SmartLab: Automated Multipurpose X-ray Diffractometer
97
Examples of Sample Mounting
Introduced below are some typical sample mounting methods.
For more information, refer to the
SmartLab Guidance Reference Manuals
, the
Package Measurements Help Topics of the online help section of the
SmartLab
Guidance software
.
Powder samples
Place powder samples in the indentation on the glass sample holder or aluminum
sample holder, then insert into the height reference sample plate.
Powder sample
Bulk samples
Use a 4-inchi wafer sample plate, 6-inch wafer sample plate, or 8-inch wafer
sample plate to measure bulk samples. Select the appropriate sample spacer and
sample plate based on sample thickness. For detailed information, refer to
sample plates and sample spacers
Place the sample so that the sample surface to be measured is parallel to the
sample plate. A piece of clay may be used to secure the sample in place. If the
bulk sample is small enough to pass through the window on the provided
aluminum sample holder, you can secure the sample in the aluminum sample
holder and use the height reference sample plate.
Bulk sample on height reference sample plate
Sample for transmission SAXS measurements
For transmission SAXS measurements, clamp a fibrous or film sample to a
sample holder and secure it in place, then insert the holder into a sample plate.
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