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horiba TPNA-500, Instruction Manual

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horiba TPNA-500 Instruction Manual Download Page 16

Others (writing of setting) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

189

Maintenance  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  190

Periodic maintenance procedure  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

190

Waste liquid processing  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

191

Replacing the reagent bottle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

193

Replacement of the pure water cartridge (For the built in pure water cartridge)

201

Supplying pure water into the pure water tank (for models equipped with a pure water 
tank)  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

204

Checking and cleaning the overflow tank (option)  . . . . . . . . . . . . . . . . . . . . . .

207

Checking and cleaning the dilution tube and cell measurement tube. . . . . . . .

209

Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  214

When measurement cannot be started. . . . . . . . . . . . . . . . . . . . . . . . . . 

214

Measurement not working right. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

215

Alarm list and operation outline. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

217

Cause and corrective action for alarms  . . . . . . . . . . . . . . . . . . . . . . . . . 

218

Material. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  224

Measurement principle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

224

Total nitrogen: Ultraviolet oxidative dissolution method . . . . . . . . . . . . . . . . . .

224

Total phosphorus: Ultraviolet oxidative dissolution - Molybdenum blue spectrophotomet-
ric method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

225

Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

226

Accessories and consumables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

229

Accessories. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

229

Consumables  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

230

List of reagent consumptions  . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

231

Time chart . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 

233

Sequence: Preprocess, Pre-Wash, Post-Wash  . . . . . . . . . . . . . . . . . . . . . . . .

234

Sequence: Zero calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

235

Sequence: Measurement/span calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . .

236

TURB. COEFFICIENT SET (Option)  . . . . . . . . . . . . . . . . . . . . . . . . . . . 

242

Summary of Contents for TPNA-500

Page 1: ...Automatic Total Nitrogen Phosphorus Monitoring System TPNA 500 Instruction Manual CODE GZ0000371324D...

Page 2: ...le to improper operation Any malfunction attributable to repair or modification by any person not authorized by HORIBA Advanced Techno Co Ltd Any malfunction or damage attributable to the use in an en...

Page 3: ...ective 2012 19 EU and or waste batteries and accumulators under the Directive 2006 66 EC in the European Union The symbol might be put with one of the chemical symbols below In this case it satisfies...

Page 4: ...igned to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and...

Page 5: ...w away this product without any good reason Name and amount of hazardous substance used in a product Unit name Hazardous substance Lead Pb Mercury Hg Cadmium Cd Hexavalent chromium Cr VI Polybromo bip...

Page 6: ...esult in death or serious injury This is to be limited to the most extreme situations This indicates a potentially hazardous situation which if not avoided could result in death or serious injury This...

Page 7: ...skin or in your eyes rinse it off with a plenty of water immediately and contact your doctor If you swallow it accidentally contact your doctor immediately Chemical hazard Some reagents are poisonous...

Page 8: ...Attachment location and type of warning labels Attachment location of warning labels 1 2 6 5 3 4 For automatic hydrochloric acid cleaning specification...

Page 9: ...Type 1 2 4 3 5 2 type labels 6 For automatic hydrochloric acid cleaning specification...

Page 10: ...careful when handling chemicals A new reagent bottle is fully charged with reagent If you grab the side of the bottle while the cap is open the reagent may spill out When opening the cap of the reage...

Page 11: ...s manual Note This interprets the necessary points for correct operation and notifies the important points for handling the product Reference This indicates the part where to refer for information Tip...

Page 12: ......

Page 13: ...peroxodisulfate aqueous solution Reagent A 35 Preparing sodium hydroxide aqueous solution Reagent B 35 Preparing dilute sulfuric acid solution Reagent C 35 Preparing L ascorbic acid aqueous solution R...

Page 14: ...ns 58 To display the MENU item screen 62 MENU SETTING 63 OPERATION SET 63 MEAS LINE SET 75 OUTPUT SET 83 PAYLOAD SET 98 SYSTEM SET 100 MENU MAINTENANCE 111 REAG 111 PERIODIC CHECK 115 EXT ANALOG OUTPU...

Page 15: ...le 174 Data definition sheet 177 How to use data 186 MEAS STATUS 186 MEAS CURRENT ALARM 186 MEAS MEASURE VALUE 186 MEAS Hour Report History 186 MEAS Day Report History 186 MEAS EXT ANALOG INPUT 186 ME...

Page 16: ...leshooting 214 When measurement cannot be started 214 Measurement not working right 215 Alarm list and operation outline 217 Cause and corrective action for alarms 218 Material 224 Measurement princip...

Page 17: ...Principle of measurement for total nitrogen Alkaline potassium peroxodisulfate solution is added to the sample solution Irradiation by ultraviolet light then causes oxidative dissolution of nitrogen c...

Page 18: ...ste liquid tank The amount of waste liquid is approximately 17 L per month Includes alarm output contact terminals to activate a Full Drain Tank alarm when the tank reaches full capacity Tank capacity...

Page 19: ...on agitation and absorbance measurement Measurement cells for total phosphorus and total nitrogen have been integrated 11 Reagent metering section Measures the amount of each reagent to be injected 12...

Page 20: ...e for control of pure water supply 15 Pure water cartridge In the case of specifications with built in pure water cartridge it is attached Pure water necessary for the measurement is purified when you...

Page 21: ...dance Can be operated directly from the screen 3 Power switch Turns power on and off to the operation section 4 Alarm indicator Will light up when an alarm occurs 5 Access indicator Will light up when...

Page 22: ...n when an operating button has been pressed No Description Details 1 Screen title Preprocess MEAS SETTING LOG DATA etc 2 Component Displays currently active items 3 Details of display item Displays me...

Page 23: ...reen will show details of each item 1 2 3 4 No Description Details 1 Screen title ALARM HISTORY etc 2 Description of table contents Shows the currently displayed item 3 Details of display item Shows d...

Page 24: ...ents are measured and injected into the dissolution sections Dissolution Solutions are exposed to ultraviolet light and heated to cause dissolution of the compounds in the sample Measurement Reagents...

Page 25: ...rity icons Item Icon Description Alarm activated Critical red An alarm is activated For details on how to check past alarm refer to DATA ALARM HISTORY page 147 Minor yellow No alarm No display No alar...

Page 26: ...Before Using the Product 10 How to change authority 1 Press the icon 2 Press the relevant authority button 3 Enter your password and press ENTER...

Page 27: ...l line Ground the shielded side to the receiving side For noise protection connect the surge absorber or noise killer in parallel with the contact output signal lines Input output terminal standard 1...

Page 28: ...malfunction Do not connect the power cable to the signal wiring section It could cause malfunction of the equipment For analog input output and contact input output For RS communication 0 75 mm2 to 2...

Page 29: ...Outputs the TP concentration for L1 TN Conc L1 Outputs the TN concentration for L1 TP Load L1 Outputs the TP load for L1 TN Load L1 Outputs the TN load for L1 Flow L1 Outputs the L1 flow rate No alloc...

Page 30: ...output range Example of 4 mA to 20 mA output Example of 0 mA to 16 mA output Measurement item Range 4 mA output 20 mA output TP Conc L1 10 mg L 0 mg L 10 mg L Measurement item Range 0 mA output 16 mA...

Page 31: ...allocation 1 AO 00 TP Conc L1 2 AO 00 3 AO 01 TN Conc L1 4 AO 01 5 AO 02 TP Load L1 6 AO 02 7 AO 03 TN Load L1 8 AO 03 Terminal No Output No Initial allocation 61 AO 04 COD Conc L1 62 AO 04 63 AO 05 C...

Page 32: ...ndard is shown below The voltage output 0 V to 1 V DC 1 V to 5 V is also available as an option Signal type Input output circuit Standard Analog signal output Current signal output 0 mA to 16 mA DC 4...

Page 33: ...pecifications Item Standard specification Only available for 3 component specification Only available for 2 point meter specification Measurement item and analog input range Example of flow meter Inpu...

Page 34: ...nt input standard is shown below The voltage input 1 V to 5 V DC is also available as an option Terminal No Output No Initial allocation 9 AI00 Flow Meter L1 10 AI00 Terminal No Output No Initial allo...

Page 35: ...ure History Hour Report Day Report Alarm History Calib History and OperateData Clock Err An error has occurred in the clock of the meter Int Power An error has occurred in the power supply unit inside...

Page 36: ...ror has occurred in the cell motor of the UV meter Lamp UV An error has occurred in the light source of the UV meter CAN Comm UV An error has occurred during communication with the UV meter when the U...

Page 37: ...ter Item Description Terminal No Output No Initial allocation 29 PO 00 TP Hi Conc L1 30 PO 00 31 PO 01 TN Hi Conc L1 32 PO 01 33 PO 02 TP Hi Load L1 34 PO 02 35 PO 03 TN Hi Load L1 36 PO 03 37 PO 04 M...

Page 38: ...92 PO 17 93 PO 18 COD Hi Load L1 94 PO 18 95 PO 19 No allocation 96 PO 19 97 PO 20 No allocation 98 PO 20 99 PO 21 No allocation 100 PO 21 Terminal No Output No Initial allocation 89 PO 16 TP Hi Conc...

Page 39: ...ler surge absorber AC or DC load or diode DC load etc in parallel with the load in order to prevent noise generation Signal type Input output circuit Standard Contact output signal Contact rating 250...

Page 40: ...10 seconds after the OFF release status Level reading Level reading Samp Lack L1 Accepts Samp Lack L1 Level reading Level reading Line Select L1 Accepts Line Select L1 The signal is accepted when the...

Page 41: ...ent calibration cleaning start is input during pulse setting only the standby signal is accepted Item Description Input condition Start signal type For level setting For pulse setting Samp Lack L2 Acc...

Page 42: ...I 03 Flow Power L1 18 PI 03 G 19 PI 04 Flow No Drain L1 20 PI 04 G 21 PI 05 Meas Start 22 PI 05 G 23 PI 06 Cal Start 24 PI 06 G 25 PI 07 Modify Date 26 PI 07 G 27 PI 08 No allocation 28 PI 08 G Termin...

Page 43: ...lect L2 72 PI 09 G 73 PI 10 Flow Mainte L2 74 PI 10 G 75 PI 11 Flow Err L2 76 PI 11 G 77 PI 12 Flow Power L2 78 PI 12 G 79 PI 13 Flow No Drain L2 80 PI 13 G 81 PI 14 No allocation 82 PI 14 G 83 PI 15...

Page 44: ...tact input may not be accepted Be sure to keep the contact ON for the time specified in the input conditions Signal type Input output circuit Standard Contact input signal Contact rating ON resistance...

Page 45: ...d wire or round pins D SUB 9 pin female connector Interface Configured at the factory RS 485 standard RS 232C option Protocol Modbus RTU Communication speed Select one of the following 38400 bps 19200...

Page 46: ...not be performed The printer paper for the TPNA 500 is a highly sensitive thermal paper for high speed printers For purchase of the printer paper specify the parts code listed in Accessories and consu...

Page 47: ...correctly Reagent bottle A label with different color is attached to each reagent bottle WARNING Chemical hazard Some reagents are poisonous and thus it is extremely dangerous if they are touched by h...

Page 48: ...ent bottle check that the color of the tube matches that of the label of the reagent bottle and attach the nozzle unit Replacement example of reagent C bottle Reagent unit Knurled screw Reagent B Reag...

Page 49: ...reagent bottle in the reagent tray as illustrated below 5 Return the reagent tray to its original position and tighten the knurled screw Knurled screw Reagent B Reagent D Span solution Reagent F Reag...

Page 50: ...ic acid aqueous solution Reagent D Mixed reagent Reagent E Hydrochloric acid solution Reagent F Span solution Consumption of reagents per measurement Application Reagent Concentration Consum ption Rea...

Page 51: ...ion Reagent C 1 Measure 60 mL of sulfuric acid special grade 96 or above in a measuring cylinder 2 Measure 180 mL of pure water in a measuring cylinder and pour it into a heat resistant container 3 Sl...

Page 52: ...rate sesquihydrate 2 Pour approximately 200 mL of pure water into a container 3 Dissolve the above measured reagent completely in this container 4 Add pure water to make it a total of 250 mL Preparing...

Page 53: ...ion measurement values total nitrogen or List of calibration solution measurement values total phosphorus 1 Measure the undiluted solution for nitrogen calibration according to the value specified in...

Page 54: ...218 1000 10 1000 20 20 1000 7 218 1000 20 1000 50 50 1000 7 218 1000 50 1000 100 100 0 722 1000 200 200 1 444 1000 500 500 3 609 1000 1000 1000 7 218 1000 Equipment range Preparation concentration Und...

Page 55: ...4 Supply pure water into the pure water tank 5 After the pure water supply return the tank to its original condition Note When the customer supplies pure water use the water of class A2 or above as sp...

Page 56: ...g Cl L 10 or less 2 or less 1 or less 1 or less Sulfate ion g SO4 L 10 or less 2 or less 1 or less 1 or less TP measurement range mg L TN measurement range mg L 2 5 10 20 50 100 200 500 1000 0 5 36 36...

Page 57: ...rts of the pure water cartridge 2 Pull down the safety lever and push in the pure water cartridge with the in out ports heading forward then pull up the safety lever Note If the safety lever can not b...

Page 58: ...s Depending on the workmanship of the pipe construction 4 Press MENU MAINTENANCE SEPARATE ACTION on the screen The SEPARATE ACTION 5 5 menu will be opened 5 Press Pure water purge to start purging of...

Page 59: ...ls will be a cause to reduce the performance of the pure water generation The pure water cartridge should be stored in the cool and dark room Water quality standard for tap water Items Criteria nitrat...

Page 60: ...of pure water supply from a customer 1 Confirm that plumbing is carried out definitely Open V 1 valve and supply pure water to purge the plumbing next Basic purge time about 5 minutes 2 When a purge w...

Page 61: ...protective goggles and gloves Dissolve the reagent in a well ventilated area such as a draft chamber Always pour hydrochloric acid into pure water Never pour pure water into hydrochloric acid 35 to 3...

Page 62: ...pour 600 mL of hydrochloric acid prepared in step 1 into the container while agitating pure water in the container 4 Pour pure water into the solution prepared in step 3 to make it a total of 4 L 5 Po...

Page 63: ...12 and 24 hours Measurement is performed at the specified interval from the measurement start time 4 External control Remote contact The operation is controlled according to the external contact input...

Page 64: ...vironment for factories that discharge waste liquid to the closed water area if there is no correlation among the measurement values obtained by the automatic total nitrogen phosphorus monitoring syst...

Page 65: ...power starts up the equipment enters a warm up state an alarm is displayed Once power has been applied to the analyzer the alarm will be canceled 10 minutes after the pump reaches a temperature of 35...

Page 66: ...nd main power switch 8 Clean the overflow tank When shutting down the analyzer for more than two weeks 1 Stop the equipment refer to STOP RESERVE page 158 2 Turn ON the maintenance switch 3 Perform th...

Page 67: ...ution in the same manner as above Store the removed reagent bottles in a cool and dark place 12 Use a beaker etc to hold the nozzle unit for each reagent line 13 Perform the following operation 14 Pre...

Page 68: ...play 1 Turn ON the power switch and main power switch 2 Clean the overflow tank 3 Set the reagent bottle in place refer to Installation of reagent bottle page 31 4 Start calibration refer to Calibrati...

Page 69: ...always perform zero calibration and then span calibration in this order Description of each calibration Calibration Description Zero calibration Measure the blank water and perform calibration by ref...

Page 70: ...perform calibration while the equipment is stopped refer to Calibration procedure page 55 Press START CALIBRATION in the main screen and then input the calibration start signal To forcibly perform cal...

Page 71: ...pure water remain The calibration cycle and count are set refer to AUTO CAL SET page 70 Operation procedure 1 Press START in the main screen 2 Zero calibration and span calibration will be performed a...

Page 72: ...ation steps from the main screen to the target screen are skipped as follows The operations from the target screen are explained by using a screen shot Main screen This is the main screen that is init...

Page 73: ...settings for the meter Page 122 DATA LOG DATA Allows you to check the values of the past data Page 131 GRAPH Allows you to use graphs to check past and current data Page 135 CALIBRATION HISTORY Allow...

Page 74: ...e 74 OFF LINE MODE MEAS LINE SET page 75 LINE CHANGE SET page 76 Line No L1 to L2 Line Select L1 to L2 CONV COEF SET page 77 Revision a L1 to a L2 Revision b L1 to b L2 CONC ALARM SET page 79 Hi Limit...

Page 75: ...ion COMMUNICATION SET page 108 Machine ID Baudrate Parity LANGUAGE SET page 109 Language TOUCH PANEL ADJUSTMENT page 110 MAINTENANCE page 111 REAG page 111 REAG VOLUME CHECK CHANGE REAG REAG VOLUME IN...

Page 76: ...INPUT page 127 ch00 to ch13 DATA page 128 LOG DATA page 131 MEASURE VALUE page 131 Measurement element Line Date PRINT HOUR REPORT page 133 Measurement element Line Date PRINT GRAPH page 135 MEASURE V...

Page 77: ...CALIBRATION HISTORY page 146 Measurement element PRINT ALARM HISTORY page 147 PRINT SAVE TO USB page 148 DATA CLEAR page 156 Setting Alarm History Calibration History Measure History Hour Report Hist...

Page 78: ...displayed 2 Select the relevant item using button displayed on the MENU screen The screen for the selected menu item will be displayed Reference MENU SETTING page 63 MENU MAINTENANCE page 111 MENU CHE...

Page 79: ...analog output Page 83 PAYLOAD SET Specifies the load calculation Page 98 SYSTEM SET Specifies the clock authority LCD printing communication and language Page 100 Item Description Reference OPERATION...

Page 80: ...commands Start Signal Pulse Pulse Starts measurement by the pulse input Level Performs measurement according to the measurement mode while the signal is input Measure Mode Schedule Repeat Performs me...

Page 81: ...s Start Time 0 to 59 0 min Specifies the time minute to start the measurement Meas Schedule Pattern 1 to 7 Measure L1 Allows you to select from Measure L1 Stop and Measure L2 Weekly Pattern Day of the...

Page 82: ...DULE 1 2 WEEKLY PATTERN 1 2 Meas Start Meas Weekly Pattern MEAS SCHEDULE 2 2 Schedule 1 WEEKLY PATTERN 2 2 Specify various settings Pattern 1 Specify AUTO MEAS SCHE SET OPERATION SET 1 2 AUTO MEAS SCH...

Page 83: ...When it is not set to 0 hours measurement is started from the specified measurement start time Item Setting range Default value Description Operation Cycle 0 hour 1 hour 2 hours 3 hours 4 hours 6 hour...

Page 84: ...ASH SET screen will be displayed 2 Specify the hydrochloric acid cleaning Note Be sure that different dates are specified for the start date of automatic hydrochloric acid cleaning and automatic reage...

Page 85: ...1 3 Function Cycle Start Date AUTO Start Date Function L2 Cycle Sample Line Wash L2 Function Cycle Start Date Start Date Sample Line AUTO HCl WASH SET 2 3 AUTO HCl WASH SET 3 3 Input a value OPERATION...

Page 86: ...s the zero calibration value SPAN Cal Count 0 to 10 2 Determines the number of times to perform calibration per span calibration When 2 is specified the average of the results of two calibrations will...

Page 87: ...tion Start Date ZERO Cal Count AUTO CAL SET 2 3 SPAN Cal Count Pre Wash Count Post Wash Count ZERO Cal Count SPAN Cal Count Pre Wash Count Post Wash Count AUTO CAL SET 3 3 SPAN SPAN Conc TP SPAN Conc...

Page 88: ...cleaning and the automatic calibration both the automatic reagent line cleaning and automatic calibration are performed simultaneously Example When 1 time is specified for all the Pre Wash ZERO CAL SP...

Page 89: ...Function 73 AUTO Start Date Cycle Function Function AUTO WASH SET Cycle Start Date Input a value OPERATION SET 1 2 WASH SET...

Page 90: ...INE SET in the OPERATION SET 2 2 screen The OFF LINE SET screen will be displayed 2 Specify the off line measurement Item Setting range Default value Description OFF LINE MODE ON OFF OFF Specifies whe...

Page 91: ...Description Reference LINE CHANGE SET Specifies the allocation of the measurement line Page 76 CONV COEF SET Specifies the conversion coefficient Page 77 CONC ALARM SET Specifies the TP TN concentrat...

Page 92: ...Default value Description Line No L1 to L2 1 to 99 1 Specifies the sample line to be used Line Select L1 to L2 Stop Working Working Select either Stop or Working for the line Note L2 can be selected...

Page 93: ...EAS LINE SET screen The CONV COEF SET TP or CONV COEF SET TN screen will be displayed Item Setting range Default value Description Revision a L1 to a L2 999 9 to 999 9 0 0000 Specifies the conversion...

Page 94: ...b L1 CONV COEF SET TN Revision Element Revision Input a value Input a value Input a value Input a value CONV COEF SET COD Element Revision Revision Revision a L1 Input a value Revision b L1 Input a va...

Page 95: ...000 mg L 0 0000 mg L Specifies the upper limit alarm value for the TP TN concentration H Hi Limit L1 to L2 0 0000 mg L to 2000 mg L 0 0000 mg L Specifies the final upper limit alarm value for the TP T...

Page 96: ...TN Element H Hi Limit L1 Hi Limit L1 Hi Limit L1 H Hi Limit L1 Input a value Input a value Input a value Input a value CONC ALARM SET COD Element H Hi Limit L1 Hi Limit L1 Hi Limit L1 H Hi Limit L1 I...

Page 97: ...ate alarm value Note 1 L2 can be selected only for the two point meter specification Note 2 When these parameters are set to 0 0000 no alarm will be activated Main MENU SETTING MEAS LINE SET MENU MEAS...

Page 98: ...value Description Hi Limit L1 to L2 0 00 m3 d to 9999999 m3 d 0 00 m3 d Specify the flow rate alarm value Note 1 L2 can be selected only for the two point meter specification Note 2 When these parame...

Page 99: ...gs refer to Contact output page 19 Item Description Reference EXT POINT OUTPUT SET Specifies the external contact output Page 83 EXT ANALOG OUTPUT SET Specifies the analog output Page 90 DATA OUTPUT S...

Page 100: ...Function 84 EXT PO SET OUTPUT SET EXT POINT EXT PO ASSIGN OUTPUT SET EXT PO ASSIGN 1 4 EXT PO ASSIGN 2 4 EXT PO ASSIGN 3 4 Specify various settings EXT PO ASSIGN EXT PO ASSIGN 4 4...

Page 101: ...period for which the signal is turned ON in synchronization with the measurement sequence OFF 3600 sec The time period for which the signal is turned OFF in synchronization with the measurement seque...

Page 102: ...ter Filter Water Supply Adc Read Press Error Samp Lack L1 TP Hi Conc L1 TP H Hi Conc L1 TP Hi Load L1 TN Hi Conc L1 TN H Hi Conc L1 TN Hi Load L1 COD Hi Conc L1 COD H Hi Conc L1 COD Hi Load L1 Hi Flow...

Page 103: ...TOTAL ALARM 2 TOTAL ALARM3 TOTAL ALARM 4 TOTAL ALARM 5 TOTAL ALARM 6 01 Int memory Err 02 Clock Err 03 Int Power 04 Int comm Err 05 Heat High Temp 06 Lamp Err 07 Temp Sensor Err 08 Lo Temp Machine 09...

Page 104: ...Function 88 34 35 36 37 38 39 40 No allocation 41 42 43 44 45 46 47 48 49 50 Default value TOTAL ALARM 1 TOTAL ALARM 2 TOTAL ALARM3 TOTAL ALARM 4 TOTAL ALARM 5 TOTAL ALARM 6...

Page 105: ...ayed 2 Press MAINTE OUTPUT SET The MAINTE OUTPUT screen will be displayed 3 Specify the contact output Item Setting range Default value Description Point Output ON OFF ON Specifies ON OFF of the conta...

Page 106: ...the full scale of the measurement range Output Limit 100 110 Outputs a signal up to the range of 100 for the full scale of the measurement range 110 Outputs a signal up to the range of 110 for the ful...

Page 107: ...91 EXT ANALOG EXT ANALOG OUTPUT OUTPUT SET Select various Output Limit Output Output Level EXT DA ASSIGN Output Output Output F S EXT DA F S Select Select Input a value OUTPUT SET settings Level Assi...

Page 108: ...tration analog output during alarm activation Page 94 MAINTE OUTPUT SET Specifies the TP TN concentration analog output during maintenance Page 95 WARMUP OUTPUT SET Specifies the TP TN concentration a...

Page 109: ...Function 93 DATA OUTPUT DATA OUTPUT SET CAL OUTPUT OUTPUT SET SET CAL OUTPUT Output Preset Output Mode Preset Input a value Mode...

Page 110: ...alarm activation to the previous value Preset Locks TP TN concentration analog output during alarm activation to a preset value Direct Outputs the measurement value to the TP TN concentration analog...

Page 111: ...g output during maintenance to the previous value Preset Locks the TP TN concentration analog output during maintenance to the preset value Direct Outputs the measurement value to the TP TN concentrat...

Page 112: ...nalog output during warm up to the previous value Preset Locks the TP TN concentration analog output during warm up to the preset value Direct Outputs the TP TN concentration analog output during warm...

Page 113: ...be displayed When set ON negative values are displayed and printed as is When set OFF all negative values are displayed as 0 3 Specify that values exceeding full scale are to be displayed When set ON...

Page 114: ...100 100 110 110 110 110 Analog output 0 to 100 0 to 110 Display printing 0 to F S Actual measure ment value to F S 0 to actual measure ment value Actual measure ment value 0 to F S Actual measure ment...

Page 115: ...Function 99 Date Function Date Hourly Date Unit Flow F S L1 Hourly Daily Function Date Daily Unit Flow F S L1 PAYLOAD SET SETTING PAYLOAD Select Input a value Input a value Input a value SET...

Page 116: ...1 AUTHORITY SET Specifies the password for power user authority Page 103 LCD ADJUST Specifies the LCD screen settings Page 104 PRINT OUT SET Specifies the printing settings on the printer Page 105 COM...

Page 117: ...099 12 31 23 59 Current time The time entered here is set as the current time Modify function ON OFF Select whether to enable ON or disable OFF the time modification function at the desired timing OFF...

Page 118: ...Function 102 SYSTEM SET 1 2 CLOCK SETTING SYSTEM SET ADJUST Date Date Modify Modify function Modify input Modify Modify Modify date CLOCK ADJUST Input a value function input date...

Page 119: ...ety of equipment settings is specified The password must be handled by personnel who are sufficiently familiar with the features of the product If a changed password is forgotten it cannot be canceled...

Page 120: ...e Description LCD OFF time OFF 10 min 20 min 30 min 60 min 10 min Specifies the time to automatically turn OFF the LCD Contrast From darkest to lightest Center Allows you to adjust the contrast of the...

Page 121: ...ue Description Print Hourly ON OFF ON Allows you to select whether or not to use the automatic printing function hourly Print Daily ON OFF ON Allows you to select whether or not to use the automatic p...

Page 122: ...Whether or not to print the item can be selected by pressing PRINT OUT SET Print Daily Tip In default setting data is printed as in the example of Real time printing no load calculation When the load...

Page 123: ...en Items to be printed by setting from the screen Calibration history DATA CAL HISTORY screen PRINT Alarm information DATA ALARM HISTORY screen PRINT Measurement history DATA LOG DATA MEASURE VALUE sc...

Page 124: ...ings Item Setting range Default value Description Machine ID 1 to 247 1 Specifies the ID number of the meter Baudrate 9600 bps 19200 bps 38400 bps 19200 bps Allows you to select the communication spee...

Page 125: ...The LANGUAGE SET screen will be displayed 3 Specifies the language settings Item Setting range Default value Description Language Japanese English Specifies the language to be displayed English Chine...

Page 126: ...UCH PANEL ADJUSTMENT TOUCH PANEL ADJUSTMENT screen will be displayed 3 Adjust the touch panel Item Description TOUCH PANEL ADJUSTMENT Adjust the position aberration of the touch panel MENU Main Refer...

Page 127: ...it Page 117 SEPARATE ACTION Specifies and updates the separate action Page 119 Item Setting range Reagent capacity Description REAG VOLUME CHECK Reag A 1000 mL Allows you to check the remaining amoun...

Page 128: ...AG in the MAINTENANCE screen The REAG screen will be displayed 2 Check the reagent volume MENU Main Refer to To display the MENU item screen page 62 SETTING MAINTENANCE MENU 1 2 MAINTENANCE REAG REAG...

Page 129: ...edure 1 Replace all the reagent bottles at the same time Replacing the reagent bottle page 193 MENU Main Refer to To display the MENU item screen page 62 SETTING MAINTENANCE MENU 1 2 MAINTENANCE REAG...

Page 130: ...screen will be displayed 2 Enter the remaining amount of reagent MENU Main Refer to To display the MENU item screen page 62 SET MAINTENANCE MENU 1 2 MAINTENANCE REAG REAG REAG REAG VOLUME REAG VOLUME...

Page 131: ...MAINTENANCE screen The PERIODIC CHECK screen will be displayed 2 Check the periodic inspection date MENU Main Refer to To display the MENU item screen page 62 SETTING MAINTENANCE MENU MAINTENANCE PERI...

Page 132: ...centration analog zero output ch00 0001 to 0FFE 03D0 ch01 Adjusts the TN concentration analog zero output ch02 0001 to 0FFE 03D0 ch02 Adjusts the TP load analog zero output ch03 0001 to 0FFE 03D0 ch03...

Page 133: ...m Setting range Default value Description Measure Line Measure L1 Measure L1 Selects the target Measure L2 Meas L1 HCl Meas L2 HCl ZERO Cal SPAN Cal Cleaning Pre Wash Post Wash Preprocess Start Sequen...

Page 134: ...Function 118 MAINTENANCE STEP STEP ACTION SET Select various settings DECIDE START ACTION...

Page 135: ...he reagent E bottle SEPARATE ACTION 4 5 Drain Reag F Drains the residual reagent from the reagent F line into the reagent F bottle Drain Span Water Drains the residual reagent from the dilution tube o...

Page 136: ...120 Operation procedure 1 Press SEPARATE ACTION in the MAINTENANCE screen The SEPARATE ACTION screen will be displayed MENU Main Refer to To display the MENU item screen page 62 SETTING MAINTENANCE M...

Page 137: ...formed and then press YES The specified operation will be started SEPARATE MAINTENANCE SEPARATE SEPARATE SEPARATE SEPARATE SEPARATE The operation starts Select ACTION ACTION 1 5 ACTION 2 5 ACTION 3 5...

Page 138: ...ts ON OFF status Page 123 EXT POINT OUTPUT Allows you to check the external contact output item and its ON OFF status The ON OFF status can be switched Page 124 EXT ANALOG INPUT Allows you to check th...

Page 139: ...Press EXT POINT INPUT in the CHECK 1 2 screen The EXT POINT INPUT screen will be displayed The external contact input item and its ON OFF status can be checked MENU Main Refer to To display the MENU i...

Page 140: ...d its ON OFF status can be checked 2 To toggle ON OFF status select the item and press O Note After approximately 10 minutes have passed with no button operation occurring on the screen within the out...

Page 141: ...t value Operation procedure 1 Press EXT ANALOG INPUT in the CHECK 1 2 screen The EXT AD screen will be displayed The external analog input item and its input value can be checked MENU Main Refer to To...

Page 142: ...ss OUTPUT Note After approximately 10 minutes have passed with no button operation occurring on the screen within the outlined area shown in the illustration below output will revert to the setting sp...

Page 143: ...procedure 1 Press INT ANALOG INPUT in the CHECK 2 2 screen The INT AI screen will be displayed The internal analog input item and its input value can be checked MENU Main Refer to To display the MENU...

Page 144: ...creen will be displayed 2 Select an item with the relevant button displayed in the DATA screen The screen for the selected data item will be displayed DATA LOG Main screen DATA 1 2 LOG DATA MEASURE ME...

Page 145: ...ALUE MEASURE TREND TREND GRAPH GRAPH HOUR REPORT HOUR Refer to the previous page OPTICAL OPTICAL SIGNAL TREND GRAPH TREND CALIBRATION HISTORY Continued on the next page VALUE GRAPH MEASURE VALUE REPOR...

Page 146: ...on 130 DATA 1 2 GRAPH Refer to the previous page CALIBRATION CAL HISTORY ALARM ALARM HISTORY SAVE SAVE TO USB Select various DATA 2 2 DATA CLEAR 1 2 DATA DATA CLEAR 2 2 HISTORY HISTORY TO USB CLEAR se...

Page 147: ...e will be displayed To change the measurement element or line press the button of the measurement element line and select the element line you wish to view Then press DECIDE To print press PRINT The l...

Page 148: ...OG DATA MEASURE VALUE Measurement Line to be Date Line to be displayed Select a line Date Scroll the display PRINT Start printing Line Select Date selection Change the date Measurement element Select...

Page 149: ...levant date button and select the measurement date you wish to view and press DECIDE The data on the specified date will be displayed To change the measurement element or line press the button of the...

Page 150: ...RY LOG DATA HOUR REPORT Measurement Line to be Date Line to be displayed Select a line Date Scroll the display PRINT Start printing Line Select Date selection Change the date Element selection Measure...

Page 151: ...Page 137 HOUR REPORT HISTORY Displays the graph of the past hourly report data The display settings of the graph can be specified Page 139 OPTICAL SIGNAL Displays the graph of the past optical signal...

Page 152: ...H MEASURE MEASURE VALUE SET GRAPH SET 1 2 GRAPH SET 2 2 Measure Measure Scale Start Time Start Time Period Vertical Top Scale Period Vertical Top Line Vertical Vertical Under Meas Meas Element Input a...

Page 153: ...APH SET screen will be displayed 4 Specify the graphical display conditions on the GRAPH SET screen Item Setting range Setting Measure Line L1 L2 Specifies the line to be displayed in a graphical form...

Page 154: ...38 DATA 1 2 GRAPH GRAPH TREND GRAPH MEASURE VALUE SET TREND GRAPH GRAPH SET Measure Scale Vertical Top Vertical Vertical Scale Vertical Under Measure Line Meas Meas Element Input a value Line Top Unde...

Page 155: ...tting Measure Line L1 L2 Specifies the line to be displayed in a graphical form Component Flow Water Payload Specifies the components Scale Water 0 01 to 1000 Flow 1 to 999999 Payload 0 00 to 9999999...

Page 156: ...REPORT SET GRAPH SET 1 2 GRAPH SET 2 2 Measure Line MEASURE Scale Start Period Component Line Vertical Component Scale Start Time Period Vertical Top Vertical Under Vertical Meas Element Meas Input a...

Page 157: ...e Line L1 L2 ZERO SPAN Specifies the line to be displayed in a graphical form Start Time 2009 01 01 00 to 2099 12 31 23 Specifies the display start date Vertical Top 25 50 75 100 Specifies the upper l...

Page 158: ...1 2 GRAPH GRAPH OPTICAL SET OPTICAL SIGNAL GRAPH SET 1 2 Measure Vertical Top Vertical Vertical Start Time Vertical Under Measure Line Start Time GRAPH SET 2 2 Pulse Type Meas Element Meas SIGNAL Line...

Page 159: ...cked Pressing moves the red line for each second allowing you to check the data OPTICAL SIGNAL 1 Touch the graphic area on the screen once 2 The red line will go off 3 Pressing goes to the previous ne...

Page 160: ...y conditions on the GRAPH SET screen Item Setting range Setting Vertical Top 25 50 75 100 Specifies the upper limit on the vertical axis of the graph for the full scale of the measurement range Vertic...

Page 161: ...145 GRAPH SET Vertical Vertical Vertical Top Vertical Under DATA 1 2 GRAPH GRAPH TREND GRAPH TREND SET Pulse Type Meas Element Pulse Type Meas Measure Measure Line GRAPH OPTICAL SIGNAL Top Under Elem...

Page 162: ...he button of the measurement element and select the element you wish to view Then press DECIDE Tip Pressing in the history display screen moves to the previous next history allowing you to check the d...

Page 163: ...HISTORY screen will be displayed Tip Pressing in the history display screen moves to the previous next history allowing you to check the data 2 Press PRINT and specify the date and press DECIDE The al...

Page 164: ...other USB memory devices we do not guarantee the operation If the memory storage capacity of the equipment is exceeded data will be deleted in order starting with the oldest The memory capacity of the...

Page 165: ...gnal values Page 153 Optical signal PUL2 CSV Stores 75 latest REF signal values for TN Optical signal PUL3 CSV Stores 75 latest SMP signal 220 nm values for TN Optical signal PUL4 CSV Stores 75 latest...

Page 166: ...Revision parameter B CONC ALARM Concentration alarm ABS 1 UV absorbance Abs ABS 2 VIS absorbance Abs ABS 3 UV VIS absorbance Abs ABS 1 ALARM UV absorbance alarm ABS 2 ALARM VIS absorbance alarm ABS 3...

Page 167: ...ity AVE CONC Average water quality LOAD Load FLOW ALARM Flow rate alarm CONC ALARM Water quality alarm LOAD ALARM Load alarm Header Description YY MM DD HH MM SS Occurrence date and time ALARM LINE Li...

Page 168: ...NC Standard solution concentration FACTOR Factor PARA_a Calculation parameter A PARA_b Calculation parameter B PARA_c Calculation parameter C PARA_k Calculation parameter K PARA_a1 Calculation paramet...

Page 169: ...ARA_b1 PARA_c1 ZERO RESULT Zero calibration result OK NG HOLD SPAN RESULT Span calibration result OK NG HOLD UV_ZERO UV zero calibration value VIS_ZERO VIS zero calibration value UV_SPAN UV span calib...

Page 170: ...entration alarm ABS 1 UV absorbance Abs ABS 2 VIS absorbance Abs ABS 3 UV VIS absorbance Abs ABS 1 ALARM UV absorbance alarm ABS 2 ALARM VIS absorbance alarm ABS 3 ALARM UV VIS absorbance alarm Header...

Page 171: ...real time When measurement is completed Note Whether or not to print it can be selected PRINT OUT SET page 105 Hourly report printing real time When hourly report calculation is completed Note Whether...

Page 172: ...al 1 min Data History All Items Operation procedure 1 Press DATA CLEAR in the DATA 2 2 screen The DATA CLEAR screen will be displayed 2 Select an item in the DATA CLEAR screen and then press YES The s...

Page 173: ...n be started MEAS CALIBRATION WASH E LINE Not supported Operation procedure 1 Press START in the main screen The START screen will be displayed 2 Select an item in the START screen and then press YES...

Page 174: ...cessing screen The STOP screen will be displayed 2 Select an item in the STOP screen and then press YES According to the selected item the current operation is stopped or reserved to be stopped Item D...

Page 175: ...peration procedure STOP CANCEL 1 Press STOP in the stop reservation screen 2 Press STOP CANCEL in the STOP screen Cancels the reservation for stopping the operation STOP Continued from the previous pa...

Page 176: ...te If power to the equipment is turned OFF without pressing the SHUTDOWN key data in system internal memory or on the CF card could be corrupted To power down the equipment be sure to follow the opera...

Page 177: ...chine ID Baudrate Parity COMMUNICATION SET page 108 Software overview Function code Item Description Remarks Physical I F RS 485 Option Two wire RS 232C When the optional RC 232C is selected it is nec...

Page 178: ...code page 161 02 Illeglal Data Address Includes the case in which data is accessed by the non standard size Example Two byte access to four byte data Note When an access is made to an unused address...

Page 179: ...ime of process being measured 256 4 clk Yes No Final alarm occurrence date and time MEAS CURRENT ALARM 260 2 long Yes No Common alarm bit 00 31 Common alarm Data definition sheet page 177 262 2 long Y...

Page 180: ...og input count value 05 1286 1 short Yes No External analog input count value 06 1287 1 short Yes No External analog input count value 07 1288 1 short Yes No External analog input count value 08 1289...

Page 181: ...Yes External analog input current value 03 5640 2 float Yes Yes External analog input current value 04 5642 2 float Yes Yes External analog input current value 05 5644 2 float Yes Yes External analog...

Page 182: ...analog output value 14 6161 1 short Yes Yes External analog output value 15 6162 1 short Yes Yes External analog output value 16 6163 1 short Yes Yes External analog output value 17 6164 1 short Yes...

Page 183: ...31 6404 2 long Yes Yes External contact output 32 63 7168 1 short Yes Yes Channel ADJUST EXT ANALOG INPUT ADJUST 7169 1 short Yes Yes Mode 0 ZERO 1 SPAN 7170 1 short Yes No Unused area Reading Consta...

Page 184: ...request time range are recorded and then acknowledged When the data area is read after 3 has been written the currently memorized data are acknowledged If there are no data FF is set 16396 35 mes_d at...

Page 185: ...ed 17929 1 short Yes No Unused area Reading Constantly 0 Writing Ignored 17930 1 short Yes No Unused area Reading Constantly 0 Writing Ignored 17931 1 short Yes Yes Request status 0 No response 1 Init...

Page 186: ...4 1 short Yes No Optical signal history 01 Request data number 00 18965 1 short Yes No Optical signal history 01 Request data number 01 18966 1 short Yes No Optical signal history 01 Request data numb...

Page 187: ...988 1 short Yes No Optical signal history 01 Request data number 24 18989 1 short Yes No Optical signal history 01 Request data number 25 18990 1 short Yes No Optical signal history 01 Request data nu...

Page 188: ...number 48 19013 1 short Yes No Optical signal history 01 Request data number 49 24576 9 cpu_inf o Yes No Main program information Data format example page 174 Others Program information 24585 9 cpu_in...

Page 189: ...Modbus 173 Other than above Yes No Unused area Reading Constantly 0 Writing Ignored Register Modbus address Length Data format Read Write Item name Read write content Classification...

Page 190: ...8 bits Digit 24 26 Abs 1 wval_t Lower 8 bits Unit 27 Constantly 0 3 mes_info 0 Mesctl status number 28 30 Abs 2 wval_t 1 Measurement line 31 Constantly 0 2 Reserved 32 Alm_Abs 0 short 25 alm_info 0 3...

Page 191: ...ort 24 25 Parameter 3 float 25 Constantly 0 26 27 Parameter 4 float 26 28 Payload wval_t 28 29 Parameter 5 float 29 Payload alarm short 30 31 Parameter 6 float 7 memalm 0 3 Date time clk 32 UV meter c...

Page 192: ...haracter for number P ASCII 3 Upper 8 bits Seventh character for number P ASCII Lower 8 bits Eighth character for number P ASCII 4 Upper 8 bits Ninth character for number P ASCII Lower 8 bits Tenth ch...

Page 193: ...3 3 L4 4 L5 5 L6 7 ZERO 8 SPAN 9 BLANK 10 WASH 12 Pre Wash 13 Post Wash 14 WASH E LINE 65535 No Line Main sequence No 0 Standby 1 MEAS 2 ZERO CAL 3 SPAN CAL 4 WASH 5 HCl WASH MEAS 6 BLANK MEAS 7 Ready...

Page 194: ...F 24 Standby 25 Inject Reag C 26 Inject Reag D 27 Inject Reag E 28 WASH E LINE 1 29 WASH E LINE 2 30 Send Liquid Inject to P cell 31 Send Liquid Inject to N cell 32 Send Liquid Pour Dilute Tube 4 33 S...

Page 195: ...Blow L1 63 Line Blow L2 64 Pure water purge 65 Press Blow 66 Standby 67 Drain Reag B 68 Drain Reag C 69 Drain Reag D 70 Drain Reag E 71 Drain Reag F 72 Drain Span Water 73 Replace Bottle 1 74 Replace...

Page 196: ...Cell Measurement Tube 88 Pull Cell Measurement Tube 89 No allocation 90 Display skip 91 Waiting reaction With Check Press 92 93 94 95 Process No 0 No display 1 Sampling 2 Decomposition 3 MEAS 4 WASH D...

Page 197: ...e UV L1 13 UV Err L1 14 UV Power L1 15 Samp Lack L2 16 Line Select L2 17 Flow Mainte L2 18 Flow Err L2 19 Flow Power L2 20 Flow No Drain L2 21 Maintenance UV L2 22 UV Err L2 23 UV Power L2 24 Samp Lac...

Page 198: ...Flow Mainte L6 54 Flow Err L6 55 Flow Power L6 56 Flow No Drain L6 57 Maintenance UV L6 58 UV Err L6 59 UV Power L6 60 Common alarm 0 Power 1 Factory Setting 2 User Setting 3 Measure History 4 Hour Re...

Page 199: ...cell 33 Temp Sensor Err Pump 34 Lack Blank 35 Full Drain Tank 36 Lo Temp Machine 37 Lo Temp Bench 38 Lo Temp P cell 39 Lack Span 40 41 Lack Reag B 42 Lack Reag C 43 Lack Reag D 44 Lack Reag E 45 Lack...

Page 200: ...y Not supported 70 Adc Read 8 71 Adc Read 9 72 Press Error 1 73 Press Error 2 74 Press Error 3 75 Press Error 4 76 Press Error 5 77 Press Error 6 78 Press Error 7 Alarm for each line 0 n0 Sample Lack...

Page 201: ...larm 0 Missing data 1 Maintenance 2 Failure 3 Power 4 Less than 4 mA 5 More than 20 mA 6 No Drain 7 Calculation Disabled 8 Full scale Over 9 No data 10 Alarm 11 Hold Previous Value 12 Hi Limit Err 13...

Page 202: ...Setting of measurement line 2 Setting of measurement element 3 Reading MEAS Day Report History 1 Setting of measurement line 2 Setting of measurement element 3 Reading MEAS EXT ANALOG INPUT 1 Reading...

Page 203: ...heck request 0 ADJUST EXT ANALOG INPUT ADJUST 1 Setting of CH 2 Setting of adjustment mode 3 Adjustment request Data set 0 is set and then the current value is read 4 Adjustment request Setting update...

Page 204: ...letion time 3 Setting of request line 4 Setting of request element 5 Request status Initialization 1 is set and then the data preparation is executed 6 Request status The same data 3 are set and then...

Page 205: ...gnal 1 Setting of request start time 2 Setting of request completion time 3 Setting of request data number 4 Request status Initialization 1 is set and then the data preparation is executed 5 Request...

Page 206: ...cycle depending on the equipment settings Waste liquid processing Waste liquid tank Waste liquid tank Perform waste liquid processing For details on the procedure refer to Waste liquid processing page...

Page 207: ...aste liquid tank is 20 L approximately 30 days when measurement is performed hourly When the tank becomes full of waste liquid a Full Drain Tank alarm will be output and the measurement will be stoppe...

Page 208: ...remove the tightening cap of the waste liquid tank and then remove the float sensor and waste liquid nozzle unit 4 Perform the waste liquid processing for the waste liquid tank 5 After the processing...

Page 209: ...ement method collective replacement and individual replacement Note A new reagent bottle is fully charged with reagent If you grab the side of the bottle while the cap is open the reagent may spill ou...

Page 210: ...he reagents at the same time Operation procedure 1 Press REAG in the MAINTENANCE screen and then CHANGE REAG Total refer to REAG page 111 MENU Main Refer to To display the MENU item screen page 62 SET...

Page 211: ...the reagent E bottle will be used in a later step store it temporarily 3 Remove the reagent F bottle in the same manner as step 2 above and then attach it to line E 4 Once the procedure is completed p...

Page 212: ...F bottle and then attach the temporarily stored reagent E bottle as instructed on the screen After the replacement press YES Reagent F bottle Reagent E bottle Tube Orange Label Orange Label Red Line...

Page 213: ...e label 7 After the operation has been completed press YES and perform calibration For details on the calibration procedure refer to START page 157 Once the operation is completed the remaining amount...

Page 214: ...DATA item screen page 128 SET MAINTENANCE MENU 1 2 Screen Operation name Description SEPARATE ACTION 3 5 Drain Reag A Drains the residual reagent from the reagent A line into the reagent A bottle Dra...

Page 215: ...ozzle unit to a new reagent bottle 6 Set the bottle in the reagent tray Return the reagent tray to its original position and tighten the knurled screw one location Nozzle unit Tightening cap Cap Remov...

Page 216: ...ut the replenishment amount of the solution MAINTENANCE REAG REAG REAG REAG VOLUME REAG VOLUME Input a value Reag A Reag B Reag C Reag D Reag E SPAN water Reagent Reagent capacity Label color Reagent...

Page 217: ...rument is OFF for more than 2 days the Pure water cartridge alarm will be issued When the alarm is issued purge out the residual water with pure water in the piping Check 1 Check if the Pure water car...

Page 218: ...should be replaced Replacement 1 Close the V 1 and V 3 valves 2 Press pure water purge to reduce the inner pressure 3 About 10 seconds later Press Pure water purge again 4 Pull down the safety lever...

Page 219: ...U MAINTENANCE SEPARATE ACTION on the screen The SEPARATE ACTION 5 5 menu will be opened 9 Press Pure water purge to start purging of the pure water cartridge Basic purge time about 5 minutes Depending...

Page 220: ...he measurement range and therefore the supply cycle listed below should only be used as a guide Use the table below for reference Pure water supply cycle guide Target Pure water tank Procedure Inspect...

Page 221: ...ch ON Pure water criterion JIS K0557 1998 Water used for industrial water and wastewater analysis 1 Remove the tube and connector for float sensor from the pure water tank 2 Remove the pure water tank...

Page 222: ...esh pure water 5 After supplying the fresh pure water return the tank to its original condition Note If the inside of the pure water tank is dirty it could affect the measurement values Rinse it well...

Page 223: ...y clean the tank before the suspended solids accumulate inside the tank When you perform maintenance be sure to stop the measurement and then turn the maintenance switch ON Inspection Check that the o...

Page 224: ...hile continuing to drain water 4 Remove the cap nuts and gaskets for the sample inlet and sample outlet and then clean the inside of the piping After the cleaning reattach the gaskets and cap nuts in...

Page 225: ...extremely careful not to break it Inspection Check if dirt is accumulated in the dilution tube and cell measurement tube Also check that the sample water is measured and discharged appropriately Clea...

Page 226: ...valve at the bottom of the dilution tube Then slide it to the left while holding the PharMed tube below the pinch valve 5 Remove the FEP tube from the PharMed tube Screws Front cover Measurement sect...

Page 227: ...etaining plate at the top of the dilution tube 7 While holding the dilution tube with one hand and pulling it to the front remove the dilution tube retaining plate upward 8 Clean the dilution tube Dil...

Page 228: ...ly set 11 Attach the dilution tube retaining plate to the dilution tube and then attach it to the equipment Note When attaching the dilution tube do not apply excessive load as it could bend the measu...

Page 229: ...hat the PharMed tube goes inside the tube through position of the pinch valve 15 Clean the cell measurement tube as necessary in the same manner as above 16 Reattach the front cover of the measurement...

Page 230: ...nd power switch ON Check that the power cable is correctly connected Main power switch Ground fault interrupter page 2 Power switch page 5 Signal wiring page 11 An alarm is activated A previously acti...

Page 231: ...nt blank water measurement or reagent measurement cannot be performed appropriately Perform each operation and report the error condition to HORIBA Advanced Techno The reagent has deteriorated Replace...

Page 232: ...o Checking and cleaning the overflow tank option page 207 Cell measurement blank water measurement or reagent measurement cannot be performed appropriately Perform each operation and report the error...

Page 233: ...ng operation the current operation is retried automatically If it reoccurs the operation is stopped and the equipment is switched to the maintenance mode 3 Alarm 4 Alarm for automatic restoration Whil...

Page 234: ...Techno Alarm 1 Day Report History data stored in CF memory has been corrupted Turn OFF the power and then turn it ON again If the problem cannot be resolved contact HORIBA Advanced Techno Alarm 1 Alar...

Page 235: ...t HORIBA Advanced Techno Alarm 2 Press Error 2 There is leakage from the manifold system on the reagent side Contact HORIBA Advanced Techno Alarm 2 Press Error 3 The sample measurement line is clogged...

Page 236: ...interruption in illumination from light source The output power has dropped due to deterioration of the light source There is a connection error inside the analyzer or the detector or board is faulty...

Page 237: ...Contact HORIBA Advanced Techno Alarm 5 P SPAN Cal Incompatible span solution is used The measurement cell is dirty The analyzer components are faulty Replace the span solution bottle Replace the reage...

Page 238: ...ced Techno Alarm 5 FROM Write FROM writing has failed Contact HORIBA Advanced Techno Alarm 5 EEPROM Write EEPROM writing has failed Contact HORIBA Advanced Techno Alarm 5 Printer Printer paper has run...

Page 239: ...n x flow rate has exceeded the specified upper limit value It is not a meter error Alarm 5 COD Hi Conc The COD concentration has exceeded the specified upper limit value It is not a meter error Alarm...

Page 240: ...o the dissolved sample to remove carbonate compounds which interfere with measurements Measure the ultraviolet absorption at the absorption wavelength of 220 nm for nitrite ion and obtain the total ni...

Page 241: ...le and apply ultraviolet irradiation The phosphorous compounds in the sample are dissolved to orthophosphoric acid PO4 3 Phosphoric ion generates molybdenum blue through reaction with phosphomolybdic...

Page 242: ...o points option Number of measurement ranges 3 One range standard 2 ranges option Measurement cycle 60 min Installation conditions Ambient temperature 2 C to 40 C Ambient humidity Relative humidity 85...

Page 243: ...3 A is available for the Maintenance contact Status output Meas Calibration Standby Maintenance SYNCHRONOUS IDLE 1 SYNCHRONOUS IDLE 2 Power etc Alarm output Hi limit alarm TP TN COD H Hi limit alarm T...

Page 244: ...ent capacity 1000 mL Solution B 0 2 mL per measurement capacity 250 mL Solution C 0 1 mL per measurement capacity 250 mL Solution D 0 1 mL per measurement capacity 250 mL Solution E 0 19 mL per measur...

Page 245: ...Material 229 Accessories and consumables Accessories No Parts Qty 1 Printer paper 10 rolls pack 2 Instruction manual this document 1 3 Installation Work Procedure 1 4 Tube insertion jig 1...

Page 246: ...Material 230 Consumables Parts Parts code Qty 1 Printer paper 3200378127 10 rolls pack 2 Pure water cartridge 3200555290 1 3 Line cleaning solution 3200017824 1...

Page 247: ...100 200 500 1000 0 5 36 36 40 40 48 1 36 36 40 40 48 44 2 40 40 44 44 52 48 56 5 40 40 44 44 52 48 56 64 10 48 48 52 52 60 56 64 72 72 20 44 48 48 56 52 60 68 68 50 56 56 64 60 68 76 76 100 64 72 68...

Page 248: ...mg L 2 5 10 20 50 100 200 500 1000 0 5 100 100 65 65 65 1 100 100 65 65 65 65 2 65 65 30 30 30 30 30 5 65 65 30 30 30 30 30 30 10 65 65 30 30 30 30 30 30 30 20 65 30 30 30 30 30 30 30 50 30 30 30 30...

Page 249: ...ASH E LINE 2 18 Not supported SEPARATE ACTION 1 Gage Reag B 0 26 2 Gage Reag F 0 26 3 Gage Reag C 0 26 4 Gage Reag D 0 26 5 Gage Reag E 0 26 6 Gauge Span Water 0 26 7 Gauge Samp L1 0 26 8 Wastewater P...

Page 250: ...cell 20 125 02 05 8 Gauge Blank Water 12 50 195 03 15 9 Drain water P cell 10 135 02 15 9 Gauge Meas Tube 1 30 225 03 45 10 Drain Reag A 40 175 02 55 10 Tube to P cell 1 15 240 04 00 11 Drain Reag B 3...

Page 251: ...ll 5 2719 45 19 20 Gauge Meas Tube1W 15 439 07 19 65 Cooling 130 2849 47 29 21 Tube to P cell 1 15 454 07 34 66 P Measure Zero 40 2889 48 09 22 P Inject Reag A 26 5 481 08 00 67 P Inject Reag E 26 5 2...

Page 252: ...f line mode Serial No TP measurement range 10 mg L TN measurement range 50 mg L Process time sec Accumulated time sec Accumulated time min sec 1 Drain Sample L1 20 20 00 20 2 Drain Blank 20 40 00 40 3...

Page 253: ...r N cell 10 898 14 58 52 Gauge Meas Tube 1 30 928 15 28 53 Tube to N cell 1 15 943 15 43 54 N Inject Reag A 26 5 970 16 09 55 N Inject Reag B 26 5 996 16 36 56 Stir N cell 5 1001 16 41 57 Stir P cell...

Page 254: ...96 54 55 88 Wastewater N cell 10 3306 55 05 89 Gauge Meas Tube1W 15 3321 55 20 90 N Stir Meas Tube 5 3326 55 25 91 Tube to N cell 1 15 3341 55 40 92 Drain water N cell 10 3351 55 50 93 Gauge Meas Tube...

Page 255: ...11 35 Gauge Blank 4 25 623 10 23 8 Pour Dilute Tube4 15 146 02 26 36 Pour Dilute Tube4 15 638 10 38 9 Standby 40 186 03 06 37 Standby 40 678 11 18 10 38 11 Stir Dilute Tube 5 191 03 11 39 Stir Dilute...

Page 256: ...44 Pour Dilute Tube4 15 783 13 03 17 Stir Dilute Tube 5 296 04 56 45 Stir Dilute Tube 5 788 13 08 Serial No TP measurement range 100 250 mg L Process time sec Accumulated time sec Accumulated time mi...

Page 257: ...OFF LINE MODE ON ON ON ON ON HCl WASH OFF Previously ON Previously ON Currently ON Currently ON Sample Line Wash ON OFF ON OFF Display Serial No 1 Drain Sample Chk Drain Sample HCl Drain Sample HCl Dr...

Page 258: ...nsated total nitrogen The turbidity compensation setting is not necessary to be changed under the condition that the good correlation with the manual analysis is obtained Item Description LINE CHANGE...

Page 259: ...latest values for each element Hourly report HRS CSV Stores 8760 latest values for each line and element Daily report DAY CSV Stores 365 latest values for each line and element Alarm history ALM CSV S...

Page 260: ......

Page 261: ...http www horiba adt jp Headquarters 31 Miyanonishi cho Kisshoin Minami ku Kyoto 601 8306 TEL 81 75 321 7184 FAX 81 75 321 7291...

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