to introduce calibration gas to the analyzer To perform a manually initiated auto calibration a Place the analyzer in Bypass mode by pressing the Bypass button on the handheld keypad This will dis...

Страница 146: ...d The Auto Calibration can be initiated from the GUI by pressing the Stream 1 Calibration button as shown in Figure 6 12 The Auto Calibration can be initiated from the keypad by selecting the stream t...

Страница 147: ...equencer or Timers tab and the analyzer can be operated on a manual or automated basis The Analysis tab Figure 6 13 is a live presentation of the analytical data and allows the operator to see the sta...

Страница 148: ...from File button The archive on the analyzer is quite large so retrieving data from the archive can take several minutes especially if the PC is connected to the analyzer via a serial connection Once...

Страница 149: ...rm conditions experienced by the analyzer both global and stream related but also such things as changes in configuration and power up events A detailed discussion of the Events tab is presented in Se...

Страница 150: ...s of the analog outputs relays solenoids Analog inputs Discrete inputs and what voltage input source is in use In some cases the activation or deactivation of the status indicators may suggest there i...

Страница 151: ...6 A series of videos demonstrating typical maintenance procedures for the ProTech903 analyzer is available on Galvanic Applied Sciences Inc s YouTube channel search YouTube for Galvanic Applied Scienc...

Страница 152: ...replace the tape a Check the hand held display for any alarms b Disable alarms by pressing the BYPASS button on the hand held controller c Turn off gas to the analyzer Pull back the Compression Head a...

Страница 153: ...4 back and slide the tape behind the compression head Ensure that the tape is flat against the groove in the sample chamber 8 and has no creases Figure7 2 Tape Enclosure Parts Reference h Pull the ta...

Страница 154: ...stallation without the anti coning disks and the one on the right shows the tape installation with the disks Figure7 4 Installation of Sensing Tape m Advance tape a few inches with the TAPE ADV key n...

Страница 155: ...the chassis flow meter is somewhere between 1 5 and 2 0 on the tube scale 7 5 Total Sulfur Sample System To check the Total Sulfur Sample System a Place the analyzer in the Total Sulfur Analysis mode...

Страница 156: ...or ease of identifying all the parts discussed in these procedures The total sulfur furnace is housed inside an explosion proof enclosure 1 There are two screw on end caps 2 3 that screw onto large th...

Страница 157: ...be pushed in any further Carefully tighten the nut onto the elbow DO NOT OVERTIGHTEN This may cause the tube to break Tug on the elbow slightly after tightening to ensure that the elbow is snugly att...

Страница 158: ...tion tube itself are as tight as possible Again be careful not to break the tube while tightening the fittings m Once the leak has been fixed replace the end caps remove the cap and reattach the sampl...

Страница 159: ...fers service on a call out basis and or factory assistance on the analyzer For Service and or Assistance Contact Galvanic Applied Sciences Inc 7000 Fisher Road SE Calgary Alberta T2H 0W3 Canada Tel 40...

Страница 160: ...eference 2 High Alarm High High Alarm Deviation Lock Analysis Alarms Zero High Alarm High High Alarm Deviation Lock Analysis Alarms Calibration High Alarm High High Alarm Deviation Lock The Events tab...

Страница 161: ...larm parameters affect all streams identically and are related to hardware and other physical parameters that affect the operation of the analyzer In many cases the set point for these global alarms i...

Страница 162: ...and date in the real time clock varies from the time and date of the connected PC by more than a certain amount how much Maximum Tape Advance Triggered if the motor advances the tape more than a certa...

Страница 163: ...omes exceptionally dark before the next analysis begins or if there is no tape present Bypass Bypass mode is a mode of the analyzer that disables any outputs that may be triggered by alarms and is typ...

Страница 164: ...ck wires at top of Sensor block to be 5 volts 4 Stain is not well defined causing erratic readings Compression head not correctly sealing Check the seal on the compression head Tape not seated properl...

Страница 165: ...on Analyzer Alarm List the furnace element may need to be replaced 10 4 20mA outputs not agreeing with display on the screen Ranges are not configured correctly check the analog output range values o...

Страница 166: ...P1 P2 P3 P5 9 3 AC DC Power P3 P4 P5 9 4 Solenoid Drivers P5 P6 9 5 Relays Wiring P7 P8 9 6 Digital Inputs Isolated P9 9 7 Digital Inputs Dry P10 9 8 Isolated 4 20 mA Outputs P11 9 9 Isolated 4 20 mA...

Страница 167: ...Revision 14 167 August 02 2019 Figure 9 1 DC Power Wiring Diagram Figure 9 2 AC Power Wiring Diagram...

Страница 168: ...Revision 14 168 August 02 2019 Figure 9 3 Total Sulfur Wiring Diagram Figure 9 4 AC DC Power Wiring Diagram...

Страница 169: ...Revision 14 169 August 02 2019 Figure 9 5 Solenoid Drivers Wiring Diagram Figure 9 6 Relays Wiring Diagram...

Страница 170: ...Revision 14 170 August 02 2019 Figure 9 7 Discrete Inputs Isolated Wiring Diagram Figure 9 8 Discrete Inputs Dry Contact Wiring Diagrams...

Страница 171: ...Revision 14 171 August 02 2019 Figure 9 9 Isolated 4 20 mA Outputs Wiring Diagram Figure 9 10 Isolated 4 20 mA Inputs Wiring Diagram...

Страница 172: ...Revision 14 172 August 02 2019 Figure 9 11 5V and 24 V Stepper Motor Wiring Diagram Figure 9 12 Isolated 2 5 Mbits LAN Expansion Port...

Страница 173: ...Revision 14 173 August 02 2019 Figure 9 13 Isolated RS 485 Port Figure 9 14 P17 RS232 Port to Ethernet Cable...

Страница 174: ...Revision 14 174 August 02 2019 Figure 9 15 Sensor Block Keypad Encoder and Low Tape Sensor Div 1 Wiring Diagram Figure 9 16 Sensor Block Keypad Encoder and Low Tape Sensor Div 2 Wiring Diagram...

Страница 175: ...Revision 14 175 August 02 2019 Figure 9 17 Non Isolated 4 20 mA Inputs...

Страница 176: ...entration Cycle time is user configurable typical is 3 minutes 11 2 Functions Streams One 1 stream standard with up to 4 streams optional Each stream includes H2S analysis run zero run reference1 run...

Страница 177: ...to 7 more optional 1 USB port 1 RS 232 Serial Port 1 RS 485 isolated serial Port 1 LAN Port for extended analog outputs 1 Ethernet optional Modbus communication on all ports Inputs 8 discrete inputs 4...

Страница 178: ...ent of tape used User can program low tape alerts alarms Real time clock for accurate event time stamping Software Windows based software for configuration and monitoring Software includes advanced co...

Страница 179: ...Watts at 24VDC Power Input Range 10 32 VDC and or 90 230VAC AC power is standard AC power required for total sulfur Analog Outputs 6 isolated user scalable and programmable Scaling range from 3 00 to...

Страница 180: ...r Sensor is using 24 Bit AD converter to achieve greatest sensitivity and incorporates temperature sensor Real time clock for accurate event time stamping 512 Kbytes non volatile memory for data and e...

Страница 181: ...LECTRONICS ASSEMBLY BA0071 FLOWMETER ROTOMETER W ADJUSTABLE KNOB FOR STANDARD H2S ANALYZER BA0328 FLOWMETER ROTOMETER WO ADJUSTABLE KNOB FOR STANDARD H2S ANALYZER BA1367 PERM DILUTION TUBE C00082 HUMI...

Страница 182: ...4 182 August 02 2019 Table 12 1 Total Sulfur System Spare Parts Part Number Description BA1480 THERMO SWITCH MC0651Q QUARTZ TUBE 13 LONG MC0724 O RING LOW TEMP MC0945 KALREZ O RING HIGH TEMP CONNECTED...

Страница 183: ...art Button Functions 87 Chart Manipulation Options 87 Chassis 19 COLD_R 66 Com Port Direct Option 41 Commonly Edited Parameters 133 Communicate Toolbar 71 Communications Settings 71 Communications Set...

Страница 184: ...Manual Sequencer 1 8 115 Manual Sequencer Request Checkbox 114 Maximum Tape Advance 82 Menu Bar 70 MODBUS ADD 65 Modbus Address field 42 Modbus Tab 117 Modbus Trees 118 Modem Option 41 Modicon 16 119...

Страница 185: ...is 102 STATE code 56 Status Bar 74 Status Indicator Lines 56 Status Tab 80 Stream Calibration Used 104 Streams 60 Streams Tab 99 Supply Reel 21 Switching Field 103 Synchronize Time 72 System Menu 70 T...

Страница 186: ...Section 13 Figures FIGURE 2 1 SCHEMATIC OF PROTECH903 FLOW PATH 16 FIGURE 2 2 INTRINSICALLY SAFE BARRIER PERIPHERAL INTERFACE CONNECTIONS 19 FIGURE 2 3 CHASSIS ALL COVERS REMOVED 20 FIGURE 2 4 TAPE TR...

Страница 187: ...NEL OF THE ANALYZER 54 FIGURE 4 2 THE LCD DISPLAY MAIN PAGE 56 FIGURE 4 3 THE KEYPAD 59 FIGURE 4 4 THE STREAMS MENU 60 FIGURE 4 5 STREAM SELECTION MENU 61 FIGURE 4 6 FIRST STREAM MENU PAGE 61 FIGURE 4...

Страница 188: ...TAB 129 FIGURE 5 44 DIRECT BOARD CONTROL WARNING 130 FIGURE 6 1 WRITE CURRENT PAGE TO ANALYZER BUTTON 134 FIGURE 6 2 PERMANENT CONFIGURATION WRITE TO THE ANALYZER BUTTON 134 FIGURE 6 3 STREAMS TAB 13...

Страница 189: ...NG DIAGRAMS 170 FIGURE 9 9 ISOLATED 4 20 MA OUTPUTS WIRING DIAGRAM 171 FIGURE 9 10 ISOLATED 4 20 MA INPUTS WIRING DIAGRAM 171 FIGURE 9 11 5V AND 24 V STEPPER MOTOR WIRING DIAGRAM 172 FIGURE 9 12 ISOLA...

Страница 190: ...Revision 14 190 August 02 2019...

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