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2-10
SETUP
2.3.4.3.1 Titration Vessel Components
Warning: Always apply a thin layer of joint grease (supplied) to ground-glass joints before
attaching. Improperly-greased joints may become permanently seized!
To assemble the titration vessel, see Figure 4 and follow the steps below:
Karl Fischer Detector Electrode
The Karl Fischer detector electrode (F) consists of two parallel, platinum pins sealed into a
10mm diameter glass body. Two steel pins connect the platinum elements to a standard BNC
connector, which allows for easy attachment to the
HI 904
.
Attach to the titration vessel (A) in the dedicated ground-glass port.
Karl Fischer Generator Electrode
The Karl Fischer generator electrode (D) consists of two platinum electrodes (anode and
cathode) on a glass body. The anode and cathode may be separated by a diaphragm that is
built into the body of the generator. The
HI 904
can be used with both diaphragm and
diaphragm-less generators.
Attach the generator electrode (D) to the titration vessel (A) in the dedicated ground-glass
port.
Desiccant Cartridge
The desiccant cartridge (E) provides a dry path for pressure equalization between the ambient
air and the inside of the titration vessel.
Attach the desiccant cartridge (E) to the top of the generator electrode (D) in the dedicated
ground-glass port.
Figure 4
Summary of Contents for HI 904
Page 1: ...1 QUICK START GUIDE HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 0 www hannainst com...
Page 4: ...4 QUICK START GUIDE...
Page 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View...
Page 17: ...1 INSTRUCTION MANUAL HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 00 www hannainst com...
Page 20: ...4...
Page 22: ...1 2 INTRODUCTION...
Page 24: ...2 2 SETUP...
Page 27: ...2 5 SETUP 2 3 Installation 2 3 1 Titrator Top View...
Page 28: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View...
Page 38: ...3 2 USER INTERFACE...
Page 46: ...3 10 USER INTERFACE...
Page 48: ...4 2 GENERAL OPTIONS...
Page 82: ...5 24 METHODS...
Page 84: ...6 2 TITRATION...
Page 94: ...6 12 TITRATION...
Page 96: ...7 2 AUXILIARY FUNCTIONS...
Page 104: ...8 2 MAINTENANCE PERIPHERALS...
Page 112: ...8 10 MAINTENANCE PERIPHERALS...
Page 124: ...9 12 METHODS OPTIMIZATION...
Page 125: ...A3 2 APPENDIX 3...
Page 126: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 127: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3...
Page 128: ...A1 2 APPENDIX 1...
Page 132: ...A2 2 APPENDIX 2...
Page 134: ...A2 4 APPENDIX 2...
Page 135: ...A3 1 APPENDIX 3 Appendix 3 Accessories A3 TITRATOR COMPONENTS A3 3...
Page 136: ...A3 2 APPENDIX 3...
Page 140: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 141: ...1 GENERAL APPLICATIONS BROCHURE HI 904 KARL FISCHER COULOMETRIC TITRATOR www hannainst com...
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Page 150: ...2 TITRATION THEORY...
Page 166: ...18 TITRATION THEORY A B Figure 8 Potential glass electrode mV C...