Dionex ICS-3000, Руководство оператора

Страница: 308 / 392

ICS-3000 Ion Chromatography System
292
Doc. 065031-04 1/08
5. Select the Pump tab and select the following parameters:
a. Under Flow Control , set Flow to the flow rate recommended for
your application.
b. Click the Motor switch to start the pump flow.
c. Gradient pump only: Under Gradient Control , enter 100% for
the reservoir containing the ASTM Type I (18 megohm-cm)
filtered and deionized water.
6. Allow the pump to run for at least 10 minutes.
7. Click Motor to turn off the pump flow.
8. Disconnect the hydration tubing assembly from the
ELUENT OUT
and
REGEN IN
ports on the CR-TC.
9. Disconnect the pump outlet line from the
ELUENT IN
port on the CR-
TC.
9.13.3 Completing the New CR-TC Plumbing
Reinstall the EluGen Cartridge
1. Reconnect the EluGen cartridge inlet and outlet lines.
2. Turn the EluGen cartridge right-side up, and check for bubbles in the
eluent generation chamber. If necessary, shake and tap the cartridge to
remove bubbles.
3. Reinstall the EluGen cartridge in the holder. Remove the 10-32 plug
from the vent opening and reinstall the luer adapter and vent line.
4. Push the cartridge’s electrical cable connector onto the
EGC 1
(or
EGC
2
) bulkhead connector. Twist the ring on the cable connector
fingertight to secure it.
5. Refer to Figure 9-19 to plumb the four ports on the new CR-TC.
To avoid damaging the suppressor, always turn off the suppressor
before hydrating the CR-TC. The pump flow is on during conditioning;
however, no flow reaches the suppressor.