Thermo Scientific ARL EQUINOX 5000, Инструкция пользователя

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Contents
1 Revision Table................................................................................................... 2
2 Introduction ....................................................................................................... 5
3 Safety ................................................................................................................. 6
3.1 General Safety Guidelines ................................................................................... 6
3.2 Hazard Statements and Symbols ......................................................................... 7
3.3 Symbols on the Instrument .................................................................................. 7
3.4 Emergency Stop .................................................................................................. 8
3.5 Electricity ............................................................................................................. 8
3.6 High Voltage Generator ....................................................................................... 9
3.7 Protection Enclosure and X-Ray Tubeshield ........................................................ 9
3.8 Security Beacons ............................................................................................... 10
3.9 Gas Safety ......................................................................................................... 11
4 General Information ........................................................................................ 12
4.1 Front View ......................................................................................................... 12
4.2 Rear View .......................................................................................................... 13
4.3 X-Ray Goniometer Description .......................................................................... 16
4.3.1 ARL EQUINOX 5000 Goniometer Description ........................................ 16
4.3.2 ARL EQUINOX 5500 Goniometer Description ........................................ 17
4.4 X-Ray Optic Configurations ............................................................................... 17
4.4.1 Monochromator Configuration ................................................................ 18
4.4.2 Mirror Configuration ................................................................................ 20
4.4.3 Mirror-Monochromator Configuration ...................................................... 21
4.5 Beam Stop and Anti-diffusion Blade ................................................................... 22
4.6 Front Panel ........................................................................................................ 23
4.7 Connections Inside the ARL EQUINOX 5000/5500 ............................................ 23
4.7.1 Sample Holders Connections ................................................................. 24
4.7.2 Service Connections .............................................................................. 25
4.7.3 Vacuum for Mirror ................................................................................... 26
4.7.4 Furnaces Connections ............................................................................ 27
5 Connection Specifications ............................................................................. 28
5.1 Electrical Connection ......................................................................................... 28
5.2 Cooling Fluid ...................................................................................................... 29
5.3 Gas Specification ............................................................................................... 30
5.3.1 Specifications of the Detector Gas.......................................................... 31
5.3.2 Gas Impurities Specifications ................................................................. 31
5.4 Environment ...................................................................................................... 31
6 Installation ....................................................................................................... 32
6.1 Location ............................................................................................................. 32
6.2 Assembly Instructions of Diffractometer's Parts ................................................. 32