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2-13
SETUP
2.3.5 Reagent, Waste Bottle Assembly
The bottle top assemblies are equipped with desiccant cartridges containing molecular sieves,
which ensures that the air passing through the reagent handling system has been dried.
The
molecular sieves have a limited capacity to absorb moisture and is typically exhausted after 3
to 5 weeks. Molecular sieves, indicating or otherwise, can be regenerated at 300°C.
The bottle tops are constructed of PTFE and have been designed to accommodate reagent
bottles with GL-45 type threaded tops.
The waste and reagent bottle top assemblies include blue PTFE tubing for the handling of
liquid Karl Fischer reagent and a clear flexible silicone based tubing for use with the air
pump.
Caution: Most Karl Fischer reagents give off harmful
vapors. Consult manufacturer’s MSDS for safe handling
guidelines.
To assemble the reagent or waste bottle, see Figure 6 and
follow the next steps:
• Insert a PTFE top (J) into a GL45 cap (E).
• Screw on the desiccant cap with hose barb (F).
• Insert a desiccant cartridge (B) with hose-barbed cap
(A) through a 10-mm fitting (F) and 10-mm o-ring (G).
• Insert and screw the desiccant fitting into the corresponding
hole. Fasten the desiccant cartridge assembly to PTFE
top (J) with 10-mm fitting (F).
• Insert the reagent / waste tube (D) in the 5-mm fitting
(H) and attach the o-ring (I).
• Insert and screw the tube fitting into the corresponding
hole.
• Screw GL45 (E) cap with full assembly onto reagent
bottle.
• Add the air tube (C) to the desiccant cap (A) and connect
it to the corresponding position on the air pump. The
“Fill” position connects to the reagent bottle assembly.
The “Empty” position connects to the waste bottle
assembly.
Figure 6
Summary of Contents for HI 904
Page 1: ...1 QUICK START GUIDE HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 0 www hannainst com...
Page 4: ...4 QUICK START GUIDE...
Page 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View...
Page 17: ...1 INSTRUCTION MANUAL HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 00 www hannainst com...
Page 20: ...4...
Page 22: ...1 2 INTRODUCTION...
Page 24: ...2 2 SETUP...
Page 27: ...2 5 SETUP 2 3 Installation 2 3 1 Titrator Top View...
Page 28: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View...
Page 38: ...3 2 USER INTERFACE...
Page 46: ...3 10 USER INTERFACE...
Page 48: ...4 2 GENERAL OPTIONS...
Page 82: ...5 24 METHODS...
Page 84: ...6 2 TITRATION...
Page 94: ...6 12 TITRATION...
Page 96: ...7 2 AUXILIARY FUNCTIONS...
Page 104: ...8 2 MAINTENANCE PERIPHERALS...
Page 112: ...8 10 MAINTENANCE PERIPHERALS...
Page 124: ...9 12 METHODS OPTIMIZATION...
Page 125: ...A3 2 APPENDIX 3...
Page 126: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 127: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3...
Page 128: ...A1 2 APPENDIX 1...
Page 132: ...A2 2 APPENDIX 2...
Page 134: ...A2 4 APPENDIX 2...
Page 135: ...A3 1 APPENDIX 3 Appendix 3 Accessories A3 TITRATOR COMPONENTS A3 3...
Page 136: ...A3 2 APPENDIX 3...
Page 140: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 141: ...1 GENERAL APPLICATIONS BROCHURE HI 904 KARL FISCHER COULOMETRIC TITRATOR www hannainst com...
Page 142: ......
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Page 150: ...2 TITRATION THEORY...
Page 166: ...18 TITRATION THEORY A B Figure 8 Potential glass electrode mV C...