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Troubleshooting
280
Problem
Possible Cause(s)
Corrective Action
Cannot obtain
suggested BEC value
You may not be comparing the
appropriate BEC value for the
wavelength you are using.
Refer to the Syngistix Software Guide
on the Syngistix Document Pack CD
for details
.
The torch position may need
adjustment.
Refer to the torch adjustment
procedures for your instrument.
The plasma viewing position
may need to be optimized.
Refer to the Lateral (radial view mode)
and X/Y (axial view mode) torch view
procedures. See
.
RF power, nebulizer argon
flow, and/or plasma viewing
height may need adjustment.
Adjust as necessary. Also, check that
you are using the recommended
settings for your instrument.
The purge windows may
require cleaning.
Refer to the instructions for removing
and cleaning the purge windows for
your instrument
.
Results
erroneously
high
Corrections may not have been
made for the reagent blank.
Aspirate a blank and rerun standards
and samples.
Standard solutions may have
deteriorated or may have been
improperly made.
Restandardize with a proven standard.
Background emission may be
present.
Use background correction.
Table 6-1.
Performance Problems: Troubleshooting Table
Summary of Contents for AVIO 200
Page 1: ...AVIO 200 SPECTROMETER Hardware Guide ICP OPTICAL EMISSION ...
Page 2: ......
Page 3: ...AvioTM 200 Spectrometer Customer Hardware and Service Guide ...
Page 12: ...Contents 10 ...
Page 30: ...28 ...
Page 31: ...Safety Practices 1 ...
Page 32: ...30 Safety Practices ...
Page 56: ...54 Safety Practices ...
Page 57: ...Preparing Your Laboratory 2 ...
Page 58: ...Preparing Your Laboratory 56 ...
Page 70: ...Preparing Your Laboratory 68 ...
Page 71: ...System Description 3 ...
Page 72: ......
Page 97: ...Installation 4 ...
Page 98: ......
Page 119: ...Installation 117 Figure 4 8 Replacing the torch 1 3 4 6 8 2 9 10 5 7 ...
Page 121: ...Installation 119 1 2 7 9 8 10 3 4 5 6 ...
Page 164: ...Installation 162 ...
Page 165: ...Maintenance 5 ...
Page 166: ......
Page 184: ...Maintenance 182 1 2 7 9 8 10 3 4 5 6 ...
Page 188: ...Maintenance 186 Figure 5 8 Replacing the Torch 1 3 4 6 8 2 9 10 5 7 ...
Page 272: ...Maintenance 270 ...
Page 273: ...Troubleshooting 6 ...
Page 274: ......
Page 293: ...Troubleshooting 291 Figure 6 1 Normal Plasma Conditions at 0 torch position ...
Page 294: ...Troubleshooting 292 Figure 6 2 Normal Plasma at 3mm position ...
Page 297: ...Troubleshooting 295 Figure 6 5 Injector too far forward ...
Page 298: ...Troubleshooting 296 Figure 6 6 No Aux Gas Torch may be glowing ...
Page 299: ...Troubleshooting 297 Figure 6 7 Air Leak or Spray Chamber Temperature too high ...
Page 300: ...Troubleshooting 298 Figure 6 8 Thin Plasma due to leak in Plasma Gas Line ...
Page 308: ......