
Genevac HT-8 & HT-12 Series II Evaporating Systems
Page 36 of
64
04-4541
Issue 1-9 – June 2008
5.8
How to start a run
This section will describe a typical evaporation run of
DMSO.
In this example, two sets of eight 28 x 60 mm
scintillation vials each containing 5 ml of DMSO were
held in solid aluminium sample holders.
SampleGuard control temperature was set at 40
degrees centigrade and the pressure to full vacuum.
To prevent condensation, the chamber was
preheated to 40 degrees centigrade.
Switch on the pump, evaporator and condenser.
Display the
Run Data
screen and input the following
data.
Run Data Locked
...................................................................
No
Next Run Number
.....................................................................
0
Run Name
..........................................
DMSO 28 x 60 mm tubes
Sample Holder Type
..........................
Solid Aluminium 28 x 60
Sample Volume
.........................................................................
5
Solvent
.............................................................................
DMSO
SampleGuard Control Temperature
......................................
40
SampleGuard Control Channel
................................................
1
Coolheat Enable Pressure
...................................................
100
Chamber Temperature Control
..............................................
40
Rotor Speed
........................................................................
Low
Heat Off Elapsed Time
......................................................
01:40
End of Run Elapsed Time
................................................
01:40
Controlled Pressure
.................................................................
0
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