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9-1
METHODS OPTIMIZATION
Chapter 9. Contents
9
OPTIMIZATION ..................................................................................... 9 - 3
9.1
Titrator Settings ................................................................................... 9 - 3
9.1.1 Control Parameters.................................................................................... 9 - 3
9.1.1.1 Endpoint Potential and Polarization Current ........................................................9 - 3
9.1.1.2 Titration Speed ...............................................................................................9 - 4
9.1.1.3 Signal Averaging .............................................................................................. 9 - 4
9.1.2 Termination Parameters .............................................................................. 9 - 5
9.1.2.1 Stability Time ..................................................................................................9 - 5
9.1.2.2 Drift Stop Termination Criteria ...........................................................................9 - 5
9.1.2.2.1 Relative Drift Stop ...................................................................................9 - 5
9.1.2.2.2 Absolute Drift Stop ..................................................................................9 - 6
9.1.3 Method Options .......................................................................................... 9 - 6
9.1.3.1 Pre-Analysis Stir Time ...................................................................................... 9 - 6
9.1.3.2 Stirring Speed ..................................................................................................9 - 6
9.1.3.3 Background Drift Rate Entry .............................................................................9 - 6
9.2
The Sample ........................................................................................... 9 - 7
9.2.1 Proper Sampling Procedure ......................................................................... 9 - 7
9.2.2 Determining the Optimal Sample Size .......................................................... 9 - 7
9.2.3 Solid Samples............................................................................................. 9 - 7
9.2.4 Liquid Samples ........................................................................................ 9 - 8
Summary of Contents for HI 904
Page 1: ...1 QUICK START GUIDE HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 0 www hannainst com...
Page 4: ...4 QUICK START GUIDE...
Page 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View...
Page 17: ...1 INSTRUCTION MANUAL HI 904 KARL FISCHER COULOMETRIC TITRATOR Revision 1 00 www hannainst com...
Page 20: ...4...
Page 22: ...1 2 INTRODUCTION...
Page 24: ...2 2 SETUP...
Page 27: ...2 5 SETUP 2 3 Installation 2 3 1 Titrator Top View...
Page 28: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View...
Page 38: ...3 2 USER INTERFACE...
Page 46: ...3 10 USER INTERFACE...
Page 48: ...4 2 GENERAL OPTIONS...
Page 82: ...5 24 METHODS...
Page 84: ...6 2 TITRATION...
Page 94: ...6 12 TITRATION...
Page 96: ...7 2 AUXILIARY FUNCTIONS...
Page 104: ...8 2 MAINTENANCE PERIPHERALS...
Page 112: ...8 10 MAINTENANCE PERIPHERALS...
Page 124: ...9 12 METHODS OPTIMIZATION...
Page 125: ...A3 2 APPENDIX 3...
Page 126: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 127: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3...
Page 128: ...A1 2 APPENDIX 1...
Page 132: ...A2 2 APPENDIX 2...
Page 134: ...A2 4 APPENDIX 2...
Page 135: ...A3 1 APPENDIX 3 Appendix 3 Accessories A3 TITRATOR COMPONENTS A3 3...
Page 136: ...A3 2 APPENDIX 3...
Page 140: ...A3 6 APPENDIX 3 MAN HI904 09 13...
Page 141: ...1 GENERAL APPLICATIONS BROCHURE HI 904 KARL FISCHER COULOMETRIC TITRATOR www hannainst com...
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Page 150: ...2 TITRATION THEORY...
Page 166: ...18 TITRATION THEORY A B Figure 8 Potential glass electrode mV C...