94
5977 Series MSD Operation Manual
4
Operating in Chemical Ionization (CI) Mode
N/A
Not available
Table 15
Reagent gas settings
Reagent gas
Methane
Isobutane
Ammonia
EI
Ion polarity
Positive
Negative
Positive
Negative
Positive
Negative
N/A
Emission 150
A
50
A
150
A
50
A
150
A
50
A
35
A
Electron
energy
150 eV
150 eV
150 eV
150 eV
150 eV
150 eV
70 eV
Filament
1
1
1
1
1
1
1 or 2
Repeller
3 V
3 V
3 V
3 V
3 V
3 V
30 V
Ion focus
130 V
130 V
130 V
130 V
130 V
130 V
90 V
Entrance
lens offset
20 V
20 V
20 V
20 V
20 V
20 V
25 V
EM volts
1200
1400
1200
1400
1200
1400
1300
Shutoff valve
Open
Open
Open
Open
Open
Open
Closed
Gas select
A
A
B
B
B
B
None
Suggested
flow
20%
40%
20%
40%
20%
40%
N/A
Source temp
250
°C
150
°C
250
°C
150
°C
250
°C
150
°C
230
°C
Quad temp
150
°C
150
°C
150
°C
150
°C
150
°C
150
°C
150
°C
Interface
temp
280
°C
280
°C
280
°C
280
°C
280
°C
280
°C
280
°C
Autotune
Yes
Yes
No
Yes
No
Yes
Yes
Содержание G7035A
Страница 1: ...Agilent Technologies Agilent 5977 Series MSD Operation Manual ...
Страница 30: ...30 5977 Series MSD Operation Manual 1 Introduction ...
Страница 88: ...88 5977 Series MSD Operation Manual 3 Operating in Electron Ionization EI Mode ...
Страница 112: ...112 5977 Series MSD Operation Manual 4 Operating in Chemical Ionization CI Mode Figure 18 PCI autotune report ...
Страница 114: ...114 5977 Series MSD Operation Manual 4 Operating in Chemical Ionization CI Mode Figure 19 NCI autotune ...
Страница 170: ...170 5977 Series MSD Operation Manual 6 CI Maintenance ...
Страница 171: ......
Страница 172: ... G3870 90003 G3870 90003 Agilent Technologies Agilent Technologies Inc Printed in USA February 2013 ...