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BA362C/07/en/07.06
51517621

Valid as of:
Software version 5.9

Operating Instructions

Stamolys CA71HY 

Analyzer for Photometric Determination of Hydrazine

Содержание StamoLys CA 71 HY

Страница 1: ...BA362C 07 en 07 06 51517621 Valid as of Software version 5 9 Operating Instructions Stamolys CA71HY Analyzer for Photometric Determination of Hydrazine...

Страница 2: ...meter SCHRITTMOTOR SCHRITTMOTOR LECKF LECKF ALARM 2 ALARM 2 OPTION OPTION ST RUNG ALARM 1 ALARM 1 F5 F4 M 0 2 A M 0 2 A M 0 2 A M 0 2 A COM NC NO COM NC NO Kanal 1 Kanal 1 Kanal 2 Kanal 2 Channel 2 Ch...

Страница 3: ...2 Local operation 22 5 3 Calibration 29 6 Commissioning 31 6 1 Function check 31 6 2 Switching on 31 7 Maintenance 33 7 1 Maintenance schedule 33 7 2 Replacing reagents 33 7 3 Replacing pump hoses 34...

Страница 4: ...lectrical cables and hose connections are not damaged Do not operate damaged products and secure them against unintentional commissioning Mark the damaged product as defective Faults at the measuring...

Страница 5: ...alerts you to hazards They could cause serious injuries as well as damage to the instrument if ignored Caution This symbol alerts you to possible faults which could arise from incorrect operation The...

Страница 6: ...er specifications Sample transfer 1 From one measuring point one channel version 2 From two measuring points two channel version Power supply 0 230 V AC 50 Hz 1 115 V AC 60 Hz 2 115 V AC 50 Hz 3 230 V...

Страница 7: ...nch 1 6 mm x 3 2 mm 0 06 inch x 0 13 inch 6 4 mm x 3 2 mm 0 25 inch x 0 13 inch 2 T hose connectors of each 1 6 mm x 1 6 mm x 1 6 mm 0 06 inch x 0 06 inch x 0 06 inch 3 2 mm x 3 2 mm x 3 2 mm 0 13 inc...

Страница 8: ...supply from canister with standard Hose at rear supply from canister with cleaner a0006574 Fig 2 Analyzer cabinet version without hoses 1 2 3 4 5 Reagent pump P2 supply from canister Display Serial i...

Страница 9: ...it reliably against impact and moisture for storage and transportation The original packaging provides optimum protection In addition the permitted ambient conditions must be observed see Technical da...

Страница 10: ...6 30 250 9 84 125 4 92 165 6 50 21 0 83 26 1 02 21 0 83 119 4 69 78 3 07 47 1 85 648 25 5 360 14 2 436 17 2 243 9 57 200 7 87 120 4 72 326 12 8 16 0 63 27 1 06 120 4 72 555 21 8 465 18 3 500 19 7 7 11...

Страница 11: ...hannel version level monitoring is only possible for one channel One collecting vessel can be mounted on the housing A second vessel would have to be made available near the device a0001363 Fig 6 Coll...

Страница 12: ...ws 6 mm 0 24 For the installation dimensions please see the previous chapter 2 Using a spirit level check that the cabinet is hanging or standing straight Only in this way can any air bubbles present...

Страница 13: ...itioning using ultrafiltration for contaminated media e g from the primary settling tank For questions regarding sample conditioning and its automation please contact Service or the sales center respo...

Страница 14: ...e for both analyzers Bear this in mind when selecting maintenance intervals for CAT430 and when setting the buffer volume at the collecting vessel a0001728 Fig 13 Installation example 1 Sample from CA...

Страница 15: ...e frame of the analyzer to reach the terminal block Beforehand release the hoses from the outlet pipe Otherwise there is a danger of flooding Connect the hoses again after folding the frame back in Fo...

Страница 16: ...emmen f hren auch bei ausgeschaltetem Ger t Spannung Terminals voltage to ground even when the unit is switched off Terminals voltage to ground even when the unit is switched off V 4 V 4 31 30 29 0V n...

Страница 17: ...ready To start measurement the voltage must stay at 0 V for at least 5 seconds Function Designation Terminal One channel version Terminal Two channel version Mains L 3 3 N 2 2 PE1 1 Brass screw with b...

Страница 18: ...t analog output 1 and analog output 2 route the cable cores of the two data cables through the interference suppressor 4 2 2 One channel version a0001746 Fig 18 Interference protection of the signal c...

Страница 19: ...nished 5 s Analog output l 1 channel 1 0 or 4 mA start of measuring range 20 mA end of measuring range l 2 channel 2 0 or 4 mA start of measuring range 20 mA end of measuring range Channel selection M...

Страница 20: ...uired not a crossed one The interface does not have to be configured at the analyzer The following commands can be sent from the PC in order to read out data D Data memory Measured values C Data memor...

Страница 21: ...easure the current values at the terminals of the analyzer and not at the PLC DSC or data logger If these current values are correct please check your PLC DCS the data logger and or the electrical cab...

Страница 22: ...on Indicator LED function H Auto measuring option Back to the main menu from all sub menus Alarm value 1 exceeded Backwards in the sub menu horizontal see Appendix Alarm value 2 exceeded V Backwards i...

Страница 23: ...et been reached or The measuring interval has not yet elapsed Note Measuring flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample coll...

Страница 24: ...sults from factors such as reagent aging aging of constructive components etc The calibration factor compensates for these effects CA 71 checks the registered calibration factor logically If the facto...

Страница 25: ...for alarm value 2 channel 1 works as an NO or NC contact Alarm value AV 1 2 Two channel version only Setting as to whether the contact for alarm value 1 channel 2 works as an NO or NC contact Alarm v...

Страница 26: ...m After each change the instrument does not wait for the measuring interval If the measurement is to start immediately set the time in the past Measuring interval 2 to 120 minutes 10 Time between two...

Страница 27: ...automatically deleted If this does not happen automatically error messages can be deleted by quickly switching the analyzer off and back on again 1 flushing 01 01 96 00 00 to 31 12 95 23 59 Time of 1...

Страница 28: ...that they run in the same ratio as for filling the sample reagent mixture in measurement mode s stop and g go Note G can only be selected if P1 and P2 are Off The following valve combinations are poss...

Страница 29: ...g table provides an overview of the standard calibration data Note Compare these values to your own data After changes in the CONFIGURATION menu and in the event of software updates you can check and...

Страница 30: ...value and then press H twice to return to the main menu AUTO MEASURING 6 Press F again This takes you back to the measuring mode The calibration is now carried out automatically Caution After the cal...

Страница 31: ...t the device parameters proceed as follows 1 Plug in the analyzer s plug with grounding contact into the socket 2 Press the H key until AUTO MEASURING is displayed 3 Select the CONFIGURATION menu and...

Страница 32: ...lect V1 S V2 R with F or K switch to R or S with V and then switch the P1 sample pump on Leave the pump running until you can tell that there is cleaning agent at the T hose connector Switch P1 back o...

Страница 33: ...splash and heat may build up If you store the reagents correctly in the dark not over 20 C they will keep unopened for a minimum of 12 weeks from the date of production batch number When this period...

Страница 34: ...ple see CONFIGURATION The value determined is saved by the analyzer as the frequency offset 7 Then carry out a calibration see chapter Calibration 7 3 Replacing pump hoses Warning When removing hoses...

Страница 35: ...CONFIGURATION and carry out calibration Calibration Caution Make sure you connect the new pump hoses to the correct connections at the T hose connector For the order numbers of the pump hoses see the...

Страница 36: ...ack hoses press the black button on the valve and disconnect the hoses 3 Spray the new hoses and valves with silicone spray before inserting them 4 Reverse the sequence of operations to install the ne...

Страница 37: ...assemblies Removing the old cell 1 Rinse first with water and then with air see SERVICE 2 Switch the analyzer off 3 Unscrew the four screws on the photometer housing and remove it 4 Release the nuts...

Страница 38: ...the instrument out of service thoroughly rinse all the lines with clean water Proceed as follows 1 Remove the reagent and standard hoses from the canisters and immerse them in a tank containing clean...

Страница 39: ...HY1 active 1 l Order No CAY540 V10AAE Reagent HY1 inactive 1 l Order No CAY540 V10AAH Cleaner 1 l Order No CAY541 V10AAE Standard 400 g l N2H4 Order No CAY542 V10C50AAE Note Please note the disposal i...

Страница 40: ...reagents Standard dosing defective Check the valves for contamination obstructions visual inspection Replace valve hoses if necessary Incorrect photometer Check the setting in the CONFIGURATION menu...

Страница 41: ...lush with 12 5 bleaching lye first and then with 5 hydrochloric acid Measured values inaccurate Standard is dosed to the sample Check the valves and valve settings Replace valve hoses if necessary Cou...

Страница 42: ...nt precipitation EDTA not with CA71HA Not enough sample conditioning Shorten the cleaning intervals of sample conditioning Error Possible cause Tests and or corrective measures a0006410 Fig 24 Overvie...

Страница 43: ...512088 Item Spare part Order number 130 133 Maintenance kit CAV740 1 set of pump hoses blue yellow item 113 12 piece 51506434 1 set of pump hoses black black 12 piece 51506497 1 pack of hose connector...

Страница 44: ...SI Shortened reaction time AM C 90 s SI A 0 Hz signal error only after 90 s Reason for crashing during frequency display in SERVICE eliminated Restart after power failure BA364C 07 xx 06 04 03 2004 5...

Страница 45: ...ent consumption Approx 0 2 A at 230 V Approx 0 5 A at 115 V Fuses 1 x slow blow 0 5 A for analyzer electronics 2 x semi delay 0 2 A for photometer Time between two measurements tmeas reaction time rin...

Страница 46: ...pplied Degree of protection IP 43 Sample temperature 5 to 40 C 40 to 100 F Sample flow rate Min 5 ml min 0 0013 gal min Consistency of the sample Low solid content dry matter 50 mg l ppm Sample inlet...

Страница 47: ...Stamolys CA71HY Technical data Endress Hauser 47...

Страница 48: ...Appendix Stamolys CA71HY 48 Endress Hauser 11 Appendix 11 1 Operating matrix One channel version a0001907 en...

Страница 49: ...Stamolys CA71HY Appendix Endress Hauser 49 a0001908 en...

Страница 50: ...Appendix Stamolys CA71HY 50 Endress Hauser Two channel version a0001909 en...

Страница 51: ...Stamolys CA71HY Appendix Endress Hauser 51 a0001910 en...

Страница 52: ...131 132 133 134 10 pieces each C Flex hose for valves 1 40 m Quantity Order No Designation CAY540 V10AAE Reagent HY1 active 1 l CAY540 V10AAH Reagent HY1 inactive 1 l CAY541 V10AAE Cleaner 1 l CAY542...

Страница 53: ...51506491 10 T hose connector 6 4 mm x 6 4 mm x 6 4 mm 51506493 10 Hose connector 6 4 mm x 6 4 mm 51506494 133 10 Hose connector 3 2 mm x 6 4 mm 51506492 134 10 Y hose connector 1 6 mm x 1 6 mm x 1 6...

Страница 54: ...tion Delay to sample s Analog output 0 20 mA 4 20 mA AV 1 NC NO AV 2 NC NO Error contact NC NO Frequency offset Hz Zero frequency base line dist water without reagent Hz Measuring range start mg l g l...

Страница 55: ...sing Filling time Reaction time RPM K floating mean N Points C1 mg l g l F 1 Hz C2 mg l g l F 2 Hz C3 mg l g l F 3 Hz C4 mg l g l F 4 Hz C5 mg l g l F 5 Hz C6 mg l g l F 6 Hz C7 mg l g l F 7 Hz C8 mg...

Страница 56: ...Appendix Stamolys CA71HY 56 Endress Hauser 11 4 Maintenance schedule a0001911 en...

Страница 57: ...Housing GFR 10 Stainless steel 9 Without 10 I Icons 5 Incoming acceptance 9 Input 45 Installation 4 8 Examples 14 Installation instructions 9 12 Interference suppressor 18 39 L LANGUAGE 27 Level monit...

Страница 58: ...Valve hoses 36 Return 4 44 S Safety conventions 5 Scope of delivery 7 Serial interface 20 SERVICE 28 Shielding 18 Signal connections 18 Software history 43 Spare parts 42 Stainless steel housing 9 Sta...

Страница 59: ......

Страница 60: ...www endress com worldwide BA362C 07 en 07 06 Printed in Germany FM SGML 6 0 DT 51517622...

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